JP3506033B2 - Method of manufacturing hot-rolled steel bars or wires - Google Patents

Method of manufacturing hot-rolled steel bars or wires

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Publication number
JP3506033B2
JP3506033B2 JP06217799A JP6217799A JP3506033B2 JP 3506033 B2 JP3506033 B2 JP 3506033B2 JP 06217799 A JP06217799 A JP 06217799A JP 6217799 A JP6217799 A JP 6217799A JP 3506033 B2 JP3506033 B2 JP 3506033B2
Authority
JP
Japan
Prior art keywords
rolled
rolling
surface temperature
finish rolling
phase
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP06217799A
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Japanese (ja)
Other versions
JP2000256741A (en
Inventor
豊 根石
浩一 黒田
健一 河添
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nippon Steel Corp
Original Assignee
Sumitomo Metal Industries Ltd
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Filing date
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Priority to JP06217799A priority Critical patent/JP3506033B2/en
Publication of JP2000256741A publication Critical patent/JP2000256741A/en
Application granted granted Critical
Publication of JP3506033B2 publication Critical patent/JP3506033B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【発明の属する技術分野】本発明は、多スタンドの粗圧
延列と中間圧延列および仕上げ圧延列からなる圧延機を
用いた熱間圧延による棒鋼や線材(以下、棒・線材とも
いう)の製造方法に係わり、より詳しくは、表層部が球
状の炭化物が均一に分散した球状組織、その他の部分が
微細な軟質組織で、しかも表層部に脱炭相からなる異常
組織のない熱間圧延棒・線材を高能率に製造することが
可能な方法に関する。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to the production of steel bars and wire rods (hereinafter also referred to as "bars / wire rods") by hot rolling using a rolling mill consisting of a multi-stand rough rolling row, intermediate rolling row and finish rolling row. Related to the method, in more detail, the surface layer has a spherical structure in which spherical carbides are uniformly dispersed, the other part has a fine soft structure, and the surface layer part is a hot-rolled bar with no abnormal structure composed of a decarburized phase. The present invention relates to a method capable of manufacturing a wire rod with high efficiency.

【0002】[0002]

【従来の技術】熱間圧延で製造されたJIS G 3502に規定
されるピアノ線材、同G 3507に規定される冷間圧造用炭
素鋼線材、さらには同G 4051,同G 4104、同G 4105など
に規定される機械構造用炭素鋼と合金鋼、同G 4805に規
定される軸受鋼、同G 4801に規定されるばね鋼および同
G 4401、同G 4401などに規定される工具鋼などを母材と
する棒・線材は、2次加工、3次加工と称される伸線、
引抜き、切断、鍛造、切削などの冷間での加工工程を経
て所要の製品に仕上げられる。
2. Description of the Related Art Piano wire rods specified by JIS G 3502 manufactured by hot rolling, carbon steel wire rods for cold heading specified by G 3507, G 4051, G 4104, G 4105. Machine structural carbon steels and alloy steels, G4805 bearing steels, G4801 spring steels, and alloy steels
Bars and wire rods that use G 4401, G 4401, etc. as the base material for tool steel are wire-drawing called secondary processing and tertiary processing,
The required products are finished through cold working processes such as drawing, cutting, forging, and cutting.

【0003】しかし、上記の熱間圧延されたままの棒・
線材の多くは、通常、その組織中にパーライト相、べー
ナイト相あるいはマルテンサイト相といった硬質相を有
し、冷間加工性が劣る。したがって、これらの棒・線材
の製造時には、熱間圧延後に焼鈍や球状化などの軟化熱
処理を施して強度を下げることで延性を高め、冷間加工
性を向上させる方法が採られてきた。
However, the above-mentioned hot-rolled bar
Most of the wire rods usually have a hard phase such as a pearlite phase, a bainite phase or a martensite phase in their structure, and are inferior in cold workability. Therefore, at the time of manufacturing these rods / wires, there has been adopted a method of enhancing the ductility by lowering the strength by performing a softening heat treatment such as annealing or spheroidizing after hot rolling to improve the cold workability.

【0004】ところが、上記の軟化熱処理には、10〜
20時間という長時間を必要とすることが多い。このた
め、生産性の向上や省エネルギーの観点から、熱処理の
時間短縮や工程省略が可能な方法の開発が強く望まれよ
うになってきた。
However, the above softening heat treatment requires 10 to
It often requires a long time of 20 hours. Therefore, from the viewpoint of improving productivity and saving energy, it has been strongly desired to develop a method capable of shortening the heat treatment time and omitting the steps.

【0005】そこで、棒・線材の連続熱間圧延時におけ
る圧延条件や冷却条件を種々調整して圧延組織を変化さ
せ、熱間圧延のままで軟化組織を得る方法や熱処理時間
の短縮化を可能にした方法が種々提案されている(例え
ば、特開昭56−41325号公報、同60−2559
22号公報、同62−139817号公報、同64−5
5330号公報、特開平4−173921号公報)。
Therefore, it is possible to change the rolling structure by variously adjusting the rolling conditions and the cooling conditions during the continuous hot rolling of the rod / wire and to obtain the softened structure as it is in the hot rolling or to shorten the heat treatment time. Various methods have been proposed (for example, JP-A-56-41325 and JP-A-60-2559).
No. 22, gazette 62-139817, gazette 64-5.
5330, JP-A-4-173921).

【0006】すなわち、上記各公報のうち、特開昭56
−41325号公報に示される方法は、熱間圧延後の調
整冷却段階において、線材を700〜850℃に急冷す
る工程、この急冷工程時における過冷防止と復熱による
再結晶の進行を完了させるために700〜775℃まで
保持または冷却速度5℃/秒以下で冷却する工程、パー
ライト相のラメラ間隔の粗大化とフェライト相中の過飽
和炭素の平衡状態への移行を図るために600〜675
℃まで冷却速度0.025〜0.25℃/秒で冷却した
後に任意な冷却速度で急冷する工程を連続して行い、そ
の際熱間圧延は圧延直後の線材温度を900℃以下にす
るのがよいとする方法である。この方法によれば、確か
に、熱間圧延のままで軟化組織を有する線材が得られ
る。しかし、この方法では、調整冷却の終了間際に、6
00〜675℃の温度範囲を0.025〜0.25℃/
秒という非常に遅い冷却速度で冷却を行うので、材料の
表層部に脱炭相が発生するのを避けることができず、表
層部に異常組織を有する製品しか得られないという欠点
を有している。
That is, of the above publications, Japanese Patent Laid-Open No.
The method disclosed in JP-A-41325 completes a step of rapidly cooling a wire rod to 700 to 850 ° C. in a controlled cooling stage after hot rolling, prevention of overcooling in this rapid cooling step, and progress of recrystallization by reheat. In order to maintain the temperature at 700 to 775 ° C or to cool at a cooling rate of 5 ° C / sec or less, 600 to 675 in order to coarsen the lamellar spacing of the pearlite phase and shift the supersaturated carbon in the ferrite phase to the equilibrium state.
The process of cooling at a cooling rate of 0.025 to 0.25 ° C./sec to the temperature of 0 ° C. and then rapidly cooling at an arbitrary cooling rate is continuously performed. At that time, the temperature of the wire rod immediately after rolling is set to 900 ° C. or less. Is a good method. According to this method, it is possible to obtain a wire rod having a softened structure as hot rolled. However, in this method, the
The temperature range of 00 to 675 ° C is 0.025 to 0.25 ° C /
Since the cooling is performed at a very slow cooling rate of 2 seconds, it is unavoidable that a decarburization phase occurs in the surface layer of the material, and there is a drawback that only a product with an abnormal structure in the surface layer can be obtained. There is.

