JP3035610B1 - How to extract vanilla tincture - Google Patents

How to extract vanilla tincture

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Publication number
JP3035610B1
JP3035610B1 JP10296551A JP29655198A JP3035610B1 JP 3035610 B1 JP3035610 B1 JP 3035610B1 JP 10296551 A JP10296551 A JP 10296551A JP 29655198 A JP29655198 A JP 29655198A JP 3035610 B1 JP3035610 B1 JP 3035610B1
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JP
Japan
Prior art keywords
vanilla
rich
extraction
product
sodium lactate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
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JP10296551A
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Japanese (ja)
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JP2000119684A (en
Inventor
雄児 福田
利枝 中田
Original Assignee
株式会社ミコヤ香商
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Abstract

【要約】 【課題】 バニラ様の香気香味付与能が強化され、且つ
バニラ抽出物独特のサヤ臭域いはビーンズ臭をほぼ消滅
させ、濃厚芳醇で且つ深みが有り天然感に富み、焼き菓
子・生菓子等に添加して食した時にのみバニラ特有の甘
さが口の中で広がり、添加した製品は保水性に富むよう
になるバニラチンキの抽出方法を提供する。 【解決手段】 キュアリング処理後のバニラビーンズ
を、乳酸ナトリウムと含水アルコールとの混合物の存在
下で抽出処理する。
Abstract: PROBLEM TO BE SOLVED: To enhance the vanilla-like flavor imparting ability, and to almost eliminate the bean smell in the vanilla extract peculiar, to be rich, rich and rich in natural feeling and to make baked confectionery. The present invention provides a method for extracting vanilla tincture, in which the sweetness unique to vanilla spreads in the mouth only when added to raw confectionery and eaten, and the added product becomes rich in water retention. SOLUTION: The vanilla beans after the curing treatment are subjected to an extraction treatment in the presence of a mixture of sodium lactate and hydroalcohol.

Description

【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【0001】[0001]

【発明の属する技術分野】本発明は、香気香味付与能が
強化され、且つ被添加物の保水性を向上させ得るバニラ
チンキの抽出方法に関する。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a method for extracting vanilla tincture, which has an enhanced aroma and flavor imparting ability and can improve the water retention of an additive.

【0002】[0002]

【従来の技術】バニラフレ−バ−に特有の香気はバニラ
ビ−ンズを収穫後、キュアリングと呼ばれる、バニラビ
−ンズを乾燥、発酵、熟成する工程を経て形成される。
現在では、バニラビ−ンズを含水アルコ−ル等で抽出し
て得られるバニラチンキ(抽出処理液)の形で利用され
ている。
2. Description of the Related Art The aroma peculiar to vanilla flavor is formed through a process of drying, fermenting, and aging vanilla beans, which is called curing after harvesting the vanilla beans.
At present, vanilla beans are used in the form of vanilla tincture (extraction solution) obtained by extracting with water-containing alcohol.

【0003】[0003]

【発明が解決しようとする課題】しかしながら、バニラ
ビ−ンズを含水アルコ−ルなどで抽出して製造するバニ
ラチンキは、抽出時間もかかり、且つバニラ抽出物独特
のサヤ臭域いはビ−ンズ臭を有しており、また一般的に
該抽出物のバニラ様の香気香味付与能が比較的弱いた
め、飲食品にバニラ特有の香気香味を付与するには、か
なりの量を添加しなければならないという欠点を有して
いた。
However, the vanilla tincture produced by extracting vanilla beans with a hydrous alcohol or the like requires a long extraction time and has a unique smell or bean odor unique to the vanilla extract. And the extract generally has a relatively weak vanilla-like flavor and flavor imparting ability, so that in order to impart a vanilla-specific flavor to food and drink, a considerable amount must be added. Had disadvantages.

【0004】そこで上記のサヤ臭域いはビ−ンズ臭を取
り除き、マイルドな熟成感を有するバニラチンキを得る
ために、少なくとも1ヵ月上貯蔵熟成させる方法が行わ
れているが、この方法は貯蔵時間が長いことにより作業
効果が悪く、工業的製法の見地から満足できるものでは
なかった。また、バニラビ−ンズを含水アルコ−ル等で
抽出して得られたバニラチンキは、食品類等に添加した
場合の保水性が必ずしも満足できるものではなかった。
[0004] In order to remove the bean odor from the above-mentioned odorous area and obtain a vanilla tincture having a mild ripening sensation, a method of storing and ripening it for at least one month has been carried out. However, the working effect was poor due to the long time, and it was not satisfactory from the viewpoint of an industrial production method. In addition, vanilla tincture obtained by extracting vanilla beans with a hydrated alcohol or the like was not always satisfactory in water retention when added to foods and the like.

【0005】[0005]

【課題を解決するための手段】本発明者らは、これらの
課題を解決すべく鋭意研究した。その結果、キュアリン
グ処理後のバニラビ−ンズを、乳酸ナトリウムと含水ア
ルコ−ルとの混合物の存在下で抽出処理すると、乳酸ナ
トリウムの影響により、バニラビ−ンズに溶媒が急速に
浸透し、短時間に効率よくバニラチンキの抽出ができる
と共に、被添加物の保水性が向上する等、上記の課題を
一挙に解決できることを発見した。
Means for Solving the Problems The present inventors have intensively studied to solve these problems. As a result, when the vanilla beans after the curing treatment are extracted in the presence of a mixture of sodium lactate and aqueous alcohol, the solvent rapidly permeates into the vanilla beans due to the effect of sodium lactate, and It has been found that the above problems can be solved at once, for example, vanilla tincture can be efficiently extracted and the water retention of the additive can be improved.

【0006】従って本発明の目的は、バニラ様の香気香
味付与能が強化され、且つバニラ抽出物独特のサヤ臭域
いはビ−ンズ臭をほぼ消滅させ、濃厚芳醇で且つ深みが
有り天然感に富み、焼き菓子・生菓子等に添加して食し
た時にのみバニラ特有の甘さが口の中で広がり、添加し
た製品は保水性に富むようになるバニラチンキの抽出方
法を提供することにある。
Accordingly, an object of the present invention is to enhance the ability to impart vanilla-like aroma and flavor, and to almost eliminate the bean odor in the vanilla extract's unique odorous odor, to provide a rich, rich, deep and natural feeling. It is an object of the present invention to provide a method for extracting vanilla tincture, which is rich in vegetables and has a characteristic sweetness of vanilla spread in the mouth only when added to baked confectionery, raw confectionery, etc., and the added product becomes rich in water retention.

