JP3558967B2 - Production method of brown wheat vinegar - Google Patents

Production method of brown wheat vinegar Download PDF

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Publication number
JP3558967B2
JP3558967B2 JP2000183027A JP2000183027A JP3558967B2 JP 3558967 B2 JP3558967 B2 JP 3558967B2 JP 2000183027 A JP2000183027 A JP 2000183027A JP 2000183027 A JP2000183027 A JP 2000183027A JP 3558967 B2 JP3558967 B2 JP 3558967B2
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Prior art keywords
brown
fermentation
barley
carbon dioxide
wheat
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Expired - Fee Related
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JP2000183027A
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JP2002000254A (en
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瀧男 案浦
龍巳 案浦
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瀧男 案浦
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Description

【0001】
【発明の属する技術分野】
本発明は玄麦と玄米の有効成分を多量に含んだ食酢の製造方法に関するものである。
また、本発明は、玄麦及び玄米を原料とし、糖化、アルコール発酵、酢酸発酵の3者並行複発酵を行い、短時間にこくのある食酢を製造する方法に関するものである。
【0002】
【従来の技術】
従来、玄米を原料とする食酢は黒酢として、九州南部でよく製造されている。黒酢は、一般に、蒸煮玄米に黒麹菌を接種し、黒麹とし、これを壺に仕込み、1〜3年の長時間かけて、糖化−アルコール発酵−酢酸発酵−熟成を行って、製造されている。また、黒酢には生理活性成分が含まれて、体によいことも知られている。
【0003】
【発明が解決しようとする課題】
本発明では、玄麦と玄米に含まれる各種生理活性成分を多量を含ませた食酢を製造することを第一の課題とした。
また、本発明では、玄麦と玄米の表皮に多く含まれる各種生理活性成分が酢によって溶出される傾向が強いところから、酢酸発酵又は熟成が完全に完了するまで原料を発酵培養液中に存在させて生理活性成分の溶出を持続させる特別の発酵法を確立することを第二の課題とした。
【0004】
【課題を解決するための手段】
本発明は、玄麦及び玄米を原料として、糖化、アルコール発酵及び酢酸発酵の3者並行複発酵を行うことによって、発酵時間を短縮するとともに玄麦と玄米の生理活性成分を十分溶出させることに成功したのである。
【0005】
本発明における「3者並行複発酵」とは、清酒製造における糖化とアルコール発酵の並行複発酵を酢酸発酵まで含ませ、3者を並行して発酵させるものである。玄麦と玄米の澱粉質の糖化は初期に始まり、ゆっくり全発酵期間に糖化を続け、一方生理活性成分の溶出は酢酸発酵が始まるころから次第に高まり、酢酸発酵終了時に最高となり、酢酸菌膜を除いた後の3ケ月間の熟成期間でもなお溶出は続くものと考えられる。
【0006】
本発明における原料は、玄麦と玄米である。
玄麦としては、玄小麦、玄大麦、玄燕麦、玄ハト麦などの玄各種麦の1もしくは2以上で、これに表皮部分、例えばふすまやその粉砕物などを一緒に使用してもよい。
また、玄米はもみを除去した玄米そのものであるが、これに表皮部分、例えば胚芽や糠や脱脂糠などを一緒に使用してもよい。
【0007】
玄麦と玄米の使用割合は、全体を100重量部とすれば、玄麦5〜95重量部に対し、玄米95〜5重量部程度でよく、好ましいのは玄麦20〜80重量部に対し、玄米80〜20重量部で、より好ましいのは、玄麦30〜70重量部で、玄米30〜70重量部程度で、最も好ましいのは半々程度である。