【0007】特開昭60−255922号公報に示され
る方法は、仕上げ圧延を2つに分けて行い、第1仕上げ
圧延後の線材を500℃を超え850℃以下に急冷した
後、第2仕上げ圧延を施して20〜80%の塑性歪みを
付与し、その塑性歪みを保持したまま冷却速度1〜10
℃/秒で冷却する方法である。この方法によれば、確か
に、微細分散した初析フェライト相中に微細なパーライ
ト相またはベイナイト相が混在した組織の線材が得ら
れ、熱間圧延後における球状化熱処理に要する時間を短
縮することが可能である。しかし、この方法は、鋼がC
r、Mo、NiおよびMnなどを多く含む焼入性の高い
合金鋼(例えばSCM430やSCM440など)の場
合、硬質相であるベイナイト相が多く存在するため、圧
延のままの引張強さが非常に高く軟質化が困難であり、
圧延のままでの伸線加工が困難な製品しか得られないと
いう欠点を有している。
In the method disclosed in Japanese Patent Laid-Open No. 60-255922, finish rolling is performed in two steps, and the wire rod after the first finish rolling is rapidly cooled to more than 500 ° C. and 850 ° C. or less and then to the second finish. Rolling is applied to give a plastic strain of 20 to 80%, and the cooling rate is 1 to 10 while maintaining the plastic strain.
This is a method of cooling at ° C / sec. According to this method, it is possible to obtain a wire having a structure in which fine pearlite phase or bainite phase is mixed in the finely dispersed proeutectoid ferrite phase, and to reduce the time required for spheroidizing heat treatment after hot rolling. Is possible. However, this method
In the case of alloy steels containing a large amount of r, Mo, Ni, Mn and the like and having high hardenability (for example, SCM430 and SCM440), since there are many bainite phases that are hard phases, the tensile strength as rolled is very high. High and difficult to soften,
It has the drawback that only products that are difficult to draw in the as-rolled state can be obtained.

【0008】特開昭62−139817号公報に示され
る方法は、仕上げ圧延を650〜850℃で開始する一
方、950℃未満で終了し、圧延終了後直ちに650〜
750℃に急冷して非同心円状に捲き取り、その後冷却
速度0.5℃/秒以上で500℃まで冷却する方法であ
る。この方法によれば、確かに、微細なフェライト相と
パーライト相の混合組織の線材が得られ、熱間圧延後に
おける球状化熱処理に要する時間を短縮することが可能
である。しかし、この方法は、鋼が上記と同じ焼入性の
高い合金鋼の場合、冷却速度0.5℃/秒以上で冷却す
ると、硬質相であるベイナイト相やマルテンサイト相が
生成するために、微細なフェライト相とパーライト相の
混合組織にはならず、上記の場合と同様に、圧延のまま
の引張強さが非常に高く軟質化は困難であり、圧延のま
までの伸線加工が困難な製品しか得られないという欠点
を有している。
In the method disclosed in Japanese Patent Laid-Open No. 62-139817, finish rolling is started at 650 to 850 ° C., while finish rolling is completed at less than 950 ° C.
It is a method in which it is rapidly cooled to 750 ° C., wound into a non-concentric shape, and then cooled to 500 ° C. at a cooling rate of 0.5 ° C./sec or more. According to this method, it is possible to obtain a wire having a mixed structure of fine ferrite phase and pearlite phase, and it is possible to shorten the time required for the spheroidizing heat treatment after hot rolling. However, in this method, when the steel is an alloy steel having the same high hardenability as described above, when cooled at a cooling rate of 0.5 ° C./sec or more, a bainite phase and a martensite phase, which are hard phases, are generated, It does not form a fine microstructure of ferrite and pearlite phases, and as in the case above, the tensile strength as rolled is extremely high and it is difficult to soften it, making it difficult to perform wire drawing as rolled. It has the drawback that only good products can be obtained.

【0009】特開昭64−55330号公報に示される
方法は、素材鋼片をAc3点以上またはAccm 点以上に加
熱して熱間圧延を施す一方、少なくとも仕上げ圧延段階
においてオーステナイト未再結晶域で加工率10〜80
%の圧延を行った後、冷却速度1.5〜100℃/秒で
Ms点直上の温度域まで冷却する方法である。この方法
によれば、確かに、熱間圧延後の球状化熱処理に要する
時間を短縮することが可能である。しかし、この方法
も、鋼が焼入性の高い合金鋼の場合、仕上げ圧延後の冷
却が極めて速いために、硬質相であるベイナイトやマル
テンサイト組織が生成し、微細なフェライト相とパーラ
イト相の混合組織にはならず、圧延のままの引張強さが
非常に高くて軟質化が困難で、圧延のままでの伸線加工
が困難な製品しか得られないという欠点を有している。
In the method disclosed in Japanese Patent Laid-Open No. 64-55330, the material steel slab is heated to an Ac 3 point or more or an Ac cm point or more and hot-rolled, while at least a finish rolling stage is performed in an austenite unrecrystallized region. With a processing rate of 10-80
%, And then cooling to a temperature range just above the Ms point at a cooling rate of 1.5 to 100 ° C./sec. According to this method, it is possible to shorten the time required for the spheroidizing heat treatment after hot rolling. However, also in this method, when the steel is an alloy steel having high hardenability, the cooling after finish rolling is extremely fast, so that a bainite or martensite structure that is a hard phase is generated, and a fine ferrite phase and a pearlite phase are formed. It has a drawback that it does not form a mixed structure, has a very high tensile strength as rolled, is difficult to soften, and only a product that is difficult to wire-draw as rolled is obtained.

【0010】特開平4−173921号公報に示される
方法は、素材鋼片をAc1点〜Acm点またはAc3点以下に
1分〜20時間未満保持する第1加熱と、Acm点または
Ac3点〜1050℃未満に加熱して未溶解炭化物とオー
ステナイト相の混合組織にする第2加熱の2工程に分け
て加熱する一方、仕上げ圧延をAr3点またはArcm 点〜
Ac3点またはAcm点の温度域にて30%以上の加工を加
えて終了した後、660〜740℃に30分以上保持す
るか、または圧延終了温度から650℃までを冷却速度
100℃/h未満で冷却する方法である。この方法によ
れば、確かに、熱間圧延のままで球状組織を有する線材
が得られ、かつ熱間圧延後の熱処理に要する時間を短縮
したり熱処理そのものを省略することも可能である。し
かし、この方法は、仕上げ圧延後の線材を、660〜7
40℃の温度域に長時間保持するので、材料の表層部に
脱炭相が発生するのを避けることができず、表層部に異
常組織を有する製品しか得られないという欠点を有して
いる。また、熱間圧延のままで2次加工に供した場合、
2次加工において最終的に必要とされる球状組織を得る
には、通常の熱処理に要する以上の時間が必要となる場
合があるという欠点も有している。
In the method disclosed in Japanese Patent Laid-Open No. 4-173921, the first heating for keeping the raw steel billet at the Ac 1 point to the Acm point or the Ac 3 point or less for 1 minute to less than 20 hours and the Acm point or the Ac 3 point. Point to less than 1050 ° C. and heating in two steps of the second heating to form a mixed structure of undissolved carbide and austenite phase, while finish rolling is performed at the Ar 3 point or the Arcm point
After finishing by adding 30% or more of processing in the temperature range of Ac 3 points or A cm points, hold at 660 to 740 ° C for 30 minutes or more, or from the rolling end temperature to 650 ° C at a cooling rate of 100 ° C / h. It is a method of cooling at less than. According to this method, it is possible to obtain a wire rod having a spherical structure as it is while hot rolling, and it is possible to shorten the time required for heat treatment after hot rolling or omit the heat treatment itself. However, in this method, the wire rod after finish rolling is 660 to 7
Since it is kept in the temperature range of 40 ° C. for a long time, it is inevitable that a decarburization phase occurs in the surface layer of the material, and only a product having an abnormal structure in the surface layer can be obtained. . Also, when subjected to secondary processing as hot rolling,
There is also a drawback that in order to obtain the spherical structure finally required in the secondary processing, it may take more time than usual heat treatment.