【0007】本発明におけるキュアリング処理後のバニ
ラビ−ンズとしては、市場で容易に入手することが出来
る任意の品種のものが利用できる。かかるバニラビ−ン
ズとしては、ブルボンバニラビ−ンズ、インドネシアバ
ニラビ−ンズ、タヒチバニラビ−ンズ等を挙げることが
できる。本発明における抽出溶媒としての水溶性有機溶
媒としては、例えばエタノ−ルなどのアルコ−ル類と、
乳酸ナトリウムとの混合物がよく、この水溶性有機溶媒
を単独で抽出溶媒として用いることもできるが、該有機
溶媒と水とを混合して使用するのが好ましく、この混合
溶媒の水含有量は通常約40%〜60重量%の範囲内が
好ましい。
[0007] As the vanilla beans after the curing treatment in the present invention, any kind of vanilla beans that can be easily obtained on the market can be used. Examples of such vanilla beans include Bourbon vanilla beans, Indonesian vanilla beans, Tahiti vanilla beans and the like. Examples of the water-soluble organic solvent as the extraction solvent in the present invention include alcohols such as ethanol,
A mixture with sodium lactate is good, and this water-soluble organic solvent can be used alone as an extraction solvent.However, it is preferable to use a mixture of the organic solvent and water, and the water content of the mixed solvent is usually Preferred is in the range of about 40% to 60% by weight.

【0008】乳酸ナトリウムはこれをそのまま抽出溶媒
に添加してもよいが、通常は50%水溶液の状態で添加
するのが好ましい。
Although sodium lactate may be added to the extraction solvent as it is, it is usually preferable to add it in the form of a 50% aqueous solution.

【0009】[0009]

【発明の実施の形態】本発明の方法を実施する際の一態
様を例示すれば、バニラビ−ンズ材料100重量部に、
乳酸ナトリウム50%水溶液90〜95重量部、エタノ
ール2.5〜3倍重量部、水3〜3.5倍重量部を二度
に分けて添加して、エタノール蒸気存在下の密閉系で、
室温乃至50°Cの温度において4時間乃至36時間静
置もしくは攪拌抽出し、自然冷却後、ろ過などの固液分
離操作によって除去することにより、バニラチンキを得
ることができる。
BEST MODE FOR CARRYING OUT THE INVENTION One embodiment of carrying out the method of the present invention is as follows: 100 parts by weight of a vanilla bean material is
90 to 95 parts by weight of a 50% aqueous solution of sodium lactate, 2.5 to 3 parts by weight of ethanol, and 3 to 3.5 parts by weight of water are added in two portions, and in a closed system in the presence of ethanol vapor,
Vanilla tincture can be obtained by leaving at room temperature to 50 ° C. for 4 hours to 36 hours or extracting with stirring or stirring, and after natural cooling, removing by a solid-liquid separation operation such as filtration.

【0010】このようにして得ることの出来るバニラチ
ンキは、従来のバニラ抽出物と比較しバニラ様の香気香
味付与能が強く、且つバニラ抽出物独特のサヤ臭域いは
ビ−ンズ臭がなく、濃厚芳醇で且つ深みが有り天然感に
富み、マイルドな塾生感に優れた風味を有している。か
くして本発明のバニラチンキは、各種製品の香気香味付
与剤に添加して利用することが出来、その添加量は、利
用目的あるいは香気香味付与剤の種類によっても異なる
が、一般的には、香気香味付与剤全体量に対して約0.
1〜約2重量%の範囲内を例示することができ且つ、焼
き菓子・生菓子等に添加し食した時にのみバニラ特有の
甘さが口の中で広がり、添加した製品は保水性に富むよ
うになる。
[0010] The vanilla tincture obtained in this way has a stronger vanilla-like aroma and flavor imparting ability than the conventional vanilla extract, and has a bean smell unique to the vanilla extract, It is rich, rich and rich with a rich natural feel and has a mild taste of juku-juku. Thus, the vanilla tincture of the present invention can be used by being added to the flavoring agent of various products, and the amount of addition varies depending on the purpose of use or the type of the flavoring agent. About 0. 0 to the total amount of the imparting agent.
The range of 1 to 2% by weight can be exemplified, and when added to baked confectionery, raw confectionery, etc., only when eaten, the unique sweetness of vanilla spreads in the mouth, and the added product is rich in water retention. Become.

【0011】本発明によれば、バニラチンキを有効成分
とする香気香味付与剤を提供することが出来、該付与剤
を利用して飲食品類などに特徴のあるバニラエキスの香
気香味を付与することができる。例えば、果汁飲料類、
果実酒類、乳飲料類、炭酸飲料類のごとき飲料類;アイ
スクリーム類、シャーベット類、アイスキャンデーのご
とき冷菓子類;シュークリーム類、カスタード類、フィ
ナンシェ類、生クリーム類のごとき洋菓子類;和菓子
類;ジャム類、チューインガム類、パン類、コーヒー、
ココア、紅茶、お茶、タバコのごとき諸好品類;和風ス
ープ類、洋風スープ類のごときスープ類;風味調味料、
各種インスタント飲料及至食品類、各種スナック食品類
などに本発明のバニラチンキの適当量を添加することに
より、食品中のpHの変化を少なくし、コクを与え、保
湿作用、離水防止効果、吸水性が著しく上がり、食した
時にのみバニラ特有の甘さが口の中で広がるバラエティ
ーに富んだ飲食品類を提供することができる。
According to the present invention, it is possible to provide a flavor imparting agent comprising vanilla tincture as an active ingredient, and to impart a flavor flavor of a vanilla extract characteristic to foods and drinks using the imparting agent. it can. For example, fruit juice drinks,
Beverages such as fruit liquors, milk drinks, carbonated drinks; ice creams, sorbets, cold candy such as popsicles; western confectionery such as cream puffs, custards, financiers, fresh cream; Japanese confectionery; Jams, chewing gums, breads, coffee,
Goods such as cocoa, black tea, tea, and tobacco; Japanese soups, soups such as Western soups;
By adding an appropriate amount of the vanilla tincture of the present invention to various instant drinks and foods, various snack foods, etc., the change in pH in the food is reduced, the body is given richness, the moisturizing effect, the effect of preventing water separation, the water absorption are improved. It is possible to provide a variety of foods and beverages that rise remarkably and spread the sweetness unique to vanilla in the mouth only when eaten.