【0008】
玄麦と玄米は各別に蒸煮され、種黒麹菌(アスペルギルス・ニガーIFO4343などがある。)を接種し、通風製麹し、各別の麹を製造する。表皮又はその処理物は蒸煮前に混合しておくとよい。2日程度で製麹は完了する。
【0009】
玄麦麹と玄米麹は、混合してタンクに半容量程度投入し、次いで全容量まで水を加える。これに蒸気を吹き込み全体を30〜35℃程度として、2週間程度維持し、その間時折撹拌して、糖化を開始させる。
【0010】
麹のタンク投入後2週間程して、耐酸性酵母種培養液(耐酸性アルコール発酵酵母であればいかなるものでもよく、協会9号などでもよい)を添加し、時折適宜撹拌し、アルコール発酵の開始を待つ。
【0011】
別途、底部がタンク内一杯に拡がり、高さは液面下になるよう台円錐体の骨組みを作り、これにアルコール含有液は通すが、炭酸ガス気泡は通さない金網を周囲に張って、上方一ヶ所又は複数箇所に集め、そこから炭酸ガス気泡が逃げるように開放とした炭酸ガス集中装置を作成しておく。
【0012】
アルコール発酵が始まったら、この炭酸ガス集中装置をタンクの中に設置し、別のタンクから酢酸発酵の終了した培養液を酢酸菌膜と一緒に、酸度が1%程度になる量添加する。また、この場合、アルコール発酵が弱いと思われたら、アルコールを補填しておくこともできる。
酢酸菌としては、このように酢酸菌膜を培養液と一緒に循環させて使用するのが一般的であるが、初発は酢醸造蔵から分離された酢酸菌でよく、またアセドバクター・アセチIFO3288などでもよい。
【0013】
酢酸菌を添加した後は酢酸菌が全面によく生育して膜を作るが、一ヶ所又は複数箇所において、炭酸ガス気泡が逃げるようにした部分だけは炭酸ガスの気泡が大量に出て、菌膜を作らせない状態が続くのである。
【0014】
酢酸発酵を2〜3カ月続け、アルコール濃度が0.2%程度まで下ったら、酢酸発酵を止めるために、酢酸菌膜を全部除去し、そのまま3カ月程度静置し、熟成させ、次いで粕を分離する。
粕の分離は、酒絞りと同様に、絞り袋に全もろみを入れ、ふねに入れ重りを加え、ゆっくり絞るのがよい。
【0015】
絞った液は酢酸約5%の美味な玄麦玄米酢となっているが、そのまま又は小分けして半年から1年放置、熟成させれば、更にまろやかで美味な玄麦玄米酢となるのである。
次に本発明の実施例を示す。
【0016】
【実施例】
玄米1tを蒸煮し、種黒麹菌を接種し、2日間通風製麹し、玄米麹を作った。
また、玄小麦1tを蒸煮し、種黒麹菌を接種し、2日間通風製麹し、玄麦麹を作った。
【0017】
4tタンクに玄米麹750kgと玄麦麹750kgを混合するように投入した。その上から水を加え、4tタンクの7分目まで水を入れ、底部から蒸気を吹き込み、麹を撹拌しながら全体を30〜35℃に加温し、糖化を開始し、2週間程度時折かいを入れて撹拌した
【0018】
2週間後、タンクに耐酸性種酵母を添加し、かいを入れて撹拌し、アルコール発酵開始の炭酸ガス気泡を確認して、炭酸ガス気泡を中央部に集めるように金網を張った台円錐体状の炭酸ガス集中装置を液面下にセットし、次いで、別のタンクで製造した酢酸発酵液を菌膜と一緒に、酸度が1%になる量(5%酢酸液であればは約2割の添加となる)添加し、酢酸発酵を開始した
【0019】
直ちに、酢酸菌膜を全面に作るが、中央部だけはアルコール発酵の持続による炭酸ガス気泡の吹き上げによって菌膜がこわされ丸く穴が開いたようになり、長い間炭酸ガス気泡は観察され
【0020】
酢酸発酵は、3カ月程度でアルコールが0.2%まで低下したとき、菌膜を全部分離して、終了させ
菌膜を分離して、そのまま3カ月程度静置し、熟成させ
次いで、もろみ全体を搾り袋に順次入れ、ふねに積み込み、水圧をかけて、ゆっくり搾り玄麦玄米酢を得
得られた玄麦玄米酢は1年程度静置し、熟成させて、出荷し
【0021】
【発明の効果】
本発明では、玄麦及び玄米を原料として、糖化、アルコール発酵、酢酸発酵の3者並行複発酵を行うことにより、玄麦、玄米の生理活性有効成分を多量溶出させたまろやかな食酢を短時間に製造することができた。
[0001]
TECHNICAL FIELD OF THE INVENTION
The present invention relates to a method for producing vinegar containing a large amount of active ingredients of brown barley and brown rice.