【0011】[0011]

【発明が解決しようとする課題】本発明の目的は、表層
部が球状の炭化物が均一に分散した球状組織、その他の
部分が微細な軟質組織で、しかも表層部に脱炭相からな
る異常組織のない熱間圧延棒鋼または線材を高能率に製
造することが可能、具体値に熱間圧延後における熱処理
に要する時間が短くてすむ方法を提供することにある。
The object of the present invention is to provide a spherical structure in which spherical carbides are uniformly dispersed in the surface layer portion, a fine soft structure in the other portion, and an abnormal structure composed of a decarburized phase in the surface layer portion. It is an object of the present invention to provide a method capable of producing a hot-rolled steel bar or a wire rod without a high efficiency with a high efficiency and requiring a short time for heat treatment after the hot-rolling to a specific value.

【0012】[0012]

【課題を解決するための手段】本発明の要旨は、次の熱
間圧延棒鋼または線材の製造方法にある。
The gist of the present invention resides in the following method for producing a hot rolled steel bar or wire rod.

【0013】下記〜の条件で順次処理することを特
徴とする熱間圧延棒鋼または線材の製造方法。
A method for producing a hot-rolled steel bar or a wire rod, which is characterized in that the treatments are sequentially performed under the following conditions.

【0014】素材鋼片を900〜1250℃に加熱す
る。
The raw steel billet is heated to 900 to 1250 ° C.

【0015】多スタンドの粗圧延列と中間圧延列およ
び仕上げ圧延列からなる圧延機の中間圧延列の最終スタ
ンドにおける圧延を、被圧延材の表面温度700〜90
0℃、減面率20%以上で行う。
The surface temperature of the material to be rolled is 700 to 90 at the final stand of the intermediate rolling train of the rolling mill consisting of the rough rolling train, the intermediate rolling train and the finishing rolling train of multiple stands.
It is performed at 0 ° C. and a reduction rate of 20% or more.

【0016】仕上げ圧延前に、被圧延材の表面温度が
Ms点以下になるように冷却速度5℃/秒以上で冷却す
る強制冷却処理を少なくとも1回行う。
Before the finish rolling, a forced cooling treatment is performed at least once so that the surface temperature of the material to be rolled is kept at the Ms point or lower at a cooling rate of 5 ° C./sec or more.

【0017】前記強制冷却処理後の被圧延材の表面温
度が被圧延材内部の保有熱により上昇して650〜75
0℃になった後、または加熱速度5℃/秒以上で加熱し
てその表面温度を650〜750℃にした後、直ちに減
面率5%以上で仕上げ圧延を行う。
The surface temperature of the material to be rolled after the forced cooling is increased by the heat retained inside the material to be rolled to 650 to 75.
After reaching 0 ° C. or after heating at a heating rate of 5 ° C./sec or more to bring the surface temperature to 650 to 750 ° C., immediately finish rolling is performed at a surface reduction rate of 5% or more.

【0018】仕上げ圧延後の被圧延材を、その表面温
度650〜750℃の温度範囲内に少なくとも5分間保
持した後、大気冷却する。
The material to be rolled after finish rolling is kept in the temperature range of 650 to 750 ° C. for at least 5 minutes and then cooled to the atmosphere.

【0019】また、上記の本発明においては、素材鋼片
には、重量%で、C:0.01〜1.2%、Si:0.
01〜2%、Mn:0.01〜2%、Al:0.001
〜0.1%、Cr:0〜2%、Mo:0〜0.6%、C
u:0〜2%、Ni:0〜4%、Ti:0〜0.1%、
N:0〜0.03%、V:0〜0.4%、Nb:0〜
0.15%、B:0〜0.005%、S:0〜0.1
%、Pb:0〜0.35%、Ca:0〜0.01%を含
有し、残部がFeおよび不可避的不純物からなり、不純
物中のPが0.05%以下の化学組成を有する鋼を用い
るのが好ましい。
Further, in the above-mentioned present invention, in the material steel billet, C: 0.01-1.2%, Si: 0.
01 to 2%, Mn: 0.01 to 2%, Al: 0.001
~ 0.1%, Cr: 0-2%, Mo: 0-0.6%, C
u: 0 to 2%, Ni: 0 to 4%, Ti: 0 to 0.1%,
N: 0 to 0.03%, V: 0 to 0.4%, Nb: 0
0.15%, B: 0 to 0.005%, S: 0 to 0.1
%, Pb: 0 to 0.35%, Ca: 0 to 0.01%, the balance Fe and unavoidable impurities, and P in the impurities has a chemical composition of 0.05% or less. It is preferably used.

【0020】上記の本発明は、下記の知見に基づいて完
成させた。すなわち、本発明者らは、上記の従来方法よ
りも熱間圧延後における熱処理に要する時間が短くで
き、しかも表層部が球状の炭化物が均一に分散した球状
組織、その他の部分が微細な軟質組織で、かつ表層部に
脱炭相からなる異常組織のない熱間圧延棒・線材を得る
ための製造条件の究明に努めた結果、次のことを知見し
た。
The present invention described above was completed based on the following findings. That is, the present inventors can shorten the time required for heat treatment after hot rolling than the above-mentioned conventional method, and the surface layer portion has a spherical structure in which spherical carbides are uniformly dispersed, and other portions have a fine soft structure. In addition, as a result of efforts to investigate the manufacturing conditions for obtaining the hot-rolled bar / wire having an abnormal structure composed of the decarburized phase in the surface layer, the following was found.

【0021】仕上げ圧延前の被圧延材に、その表面温度
がMs以下になるまで冷却速度5℃/秒以上で冷却する
強制冷却処理を少なくとも1回施すとともに、この強制
冷却処理後の被圧延材の表面温度が650〜750℃に
なってから減面率5%で仕上げ圧延を施し、仕上げ圧延
後の被圧延材をその表面温度650〜750℃の温度域
に5分以上保持する。その場合には、被圧延材内部の組
織がフェライト相とパーライト相の混合組織であるにも
かかわらず、球状炭化物の生成が促進され、熱間圧延後
における熱処理時間を短かくしても、表層部が球状の炭
化物が均一に分散した球状組織、その他の部分が微細な
軟質組織で、しかも表層部に脱炭相からなる異常組織の
ない所望の製品が得られる。
The material to be rolled before finish rolling is subjected to at least one forced cooling treatment for cooling it at a cooling rate of 5 ° C./sec or more until the surface temperature thereof becomes equal to or lower than Ms, and the material to be rolled after this forced cooling treatment. After the surface temperature of the steel sheet reaches 650 to 750 ° C, finish rolling is performed at a surface reduction rate of 5%, and the material to be rolled after the finish rolling is held in the temperature range of the surface temperature of 650 to 750 ° C for 5 minutes or more. In that case, even though the structure inside the material to be rolled is a mixed structure of ferrite phase and pearlite phase, the formation of spherical carbides is promoted, and even if the heat treatment time after hot rolling is shortened, the surface layer portion is It is possible to obtain a desired product having a spherical structure in which spherical carbides are uniformly dispersed, a fine soft structure in the other portions, and having no abnormal structure composed of a decarburized phase in the surface layer.