【0012】[0012]

【実施例】以下、比較例及び実施例によって本発明の態
様をさらに具体的に説明する。但し、実験に関してはバ
ニラチンキのままだとエタノール臭が強く立つので、バ
ニラオレオレジンにして比較することとなる。 実施例1 三角フラスコに、約1cmにカットしたバニラビーンズ
(ブルボン産)15g、99%エタノール23.1g、
50%乳酸ナトリウム水溶液14g、水18.9gを仕
込み、三角フラスコ内の抽出温度50°Cで4時間攪拌
しながら抽出する。抽出終了後、20°Cに自然冷却
し、一昼夜(24時間)放置後、ガーゼ等でデカント分
離する。抽出し終わったカットバニラビーンズに翌日ま
た99%エタノール19.39g、50%乳酸ナトリウ
ム水溶液11.75g、水15.86gを仕込み、その
後は上記条件と同条件で処理し、合計90gのバニラチ
ンキを得た。そこで得たバニラチンキを15gまでバス
にて揮発凝縮させ、15gのオレオレジン10fを摂取
する(実施例1;本発明品NO.1)。pH;6.7
(±0.1)。
The embodiments of the present invention will be described more specifically with reference to comparative examples and examples. However, regarding the experiment, if the vanilla tincture is left as it is, the ethanol odor becomes strong. Therefore, comparison is made with vanilla oleoresin. Example 1 In an Erlenmeyer flask, 15 g of vanilla beans (from Bourbon) cut to about 1 cm, 23.1 g of 99% ethanol,
14 g of a 50% aqueous sodium lactate solution and 18.9 g of water are charged, and the mixture is extracted while stirring at an extraction temperature of 50 ° C. in an Erlenmeyer flask for 4 hours. After the completion of the extraction, the mixture is naturally cooled to 20 ° C., left for 24 hours, and then decanted with gauze or the like. The extracted vanilla beans were charged with 19.39 g of 99% ethanol, 11.75 g of a 50% aqueous sodium lactate solution, and 15.86 g of water the next day, and then treated under the same conditions as above to obtain a total of 90 g of vanilla tincture. Was. The vanilla tincture thus obtained is volatilized and condensed in a bath up to 15 g, and 15 g of oleoresin 10f is taken (Example 1; product No. 1 of the present invention). pH; 6.7
(± 0.1).

【0013】参考例1(時間の変化) 実施例1における抽出時間を2時間にした他は、実施例
1と同一条件によりバニラオレオレジンを製造した(参
考例1;参考品NO.1)。 参考例2(時間の変化) 実施例1における抽出時間を6時間にした他は、実施例
1と同一条件によりバニラオレオレジンを製造した(参
考例2;参考品NO.2)。
Reference Example 1 (Change in time) Vanilla oleoresin was produced under the same conditions as in Example 1 except that the extraction time in Example 1 was changed to 2 hours (Reference Example 1; Reference No. 1). Reference Example 2 (Change in time) Vanilla oleoresin was produced under the same conditions as in Example 1 except that the extraction time in Example 1 was changed to 6 hours (Reference Example 2; Reference No. 2).

【0014】参考例3(時間の変化) 実施例1における抽出時間を8時間にした他は、実施例
1と同一条件によりバニラオレオレジンを製造した(参
考例3;参考品NO.3)。抽出時間の変化に関して実
施例1及び参考例1乃至参考例3(参考品NO.1乃至
参考品NO.3)における抽出時間の変化に伴い生じる
抽出量の変化を、液体クロマトグラフィにて検査した結
果、4時間以上抽出しても劇的な変化は見られないた
め、物理的な考えも含めて今後の実験の抽出時間は、4
時間のみの時間で行うこととする。
Reference Example 3 (Change in time) Vanilla oleoresin was produced under the same conditions as in Example 1 except that the extraction time in Example 1 was changed to 8 hours (Reference Example 3; Reference No. 3). As to the change of the extraction time, the result of examining the change of the amount of extraction caused by the change of the extraction time in Example 1 and Reference Examples 1 to 3 (Reference No. 1 to Reference No. 3) by liquid chromatography. Since no dramatic change was observed even after extraction for more than 4 hours, the extraction time for future experiments including
It should be done only in time.

【0015】参考例4(抽出温度の変化) 実施例1における抽出温度を45°Cにした他は、実施
例1と同一条件によりバニラオレオレジンを製造した
(参考例4;参考品NO.4)。 参考例5(抽出温度の変化) 実施例1における抽出温度を55°Cにした他は、実施
例1と同一条件によりバニラオレオレジンを製造した
(参考例5;参考品NO.5)。
Reference Example 4 (Change in extraction temperature) A vanilla oleoresin was produced under the same conditions as in Example 1 except that the extraction temperature in Example 1 was changed to 45 ° C (Reference Example 4; Reference product No. 4). ). Reference Example 5 (Change in extraction temperature) A vanilla oleoresin was produced under the same conditions as in Example 1 except that the extraction temperature in Example 1 was 55 ° C (Reference Example 5; Reference product No. 5).

【0016】参考例6(抽出温度の変化) 実施例1における抽出温度を60°Cにした他は、実施
例1と同一条件によりバニラオレオレジンを製造した
(参考例6;参考品NO.6)。抽出温度の変化に関し
て実施例1及び参考例4乃至参考例6(参考品NO.4
乃至参考品NO.6)における抽出温度の変化を伴う抽
出量の変化を液体クロマトグラフィにて検査した結果、
50°C以上に抽出温度を上昇させても劇的な変化は見
られないため、熟効率を考慮に入れて今後の実験は、5
0°Cのみの抽出温度で行うこととする。
Reference Example 6 (Change in extraction temperature) Vanilla oleoresin was produced under the same conditions as in Example 1 except that the extraction temperature in Example 1 was changed to 60 ° C (Reference Example 6; Reference product No. 6). ). Example 1 and Reference Examples 4 to 6 (Reference Product No. 4) regarding the change in extraction temperature
Or reference goods NO. As a result of examining the change in the extraction amount accompanying the change in the extraction temperature in 6) by liquid chromatography,
Even if the extraction temperature is increased to 50 ° C. or higher, no dramatic change is observed.
It is performed at an extraction temperature of only 0 ° C.

【0017】参考例7(50%乳酸ナトリウム水溶液0
%の時) 実施例1における50%乳酸ナトリウム水溶液を含水ア
ルコールに差し替えてみる。即ち、99%エタノール3
0.8g、50%乳酸ナトリウム水溶液0g、水25.
2gを仕込み、三角フラスコ内の抽出温度50°Cで4
時間攪拌しながら抽出する。抽出終了後、20°Cに自
然冷却し、一昼夜(24時間)放置後、ガーゼ布でデカ
ント分離する。抽出し終わったカットバニラビーンズに
翌日また99%エタノール25.85g、水25.85
gを仕込んだ他は、実施例1と同条件によりバニラオレ
オレジンを製造した(参考例7;参考品NO.7)。p
H;4.1(±0.1)。
Reference Example 7 (50% aqueous solution of sodium lactate 0
%) The 50% aqueous solution of sodium lactate in Example 1 is replaced with aqueous alcohol. That is, 99% ethanol 3
0.8 g, 50 g of a 50% aqueous sodium lactate solution, water 25.
Charge 2 g and extract at 50 ° C in an Erlenmeyer flask.
Extract while stirring for hours. After completion of the extraction, the mixture is naturally cooled to 20 ° C., left for 24 hours, and then decanted with a gauze cloth. Next day, 25.85 g of 99% ethanol and 25.85 water were added to the cut vanilla beans after the extraction.
g was prepared and vanilla oleoresin was produced under the same conditions as in Example 1 (Reference Example 7; Reference product No. 7). p
H; 4.1 (± 0.1).

