JP3422701B2 - Flow cell holder for particle size distribution analyzer - Google Patents

Flow cell holder for particle size distribution analyzer

Info

Publication number
JP3422701B2
JP3422701B2 JP33788698A JP33788698A JP3422701B2 JP 3422701 B2 JP3422701 B2 JP 3422701B2 JP 33788698 A JP33788698 A JP 33788698A JP 33788698 A JP33788698 A JP 33788698A JP 3422701 B2 JP3422701 B2 JP 3422701B2
Authority
JP
Japan
Prior art keywords
cell
holder
supporting
flow cell
recess
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP33788698A
Other languages
Japanese (ja)
Other versions
JP2000162118A (en
Inventor
拓司 黒住
嘉之 中嶋
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Horiba Ltd
Original Assignee
Horiba Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Horiba Ltd filed Critical Horiba Ltd
Priority to JP33788698A priority Critical patent/JP3422701B2/en
Publication of JP2000162118A publication Critical patent/JP2000162118A/en
Application granted granted Critical
Publication of JP3422701B2 publication Critical patent/JP3422701B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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  • Length Measuring Devices By Optical Means (AREA)
  • Optical Measuring Cells (AREA)
  • Investigating Or Analysing Materials By Optical Means (AREA)

Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【発明の属する技術分野】本発明は、分散媒に粒子群を
分散させた試料液が流通するフローセルを支持する粒子
径分布測定装置のフローセルホルダに関する。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a flow cell holder of a particle size distribution measuring device for supporting a flow cell in which a sample solution in which a particle group is dispersed in a dispersion medium flows.

【0002】[0002]

【従来の技術】粒子による光の回折または散乱現象を利
用した粒子径分布測定装置では、分散した試料粒子に例
えばレーザ光等を照射することによって生ずる回折光ま
たは散乱光の強度分布、つまり、回折角または散乱角と
光強度との関係を複数のセンサ素子で測定し、これにフ
ラウンホーファ回折またはミー散乱の理論に基づく演算
処理を施すことによって、試料粒子の粒度分布が算出さ
れる。
2. Description of the Related Art In a particle size distribution measuring device utilizing the diffraction or scattering phenomenon of light by particles, the intensity distribution of diffracted light or scattered light generated by irradiating dispersed sample particles with, for example, laser light The particle size distribution of the sample particles is calculated by measuring the relationship between the bending angle or the scattering angle and the light intensity with a plurality of sensor elements and performing arithmetic processing based on the Fraunhofer diffraction or Mie scattering theory.

【0003】前記粒子径分布測定装置は、例えば、図5
に示すような構成になっている。同図において、1は分
散バスで、その内部にはモータ2によって回転する攪拌
羽根3が設けられているとともに、底面4の外部には図
外の発振器によって振動する超音波振動子5が設けられ
ている。6は試料粒子を含む分散媒7を収容したタン
ク、8は分散媒供給管で、電磁弁などの開閉弁9を備
え、分散バス1の開口に開放接続されている。
The particle size distribution measuring device is, for example, as shown in FIG.
The configuration is as shown in. In the figure, reference numeral 1 is a dispersion bath, inside of which a stirring blade 3 rotated by a motor 2 is provided, and outside of a bottom surface 4 an ultrasonic transducer 5 vibrated by an oscillator (not shown) is provided. ing. 6 is a tank containing a dispersion medium 7 containing sample particles, 8 is a dispersion medium supply pipe, which is provided with an opening / closing valve 9 such as an electromagnetic valve, and is openly connected to the opening of the dispersion bath 1.

【0004】10は懸濁液が充填される角筒状のガラス
製のフローセルで、厚さが精密に加工されており、分散
バス1とは、ポンプ11,切換え弁12を備えた循環流
路13によって接続され、これらとともに懸濁液の循環
系14を構成している。15はフローセル10の一側に
設けられるレーザ光源、16はフローセル10の他側に
設けられる集光レンズで、その後方の焦点位置に検出器
17が設けられており、これらによって試料粒子による
回折/散乱光の強度分布が測定される。
Reference numeral 10 denotes a square tube-shaped glass flow cell filled with a suspension, the thickness of which is precisely processed, and the dispersion bath 1 is a circulation flow path provided with a pump 11 and a switching valve 12. They are connected by 13 and together form a suspension circulation system 14. Reference numeral 15 is a laser light source provided on one side of the flow cell 10, 16 is a condenser lens provided on the other side of the flow cell 10, and a detector 17 is provided at a focus position behind the condenser lens. The intensity distribution of scattered light is measured.

【0005】そして、従来のフローセル10のフローセ
ルホルダ18は、例えば、図6に示すような構成になっ
ている。同図において、19はベースであり、ベース1
9の上面の後端に段部20が形成され、この段部20の
両側部に透孔21が形成されている。22はセル10の
下側に設けられる下ホルダであり、上面にフローセル1
0の下面開口10aが当接する当接部23が形成され、
その周縁部に環状のOリング溝24が形成され、このO
リング溝24にOリング25が嵌入され、前記当接部2
3の両側に貫通孔26が2個ずつ並設され、下ホルダ2
2の導入孔(図示せず)に接続された導入パイプ27が
前方に導出されている。28はセル10の左,右の両側
に設けられるサイドホルダであり、側面にセル10の両
側部が当接する溝29が精密に加工され、サイドホルダ
28の上部,下部に2個ずつ螺孔30が形成されてい
る。31はセル10の上側に設けられる上ホルダであ
り、下面にセル10の上面開口10bが当接する当接部
(図示せず)が形成され、下ホルダ22と同様、当接部
の周縁部にOリング溝(図示せず)が形成され、このO
リング溝にOリング25が嵌入され、前記当接部の両側
に貫通孔26が2個ずつ並設され、上ホルダ31の排出
孔(図示せず)に接続された排出パイプ32が前方に導
出され、前記導入パイプ27および前記排出パイプ32
が前記循環流路13に接続されている。
The flow cell holder 18 of the conventional flow cell 10 has a structure as shown in FIG. 6, for example. In the figure, 19 is a base, and base 1
A step portion 20 is formed at the rear end of the upper surface of 9, and through holes 21 are formed on both side portions of the step portion 20. Reference numeral 22 denotes a lower holder provided on the lower side of the cell 10, and the flow cell 1 is provided on the upper surface.
A contact portion 23 with which the lower surface opening 10a of 0 abuts is formed,
An annular O-ring groove 24 is formed on the periphery of the O-ring groove 24.
The O-ring 25 is fitted into the ring groove 24, and the contact portion 2
Two through holes 26 are provided side by side on both sides of the lower holder 2
The introduction pipe 27 connected to the second introduction hole (not shown) is drawn out forward. Reference numeral 28 denotes side holders provided on both the left and right sides of the cell 10, and grooves 29 with which both side portions of the cell 10 contact are precisely machined on the side surface, and two screw holes 30 are provided at the upper and lower portions of the side holder 28. Are formed. Reference numeral 31 denotes an upper holder provided on the upper side of the cell 10, and a contact portion (not shown) with which the upper surface opening 10b of the cell 10 abuts is formed on the lower surface, and like the lower holder 22, a peripheral portion of the contact portion. An O-ring groove (not shown) is formed.
An O-ring 25 is fitted in the ring groove, two through holes 26 are arranged in parallel on both sides of the contact portion, and a discharge pipe 32 connected to a discharge hole (not shown) of the upper holder 31 is led out forward. The introduction pipe 27 and the discharge pipe 32.
Are connected to the circulation channel 13.