【0022】ただし、素材鋼片を1250℃を超えて加
熱した場合には、製品の表層部で脱炭が生じる。また、
圧延機の中間列の最終スタンドにおける圧延時の被圧延
材の表面温度が700℃未満または900℃超、かつ減
面率20%未満の場合には、その後、上記のMs点以下
への強制冷却処理や650〜750℃への復熱または加
熱処理などを施しても、製品の内部組織がマルテンサイ
ト相やベイナイト相などの硬質の低温変態相からなる過
冷却組織になり、均一な軟化組織が安定して得られない
場合がある。
However, when the raw steel billet is heated above 1250 ° C., decarburization occurs at the surface layer of the product. Also,
When the surface temperature of the material to be rolled at the final stand in the middle row of the rolling mill is less than 700 ° C or more than 900 ° C and the surface reduction rate is less than 20%, thereafter, forced cooling to the Ms point or less is performed. Even if heat treatment or reheat to 650 to 750 ° C. or heat treatment is performed, the internal structure of the product becomes a supercooled structure composed of a hard low-temperature transformation phase such as a martensite phase or a bainite phase, and a uniform softened structure is obtained. It may not be possible to obtain stable results.

【0023】[0023]

【発明の実施の形態】以下、本発明の各工程における処
理条件を、上記のように定めた理由について詳しく説明
する。
BEST MODE FOR CARRYING OUT THE INVENTION The reason why the processing conditions in each step of the present invention are set as above will be described in detail below.

【0024】素材鋼片の加熱温度:加熱温度が900℃
未満では、圧延機に対する負荷が大きくなる。また、鋼
片断面内の温度を均一に加熱するのに長時間かかり、生
産性が低下するだけでなく、圧延時に割れが発生するこ
とがある。一方、1250℃を超えて加熱すると、加熱
中の脱炭量が急激に増加し、製品線材の表層部で脱炭が
発生するのを防げなくなることがある。したがって、素
材鋼片の加熱温度は、900〜1250℃とした。
Heating temperature of the raw steel billet: The heating temperature is 900 ° C.
When it is less than 1, the load on the rolling mill becomes large. Further, it takes a long time to uniformly heat the temperature in the cross section of the billet, which not only lowers the productivity but also causes cracks during rolling. On the other hand, if the temperature is higher than 1250 ° C, the amount of decarburization during heating may increase rapidly, and it may be impossible to prevent decarburization from occurring in the surface layer of the product wire. Therefore, the heating temperature of the raw steel billet is set to 900 to 1250 ° C.

【0025】中間圧延列の最終スタンドにおける圧延:
中間圧延列の最終スタンドでの圧延時における被圧延材
の表面温度が700℃未満であると、圧延機に対する負
荷が大きくなるだけでなく、圧延時に割れが発生するこ
とがある。一方、上記の表面温度が900℃を超える
と、仕上げ圧延入側での結晶粒度が粗くなりすぎて目的
とする微細な軟質組織が得られにくい。さらに、減面率
が20%未満であると、目的とする微細な軟質組織が得
られにくい。したがって、圧延機の中間列の最終スタン
ドにおける圧延は、被圧延材の表面温度700〜900
℃、減面率20%以上とした。
Rolling in the last stand of the intermediate rolling train:
If the surface temperature of the material to be rolled during rolling in the final stand of the intermediate rolling row is lower than 700 ° C, not only the load on the rolling mill becomes large, but also cracks may occur during rolling. On the other hand, when the surface temperature exceeds 900 ° C., the grain size on the entry side of the finish rolling becomes too coarse, and it is difficult to obtain the desired fine soft structure. Furthermore, if the area reduction rate is less than 20%, it is difficult to obtain the desired fine soft tissue. Therefore, the rolling at the final stand in the middle row of the rolling mill is performed at the surface temperature of the rolled material of 700 to 900.
C, and the area reduction rate was 20% or more.

【0026】なお、減面率は高ければ高いほどよく、そ
の上限は特に定める必要はないが、40%を超えると、
仕上げ圧延において要求される寸法精度の製品線材に仕
上げることが難しくなるので、その上限は40%とする
のがよい。
The higher the surface reduction rate, the better. The upper limit need not be specified, but if it exceeds 40%,
Since it is difficult to finish a product wire rod having the required dimensional accuracy in finish rolling, the upper limit is preferably 40%.

【0027】仕上げ圧延前における冷却と復熱処理:本
発明においては、上記圧延機の中間列の最終スタンドに
よる圧延後の被圧延材を5℃/秒以上の冷却速度で冷却
し、その表面温度をMs点以下にまで下げる強制冷却処
理を少なくとも1回行い、この強制冷却処理後の被圧延
材の表面温度がその内部保有熱によって650〜750
℃に復熱してから直ちに仕上げ圧延を行う。
Cooling and reheat treatment before finish rolling: In the present invention, the material to be rolled after rolling by the final stand in the middle row of the rolling mill is cooled at a cooling rate of 5 ° C./sec or more and its surface temperature is The forced cooling treatment for lowering the temperature to below the Ms point is performed at least once, and the surface temperature of the material to be rolled after this forced cooling treatment is 650 to 750 due to the internal heat retained therein.
After recuperating to ℃, finish rolling immediately.

【0028】このように、Ms点以下への強制冷却処理
後、表面温度が650〜750℃に復熱した被圧延材
に、後述する条件の仕上げ圧延を施す場合には、仕上げ
圧延後の被圧延材を後述の温度域に比較的短時間保持す
るだけで、熱間圧延のままで球状組織を有する製品を得
ることができる。その理由は、次のとおりである。
As described above, when the material to be rolled whose surface temperature is reheated to 650 to 750 ° C. after the forced cooling treatment to the Ms point or less is subjected to finish rolling under the conditions described later, A product having a spherical structure can be obtained as hot rolled by simply holding the rolled material in the temperature range described later for a relatively short time. The reason is as follows.

【0029】すなわち、一般的な熱間圧延中における鋼
材の組織は、通常、オーステナイト組織である。このオ
ーステナイト組織から熱履歴を変化させることで、球状
の炭化物が均一に分散した球状組織を得るには、鋼材を
Ac1変態点の近傍に数時間、具体的には最低でも2時間
保持する必要がある。これを実際の生産現場で実現する
ためには、等温長時間保持が可能な熱処理設備の導入が
必要で、設備費が嵩むほか、生産性が低下して製品の製
造コストが高くなる。
That is, the structure of the steel material during general hot rolling is usually an austenite structure. In order to obtain a spherical structure in which spherical carbides are uniformly dispersed by changing the heat history from this austenite structure, it is necessary to hold the steel material in the vicinity of the Ac 1 transformation point for several hours, specifically, at least 2 hours. There is. In order to realize this at an actual production site, it is necessary to introduce a heat treatment facility capable of holding an isothermal long period of time, which increases equipment cost and lowers productivity and increases product manufacturing cost.