In addition, the present invention relates to a method for producing vinegar with richness in a short time by using brown wheat and brown rice as raw materials, performing saccharification, alcohol fermentation, and acetic acid fermentation in parallel.
[0002]
[Prior art]
Conventionally, vinegar made from brown rice is often produced as black vinegar in southern Kyushu. Black vinegar is generally produced by inoculating black koji mold on steamed brown rice to prepare black koji, charging it into a jar, and performing saccharification-alcohol fermentation-acetic acid fermentation-ripening over a long period of 1 to 3 years. ing. It is also known that black vinegar contains a physiologically active ingredient and is good for the body.
[0003]
[Problems to be solved by the invention]
An object of the present invention is to produce vinegar containing a large amount of various physiologically active components contained in brown wheat and brown rice.
Further, in the present invention, since various physiologically active components contained in the epidermis of brown wheat and brown rice have a strong tendency to be eluted by vinegar, the raw materials are present in the fermentation broth until acetic acid fermentation or ripening is completely completed. The second task was to establish a special fermentation method to maintain the elution of the physiologically active component.
[0004]
[Means for Solving the Problems]
INDUSTRIAL APPLICABILITY The present invention has succeeded in shortening the fermentation time and sufficiently eluting the bioactive components of brown barley and brown rice by performing three-sided parallel fermentation of saccharification, alcohol fermentation, and acetic acid fermentation using brown barley and brown rice as raw materials. It is.
[0005]
In the present invention, the "three-member parallel compound fermentation" includes the simultaneous compound fermentation of saccharification and alcohol fermentation in sake production up to acetic acid fermentation and fermentation of the three members in parallel. Starch saccharification of brown barley and brown rice begins early and continues saccharification slowly during the entire fermentation period, while the elution of bioactive components gradually increases from the start of acetic acid fermentation, reaches the highest at the end of acetic acid fermentation, and removes acetic acid bacterial membranes. It is considered that the elution still continues during the ripening period of three months after the aging.
[0006]
The raw materials in the present invention are brown barley and brown rice.
The brown barley is one or more of various types of wheat, such as brown wheat, brown barley, brown oat, and brown pigeon barley, and a skin portion, for example, bran or a crushed product thereof may be used together.
Further, the brown rice is the brown rice itself from which the firs are removed, and an epidermis such as germ, bran, or defatted bran may be used together.
[0007]
If the whole is 100 parts by weight, the use ratio of brown rice to brown rice is about 5 to 95 parts by weight, and about 95 to 5 parts by weight of brown rice is preferable. More preferably, it is 30 to 70 parts by weight of brown wheat, about 30 to 70 parts by weight of brown rice, and most preferably about half.
[0008]
Brown barley and brown rice are separately steamed, inoculated with a seed black koji mold (such as Aspergillus niger IFO4343), and subjected to aeration koji making to produce different koji. It is advisable to mix the epidermis or its processed product before steaming. Koji making is completed in about 2 days.
[0009]
The brown barley koji and the brown rice koji are mixed and put into a tank at about a half volume, and then water is added to the full volume. The whole is blown with steam to maintain the temperature at about 30 to 35 ° C., and is maintained for about 2 weeks. During this time, stirring is performed occasionally to start saccharification.