【0006】そして、セル10をホルダ18に取り付け
る場合、セル10の下面開口10aの周縁部を下ホルダ
22の当接部23に当接し、セル10の両サイドにそれ
ぞれサイドホルダ28の溝29を当接し、セル用固定ね
じ33aを、下ホルダ22の各透孔26にばね座金33
bを介して挿通し、両サイドホルダ28の螺孔30に螺
合し、Oリング25をセル10の下面開口10aの周縁
部に圧接し、下ホルダ22の上面にセル10,両サイド
ホルダ28を取り付け、つぎに、上ホルダ31の当接部
をセル10の上面開口10bの周縁部に当接し、セル用
固定ねじ33aを、上ホルダ31の各透孔26にばね座
金33bを介して挿通し、両サイドホルダ28の螺孔3
0に螺合し、Oリング25をセル10の上面開口10b
の周縁部に圧接し、両サイドホルダ28の上面に上ホル
ダ31を取り付け、セル10の両面開口10a,10b
の周縁部を気密にシールし、セル10を精度良く規定の
位置に取り付けている。そして、ホルダ18をベース1
9の段部20に載置し、ベース19の透孔21,下ホル
ダ22の貫通孔26にホルダ用固定ねじ33cを挿通
し、両サイドホルダの下部の螺孔30に螺合し、ベース
19にホルダ18を取り付ける。
When the cell 10 is attached to the holder 18, the peripheral edge of the lower surface opening 10a of the cell 10 is brought into contact with the contact portion 23 of the lower holder 22, and the grooves 29 of the side holders 28 are formed on both sides of the cell 10. Abut, and fix the cell fixing screws 33a to the through holes 26 of the lower holder 22 by the spring washers 33.
Inserted through b, screwed into the screw holes 30 of both side holders 28, the O-ring 25 is pressed against the peripheral edge of the lower surface opening 10a of the cell 10, and the cell 10 and both side holders 28 are attached to the upper surface of the lower holder 22. Then, the contact portion of the upper holder 31 is brought into contact with the peripheral portion of the upper surface opening 10b of the cell 10, and the cell fixing screw 33a is inserted into each through hole 26 of the upper holder 31 via the spring washer 33b. Then, the screw holes 3 of the both side holders 28
0 and screw the O-ring 25 to the top opening 10b of the cell 10.
The upper holder 31 is attached to the upper surfaces of both side holders 28 by pressure contact with the peripheral edges of
The peripheral edge of the cell is hermetically sealed, and the cell 10 is attached to the prescribed position with high accuracy. Then, the holder 18 is used as the base 1
The holder fixing screw 33c is inserted into the through hole 21 of the base 19 and the through hole 26 of the lower holder 22 and screwed into the screw holes 30 in the lower portions of both side holders. The holder 18 is attached to.

【0007】[0007]

【発明が解決しようとする課題】従来の前記フローセル
ホルダ18の場合、フローセル10の取り付けに際し、
複数本のセル用固定ねじ33aを使用しているため、セ
ル10のセルホルダ18への取り付け,およびセルホル
ダ18からの取り外しが困難であり、しかも、フローセ
ル10のメンテナンスを行う際、全てのセル用固定ねじ
33aを下ホルダ22,上ホルダ31および両サイドホ
ルダ28から取り外す必要があり、その作業が煩雑で、
多大の時間を要するという問題がある。また、セル10
の厚さおよび両サイドホルダ28の溝29を精密に加工
しても、セル10の厚さと両サイドホルダ28の溝29
との間に隙間が生じ、この隙間によりセル10ががたつ
く。しかも、下ホルダ22に両サイドホルダ28が左右
に少しでもずれて取り付けられたり、加工された左,右
の溝29の位置が少しでもずれていたりすると、セル1
0がひねられて割れる恐れがある。さらに、セル10と
両サイドホルダ28とのがたつき、セル10の割れを避
けようとすると、より精密な加工が必要になるという問
題がある。
In the case of the conventional flow cell holder 18, when the flow cell 10 is attached,
Since a plurality of cell fixing screws 33a are used, it is difficult to attach the cell 10 to the cell holder 18 and remove it from the cell holder 18, and further, when performing maintenance on the flow cell 10, fixing all cells. Since it is necessary to remove the screws 33a from the lower holder 22, the upper holder 31, and both side holders 28, the work is complicated,
There is a problem that it takes a lot of time. Also, the cell 10
Even if the thickness of the cell 10 and the groove 29 of both side holders 28 are precisely machined, the thickness of the cell 10 and the groove 29 of both side holders 28 are
A gap is generated between the cells 10 and, and the cell 10 rattles due to this gap. Moreover, if both side holders 28 are attached to the lower holder 22 with a slight left or right displacement, or if the positions of the processed left and right grooves 29 are slightly displaced, the cell 1
There is a risk that 0 will be twisted and cracked. Furthermore, if it is attempted to avoid the rattling of the cell 10 and both side holders 28 and the cracking of the cell 10, there is a problem that more precise processing is required.

【0008】本発明は、前記の点に留意してなされたも
のであり、その目的は、フローセルのセルホルダへの取
り付け,およびセルホルダからの取り外しを容易にし、
セルのメンテナンスを行う際の作業性を向上するととも
に、セルおよびホルダの取付誤差,加工誤差によるセル
のがたつき,割れ,歪みを防止し、セルを簡単,かつ,
精度よく正確な位置に取り付けることができる粒子径分
布測定装置のフローセルホルダを提供することにある。
The present invention has been made in view of the above points, and an object thereof is to facilitate attachment and detachment of a flow cell to and from a cell holder,
Improves workability when performing cell maintenance, and prevents rattling, cracking, and distortion of the cell due to cell and holder mounting errors and processing errors, making the cell simple and
It is an object of the present invention to provide a flow cell holder for a particle size distribution measuring device, which can be mounted in a precise position with high accuracy.