【0030】ところが、熱間圧延中の鋼材をMs点以下
にまで冷却して一旦マルテンサイト組織を生成させた
後、鋼材内部の保有熱により表面温度を上記の650〜
750℃にまで復熱させると、生成したマルテンサイト
組織中のε炭化物を核にして比較的短時間に球状のθ炭
化物が生成する。熱間圧延のままで球状組織が得られる
のはそのためである。
However, after the steel material being hot-rolled is cooled to the Ms point or lower to once generate a martensitic structure, the surface temperature is kept at 650 to 650 by the heat retained inside the steel material.
When reheated to 750 ° C., spherical ε-carbide is produced in a relatively short time with ε-carbide in the produced martensite structure as a nucleus. This is why the spherical structure can be obtained by hot rolling.

【0031】ここで、強制冷却処理に際しての冷却速度
を5℃/秒以上としたのは、冷却速度が5℃/秒未満で
あると、たとえMs点以下に冷却してもマルテンサイト
変態せず、その組織がマルテンサイト組織にならない場
合があるためである。
Here, the cooling rate in the forced cooling treatment is set to 5 ° C./sec or more, because if the cooling rate is less than 5 ° C./sec, martensite transformation does not occur even if cooled below the Ms point. This is because the organization may not be a martensite organization.

【0032】上記の冷却速度は、供給水量が調整可能な
水冷装置や浴温が調整可能な塩浴槽などの適宜な冷却手
段を、上記中間圧延列の最終スタンドと仕上げ圧延列の
第1スタンドとの間に設置することで制御可能である。
For the above cooling rate, a suitable cooling means such as a water cooling device capable of adjusting the amount of supplied water or a salt bath capable of controlling the bath temperature is used for the final stand of the intermediate rolling train and the first stand of the finish rolling train. It can be controlled by installing it in between.

【0033】また、復熱後の表面温度を650〜750
℃としたのは、復熱後の表面温度が650℃未満である
と球状炭化物の生成が十分でなく、750℃を超えると
生成したマルテンサイト組織がオーステナイト組織に逆
変態しやすいためである。
The surface temperature after recuperation is set to 650 to 750.
The reason why the temperature is set to be 0 ° C is that if the surface temperature after recuperation is less than 650 ° C, the formation of spherical carbides is not sufficient, and if it exceeds 750 ° C, the formed martensite structure is likely to undergo reverse transformation to an austenite structure.

【0034】なお、強制冷却処理後の復熱処理は、鋼材
内部の保有熱による昇温を待つのではなく、誘導加熱コ
イルなどからなる加熱手段を用いて積極的に加熱昇温さ
せるようにしてもよい。この場合、仕上げ圧延への移行
時間の短縮化が図れ、生産性が向上する。
In the post-heat treatment after the forced cooling treatment, instead of waiting for the temperature rise due to the heat retained inside the steel material, the heating means such as an induction heating coil may be used to actively heat and raise the temperature. Good. In this case, the transition time to finish rolling can be shortened and productivity is improved.

【0035】ただし、加熱手段による加熱昇温時の加熱
速度は、5℃/秒以上とする必要がある。これは、加熱
速度が5℃/秒未満であると、上記の表面温度に復熱さ
せるのに要する加熱時間が長くなりすぎ仕上げ圧延への
移行時間の短縮化が図れなくなり、逆に中間圧延列の最
終スタンドと仕上げ圧延列の第1スタンドとの間隔が長
大な設備レイアウトにする必要が生じ、設備費が嵩んで
製品の製造コスト上昇を招くようになるためである。
However, the heating rate at the time of heating by the heating means must be 5 ° C./sec or more. This is because if the heating rate is less than 5 ° C / sec, the heating time required to reheat to the above surface temperature becomes too long and the transition time to finish rolling cannot be shortened. This is because it is necessary to make the equipment layout in which the distance between the last stand and the first stand of the finish rolling row is long, which increases the equipment cost and increases the manufacturing cost of the product.

【0036】以上の理由から、本発明では、圧延機の中
間圧延列の最終スタンドによる圧延後の被圧延材を、そ
の表面温度がMs点以下になるまで5℃/秒以上の冷却
速度で少なくとも1回強制冷却し、この強制冷却後の被
圧延材の表面温度が内部の保有熱によって650〜75
0℃に復熱するか、または加熱手段を用いて650〜7
50℃に加熱してから直ちに仕上げ圧延を行うこととし
た。
For the above reasons, in the present invention, the material to be rolled after being rolled by the final stand of the intermediate rolling row of the rolling mill is at least cooled at a cooling rate of 5 ° C./sec or more until the surface temperature becomes equal to or lower than the Ms point. After forced cooling once, the surface temperature of the material to be rolled after the forced cooling is 650 to 75 due to the heat retained inside.
Reheat to 0 ° C or use heating means to reach 650-7
After heating to 50 ° C., finish rolling was immediately performed.

【0037】なお、上記強制冷却処理に際しての冷却速
度は、速ければ速いほどよく、その上限は特に定める必
要がないが、300℃/秒を超えると、冷却手段として
より高能力なものが必要になり、設備費が嵩んで製品の
製造コスト上昇を招くので、その上限は300℃/秒と
するのがよい。
The higher the cooling rate in the forced cooling treatment, the better, and it is not necessary to set the upper limit. However, if it exceeds 300 ° C./second, a cooling means having a higher capacity is required. Since the equipment cost increases and the manufacturing cost of the product increases, the upper limit is preferably 300 ° C./second.

【0038】また、加熱手段による加熱昇温時の加熱速
度は速ければ速いほどよく、その上限は特に定める必要
がないが、300℃/秒を超えると、上記の冷却手段の
場合と同様に、加熱手段としてより高能力なものが必要
になり、設備費が嵩んで製品の製造コスト上昇を招くの
で、その上限は300℃/秒とするのがよい。
Further, the higher the heating rate at the time of heating by the heating means, the better, and it is not necessary to set the upper limit in particular, but if it exceeds 300 ° C./sec, as in the case of the above cooling means, Since a heating means having a higher capacity is required and the equipment cost increases and the manufacturing cost of the product increases, the upper limit is preferably set to 300 ° C./second.

【0039】仕上げ圧延:仕上げ圧延は、上記したよう
に、強制冷却後の被圧延材の表面温度が650〜750
℃に復熱するか、または加熱手段を用いて650〜75
0℃に加熱してか直ちに行う。しかし、その際の減面率
が5%未満であると、仕上げ圧延によって付与される歪
みが小さすぎて細粒化が不十分なために球状炭化物が十
分に生成せず、圧延終了後における熱処理時間の短縮化
が図れない。したがって、仕上げ圧延は、減面率5%以
上で行うこととした。
Finish rolling: In finish rolling, as described above, the surface temperature of the material to be rolled after forced cooling is 650 to 750.
Reheat to ℃ or using heating means 650-75
Heat to 0 ° C or immediately. However, if the area reduction rate at that time is less than 5%, the strain imparted by the finish rolling is too small and the grain refinement is insufficient, so that spherical carbides are not sufficiently generated, and the heat treatment after the rolling is finished. The time cannot be shortened. Therefore, the finish rolling is performed at a surface reduction rate of 5% or more.