【0018】実施例2(50%乳酸ナトリウム水溶液2
0%の時) 実施例1における99%エタノール、50%乳酸ナトリ
ウム水溶液、水の割合を変えてみる。99%エタノール
24.64g、50%乳酸ナトリウム水溶液11.2
g、水20.16gを仕込み、三角フラスコ内の抽出温
度50°Cで4時間攪拌しながら抽出する。抽出終了
後、20°Cに自然冷却し、一昼夜(24時間)放置
後、ガーゼ布でデカント分離する。抽出し終わったカッ
トバニラビーンズに翌日また99%エタノール20.6
8g、50%乳酸ナトリウム水溶液9.4g、水16.
92gを仕込んだ他は、実施例1と同条件によりバニラ
オレオレジンを製造した(実施例2;本発明品NO.
2)。pH;6.6(±0.1)。
Example 2 (50% aqueous solution of sodium lactate 2
(At 0%) The ratio of 99% ethanol, 50% sodium lactate aqueous solution and water in Example 1 is changed. 24.64 g of 99% ethanol, aqueous solution of 50% sodium lactate 11.2
g and 20.16 g of water, and extraction is performed while stirring at an extraction temperature of 50 ° C. for 4 hours in an Erlenmeyer flask. After completion of the extraction, the mixture is naturally cooled to 20 ° C., left for 24 hours, and then decanted with a gauze cloth. The next day, cut the vanilla beans into 99% ethanol 20.6
8 g, 9.4 g of a 50% aqueous sodium lactate solution, water 16.
A vanilla oleoresin was produced under the same conditions as in Example 1 except that 92 g were charged (Example 2; product No. of the present invention).
2). pH; 6.6 (± 0.1).

【0019】実施例3(50%乳酸ナトリウム水溶液3
0%の時) 実施例1における99%エタノール、50%乳酸ナトリ
ウム水溶液、水の割合を変えてみる。99%エタノール
21.56g、50%乳酸ナトリウム水溶液16.8
g、水17.64gを仕込み、三角フラスコ内の抽出温
度50°Cで4時間攪拌しながら抽出する。抽出終了
後、20°Cに自然冷却し、一昼夜(24時間)放置
後、ガーゼ布でデカント分離する。抽出し終わったカッ
トバニラビーンズに翌日また99%エタノール18.0
95g、50%乳酸ナトリウム水溶液14.1g、水1
4.805gを仕込んだ他は、実施例1と同条件により
バニラオレオレジンを製造した(実施例3;本発明品N
O.3)。pH;6.8(±0.1)。
Example 3 (50% aqueous solution of sodium lactate 3
(At 0%) The ratio of 99% ethanol, 50% sodium lactate aqueous solution and water in Example 1 is changed. 21.56 g of 99% ethanol, 16.8% aqueous solution of sodium lactate 16.8
g and 17.64 g of water, and extraction was performed while stirring at an extraction temperature of 50 ° C. for 4 hours in an Erlenmeyer flask. After completion of the extraction, the mixture is naturally cooled to 20 ° C., left for 24 hours, and then decanted with a gauze cloth. After the extraction, cut vanilla beans were added to the next day with 99% ethanol 18.0.
95 g, 50% sodium lactate aqueous solution 14.1 g, water 1
A vanilla oleoresin was produced under the same conditions as in Example 1 except that 4.805 g was charged (Example 3; product N of the present invention).
O. 3). pH; 6.8 (± 0.1).

【0020】実施例4(50%乳酸ナトリウム水溶液3
5%の時) 実施例1における99%エタノール、50%乳酸ナトリ
ウム水溶液、水の割合を変えてみる。99%エタノール
20.02g、50%乳酸ナトリウム水溶液19.6
g、水16.38gを仕込み、三角フラスコ内の抽出温
度50°Cで4時間攪拌しながら抽出する。抽出終了
後、20°Cに自然冷却し、一昼夜(24時間)放置
後、ガーゼ布でデカント分離する。抽出し終わったカッ
トバニラビーンズに翌日また99%エタノール16.8
025g、50%乳酸ナトリウム水溶液16.45g、
水13.7475gを仕込んだ他は、実施例1と同条件
によりバニラオレオレジンを製造した(実施例4;本発
明品NO.4)。pH;6.8(±0.1)。
Example 4 (50% aqueous solution of sodium lactate 3
At the time of 5%) The proportions of 99% ethanol, 50% sodium lactate aqueous solution and water in Example 1 are changed. 20.02 g of 99% ethanol, 19.6 of 50% aqueous sodium lactate solution
g and 16.38 g of water, and extraction is performed while stirring at an extraction temperature of 50 ° C. for 4 hours in an Erlenmeyer flask. After completion of the extraction, the mixture is naturally cooled to 20 ° C., left for 24 hours, and then decanted with a gauze cloth. Next day, add 16.8% 99% ethanol to cut vanilla beans after extraction.
025 g, 50% sodium lactate aqueous solution 16.45 g,
A vanilla oleoresin was produced under the same conditions as in Example 1 except that 13.7475 g of water was charged (Example 4; product No. 4 of the present invention). pH; 6.8 (± 0.1).

【0021】実施例5(50%乳酸ナトリウム水溶液4
0%の時) 実施例1における99%エタノール、50%乳酸ナトリ
ウム水溶液、水の割合を変えてみる。99%エタノール
18.48g、50%乳酸ナトリウム水溶液22.4
g、水15.12g、を仕込み、三角フラスコ内の抽出
温度50°Cで4時間攪拌しながら抽出する。抽出終了
後、20°Cに自然冷却し、一昼夜(24時間)放置
後、ガーゼ布でデカント分離する。抽出し終わったカッ
トバニラビーンズに翌日また99%エタノール15.5
1g、50%乳酸ナトリウム水溶液18.8g、水1
2.69gを仕込んだ他は、実施例1と同条件によりバ
ニラオレオレジンを製造した(実施例5;本発明品N
O.5)。pH;6.9(±0.1)。
Example 5 (50% aqueous solution of sodium lactate 4
(At 0%) The ratio of 99% ethanol, 50% sodium lactate aqueous solution and water in Example 1 is changed. 18.48 g of 99% ethanol, 22.4% aqueous 50% sodium lactate solution
g and 15.12 g of water, and extraction was performed while stirring at an extraction temperature of 50 ° C. for 4 hours in an Erlenmeyer flask. After completion of the extraction, the mixture is naturally cooled to 20 ° C., left for 24 hours, and then decanted with a gauze cloth. Next day, add 15.5% 99% ethanol to cut vanilla beans after extraction.
1 g, 50% aqueous sodium lactate solution 18.8 g, water 1
A vanilla oleoresin was produced under the same conditions as in Example 1 except that 2.69 g was charged (Example 5; product N of the present invention).
O. 5). pH; 6.9 (± 0.1).