【0009】[0009]

【課題を解決するための手段】前記課題を解決するため
に、請求項1記載の粒子径分布測定装置のフローセルホ
ルダは、分散媒に粒子群を分散させた試料液が流通する
フローセルを支持するフローセルホルダに形成され,前
記セルの一側に設けられる光源と前記セルの他側に設け
られる検出器とを結ぶ光軸に対して前記セルが垂直にな
るように支持する支持面と、前記セルの他面が前記支持
面に圧接するように前記セルの一面を押圧する押圧手段
とを備えたものである。
In order to solve the above problems, a flow cell holder of a particle size distribution measuring apparatus according to claim 1 supports a flow cell in which a sample liquid in which particle groups are dispersed in a dispersion medium flows. A support surface formed on the flow cell holder for supporting the cell so as to be perpendicular to an optical axis connecting a light source provided on one side of the cell and a detector provided on the other side of the cell; And a pressing means for pressing one surface of the cell such that the other surface of the cell is in pressure contact with the supporting surface.

【0010】したがって、フローセルホルダに、セルの
一側に設けられる光源と他側に設けられる検出器とを結
ぶ光軸に対してセルが垂直になるように支持する支持面
を形成し、押圧手段によりセルの一面を押圧してセルの
他面を支持面に圧接するようにしたため、セルを簡単,
かつ,精度よく正確な位置に取り付けることができる。
Therefore, the flow cell holder is provided with a support surface for supporting the cell so that the cell is perpendicular to the optical axis connecting the light source provided on one side of the cell and the detector provided on the other side, and the pressing means is formed. Since one surface of the cell is pressed by pressing the other surface of the cell against the supporting surface,
In addition, it can be installed in a precise and accurate position.

【0011】しかも、セルを、従来のように、サイドホ
ルダに取り付けないため、セルとホルダとの間に隙間が
形成されず、セルのがたつきがない。また、セルおよび
ホルダの取付誤差,加工誤差によるセルの割れ,歪みが
ない。
Moreover, since the cell is not attached to the side holder as in the conventional case, a gap is not formed between the cell and the holder, and the cell does not rattle. Further, there is no crack or distortion of the cell due to the mounting error of the cell and the holder or the processing error.

【0012】また、請求項2記載のフローセルホルダ
は、分散媒に粒子群を分散させた試料液が流通するフロ
ーセルの下端部が下凹部に挿入される下ホルダと、前記
下凹部の底面および側壁に形成され,前記セルの一側に
設けられる光源と前記セルの他側に設けられる検出器と
を結ぶ光軸に対して前記セルが垂直になるように支持す
る支持面と、前記下ホルダの孔に接続され,前記試料液
を導入又は排出するパイプと、前記セルの上端部が上凹
部に挿入され,前記上端部を支持する上ホルダと、当該
上ホルダの孔に接続され,前記試料液を排出又は導入す
るパイプと、前記両凹部にそれぞれ設けられ,前記セル
の上面開口および下面開口の周縁部をシールするOリン
グと、前記上ホルダの一端部の両側面に突設され,前記
光軸に平行に位置したピンと、水平方向の支持片が前記
下ホルダの両側面に装着され,前記支持片の一端部から
延設された上下方向の折曲片の先端部が前記上ホルダの
一端部に位置した支持板と、前記支持片に螺合し,前記
セルの他面が前記支持面に圧接するように前記セルの一
面を押圧する押圧ボルトと、前記折曲片の先端部に形成
され,前記ピンが挿通された長孔と、一端が前記支持片
の一端部に係止し,他端が前記長孔に挿通された前記ピ
ンに係止した引張ばねと、前記上ホルダの他端部を貫通
し,前記下ホルダに螺合する取付ボルトと、前記上ホル
ダの他端部と前記取付ボルトとの間に設けられた圧縮ば
ねとを備えたものである。
Further, in the flow cell holder according to claim 2, a lower holder in which a lower end portion of a flow cell in which a sample liquid in which a particle group is dispersed in a dispersion medium flows is inserted into a lower concave portion, and a bottom surface and a side wall of the lower concave portion. And a supporting surface for supporting the cell so as to be perpendicular to an optical axis connecting a light source provided on one side of the cell and a detector provided on the other side of the cell, and the lower holder. A pipe connected to a hole for introducing or discharging the sample liquid, an upper holder for inserting the upper end of the cell into an upper recess and supporting the upper end, and a pipe for connecting the upper holder to the sample liquid. A pipe for discharging or introducing water, an O-ring that is provided in each of the recesses and seals the peripheral portions of the upper surface opening and the lower surface opening of the cell, and project from both side surfaces of one end of the upper holder. Located parallel to the axis A support plate in which a pin and a horizontal support piece are mounted on both side surfaces of the lower holder, and a tip end of a vertical bending piece extending from one end of the support piece is located at one end of the upper holder. A pressing bolt that is screwed onto the supporting piece and presses one surface of the cell so that the other surface of the cell is in pressure contact with the supporting surface; and a pin that is formed at the tip of the bent piece and that the pin is inserted. And a tension spring having one end locked to one end of the support piece and the other end locked to the pin inserted into the long hole, and the other end of the upper holder, It is provided with a mounting bolt screwed to the lower holder and a compression spring provided between the other end of the upper holder and the mounting bolt.