[0010]
About 2 weeks after putting the koji into the tank, add the acid-resistant yeast seed culture solution (any acid-resistant alcohol-fermenting yeast may be used, or the Association No. 9 or the like), and occasionally stir appropriately to conduct alcohol fermentation. Wait for the start.
[0011]
Separately, a bottom is expanded to fill the inside of the tank, and a frame of a truncated cone is formed so that the height is below the liquid level, and a wire mesh that allows alcohol-containing liquid to pass through but does not allow carbon dioxide gas bubbles to pass around, A carbon dioxide concentration device is collected at one or a plurality of locations and opened so that carbon dioxide bubbles escape therefrom.
[0012]
When alcohol fermentation has started, this carbon dioxide concentration device is installed in a tank, and a culture solution in which acetic acid fermentation has been completed is added from another tank together with an acetic acid bacterium in such an amount that the acidity becomes about 1%. In this case, if alcohol fermentation is considered weak, alcohol can be supplemented.
As the acetic acid bacterium, it is common to use the acetic acid bacterium circulated together with the culture solution as described above, but the first acetic acid bacterium may be an acetic acid bacterium isolated from the vinegar brewery, and may be Acetobacter acetyl IFO3288 or the like. May be.
[0013]
After adding the acetic acid bacteria, the acetic acid bacteria grow well on the entire surface to form a film.However, in one or more places, only a portion where the carbon dioxide gas bubbles escape allows a large amount of carbon dioxide gas bubbles to come out, and the bacteria grow. The state where a film is not made continues.
[0014]
The acetic acid fermentation is continued for 2 to 3 months, and when the alcohol concentration is reduced to about 0.2%, in order to stop the acetic acid fermentation, all the acetic acid bacteria membranes are removed, and the acetic acid fermentation is allowed to stand for about 3 months, aged, and then the cake is removed. To separate.
It is better to put the whole moromi in a squeezing bag, put the weight in a bowl, add the weight, and squeeze slowly as in the case of sake squeezing.
[0015]
The squeezed liquid is a delicious brown wheat vinegar of about 5% acetic acid, but if left alone or divided and left for half a year to one year, and then aged, it becomes a more round and delicious brown wheat vinegar.
Next, examples of the present invention will be described.
[0016]
【Example】
1 ton of brown rice was steamed, inoculated with a seed black koji mold, and made with aeration for 2 days to produce brown rice koji.
In addition, 1 ton of brown wheat was steamed, inoculated with a seed black koji mold, and made with aeration for 2 days to produce brown wheat koji.
[0017]
750 kg of brown rice koji and 750 kg of brown barley koji were put into a 4 t tank so as to be mixed. Water is added from above, water is poured into the 4t tank until the 7th minute, steam is blown from the bottom, the whole is heated to 30-35 ° C while stirring the koji, saccharification is started, and occasionally padded for about 2 weeks. It was stirred into.
[0018]
Two weeks later, acid-resistant seed yeast was added to the tank, a paddle was added, and the mixture was stirred to confirm the presence of carbon dioxide gas bubbles at the start of alcohol fermentation. A carbon dioxide concentrator is set below the liquid level, and then the acetic acid fermentation solution produced in another tank is added together with the pellicle to an amount of 1% acidity (about 2% for a 5% acetic acid solution). the addition of split) was added to initiate the acetic acid fermentation.
[0019]
Immediately make acetic acid bacteria film on the entire surface, but only the central portion is as the round holes pellicles are corrupted by blowing up of the carbon dioxide gas bubbles due to the persistence of alcoholic fermentation open, long carbon dioxide bubbles were observed.
[0020]
Acetic acid fermentation when the alcohol is lowered to 0.2% in about 3 months, the pellicle was separated whole was terminated.
The bacteria film was separated and allowed to stand as it is about three months, and aged.
Then, successively put into a bag squeezed the whole mash, loading the boat, over the water pressure to obtain a slowly squeezed crude barley brown rice vinegar.