【0040】なお、仕上げ圧延時の減面率は高ければ高
いほどよく、その上限は特に定める必要がないが、70
%を超えると加工発熱よって材料温度が上昇し、加工に
よって得られた微細粒が粒成長を起こして粗大化しやす
いので、その上限は70%とするのがよい。
It should be noted that the higher the area reduction rate during finish rolling is, the better it is.
%, The material temperature rises due to heat generation during processing, and the fine particles obtained by processing tend to grow and coarsen, so the upper limit is preferably 70%.

【0041】仕上げ圧延後の処理:仕上げ圧延後の被圧
延材は、その表面温度を650〜750℃の温度範囲に
維持した状態で少なくとも5分間保持する必要がある。
これは、上記の復熱処理の場合と同様に、その表面温度
が650℃未満であると球状炭化物の生成が十分でな
く、750℃を超えると生成したマルテンサイト組織が
オーステナイト組織に逆変態しやすいためである。
Treatment after finish rolling: The material to be rolled after finish rolling needs to be held for at least 5 minutes while maintaining the surface temperature in the temperature range of 650 to 750 ° C.
This is because, as in the case of the above-mentioned reheat treatment, when the surface temperature is less than 650 ° C, the formation of spherical carbides is not sufficient, and when it exceeds 750 ° C, the formed martensite structure is likely to undergo reverse transformation into an austenite structure. This is because.

【0042】また、保持時間が5分未満であると、球状
炭化物の生成が不十分であるとともに、内部組織である
オーステナイト相またはオーステナイト相とフェライト
相、パーライト相の混合組織中の未変態のオーステナイ
ト相が完全に変態せず、その後の冷却によってマルテン
サイト相やベイナイト相などの硬質の低温変態相からな
る過冷却組織になる場合があるためである。したがっ
て、仕上げ圧延後の被圧延材は、その表面温度を650
〜750℃の温度範囲に少なくとも5分間保持すること
とした。
If the holding time is less than 5 minutes, the formation of spherical carbides is insufficient, and untransformed austenite in the internal structure of the austenite phase or the mixed structure of the austenite phase and the ferrite phase and the pearlite phase is obtained. This is because the phase may not be completely transformed and a supercooled structure composed of a hard low-temperature transformation phase such as a martensite phase or a bainite phase may be formed by subsequent cooling. Therefore, the surface temperature of the rolled material after finish rolling is 650
It was decided to maintain the temperature range of ˜750 ° C. for at least 5 minutes.

【0043】なお、上記の保持時間は、長ければ長いほ
どよく、その上限は特に定める必要がないが、30分を
超えると、極めて長大なステルモアタイプのコンベアな
どからなる冷却設備が必要になるのに加え、その表面温
度を650〜750℃に保持するのに加熱装置が必要に
なり、設備費が嵩んで製品の製造コスト上昇を招くの
で、その上限は30分とするのがよい。
It should be noted that the longer the holding time is, the better it is, and it is not necessary to set the upper limit in particular, but if it exceeds 30 minutes, a cooling facility including an extremely long Stelmore type conveyor is required. In addition to this, a heating device is required to maintain the surface temperature at 650 to 750 ° C., which increases equipment costs and raises the manufacturing cost of the product. Therefore, the upper limit is preferably set to 30 minutes.

【0044】次に、上記本発明の方法において、素材鋼
片として用いて好ましい鋼について説明する。なお、以
下において「%」は「重量%」を意味する。
Next, in the above-mentioned method of the present invention, preferable steels to be used as the raw material billet will be explained. In the following, "%" means "% by weight".

【0045】本発明の方法に用いて好ましい鋼は、C:
0.01〜1.2%、Si:0.01〜2%、Mn:
0.01〜2%、Al:0.001〜0.1%を含有
し、不純物中のPが0.05%以下の炭素鋼または低合
金鋼である。
The preferred steel for use in the method of the present invention is C:
0.01-1.2%, Si: 0.01-2%, Mn:
It is a carbon steel or a low alloy steel containing 0.01 to 2% and Al: 0.001 to 0.1%, and P in impurities being 0.05% or less.

【0046】ここで、上記の低合金鋼とは、上記の成分
以外に任意添加元素として、2%以下のCr、0.6%
以下のMo、2%以下のCu、4%以下のNi、0.1
%以下のTi、0.03%以下のN、0.4%以下の
V、0.15%以下のNb、0.005%以下のB、
0.1%以下のS、0.35%以下のPbおよび0.0
1%以下のCaのうちから選ばれた1種または2種以上
を含有するFe基合金を意味する。
Here, the above-mentioned low alloy steel means, in addition to the above-mentioned components, 2% or less of Cr and 0.6% as optional addition elements.
Mo below, Cu below 2%, Ni below 4%, 0.1
% Or less Ti, 0.03% or less N, 0.4% or less V, 0.15% or less Nb, 0.005% or less B,
0.1% or less S, 0.35% or less Pb and 0.0
It means an Fe-based alloy containing one or more selected from Ca of 1% or less.

【0047】以下、各成分の含有量を上記のように定め
た理由について説明する。
The reason why the content of each component is determined as described above will be described below.

【0048】Cは最終製品の強度を確保するのに有効な
元素であるが、0.01%未満では所望の強度が確保で
きず、1.2%を超えると著しい靭性低下を招くので、
その含有量を0.01〜1.2%とした。
C is an element effective for securing the strength of the final product, but if it is less than 0.01%, the desired strength cannot be secured, and if it exceeds 1.2%, the toughness is remarkably deteriorated.
The content was 0.01 to 1.2%.

【0049】Siは溶鋼の脱酸および固溶強化による最
終製品の強度確保の目的で添加するが、0.01%未満
ではこれらの効果が十分でなく、2%を超えるとこれら
の効果が飽和し、逆に靭性低下を招くので、その含有量
を0.01〜2%とした。
Si is added for the purpose of securing the strength of the final product by deoxidizing molten steel and strengthening solid solution, but if it is less than 0.01%, these effects are not sufficient, and if it exceeds 2%, these effects saturate. On the contrary, since the toughness is lowered, the content is set to 0.01 to 2%.

【0050】Mnは鋼の焼入性を向上させ、最終製品の
強度を確保するのに有効な元素であるが、0.01%未
満ではその効果が十分でなく、2%を超えるとその効果
が飽和し、逆に靭性低下を招くので、その含有量を0.
01〜2%とした。
Mn is an element effective for improving the hardenability of steel and ensuring the strength of the final product. If it is less than 0.01%, its effect is not sufficient, and if it exceeds 2%, its effect is obtained. Is saturated and conversely leads to a decrease in toughness, so the content is set to 0.
It was set to 01 to 2%.

【0051】Alは溶鋼の脱酸および結晶粒の微細化を
目的として添加するが、0.001%未満ではこれらの
効果が十分でなく、0.1%を超えるとこれらの効果が
飽和し、逆に靭性低下を招くので、その含有量を0.0
01〜0.1%とした。
Al is added for the purpose of deoxidizing molten steel and refining crystal grains. If less than 0.001%, these effects are not sufficient, and if more than 0.1%, these effects saturate. On the contrary, since it causes toughness deterioration, its content is 0.0
It was set to 01 to 0.1%.