【0013】したがって、下ホルダの下凹部にフローセ
ルの下端部を挿入し、下凹部の底面および側壁に、セル
の一側に設けられる光源とセルの他側に設けられる検出
器とを結ぶ光軸に対してセルが垂直になるように支持す
る支持面を形成し、上ホルダの上凹部にフローセルの上
端部を挿入し、前記光軸に平行に位置したピンを上ホル
ダの一端部の両側面に突設し、支持板の支持片を下ホル
ダの両側に装着し、支持片にセルの一面を押圧する押圧
ボルトを螺合し、セルの他面を支持面に圧接し、支持板
の折曲片の長孔にピンを挿通し、引張ばねの一端を支持
板の支持片の一端部に係止するとともに、他端を前記長
孔に挿通されたピンに係止し、上ホルダの他端部との間
に圧縮ばねが設けられた取付ボルトを、上ホルダの他端
部を貫通して下ホルダに螺合するようにしたため、セル
を簡単,かつ,精度よく正確な位置に取り付けることが
できる。また、セルをセルホルダに取り付けた場合、取
付ボルトの圧縮ばねが圧縮されると同時に、引張ばねに
より上ホルダの一端部がピンを介して下方向に引っ張ら
れ、下凹部にセルの下面開口の周縁部が圧接するととも
に、上凹部にセルの上面開口の周縁部が圧接し、前記両
開口の周縁部を確実にシールすることができる。しか
も、上ホルダおよび下ホルダの寸法精度を高める必要が
なく、寸法精度の誤差によるセルの前記両開口からの液
漏れ、上ホルダ,下ホルダの圧接によるセルの歪み,割
れが生じない。
Therefore, the lower end of the flow cell is inserted into the lower recess of the lower holder, and the optical axis connecting the light source provided on one side of the cell and the detector provided on the other side of the cell on the bottom surface and side wall of the lower recess. A support surface is formed so that the cell is perpendicular to the upper holder, the upper end of the flow cell is inserted into the upper recess of the upper holder, and the pins positioned parallel to the optical axis are attached to both side surfaces of one end of the upper holder. The support pieces of the support plate are mounted on both sides of the lower holder.Pressing bolts that press one surface of the cell are screwed into the support piece, and the other surface of the cell is pressed against the support surface to fold the support plate. Insert the pin into the long hole of the bent piece, lock one end of the tension spring to one end of the support piece of the support plate, and lock the other end to the pin inserted into the long hole. Insert the mounting bolt, which has a compression spring between it and the end, through the other end of the upper holder and Because it is screwed into da, simple cell, and can be attached to accurately correct position. Also, when the cell is attached to the cell holder, the compression spring of the attachment bolt is compressed, and at the same time, one end of the upper holder is pulled downward by the tension spring via the pin, and the lower recess is surrounded by the lower edge of the cell. The portions are pressed together, and the peripheral portions of the upper opening of the cell are pressed against the upper concave portion, so that the peripheral portions of the both openings can be reliably sealed. Moreover, it is not necessary to increase the dimensional accuracy of the upper holder and the lower holder, and liquid leakage from the both openings of the cell due to dimensional accuracy error and distortion and cracking of the cell due to pressure contact between the upper holder and the lower holder do not occur.

【0014】さらに、セルをセルホルダから取り外す場
合、取付ボルトを下ホルダから取り外し、押圧ボルトを
緩めるだけでよく、セルを簡単に下ホルダ下凹部から取
り出すことができ、容易にメンテナンスを行うことがで
きる。
Further, when removing the cell from the cell holder, it is sufficient to remove the mounting bolt from the lower holder and loosen the pressing bolt, and the cell can be easily taken out from the lower recess of the lower holder, and maintenance can be easily performed. .

【0015】[0015]

【発明の実施の形態】実施の1形態につき、図1〜図3
を参照して説明する。それらの図において、34はセル
ホルダであり、主として、断面がL字形状の下ホルダ3
5と,直方体形状の上ホルダ43とから構成されてい
る。
BEST MODE FOR CARRYING OUT THE INVENTION FIG.
Will be described with reference to. In these drawings, 34 is a cell holder, which is mainly composed of a lower holder 3 having an L-shaped cross section.
5 and a rectangular parallelepiped upper holder 43.

【0016】前記下ホルダ35は、水平方向の基体35
aと,水平方向の基体35aの上面の一側に一体に突設
された突条体35bとからなり、突条体35bの中央に
下凹部35cが形成され、この下凹部35cに、外面が
精密に加工されたフローセル10の下端部が挿脱自在に
挿入され、下凹部35cの底面に横支持面Xが精密に加
工され、横支持面Xに環状のOリング溝35dが形成さ
れ、このOリング溝35dにOリング35eが嵌入さ
れ、Oリング35eにセル10の下面開口の周縁部が当
接する。35fは下凹部35cの他側の壁面に突設され
た支持体であり、精密に加工された縦支持面Yを有して
いる。37は基体37aから突条体37bにかけて形成
された導入孔(または排出孔)であり、導入孔37の一
端と下凹部35cとの間に連通孔38が形成され、導入
孔37の他端部に導入パイプ39が接続されて他側に導
出され、導入パイプ39,導入孔37,連通孔38,下
凹部35c,セル10の下面開口が連通している。40
は下ホルダ35の前端部に一体に突設された筒体であ
り、内面に螺溝が形成されている。
The lower holder 35 is a horizontal base body 35.
a and a ridge 35b integrally formed on one side of the upper surface of the base body 35a in the horizontal direction. A lower recess 35c is formed at the center of the ridge 35b, and the lower recess 35c has an outer surface. The precision machined lower end of the flow cell 10 is removably inserted, the lateral support surface X is precisely machined on the bottom surface of the lower recess 35c, and an annular O-ring groove 35d is formed on the lateral support surface X. The O-ring 35e is fitted in the O-ring groove 35d, and the peripheral edge of the lower surface opening of the cell 10 abuts on the O-ring 35e. Reference numeral 35f denotes a support member projectingly provided on the other side wall surface of the lower recess 35c, and has a vertically-supported vertical support surface Y. Reference numeral 37 denotes an introduction hole (or a discharge hole) formed from the base body 37a to the protrusion 37b. A communication hole 38 is formed between one end of the introduction hole 37 and the lower recess 35c, and the other end of the introduction hole 37 is formed. The introduction pipe 39 is connected to and led out to the other side, and the introduction pipe 39, the introduction hole 37, the communication hole 38, the lower recess 35c, and the lower surface opening of the cell 10 communicate with each other. 40
Is a cylindrical body integrally provided on the front end of the lower holder 35, and has a thread groove formed on the inner surface thereof.

【0017】41はL字形状の2枚の支持板であり、水
平方向の支持片41aと,支持片41aの一端部から延
設された上下方向の折曲片41bとからなり、支持片4
1aが下ホルダ35の突条体35bの両側面に固定ボル
ト42により装着され、前記折曲片41bの先端部に長
孔41cが形成され、支持片41aの両側部を2本の押
圧ボルト36が貫通して支持片41aの裏面に固着され
たナット36aに螺合し、その先端部がセル10の下端
部の一面を押圧し、セル10の下面が前記横支持面Xに
当接し、セル10の下端部の他面が前記縦支持面Yに圧
接し、セル10の一側に設けられる光源とセル10の他
側に設けられる検出器とを結ぶ光軸に対してセル10が
垂直になるように支持され、セル10が精度よく正確な
位置に取り付けられる。
Reference numeral 41 denotes two L-shaped support plates, each of which includes a horizontal support piece 41a and a vertical bending piece 41b extending from one end of the support piece 41a.
1a is attached to both side surfaces of the ridge 35b of the lower holder 35 by fixing bolts 42, a long hole 41c is formed at the tip of the bending piece 41b, and two pressing bolts 36 are provided on both sides of the supporting piece 41a. Penetrates and is screwed into a nut 36a fixed to the back surface of the support piece 41a, the tip end of the nut presses one surface of the lower end portion of the cell 10, and the lower surface of the cell 10 abuts the lateral support surface X. The other surface of the lower end of the cell 10 is in pressure contact with the vertical support surface Y, and the cell 10 is perpendicular to the optical axis connecting the light source provided on one side of the cell 10 and the detector provided on the other side of the cell 10. And the cell 10 is mounted in a precise position with high accuracy.