【0022】実施例6(50%乳酸ナトリウム水溶液5
0%の時) 実施例1における99%エタノール、50%乳酸ナトリ
ウム水溶液、水の割合を変えてみる。99%エタノール
15.4g、50%乳酸ナトリウム水溶液28g、水1
2.6gを仕込み、三角フラスコ内の抽出温度50°C
で4時間攪拌しながら抽出する。抽出終了後、20°C
に自然冷却し、一昼夜(24時間)放置後、ガーゼ布で
デカント分離する。抽出し終わったカットバニラビーン
ズに翌日また99%エタノール12.925g、50%
乳酸ナトリウム水溶液23.5g、水10.575gを
仕込んだ他は、実施例1と同条件によりバニラオレオレ
ジンを製造した(実施例6;本発明品NO.6)。p
H;6.9(±0.1)。
Example 6 (50% aqueous solution of sodium lactate 5
(At 0%) The ratio of 99% ethanol, 50% sodium lactate aqueous solution and water in Example 1 is changed. 99% ethanol 15.4g, 50% sodium lactate aqueous solution 28g, water 1
2.6 g was charged, and the extraction temperature in an Erlenmeyer flask was 50 ° C.
For 4 hours while stirring. After extraction, 20 ° C
After natural cooling for 24 hours, the mixture is decanted with a gauze cloth. After the extraction, cut vanilla beans were added to the next day.
A vanilla oleoresin was produced under the same conditions as in Example 1 except that 23.5 g of an aqueous solution of sodium lactate and 10.575 g of water were charged (Example 6; product No. 6 of the present invention). p
H; 6.9 (± 0.1).

【0023】実施例7(50%乳酸ナトリウム水溶液7
5%の時) 実施例1における99%エタノール、50%乳酸ナトリ
ウム水溶液、水の割合を変えてみる。99%エタノール
7.7g、50%乳酸ナトリウム水溶液42g、水6.
3gを仕込み、三角フラスコ内の抽出温度50°Cで4
時間攪拌しながら抽出する。抽出終了後、20°Cに自
然冷却し、一昼夜(24時間)放置後、ガーゼ布でデカ
ント分離する。抽出し終わったカットバニラビーンズに
翌日また99%エタノール6.4625g、50%乳酸
ナトリウム水溶液35.25g、水5.2875gを仕
込んだ他は、実施例1と同条件によりバニラオレオレジ
ンを製造した(実施例7;本発明品NO.7)。pH;
7.2(±0.1)。 実施例8(50%乳酸ナトリウム水溶液100%の時) 実施例1における99%エタノール、50%乳酸ナトリ
ウム水溶液、水の割合を変えてみる。99%エタノール
0g、50%乳酸ナトリウム水溶液56g、水0gを仕
込み、三角フラスコ内の抽出温度50°Cで4時間攪拌
しながら抽出する。抽出終了後、20°Cに自然冷却
し、一昼夜(24時間)放置後、ガーゼ布でデカント分
離する。抽出し終わったカットバニラビーンズに翌日ま
た99%エタノール0g、50%乳酸ナトリウム水溶液
47g、水0gを仕込んだ他は、実施例1と同条件によ
りバニラオレオレジンを製造した(実施例8;本発明品
NO.8)。pH;7.4(±0.1)。
Example 7 (50% aqueous solution of sodium lactate 7
At the time of 5%) The proportions of 99% ethanol, 50% sodium lactate aqueous solution and water in Example 1 are changed. 7.7 g of 99% ethanol, 42 g of a 50% aqueous solution of sodium lactate, water 6.
Charge 3g and extract at 50 ° C in an Erlenmeyer flask.
Extract while stirring for hours. After completion of the extraction, the mixture is naturally cooled to 20 ° C., left for 24 hours, and then decanted with a gauze cloth. The next day, vanilla oleoresin was produced under the same conditions as in Example 1 except that cut vanilla beans after extraction were charged with 6.4625 g of 99% ethanol, 35.25 g of a 50% aqueous sodium lactate solution, and 5.2875 g of water the next day ( Example 7: Invention product No. 7). pH;
7.2 (± 0.1). Example 8 (when the 50% aqueous sodium lactate solution is 100%) The proportions of 99% ethanol, 50% aqueous sodium lactate solution and water in Example 1 are changed. 0 g of 99% ethanol, 56 g of a 50% sodium lactate aqueous solution and 0 g of water are charged, and the mixture is extracted while stirring at an extraction temperature of 50 ° C. in an Erlenmeyer flask for 4 hours. After completion of the extraction, the mixture is naturally cooled to 20 ° C., left for 24 hours, and then decanted with a gauze cloth. A vanilla oleoresin was produced under the same conditions as in Example 1 except that cut vanilla beans after extraction were charged with 0 g of 99% ethanol, 47 g of a 50% aqueous sodium lactate solution, and 0 g of water the next day (Example 8; the present invention). Product No. 8). pH; 7.4 (± 0.1).

【0024】試験例1 抽出時間の変化に関して、実施例1及び、参考例1乃至
参考例3(参考品NO.1乃至参考例NO.3)におけ
る抽出時間の変化に伴い生じる抽出量の変化を、液体ク
ロマトグラフィにて検査した結果、参考例1(参考品N
O.1)のように2時間攪拌抽出しても、カラメル成
分、天然成分、バニリン成分のいずれもあまり抽出出来
なかった。また、参考例2(参考品NO.2)及び、参
考例3(参考品NO.3)のように4時間以上抽出して
も、カラメル成分、天然成分、バニリン成分のいずれに
も劇的な変化は見られないため、工業的製法の見地及び
物理的見地も含めて抽出時間は4時間が最適であるとい
う結論に達した。
Test Example 1 With respect to the change in the extraction time, the change in the amount of extraction caused by the change in the extraction time in Example 1 and Reference Examples 1 to 3 (Reference Products No. 1 to No. 3) was examined. As a result of inspection by liquid chromatography, Reference Example 1 (Reference product N
O. Even with stirring and extraction for 2 hours as in 1), none of the caramel component, natural component, and vanillin component could be extracted much. In addition, even if extracted for 4 hours or more as in Reference Example 2 (Reference Product No. 2) and Reference Example 3 (Reference Product No. 3), the caramel component, the natural component, and the vanillin component are all dramatic. Since no changes were seen, it was concluded that the extraction time was 4 hours optimal, including the industrial manufacturing and physical aspects.