【0052】Pは鋼の結晶粒界や中心部に偏析して靭性
を低下させ、特に0.05%を超えると著しい靭性低下
を引き起こすので、0.05%以下とした。
P is segregated at the grain boundaries and the central part of the steel to lower the toughness, and particularly when it exceeds 0.05%, the toughness is remarkably decreased, so P is set to 0.05% or less.

【0053】Cr、Ni、MoおよびBは、いずれも、
焼入性の向上を通じて最終製品の強度を上昇させる作用
を有する元素である。このため、その効果を得たい場合
にはこれらのうちから選ばれた1種または2種以上を添
加することができる。その効果は、Crは0.3%以
上、Niは0.1%以上、Moは0.05%以上、Bは
0.0002%以上で顕著になる。しかし、Crは2
%、Niは4%、Moは0.6%、Bは0.005%を
超えて含有させると、熱間圧延のままでベイナイト、マ
ルテンサイト組織を生じて均一な軟質組織が確保できな
くなるだけでなく、製品線材の表層部に脱炭相が発生し
やすくなる。したがって、添加する場合のこれら元素の
含有量は、Crについては0.3〜2%、Niについて
は0.1〜4%、Moについては0.05〜0.6%、
Bについては0.0002〜0.005%とするのがよ
い。
Cr, Ni, Mo and B are all
It is an element that has the effect of increasing the strength of the final product through the improvement of hardenability. Therefore, in order to obtain the effect, one kind or two or more kinds selected from these can be added. The effect becomes remarkable when Cr is 0.3% or more, Ni is 0.1% or more, Mo is 0.05% or more, and B is 0.0002% or more. However, Cr is 2
%, Ni 4%, Mo 0.6%, and B more than 0.005%, bainite and martensite structures are formed in the hot rolled state, and a uniform soft structure cannot be secured. Not only that, the decarburization phase easily occurs on the surface layer of the product wire. Therefore, the content of these elements when added is 0.3 to 2% for Cr, 0.1 to 4% for Ni, 0.05 to 0.6% for Mo,
B is preferably 0.0002 to 0.005%.

【0054】Ti、Nb、VおよびNは、いずれも、結
晶粒度を調整するのに有効な元素である。このため、そ
の効果を得たい場合にはこれらのうちから選ばれた1種
または2種以上を添加することができる。その効果は、
Tiは0.002%以上、NbとVは0.005%以
上、Nは0.001%以上で顕著になる。しかし、Ti
は0.1%、Nbは0.15%、Vは0.4%、Nは
0.03%を超えて含有させると、その効果が飽和し逆
に靭性低下を招く。したがって、添加する場合のこれら
元素の含有量は、Tiについては0.002〜0.1
%、Nbについては0.005〜0.15%、Vについ
ては0.005〜0.4%、Nについては0.001〜
0.03%とするのがよい。
Ti, Nb, V and N are all effective elements for adjusting the crystal grain size. Therefore, in order to obtain the effect, one kind or two or more kinds selected from these can be added. The effect is
It becomes remarkable when Ti is 0.002% or more, Nb and V are 0.005% or more, and N is 0.001% or more. However, Ti
If 0.1%, Nb is 0.15%, V is 0.4% and N is more than 0.03%, the effect is saturated and conversely the toughness is lowered. Therefore, the content of these elements when added is 0.002 to 0.1 for Ti.
%, Nb 0.005 to 0.15%, V 0.005 to 0.4%, and N 0.001 to 0.15%.
It is good to set it to 0.03%.

【0055】Cuは靭性と焼入性を向上させるのに有効
な元素である。このため、その効果を得たい場合には添
加することができ、その効果は0.05%以上で顕著に
なる。しかし、2%を超えて含有させると、その効果は
飽和し、逆に靭性低下を招く。したがって、添加する場
合のCu含有量は、0.05〜2%とするのがよい。
Cu is an element effective for improving toughness and hardenability. Therefore, if it is desired to obtain the effect, it can be added, and the effect becomes remarkable at 0.05% or more. However, if the content exceeds 2%, the effect is saturated and, conversely, toughness is reduced. Therefore, the Cu content when added is preferably 0.05 to 2%.

【0056】S、PbおよびCaは、いずれも、被削性
を向上させるのに有効な元素である。このため、その効
果を得たい場合にはこれらのうちから選ばれた1種また
は2種以上を添加することができる。その効果は、Sと
Pbは0.05%以上、Caは0.001%以上で顕著
になる。しかし、Sは0.1%、Pbは0.35%、C
aは0.01%を超えて含有させると、その効果が飽和
し逆に靭性低下を招く。したがって、添加する場合のこ
れら元素の含有量は、Sについては0.05〜0.1
%、Pbについては0.05〜0.35%、Caについ
ては0.001〜0.01%とするのがよい。
S, Pb and Ca are all effective elements for improving machinability. Therefore, in order to obtain the effect, one kind or two or more kinds selected from these can be added. The effect becomes remarkable when S and Pb are 0.05% or more and Ca is 0.001% or more. However, S is 0.1%, Pb is 0.35%, C
If the content of a exceeds 0.01%, the effect is saturated and conversely the toughness is lowered. Therefore, the content of these elements when added is 0.05 to 0.1 for S.
%, Pb is preferably 0.05 to 0.35%, and Ca is preferably 0.001 to 0.01%.

【0057】[0057]

【実施例】表1に示す化学組成を有する3種類の鋼から
なる素材鋼片の角ビレット(140mm角、長さ10
m)を準備した。
EXAMPLE A square billet (140 mm square, length 10 mm) of a raw billet made of three kinds of steels having the chemical compositions shown in Table 1
m) was prepared.

【0058】[0058]

【表1】 [Table 1]

【0059】準備した各角ビレットは、表2に示す各条
件にて熱間圧延して外径10mmの熱間圧延線材にし
た。
The prepared square billets were hot-rolled under the conditions shown in Table 2 to obtain hot-rolled wire rods having an outer diameter of 10 mm.

【0060】得られた各線材から試験片を採取して引張
試験とミクロ観察に供し、引張強さを調べる一方、表層
部が球状組織、その他の部分が微細な軟質組織で、しか
も表層部に脱炭相からなる異常組織があるか否かを調査
し、その結果を、表2に併せて示した。なお、表2のミ
クロ組織欄に記した記号Fはフェライト相、Pはパーラ
イト相、Bはベイナイト相を意味している。
A test piece was taken from each of the obtained wire rods and subjected to a tensile test and micro observation to examine the tensile strength, while the surface layer had a spherical structure and the other parts had a fine soft structure, and the surface layer had a fine structure. It was investigated whether or not there was an abnormal structure composed of a decarburized phase, and the results are also shown in Table 2. The symbol F in the microstructure column in Table 2 means a ferrite phase, P means a pearlite phase, and B means a bainite phase.

【0061】[0061]

【表2】 [Table 2]

【0062】表2に示す結果からわかるように、本発明
の方法(試番1〜10)によった場合には、いずれも表
層部が球状組織、その他の部分が微細な軟質組織で、し
かも表層部に脱炭相からなる異常組織が存在せず、引張
強さが725MPa以下の軟質な線材が得られた。
As can be seen from the results shown in Table 2, according to the method of the present invention (trials Nos. 1 to 10), the surface layer has a spherical structure and the other parts have a fine soft structure, and A soft wire having a tensile strength of 725 MPa or less was obtained without an abnormal structure composed of a decarburized phase in the surface layer.