【0018】前記上ホルダ43は、下面の中央に上凹部
43aが形成され、この上凹部43aに、セル10の上
端部が挿脱自在に挿入されて支持され、上凹部43aの
上面に環状のOリング溝43bが形成され、このOリン
グ溝43bにOリング43cが嵌入され、Oリング43
cにセル10の上面開口の周縁部が当接する。44は上
ホルダ43に形成された排出孔(または導入孔)であ
り、排出孔44の一端と上凹部43aとの間に連通孔4
5が形成され、排出孔44の他端部に排出パイプ46が
接続されて他側に導出され、排出パイプ46,排出孔4
4,連通孔45,上凹部43a,セル10の上面開口が
連通している。47は上ホルダ43の一端部の両側面に
突設されたピンであり、前記光軸に平行に位置し、前記
両支持板41の折曲片41bの長孔41cにピン47が
挿通され、上ホルダ43の一端部が回転自在に支持され
ている。
The upper holder 43 has an upper recess 43a formed at the center of the lower surface, and the upper end of the cell 10 is removably inserted into and supported by the upper recess 43a, and an annular shape is formed on the upper surface of the upper recess 43a. The O-ring groove 43b is formed, and the O-ring 43c is fitted into the O-ring groove 43b.
The peripheral edge of the upper surface opening of the cell 10 abuts on c. Reference numeral 44 denotes a discharge hole (or an introduction hole) formed in the upper holder 43, and the communication hole 4 is provided between one end of the discharge hole 44 and the upper recess 43a.
5, the discharge pipe 46 is connected to the other end of the discharge hole 44 and is led out to the other side.
4, the communication hole 45, the upper recess 43a, and the upper surface opening of the cell 10 communicate with each other. Reference numeral 47 denotes a pin projecting from both side surfaces of one end of the upper holder 43, which is positioned parallel to the optical axis, and the pin 47 is inserted into the long holes 41c of the bent pieces 41b of the both support plates 41. One end of the upper holder 43 is rotatably supported.

【0019】48は引張ばねであり、一端が前記両支持
板41の支持片41aのピン48aに係止し、他端が前
記ピン47に係止し、上ホルダ43の一端部を鉛直方向
に引っ張っている。49は上ホルダ43の他端部に形成
された切欠であり、この切欠49に取付ボルト50が設
けられ、取付ボルト50の先端部が切欠49の底部を貫
通して上ホルダ43の他端部から下方に導出されてい
る。51は取付ボルト50の先端部に装着された環状の
止め金であり、上ホルダ43からの取付ボルト50の逸
脱を防止している。52は切欠49の底部と取付ボルト
50の頭部との間に設けられた圧縮ばねであり、取付ボ
ルト50の先端部が下ホルダ35の筒体40に螺合して
圧縮されている。
Reference numeral 48 denotes a tension spring, one end of which is engaged with the pin 48a of the support piece 41a of the both support plates 41 and the other end of which is engaged with the pin 47, so that one end of the upper holder 43 is vertically extended. I'm pulling. Reference numeral 49 denotes a notch formed in the other end of the upper holder 43. The notch 49 is provided with a mounting bolt 50. The tip of the mounting bolt 50 penetrates the bottom of the notch 49 and the other end of the upper holder 43. Has been derived from below. Reference numeral 51 denotes an annular stopper plate attached to the tip of the mounting bolt 50, which prevents the mounting bolt 50 from deviating from the upper holder 43. A compression spring 52 is provided between the bottom of the cutout 49 and the head of the mounting bolt 50, and the tip of the mounting bolt 50 is screwed into the cylinder 40 of the lower holder 35 and compressed.

【0020】そして、図1の実線の状態は、セル10が
セルホルダ34に取り付けられた状態を示し、取付ボル
ト50が下ホルダ35の突条体35bの筒体40に螺合
し、上ホルダ43のピン47が長孔41cの上端側に位
置し、この状態で、上ホルダ43の一端部が引張ばね4
8によりピン47を介して鉛直方向に引っ張られ、セル
10の下端部が前記突条体35bの下凹部35cに挿入
され、下凹部35cの横支持面Xにセル10の下端部の
下面が当接し、押圧ボルト36がセル10の下端部の一
面を押圧し、セル10の下端部の他面が支持体35fの
縦支持面Yに圧接し、セル10の下端部が前記横支持面
Xおよび前記縦支持面Yにより支持され、セル10の上
端部が上ホルダ43の上凹部43aに挿入されて支持さ
れ、セル10が前記光軸に対して垂直に支持されてい
る。
The state of the solid line in FIG. 1 shows the state in which the cell 10 is attached to the cell holder 34, and the attachment bolt 50 is screwed into the tubular body 40 of the ridge 35b of the lower holder 35 and the upper holder 43. The pin 47 of the upper holder 43 is located on the upper end side of the elongated hole 41c.
8 is pulled vertically through the pin 47, the lower end of the cell 10 is inserted into the lower recess 35c of the protrusion 35b, and the lower surface of the lower end of the cell 10 contacts the lateral support surface X of the lower recess 35c. The pressing bolt 36 presses one surface of the lower end portion of the cell 10, the other surface of the lower end portion of the cell 10 is pressed against the vertical support surface Y of the support 35f, and the lower end portion of the cell 10 is connected to the horizontal support surface X and The cell 10 is supported by the vertical support surface Y, the upper end of the cell 10 is inserted into and supported by the upper recess 43a of the upper holder 43, and the cell 10 is supported perpendicularly to the optical axis.

【0021】この状態から、セル10をセルホルダ34
から取り外す場合、取付ボルト50を緩めて突条体35
bの筒体40から取り外すとともに、押圧ボルト36を
緩めてセル10の下端部の一面から離脱させ、、上ホル
ダ43を図1の鎖線に示す位置まで回動し、セル10を
下ホルダ35の下凹部35cから上方に引き出し、セル
10および両ホルダ35,43の内部の清掃等のメンテ
ナンスを行う。このように、セル10をセルホルダ34
から取り外す場合、取付ボルト50を緩めて上ホルダ4
3から取り外すとともに、押圧ボルト36を緩めるだけ
でよく、従来のように、複数本のねじを全て取り外して
各ホルダを解体する必要がなく、容易にメンテナンスを
行うことができる。
From this state, the cell 10 is placed in the cell holder 34.
When removing from the ridge 35, loosen the mounting bolt 50.
While removing from the tubular body 40 of b, loosening the pressing bolt 36 to separate it from the one surface of the lower end portion of the cell 10, the upper holder 43 is rotated to the position shown by the chain line in FIG. The cell 10 and the holders 35 and 43 are cleaned upward by pulling them upward from the lower recess 35c. In this way, the cell 10 is placed in the cell holder 34
When removing from the upper holder 4 loosen the mounting bolt 50
It is only necessary to loosen the pressing bolt 36 while removing it from the connector 3, and unlike the conventional case, it is not necessary to remove all the plurality of screws to disassemble each holder, and maintenance can be easily performed.