【0025】試験例2 抽出時間の変化に関して、実施例1(本発明品NO.
1)及び、参考例4(参考品NO.4)乃至参考例6
(参考品NO.6)における抽出時間の変化に伴う抽出
量の変化を、液体クロマトグラフィにて検査した結果、
参考例4(参考品NO.4)において抽出温度を45°
Cにしても、カラメル成分、天然成分、バニリン成分の
いずれもあまり抽出出来なかった。また、参考例5(参
考品NO.5)及び、参考例6(参考品NO.6)のよ
うに55°C以上に抽出温度を上昇させても劇的な変化
は見られないため、熟効率を考慮に入れて、50°Cの
抽出温度が最適であるという結論に達した。
Test Example 2 With respect to the change in the extraction time, Example 1 (Product No.
1) and Reference Example 4 (Reference Product No. 4) to Reference Example 6
As a result of examining the change of the extraction amount with the change of the extraction time in (Reference Product No. 6) by liquid chromatography,
In Reference Example 4 (Reference Product No. 4), the extraction temperature was 45 °.
Even with C, none of the caramel component, natural component, and vanillin component could be extracted much. Moreover, even if the extraction temperature is increased to 55 ° C. or higher as in Reference Example 5 (Reference Product No. 5) and Reference Example 6 (Reference Product No. 6), no dramatic change is observed. Taking into account the efficiency, it was concluded that an extraction temperature of 50 ° C. was optimal.

【0026】試験例3 乳酸ナトリウムの添加量に関して、実施例1乃至実施例
8を液体クロマトグラフィーにそれぞれかけた結果、乳
酸ナトリウム20%以下だとカラメル成分、天然成分、
バニリン成分全てにおいて低い値を示す。また、30%
以上だと天然成分及びバニリン成分の抽出は飽和状態に
なり、カラメル成分の抽出が減少していき、チンキとし
ての重要な成分を一つ欠くことになるので、一般には避
けることが望ましい。
Test Example 3 As to the amount of sodium lactate added, Examples 1 to 8 were subjected to liquid chromatography. As a result, if the amount of sodium lactate was 20% or less, caramel component, natural component,
All vanillin components show low values. In addition, 30%
As described above, the extraction of the natural component and the vanillin component becomes saturated, the extraction of the caramel component decreases, and one important component as tincture is lost.

【0027】試験例4 常法により乳脂肪分10%のアイスクリーム生地を調整
し、実施例1(本発明品NO.1)と参考例7(参考品
NO.7)で得られたバニラオレオレジンをそれぞれ
0.2%添加したアイスクリームを調整した。これらの
アイスクリームについて良く訓練された10名のパネラ
ーにより、2点の比較法による官能評価を行った。その
結果を表−1に示す。
Test Example 4 A vanilla oleoresin obtained in Example 1 (Product No. 1 of the present invention) and Reference Example 7 (No. 7) was prepared by preparing an ice cream dough having a milk fat content of 10% by a conventional method. Ice cream to which 0.2% of each gin was added was prepared. Sensory evaluation was performed on these ice creams by 10 well-trained panelists by a two-point comparison method. Table 1 shows the results.

【0028】 表−1評価項目 本発明品NO.1 参考品NO.7 香味が強く好ましく、天然感がある方 8名 2名 濃厚芳醇で熟成感が優れている方 9名 1名 試験例5 試験例4同様に、実施例2で得られた本発明品NO.2
と参考例7で得られた参考品NO.7を官能評価した結
果を表−2に示す。
Table 1 Evaluation Items of the Invention No. 1 Reference product NO. 7 Strong and preferred flavor, natural feeling 8 2 Rich, rich and excellent ripening 9 9 Test Example 5 Similarly to Test Example 4, the product of the present invention NO. 2
And the reference product No. obtained in Reference Example 7. Table 2 shows the results of sensory evaluation of No. 7.

【0029】 表−2評価項目 本発明品NO.2 参考品NO.7 香味が強く好ましく、天然感がある方 7名 3名 濃厚芳醇で熟成感が優れている方 9名 1名 試験例6 試験例4同様に、実施例3で得られた本発明品NO.3
と参考例7で得られた参考品NO.7を官能評価した結
果を表−3に示す。
Table 2 Evaluation Items of the Invention No. 2 Reference product NO. 7 Strong and preferred flavor and natural feeling 7 3 Rich and rich and excellent ripening 9 9 1 Test Example 6 Similarly to Test Example 4, the product of the present invention NO. 3
And the reference product No. obtained in Reference Example 7. Table 3 shows the results of the sensory evaluation of No. 7.

【0030】 表−3評価項目 本発明品NO.3 参考品NO.7 香味が強く好ましく、天然感がある方 7名 3名 濃厚芳醇で熟成感が優れている方 8名 2名 試験例7 試験例4同様に、実施例4で得られた本発明品NO.4
と参考例7で得られた参考品NO.7を官能評価した結
果を表−4に示す。
Table 3 Evaluation Items of the Invention No. 3 Reference product NO. 7 Strong and preferred flavor and natural feeling 7 3 Rich and rich and excellent maturation 8 2 Test Example 7 Similarly to Test Example 4, the product of the present invention NO. 4
And the reference product No. obtained in Reference Example 7. Table 4 shows the results of the sensory evaluation of No. 7.

【0031】 表−4評価項目 本発明品NO.4 参考品NO.7 香味が強く好ましく、天然感がある方 7名 3名 濃厚芳醇で熟成感が優れている方 8名 2名 試験例8 試験例4同様に、実施例5で得られた本発明品NO.5
と参考例7で得られた参考品NO.7を官能評価した結
果を表−5に示す。
Table 4 Evaluation Items of the Invention No. 4 Reference product NO. 7 Strong and preferred flavor and natural feeling 7 3 Rich and rich and excellent ripening 8 8 Test Example 8 Similarly to Test Example 4, the product of the present invention No. 5 obtained in Example 5 was used. 5
And the reference product No. obtained in Reference Example 7. Table 5 shows the results of the sensory evaluation of No. 7.