【0063】これに対し、圧延機の中間圧延列の最終ス
タンドにおける被圧延材の表面温度、仕上げ圧延前の強
制冷却の有無および冷却時の被圧延材の表面温度と冷却
速度、仕上げ圧延直前の被圧延材の表面温度、仕上げ圧
延での減面率、および仕上げ圧延後の被圧延材表面温度
650〜750℃での保持時間のうちのいずれか1つ以
上が本発明で規定する範囲を外れる比較例の方法(試番
11〜20)によった場合には、いずれも表層部が球状
組織ではなく、表層部に硬質相のベイナイト組織や脱炭
相からなる異常組織があるだけでなく、内部が粗大なフ
ェライト相とパーライト相の混合組織やフェライト相、
パーライト相およびベイナイト相の混合組織であった。
また、試番12、13、15、16、18および19
は、表層部にベーナイト相が生成したために、引張強さ
が異常に高く、軟質な線材は得られなかった。
On the other hand, the surface temperature of the material to be rolled in the final stand of the intermediate rolling train of the rolling mill, the presence or absence of forced cooling before finish rolling, the surface temperature and cooling rate of the material to be rolled at the time of cooling, the temperature immediately before the finish rolling. Any one or more of the surface temperature of the material to be rolled, the surface reduction rate in finish rolling, and the holding time at the surface temperature of the material to be rolled 650 to 750 ° C. after finish rolling deviates from the range specified in the present invention. In the case of using the method of the comparative example (trial numbers 11 to 20), not only the surface layer portion does not have a spherical structure, but the surface layer portion has an abnormal structure composed of a bainite structure of a hard phase and a decarburized phase, Mixed structure of ferrite phase and pearlite phase with coarse inside and ferrite phase,
It had a mixed structure of pearlite phase and bainite phase.
Also, trial numbers 12, 13, 15, 16, 18, and 19
However, since a bainite phase was generated in the surface layer, the tensile strength was abnormally high, and a soft wire could not be obtained.

【0064】[0064]

【発明の効果】本発明の方法によれば、圧延のままで、
表層部に脱炭相からなる異常組織が存在せず、表層部が
球状組織で内部が微細な軟質組織の棒鋼または線材を高
能率に製造することが可能である。
According to the method of the present invention, as-rolled,
It is possible to highly efficiently manufacture a steel bar or a wire rod having no abnormal structure composed of a decarburized phase in the surface layer part and having a spherical structure in the surface layer part and a soft structure having a fine inside.

───────────────────────────────────────────────────── フロントページの続き (51)Int.Cl.7 識別記号 FI C22C 38/58 C22C 38/58 (56)参考文献 特開 平4−173921(JP,A) 特開 平2−213416(JP,A) 特開 昭55−8484(JP,A) 特開 昭59−136423(JP,A) 特開 平1−205031(JP,A) 特開2000−256740(JP,A) (58)調査した分野(Int.Cl.7,DB名) C21D 8/06 C21D 9/52 C21D 9/573 B21B 1/16 C22C 38/00 - 38/60 ─────────────────────────────────────────────────── ─── Continuation of front page (51) Int.Cl. 7 Identification code FI C22C 38/58 C22C 38/58 (56) Reference JP-A-4-173921 (JP, A) JP-A-2-213416 (JP , A) JP 55-8484 (JP, A) JP 59-136423 (JP, A) JP 1-205031 (JP, A) JP 2000-256740 (JP, A) (58) Survey Fields (Int.Cl. 7 , DB name) C21D 8/06 C21D 9/52 C21D 9/573 B21B 1/16 C22C 38/00-38/60

Claims (2)

(57)【特許請求の範囲】(57) [Claims] 【請求項1】下記〜の条件で順次処理することを特
徴とする熱間圧延棒鋼または線材の製造方法。 素材鋼片を900〜1250℃に加熱する。 多スタンドの粗圧延列と中間圧延列および仕上げ圧延
列からなる圧延機の中間圧延列の最終スタンドにおける
圧延を、被圧延材の表面温度700〜900℃、減面率
20%以上で行う。 仕上げ圧延前に、被圧延材の表面温度がMs点以下に
なるように冷却速度5℃/秒以上で冷却する強制冷却処
理を少なくとも1回行う。 前記強制冷却処理後の被圧延材の表面温度が被圧延材
内部の保有熱により上昇して650〜750℃になった
後、または加熱手段を用いて加熱速度5℃/秒以上で加
熱してその表面温度を650〜750℃にした後、直ち
に減面率5%以上で仕上げ圧延を行う。 仕上げ圧延後の被圧延材を、その表面温度650〜7
50℃の温度範囲内に少なくとも5分間保持した後、大
気冷却する。
1. A method for producing a hot-rolled steel bar or wire rod, which is characterized in that the treatments are sequentially performed under the following conditions. The raw steel billet is heated to 900 to 1250 ° C. Rolling is performed in the final stand of the intermediate rolling train of the rolling mill including the rough rolling train, the intermediate rolling train, and the finish rolling train of multiple stands at a surface temperature of the rolled material of 700 to 900 ° C. and a reduction rate of 20% or more. Before finish rolling, a forced cooling treatment is performed at least once to cool the material to be rolled at a cooling rate of 5 ° C./sec or more so that the surface temperature of the material to be rolled is equal to or lower than the Ms point. After the surface temperature of the material to be rolled after the forced cooling treatment rises to 650 to 750 ° C. due to the heat retained inside the material to be rolled, or is heated at a heating rate of 5 ° C./second or more using a heating means. After setting the surface temperature to 650 to 750 ° C., finish rolling is immediately performed with a surface reduction rate of 5% or more. The surface temperature of the rolled material after finish rolling is 650 to 7
Hold in the temperature range of 50 ° C. for at least 5 minutes and then cool to the atmosphere.
【請求項2】素材鋼片に、重量%で、C:0.01〜
1.2%、Si:0.01〜2%、Mn:0.01〜2
%、Al:0.001〜0.1%、Cr:0〜2%、M
o:0〜0.6%、Cu:0〜2%、Ni:0〜4%、
Ti:0〜0.1%、N:0〜0.03%、V:0〜
0.4%、Nb:0〜0.15%、B:0〜0.005
%、S:0〜0.1%、Pb:0〜0.35%、Ca:
0〜0.01%を含有し、残部がFeおよび不可避的不
純物からなり、不純物中のPが0.05%以下の化学組
成を有する鋼を用いることを特徴とする請求項1に記載
の熱間圧延棒鋼または線材の製造方法。
2. The weight ratio of C: 0.01 to the raw steel billet.
1.2%, Si: 0.01 to 2%, Mn: 0.01 to 2
%, Al: 0.001 to 0.1%, Cr: 0 to 2%, M
o: 0-0.6%, Cu: 0-2%, Ni: 0-4%,
Ti: 0 to 0.1%, N: 0 to 0.03%, V: 0
0.4%, Nb: 0 to 0.15%, B: 0 to 0.005
%, S: 0 to 0.1%, Pb: 0 to 0.35%, Ca:
The steel according to claim 1, characterized in that a steel containing 0 to 0.01%, the balance being Fe and unavoidable impurities, and having a chemical composition in which P in the impurities is 0.05% or less is used. Method for producing hot rolled steel bar or wire rod.
JP06217799A 1999-03-09 1999-03-09 Method of manufacturing hot-rolled steel bars or wires Expired - Fee Related JP3506033B2 (en)

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