Crude barley brown rice vinegar obtained was allowed to stand for about one year, aged, were shipped.
[0021]
【The invention's effect】
In the present invention, brown wheat and brown rice are used as raw materials, and saccharification, alcohol fermentation, and acetic acid fermentation are performed in parallel to produce a mild vinegar in which a large amount of the biologically active ingredients of brown wheat and brown rice are eluted. We were able to.

Claims (5)

玄麦麹と玄米麹からなる発酵原料をタンクに入れ、水を加えて、糖化を開始し、次いで耐酸性種酵母を添加し、アルコール発酵を開始し、次いでアルコール含有液は通すが、炭酸ガス気泡は通さず、一ヶ所に集め開放する炭酸ガス集中装置を発酵液中に設置し、次に種酢酸菌を添加し、アルコール発酵による炭酸ガス気泡を一ヶ所に集め、そこから逃し、気泡が逃げるところ以外の表面の酢酸菌膜を保持しつつ、糖化、アルコール発酵及び酢酸発酵の3者並行複発酵を行なうことを特徴とする玄麦玄米酢の製造方法。Put the fermented raw material consisting of brown wheat koji and brown rice koji into a tank, add water, start saccharification, then add acid-resistant seed yeast, start alcohol fermentation, and then pass the alcohol-containing liquid, but carbon dioxide gas bubbles Install a carbon dioxide concentration device that collects and opens in one place in the fermentation liquid, then adds seed acetic acid bacteria, collects carbon dioxide bubbles from alcohol fermentation in one place, escapes from there, and escapes the bubbles A method for producing brown barley vinegar, which comprises performing three-sided parallel fermentation of saccharification, alcohol fermentation, and acetic acid fermentation while retaining the acetic acid bacterium membrane on the other surface. 玄麦麹の玄麦が、玄小麦、玄大麦、玄燕麦、玄ハト麦から選ばれた1以上であることを特徴とする請求項1に記載の玄麦玄米酢の製造方法。The method for producing brown wheat vinegar according to claim 1, wherein the brown wheat of brown wheat koji is at least one selected from brown wheat, brown barley, brown oat, and brown pigeon barley. 玄小麦、玄大麦、玄燕麦、玄ハト麦から選ばれた1以上の表皮部分を一緒に使用するものであることを特徴とする請求項1に記載の玄麦玄米酢の製造方法。The method for producing brown wheat vinegar according to claim 1, wherein at least one skin portion selected from brown wheat, brown barley, brown oat, and brown pigeon is used together. 胚芽、糠、脱脂糠から選ばれた1以上を一緒に使用するものであることを特徴とする請求項1に記載の玄麦玄米酢の製造方法。The method for producing brown barley brown rice vinegar according to claim 1, wherein one or more selected from germ, bran, and defatted bran are used together. 炭酸ガス気泡を一ヶ所に集めることが、アルコール含有液は通すが、炭酸ガス気泡は通さない金網などで作り、一ヶ所を開放した台円錐体の炭酸ガス集中装置を設置して行なわれることを特徴とする請求項1に記載の玄麦玄米酢の製造方法。Collecting carbon dioxide gas bubbles in one place is performed by using a wire mesh that allows the alcohol-containing liquid to pass through but does not pass carbon dioxide gas bubbles, and installs a trapezoidal cone-shaped carbon dioxide concentration device with one place open. The method for producing brown barley brown rice vinegar according to claim 1.
JP2000183027A 2000-06-19 2000-06-19 Production method of brown wheat vinegar Expired - Fee Related JP3558967B2 (en)

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KR101245930B1 (en) 2011-05-06 2013-03-21 순천대학교 산학협력단 The manufacturing method of salicornia herbacea vinegar using unpolished rice
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CN112980646B (en) * 2021-03-01 2022-05-13 山西农业大学 Kefir source composite probiotic fermented pear juice and oat viable bacteria vinegar drink and preparation method thereof

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