【0032】 表−5評価項目 本発明品NO.5 参考品NO.7 香味が強く好ましく、天然感がある方 7名 3名 濃厚芳醇で熟成感が優れている方 7名 3名 試験例9 試験例4同様に、実施例6で得られた本発明品NO.6
と参考例7で得られた参考品NO.7を官能評価した結
果を表−6に示す。
[0032] Table -5 endpoints present invention product NO. 5 Reference product NO. 7 Strong and preferred flavor, natural feeling 7 3 Rich, rich and excellent maturity 7 3 Test Example 9 Similarly to Test Example 4, the product of the present invention NO. 6
And the reference product No. obtained in Reference Example 7. Table 6 shows the results of the sensory evaluation of No. 7.

【0033】 表−6評価項目 本発明品NO.6 参考品NO.7 香味が強く好ましく、天然感がある方 7名 3名 濃厚芳醇で熟成感が優れている方 7名 3名 試験例10 試験例4同様に、実施例7で得られた本発明品NO.7
と参考例7で得られた参考品NO.7を官能評価した結
果を表−7に示す。
[0033] Table -6 endpoints present invention product NO. 6 Reference product NO. 7 Strong and preferred flavor and natural feeling 7 3 Rich and rich and excellent ripening 7 3 Test Example 10 Similarly to Test Example 4, the product of the present invention obtained in Example 7 was NO. 7
And the reference product No. obtained in Reference Example 7. Table 7 shows the results of the sensory evaluation of No. 7.

【0034】 表−7評価項目 本発明品NO.7 参考品NO.7 香味が強く好ましく、天然感がある方 7名 3名 濃厚芳醇で熟成感が優れている方 7名 3名 試験例11 試験例4同様に、実施例8で得られた本発明品NO.8
と参考例7で得られた参考品NO.7を官能評価した結
果を表−8に示す。
Table 7 Evaluation Items of the Invention No. 7 Reference product NO. 7 Strong and preferable flavor, natural feeling 7 3 Rich, rich and excellent ripening feeling 7 3 Test Example 11 Similarly to Test Example 4, the product of the present invention NO. 8
And the reference product No. obtained in Reference Example 7. Table 8 shows the results of the sensory evaluation of No. 7.

【0035】 表−8評価項目 本発明品NO.8 参考品NO.7 香味が強く好ましく、天然感がある方 7名 3名 濃厚芳醇で熟成感が優れている方 7名 3名 試験例12 市販されている動物性生クリーム生地を調整し、実施例
1(本発明品NO.1)と参考例7(参考品NO.7)
で得られたバニラオレオレジンをそれぞれ0.2%添加
した生クリームを調整した。これらの生クリームについ
て良く訓練された10名のパネラーにより、2点の比較
法による官能評価を行った。その結果を表−9に示す。
Table 8 Evaluation Items of the Invention No. 8 Reference product NO. 7 Strong and preferred flavor and natural feeling 7 3 Rich and rich and excellent maturity 7 3 Test Example 12 A commercially available animal raw cream dough was prepared. Invention product No. 1) and Reference example 7 (Reference product No. 7)
A fresh cream to which 0.2% of the vanilla oleoresin obtained in the above was added was prepared. Sensory evaluation was performed on these fresh creams by 10 well-trained panelists by a two-point comparison method. The results are shown in Table-9.

【0036】 表−9評価項目 本発明品NO.1 参考品NO.7 香味が強く好ましく、天然感がある方 8名 2名 濃厚芳醇で熟成感が優れている方 9名 1名 試験例13 試験例12同様に、実施例2で得られた本発明品NO.
2参考例7で得られた参考品NO.7を官能評価した結
果を表−10に示す。
Table 9 Evaluation Items of the Invention No. 1 Reference product NO. 7 Strong and preferred flavor and natural feeling 8 2 Rich and rich and excellent ripening 9 9 1 Test Example 13 Similarly to Test Example 12, the product of the present invention NO.
2 Reference product obtained in Reference Example 7 Table 10 shows the results of the sensory evaluation of No. 7.

【0037】 表−10評価項目 本発明品NO.2 参考品NO.7 香味が強く好ましく、天然感がある方 7名 3名 濃厚芳醇で熟成感が優れている方 9名 1名 試験例14 試験例12同様に、実施例3で得られた本発明品NO.
3参考例7で得られた参考品NO.7を官能評価した結
果を表−11に示す。
Table 10 Evaluation Items of the Invention No. 2 Reference product NO. 7 Strong and preferred flavor and natural feeling 7 3 Rich and rich and excellent ripening 9 9 1 Test Example 14 Similarly to Test Example 12, the product of the present invention obtained in Example 3 was NO.
3 Reference product No. 3 obtained in Reference Example 7. Table 11 shows the results of a sensory evaluation of No. 7.

【0038】 表−11評価項目 本発明品NO.3 参考品NO.7 香味が強く好ましく、天然感がある方 7名 3名 濃厚芳醇で熟成感が優れている方 8名 2名 試験例15 試験例12同様に、実施例4で得られた本発明品NO.
4参考例7で得られた参考品NO.7を官能評価した結
果を表−12に示す。
Table 11 Evaluation Items of the Invention No. 3 Reference product NO. 7 Strong and preferred flavor and natural feeling 7 3 Rich and rich and excellent maturation 8 2 Test Example 15 Similarly to Test Example 12, the product of the present invention NO.
4 Reference product No. 4 obtained in Reference Example 7. Table 12 shows the results of a sensory evaluation of No. 7.

【0039】 表−12評価項目 本発明品NO.4 参考品NO.7 香味が強く好ましく、天然感がある方 7名 3名 濃厚芳醇で熟成感が優れている方 8名 2名 試験例16 試験例12同様に、実施例5で得られた本発明品NO.
5参考例7で得られた参考品NO.7を官能評価した結
果を表−13に示す。
Table 12 Evaluation Items of the Invention No. 4 Reference product NO. 7 Strong and preferable flavor, natural feeling 7 3 Rich, rich and excellent ripening feeling 8 2 Test Example 16 Similarly to Test Example 12, the product of the present invention NO.
5 Reference product obtained in Reference Example 7 Table 13 shows the results of a sensory evaluation of No. 7.

【0040】 表−13評価項目 本発明品NO.5 参考品NO.7 香味が強く好ましく、天然感がある方 7名 3名 濃厚芳醇で熟成感が優れている方 7名 3名 試験例17 試験例12同様に、実施例6で得られた本発明品NO.
6参考例7で得られた参考品NO.7を官能評価した結
果を表−14に示す。
Table 13 Evaluation Items of the Invention No. 5 Reference product NO. 7 Strong and preferred flavor and natural feeling 7 3 Rich and rich and excellent ripening 7 3 Test Example 17 Similarly to Test Example 12, the product of the present invention NO.
Reference product No. 6 obtained in Reference Example 7 Table 14 shows the results of a sensory evaluation of No. 7.