【0022】そして、セル10をセルホルダ34に取り
付ける場合、セル10の下端部を下ホルダ35の下凹部
35aに挿入し、セル10の下面開口の周縁部を前記横
支持面Xに当接し、押圧ボルト36を緊締してセル10
の下端部の一面を押圧し、セル10の下端部の他面を前
記縦支持面Yに圧接する。つぎに、上ホルダ43を引張
ばね48に抗して、図1の実線に示す位置まで回動する
と、セル10の上端部が上凹部43aに挿入され、セル
10の上面開口の周縁部が上ホルダ43のOリング43
cに当接する。この状態で、取付ボルト50を前記突条
体35bの筒体40に螺合すると、圧縮ばね52が圧縮
されると同時に、引張ばね48により、上ホルダ43の
一端部がピン47を介して鉛直方向に引っ張られ、下凹
部35cのOリング35eにセル10の下面開口の周縁
部が圧接するとともに、上凹部43aのOリング43c
にセル10の上面開口の周縁部が圧接する。すなわち、
前記両ばね48,52の蓄勢力によって、両ホルダ3
5,43のOリング35e,43cがセル10の両開口
の周縁部にそれぞれ圧接し、前記両開口の周縁部を確実
にシールする。
When the cell 10 is attached to the cell holder 34, the lower end of the cell 10 is inserted into the lower recess 35a of the lower holder 35, and the peripheral edge of the lower surface opening of the cell 10 is brought into contact with the lateral support surface X and pressed. Tighten the bolt 36 to tighten the cell 10
One surface of the lower end of the cell 10 is pressed, and the other surface of the lower end of the cell 10 is pressed against the vertical support surface Y. Next, when the upper holder 43 is rotated against the tension spring 48 to the position shown by the solid line in FIG. 1, the upper end portion of the cell 10 is inserted into the upper recess 43a, and the peripheral edge portion of the upper surface opening of the cell 10 is raised. O-ring 43 of holder 43
abut on c. In this state, when the mounting bolt 50 is screwed into the cylindrical body 40 of the ridge 35b, the compression spring 52 is compressed, and at the same time, the tension spring 48 causes one end of the upper holder 43 to vertically pass through the pin 47. Is pulled in the direction, the peripheral portion of the lower surface opening of the cell 10 is pressed against the O-ring 35e of the lower recess 35c, and the O-ring 43c of the upper recess 43a is pressed.
The peripheral edge portion of the upper surface opening of the cell 10 is pressed against. That is,
Due to the stored force of both springs 48 and 52, both holders 3
The O-rings 35e and 43c of 5, 43 are pressed against the peripheral portions of both openings of the cell 10, respectively, and reliably seal the peripheral portions of the both openings.

【0023】このように、前記形態の場合、セル10を
図6に示すようなサイドホルダに取り付けないため、セ
ル10とホルダとの間に隙間が形成されず、セル10の
がたつきがない。また、セル10およびホルダの取付誤
差,加工誤差によるセル10の割れ,歪みがない。しか
も、従来のように、上ホルダ43および下ホルダ35を
サイドホルダに取り付けないため、これら部品の寸法精
度を高める必要がなく、寸法精度の誤差によるセル10
の前記両開口からの液漏れがなく、上ホルダ43,下ホ
ルダ35の圧接によってセル10が歪んだり、割れたり
しない。
As described above, in the case of the above-described embodiment, since the cell 10 is not attached to the side holder as shown in FIG. 6, a gap is not formed between the cell 10 and the holder and the cell 10 does not rattle. . Further, there is no crack or distortion of the cell 10 due to an attachment error or a processing error of the cell 10 and the holder. Moreover, unlike the conventional case, since the upper holder 43 and the lower holder 35 are not attached to the side holders, it is not necessary to improve the dimensional accuracy of these parts, and the cell 10 due to an error in the dimensional accuracy is not required.
There is no liquid leakage from the both openings, and the cell 10 is not distorted or broken by the pressure contact between the upper holder 43 and the lower holder 35.

【0024】なお、前記形態の場合、セル10の押圧手
段に押圧ボルト36を用いたが、これに限らず、ばね板
を用いてもよく、図4に示すような押圧体53を用いて
もよい。この押圧体53は、二個の筒体54が支持片4
1aの両側の透孔41dにそれぞれ内側から挿通され、
両透孔41dの周縁部に筒体54のフランジ56が当接
し、一側の開口端部が蓋板55により閉塞され、筒体5
4の周面に環状の止め金57が螺合し、支持片41aに
筒体54が装着されている。なお、筒体54の他側の開
口端部の直径は一側の開口端部の直径より若干小さくな
っており、前記筒体54の内部には、ばね58が設けら
れるとともに、ばね58により出方向に付勢されたボー
ル59が筒体54の他側の開口端部に出没自在に設けら
れ、筒体54の他側の開口端部からボール59の一部が
突出している。そして、セル10の下端部を下ホルダ3
5の下凹部35cに挿入した際、セル10の下端部の一
面がボール59に押圧され、セル10の下端部の他面が
縦支持面Yに圧接され、前記形態の場合と同様に、セル
10が前記光軸に対して垂直に支持される。また、セル
10の下端部を下ホルダ35の下凹部35cから取り外
す際、セル10を上方に引き出せばよい。
In the above embodiment, the pressing bolt 36 is used as the pressing means of the cell 10, but the present invention is not limited to this, a spring plate may be used, and a pressing body 53 as shown in FIG. 4 may be used. Good. In this pressing body 53, the two tubular bodies 54 are
1a is inserted into the through holes 41d on both sides from the inside,
The flange 56 of the tubular body 54 abuts on the peripheral portions of both the through holes 41d, and the opening end portion on one side is closed by the lid plate 55.
An annular stopper plate 57 is screwed onto the peripheral surface of 4, and the cylindrical body 54 is attached to the support piece 41a. The diameter of the opening end on the other side of the tubular body 54 is slightly smaller than the diameter of the opening end on the one side. Inside the tubular body 54, a spring 58 is provided and the spring 58 causes the spring 58 to project. A ball 59 urged in the direction is provided at an open end of the other side of the tubular body 54 so as to be retractable and retractable, and a part of the ball 59 projects from the open end of the other side of the tubular body 54. Then, the lower end of the cell 10 is attached to the lower holder 3
5, when inserted into the lower recess 35c of the cell 10, one surface of the lower end portion of the cell 10 is pressed by the ball 59, and the other surface of the lower end portion of the cell 10 is pressed against the vertical support surface Y. 10 is supported perpendicular to the optical axis. Further, when removing the lower end of the cell 10 from the lower recess 35c of the lower holder 35, the cell 10 may be pulled out upward.