【0041】 表−14評価項目 本発明品NO.6 参考品NO.7 香味が強く好ましく、天然感がある方 7名 3名 濃厚芳醇で熟成感が優れている方 7名 3名 試験例18 試験例12同様に、実施例7で得られた本発明品NO.
7参考例7で得られた参考品NO.7を官能評価した結
果を表−15に示す。
[0041] Table -14 evaluation item the product of the present invention NO. 6 Reference product NO. 7 Strong and preferred flavor and natural feeling 7 3 Rich and rich and excellent ripening 7 3 Test Example 18 Similarly to Test Example 12, the product of the present invention NO.
Reference product No. 7 obtained in Reference Example 7. Table 15 shows the results of a sensory evaluation of No. 7.

【0042】 表−15評価項目 本発明品NO.7 参考品NO.7 香味が強く好ましく、天然感がある方 7名 3名 濃厚芳醇で熟成感が優れている方 7名 3名 試験例19 試験例12同様に、実施例8で得られた本発明品NO.
8参考例7で得られた参考品NO.7を官能評価した結
果を表−16に示す。
Table 15 Evaluation Items of the Invention No. 7 Reference product NO. 7 Strong and preferred flavor and natural feeling 7 3 Rich and rich and excellent ripening 7 7 Test Example 19 Similarly to Test Example 12, the product of the present invention obtained in Example 8 was the same.
8 Reference product No. 8 obtained in Reference Example 7. Table 16 shows the results of a sensory evaluation of No. 7.

【0043】 表−16評価項目 本発明品NO.8 参考品NO.7 香味が強く好ましく、天然感がある方 7名 3名 濃厚芳醇で熟成感が優れている方 7名 3名 試験例20 試験例4乃至試験例19において、4°Cで1週間保存
した後、それぞれの保水性を2点比較法により評価を行
った結果、いずれも参考品NO.7よりも本発明品N
O.1乃至本発明品NO.8の方が艶があり干涸びてお
らず、保水性に優れることがわかった。
Table 16 Evaluation Items of the Invention No. 8 Reference product NO. 7 Strong and preferred flavor, natural feeling 7 3 Rich, rich and excellent maturity 7 3 Test Example 20 In Test Examples 4 to 19, after storing at 4 ° C for 1 week And the water retention of each was evaluated by a two-point comparison method. N of the present invention than 7
O. Nos. 1 to NO. It was found that No. 8 was glossy and not dry, and was superior in water retention.

【0044】表−1乃至表−16の結果及び試験例20
の結果から明らかな如く、本発明品はいずれもそれぞれ
対応する参考品に比較してバニラ様の香味付与能が強
く、濃厚芳醇で且つ深みが有り天然感に富み、焼き菓子
・生菓子等に添加した後、食した時にのみバニラ特有の
甘さが口の中で広がる感じが出せ、更に保水性に優れる
ことがわかった。
Results of Tables 1 to 16 and Test Example 20
As is clear from the results, all of the products of the present invention have a stronger vanilla-like flavor imparting ability than the corresponding reference products, and are rich in richness and depth, rich in natural feeling, and added to baked confectionery and raw confectionery. After that, only when eaten, the sweetness peculiar to vanilla spreads in the mouth, and it was found that it was excellent in water retention.

【0045】[0045]

【発明の効果】本発明によれば、バニラビーンズに溶媒
を急速に浸透させて有効成分を短時間に効率よく強制抽
出することができ、バニラ様の香気香味付与能が強く、
且つバニラ抽出物独特のサヤ臭域いはビーンズ臭がな
く、濃厚芳醇で且つ深みが有り天然感に富み、焼き菓子
・生菓子等に添加した後、食した時にのみバニラ特有の
甘さが口の中で広がり、添加した製品は保水性に富むよ
うになるバニラチンキを得ることができる。
According to the present invention, the solvent can be rapidly permeated into the vanilla beans, the active ingredient can be efficiently extracted in a short time, and the vanilla-like aroma imparting ability is strong.
And the unique smell of vanilla extract has no bean smell, it is rich, rich and deep, rich in natural sensation, added to baked confectionery, raw confectionery, etc., and the sweetness unique to vanilla only when eaten The vanilla tincture that spreads in and the added product becomes rich in water retention can be obtained.

【0046】また、乳酸ナトリウムの緩衝作用により、
得られたバニラチンキは略中性となるので(実施例1〜
8参照)、酸性臭やアルカリ臭等の異の香りを発する
こともない。
Also, due to the buffering action of sodium lactate,
Since the obtained vanilla tincture becomes substantially neutral (Examples 1 to 5)
8 reference), nor emit a different quality scent of such acidic odor and alkaline odor.

───────────────────────────────────────────────────── フロントページの続き (58)調査した分野(Int.Cl.7,DB名) C11B 9/02 A23L 1/221 C11B 1/10 C11B 9/00 ──────────────────────────────────────────────────続 き Continued on the front page (58) Field surveyed (Int.Cl. 7 , DB name) C11B 9/02 A23L 1/221 C11B 1/10 C11B 9/00

Claims (4)

(57)【特許請求の範囲】(57) [Claims] 【請求項1】 キュアリング処理後のバニラビ−ンズ
を、乳酸ナトリウムと含水アルコ−ルとの混合物の存在
下で抽出処理することを特徴とするバニラチンキの抽出
方法。
1. A method for extracting vanilla tincture, comprising extracting vanilla beans after curing treatment in the presence of a mixture of sodium lactate and water-containing alcohol.
【請求項2】 抽出処理において、攪拌抽出を4時間行
う、請求項1記載のバニラチンキの抽出方法。
2. The method for extracting vanilla tincture according to claim 1, wherein stirring extraction is performed for 4 hours in the extraction process.
【請求項3】 抽出処理を50°Cで行う、請求項1又
は2記載のバニラチンキの抽出方法。
3. The method for extracting vanilla tincture according to claim 1, wherein the extraction is performed at 50 ° C.
【請求項4】 抽出溶媒中の乳酸ナトリウムの量を20
〜30%とする、請求項1、2又は3記載のバニラチン
キの抽出方法。
4. The amount of sodium lactate in the extraction solvent is 20
The method for extracting vanilla tincture according to claim 1, 2 or 3, wherein the concentration is set to 30%.
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103289821A (en) * 2012-03-05 2013-09-11 广州市名花香料有限公司 Preparation method of Vanilla extract

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5546961B2 (en) * 2010-06-15 2014-07-09 長谷川香料株式会社 Method for producing water-soluble extract

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103289821A (en) * 2012-03-05 2013-09-11 广州市名花香料有限公司 Preparation method of Vanilla extract

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