【0025】また、上ホルダ43の保持手段に取付ボル
ト50を用いたが、これに限らず、上ホルダ43を保持
できる手段であれば何でもよい。
Further, although the mounting bolt 50 is used as the holding means for the upper holder 43, it is not limited to this and any means can be used as long as it can hold the upper holder 43.

【0026】[0026]

【発明の効果】以上説明したように、請求項1記載の粒
子径分布測定装置のフローセルホルダは、フローセルホ
ルダに、セルの一側に設けられる光源と他側に設けられ
る検出器とを結ぶ光軸に対してセルが垂直になるように
支持する支持面を形成し、押圧手段によりセルの一面を
押圧し、セルの他面を支持面に圧接するようにしたた
め、セルを簡単,かつ,精度よく正確な位置に取り付け
ることができる。しかも、セルを、従来のように、サイ
ドホルダに取り付けないため、セルとホルダとの間に隙
間が形成されず、セルのがたつきがない。また、セルお
よびホルダの取付誤差,加工誤差によるセルの割れ,歪
みを防止することができる。
As described above, in the flow cell holder of the particle size distribution measuring apparatus according to the first aspect, the flow cell holder is a light connecting the light source provided on one side of the cell and the detector provided on the other side. Since the support surface is formed so that the cell is perpendicular to the axis and one surface of the cell is pressed by the pressing means and the other surface of the cell is pressed against the support surface, the cell is simple and accurate. It can be installed in a precise position. Moreover, since the cell is not attached to the side holder as in the conventional case, a gap is not formed between the cell and the holder, and the cell does not rattle. Further, it is possible to prevent the cracking and distortion of the cell due to the mounting error of the cell and the holder and the processing error.

【0027】また、請求項2記載の粒子径分布測定装置
のフローセルホルダは、下ホルダの下凹部にフローセル
の下端部を挿入し、下凹部の底面および側壁に、セルの
一側に設けられる光源とセルの他側に設けられる検出器
とを結ぶ光軸に対してセルが垂直になるように支持する
支持面を形成し、上ホルダの上凹部にフローセルの上端
部を挿入し、前記光軸に平行に位置したピンを上ホルダ
の一端部の両側面に突設し、支持板の支持片を下ホルダ
の両側に装着し、支持片にセルの一面を押圧する押圧ボ
ルトを螺合し、セルの他面を支持面に圧接し、支持板の
折曲片の長孔にピンを挿通し、引張ばねの一端を支持板
の支持片の一端部に係止するとともに、他端を前記長孔
に挿通されたピンに係止し、上ホルダの他端部との間に
圧縮ばねが設けられた取付ボルトを、上ホルダの他端部
を貫通して下ホルダに螺合するようにしたため、セルを
セルホルダに取り付ける場合、セルの両端部を両ホルダ
の凹部にそれぞれ挿入し、取付ボルトを下ホルダに螺合
するだけでよく、セルを簡単,かつ,精度よく正確な位
置に取り付けることができる。また、セルをセルホルダ
に取り付けた場合、取付ボルトの圧縮ばねが圧縮される
と同時に、引張ばねにより上ホルダの一端部がピンを介
して下方向に引っ張られ、下凹部にセルの下面開口の周
縁部が圧接するとともに、上凹部にセルの上面開口の周
縁部が圧接し、前記両開口の周縁部を確実にシールする
ことができる。しかも、上ホルダおよび下ホルダの寸法
精度を高める必要がなく、寸法精度の誤差によるセルの
前記両開口からの液漏れ、上ホルダ,下ホルダの圧接に
よるセルの歪み,割れが生じない。
Further, in the flow cell holder of the particle size distribution measuring apparatus according to claim 2, the lower end portion of the flow cell is inserted into the lower recess of the lower holder, and the light source provided on one side of the cell on the bottom surface and side wall of the lower recess. And a detector provided on the other side of the cell, a support surface is formed to support the cell so that it is perpendicular to the optical axis, and the upper end of the flow cell is inserted into the upper recess of the upper holder. Pins protruding parallel to one end of the upper holder, supporting pieces of the supporting plate are mounted on both sides of the lower holder, and pressing bolts for pressing one surface of the cell to the supporting piece are screwed together, The other surface of the cell is pressed against the supporting surface, the pin is inserted into the elongated hole of the bent piece of the supporting plate, one end of the tension spring is locked to one end of the supporting piece of the supporting plate, and the other end is It is locked to the pin inserted in the hole and a compression spring is provided between the pin and the other end of the upper holder. Since the mounting bolts penetrate the other end of the upper holder and are screwed into the lower holder, when mounting the cell to the cell holder, insert both ends of the cell into the recesses of both holders and lower the mounting bolt. Since it is only necessary to screw it into the holder, the cell can be attached easily and accurately at an accurate position. Also, when the cell is attached to the cell holder, the compression spring of the attachment bolt is compressed, and at the same time, one end of the upper holder is pulled downward by the tension spring via the pin, and the lower recess is surrounded by the lower edge of the cell. The portions are pressed together, and the peripheral portions of the upper opening of the cell are pressed against the upper concave portion, so that the peripheral portions of the both openings can be reliably sealed. Moreover, it is not necessary to increase the dimensional accuracy of the upper holder and the lower holder, and liquid leakage from the both openings of the cell due to dimensional accuracy error and distortion and cracking of the cell due to pressure contact between the upper holder and the lower holder do not occur.

【0028】さらに、セルをセルホルダから取り外す場
合、取付ボルトを下ホルダから取り外し、押圧ボルトを
緩めるだけでよく、セルを簡単に下ホルダの下凹部から
取り出すことができ、容易にメンテナンスを行うことが
できる。
Further, when removing the cell from the cell holder, it suffices to remove the mounting bolt from the lower holder and loosen the pressing bolt, and the cell can be easily taken out from the lower recess of the lower holder, facilitating maintenance. it can.

【図面の簡単な説明】[Brief description of drawings]

【図1】本発明の形態1の斜視図である。FIG. 1 is a perspective view of a first embodiment of the present invention.

【図2】図1の切断正面図である。FIG. 2 is a cut front view of FIG.

【図3】図1の切断平面図である。FIG. 3 is a sectional plan view of FIG.

【図4】図1の押圧手段の変形例の切断平面図である。FIG. 4 is a cutaway plan view of a modification of the pressing means of FIG.

【図5】粒子径分布測定装置の概略構成図である。FIG. 5 is a schematic configuration diagram of a particle size distribution measuring device.

【図6】従来例のフローセルホルダの分解斜視図であ
る。
FIG. 6 is an exploded perspective view of a conventional flow cell holder.

【符号の説明】[Explanation of symbols]

10…フローセル、34…フローセルホルダ、35…下
ホルダ、35c…下凹部、35e…Oリング、36…押
圧ボルト、37…導入孔、39…導入パイプ、41…支
持板、41a…支持片、41b…折曲片、41c…長
孔、43…上ホルダ、43a…上凹部、43c…Oリン
グ、44…排出孔、46…排出パイプ、47…ピン、4
8…引張ばね、50…取付ボルト、52…圧縮ばね、X
…横支持面、Y…縦支持面。
10 ... Flow cell, 34 ... Flow cell holder, 35 ... Lower holder, 35c ... Lower recess, 35e ... O ring, 36 ... Press bolt, 37 ... Introduction hole, 39 ... Introduction pipe, 41 ... Support plate, 41a ... Support piece, 41b ... bent piece, 41c ... long hole, 43 ... upper holder, 43a ... upper recess, 43c ... O-ring, 44 ... discharge hole, 46 ... discharge pipe, 47 ... pin, 4
8 ... tension spring, 50 ... mounting bolt, 52 ... compression spring, X
... horizontal support surface, Y ... vertical support surface.

フロントページの続き (58)調査した分野(Int.Cl.7,DB名) G01N 15/02 G01B 11/08 G01N 15/14 G01N 21/01 G01N 21/05 Front page continued (58) Fields surveyed (Int.Cl. 7 , DB name) G01N 15/02 G01B 11/08 G01N 15/14 G01N 21/01 G01N 21/05

Claims (2)

(57)【特許請求の範囲】(57) [Claims] 【請求項1】 分散媒に粒子群を分散させた試料液が流
通するフローセルを支持するフローセルホルダに形成さ
れ,前記セルの一側に設けられる光源と前記セルの他側
に設けられる検出器とを結ぶ光軸に対して前記セルが垂
直になるように支持する支持面と、 前記セルの他面が前記支持面に圧接するように前記セル
の一面を押圧する押圧手段とを備えたことを特徴とする
粒子径分布測定装置のフローセルホルダ。
1. A light source provided on one side of the cell and a detector provided on the other side of the cell, which is formed on a flow cell holder that supports a flow cell in which a sample solution in which a group of particles is dispersed in a dispersion medium flows. A supporting surface for supporting the cell so as to be perpendicular to the optical axis connecting the two, and pressing means for pressing one surface of the cell so that the other surface of the cell is in pressure contact with the supporting surface. Flow cell holder for particle size distribution measuring device.
【請求項2】 分散媒に粒子群を分散させた試料液が流
通するフローセルの下端部が下凹部に挿入される下ホル
ダと、 前記下凹部の底面および側壁に形成され,前記セルの一
側に設けられる光源と前記セルの他側に設けられる検出
器とを結ぶ光軸に対して前記セルが垂直になるように支
持する支持面と、 前記下ホルダの孔に接続され,前記試料液を導入又は排
出するパイプと、 前記セルの上端部が上凹部に挿入され,前記上端部を支
持する上ホルダと、 当該上ホルダの孔に接続され,前記試料液を排出又は導
入するパイプと、 前記両凹部にそれぞれ設けられ,前記セルの上面開口お
よび下面開口の周縁部をシールするOリングと、 前記上ホルダの一端部の両側面に突設され,前記光軸に
平行に位置したピンと、 水平方向の支持片が前記下ホルダの両側面に装着され,
前記支持片の一端部から延設された上下方向の折曲片の
先端部が前記上ホルダの一端部に位置した支持板と、 前記支持片に螺合し,前記セルの他面が前記支持面に圧
接するように前記セルの一面を押圧する押圧ボルトと、 前記折曲片の先端部に形成され,前記ピンが挿通された
長孔と、 一端が前記支持片の一端部に係止し,他端が前記長孔に
挿通された前記ピンに係止した引張ばねと、 前記上ホルダの他端部を貫通し,前記下ホルダに螺合す
る取付ボルトと、 前記上ホルダの他端部と前記取付ボルトとの間に設けら
れた圧縮ばねとを備えたことを特徴とする粒子径分布測
定装置のフローセルホルダ。
2. A lower holder into which a lower end portion of a flow cell, through which a sample solution in which a group of particles is dispersed in a dispersion medium flows, is inserted into a lower recess, and a bottom surface and a side wall of the lower recess, the one side of the cell A supporting surface for supporting the cell so as to be perpendicular to an optical axis connecting a light source provided in the cell and a detector provided on the other side of the cell, and connecting the sample solution to the hole of the lower holder. A pipe for introducing or discharging, an upper holder for inserting the upper end of the cell into an upper recess and supporting the upper end, and a pipe for connecting to the hole of the upper holder for discharging or introducing the sample solution, O-rings that are respectively provided in both recesses and seal the peripheral portions of the upper surface opening and the lower surface opening of the cell; pins that project from both side surfaces of one end of the upper holder and that are parallel to the optical axis; The direction of the support piece is below Is mounted on both sides of the holder,
A tip of a vertically bent piece extending from one end of the support piece is screwed into the support plate located at one end of the upper holder, and the other surface of the cell is supported by the support plate. A pressing bolt that presses one surface of the cell so as to come into pressure contact with the surface, a long hole that is formed at the tip of the bent piece and through which the pin is inserted, and one end is locked to one end of the support piece. A tension spring, the other end of which is locked to the pin inserted into the elongated hole, a mounting bolt which penetrates the other end of the upper holder and is screwed into the lower holder, and the other end of the upper holder And a compression spring provided between the mounting bolt and the mounting bolt.
JP33788698A 1998-11-27 1998-11-27 Flow cell holder for particle size distribution analyzer Expired - Fee Related JP3422701B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP33788698A JP3422701B2 (en) 1998-11-27 1998-11-27 Flow cell holder for particle size distribution analyzer

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP33788698A JP3422701B2 (en) 1998-11-27 1998-11-27 Flow cell holder for particle size distribution analyzer

Publications (2)

Publication Number Publication Date
JP2000162118A JP2000162118A (en) 2000-06-16
JP3422701B2 true JP3422701B2 (en) 2003-06-30

Family

ID=18312932

Family Applications (1)

Application Number Title Priority Date Filing Date
JP33788698A Expired - Fee Related JP3422701B2 (en) 1998-11-27 1998-11-27 Flow cell holder for particle size distribution analyzer

Country Status (1)

Country Link
JP (1) JP3422701B2 (en)

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* Cited by examiner, † Cited by third party
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