JP2989766B2 - Case hardened steel with excellent fatigue properties and machinability - Google Patents

Case hardened steel with excellent fatigue properties and machinability

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Publication number
JP2989766B2
JP2989766B2 JP7337257A JP33725795A JP2989766B2 JP 2989766 B2 JP2989766 B2 JP 2989766B2 JP 7337257 A JP7337257 A JP 7337257A JP 33725795 A JP33725795 A JP 33725795A JP 2989766 B2 JP2989766 B2 JP 2989766B2
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Japan
Prior art keywords
less
inclusions
steel
machinability
bending fatigue
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JP7337257A
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Japanese (ja)
Other versions
JPH09176784A (en
Inventor
澄恵 野村
義武 松島
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Kobe Steel Ltd
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Kobe Steel Ltd
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Description

【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【0001】[0001]

【発明の属する技術分野】本発明は、浸炭焼入れ処理も
しくは浸炭・窒化焼入れ処理により表面硬化処理の行な
われる機械部品用素材として用いられる肌焼鋼の改質技
術に関し、特に自動車等の歯車、シャフト、等速ジョイ
ント等の機械部品として優れた疲労特性を発揮すると共
に、被削性にも優れた肌焼鋼に関するものである。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a technology for modifying case hardened steel used as a material for machine parts subjected to surface hardening by carburizing and quenching or carburizing / nitriding quenching, and particularly to gears and shafts for automobiles and the like. The present invention relates to a case hardened steel which exhibits excellent fatigue characteristics as a mechanical component such as a constant velocity joint and has excellent machinability.

【0002】[0002]

【従来の技術】肌焼鋼は、例えば自動車や建設機械等の
機械部品のうち特に高疲労特性の求められる部品等に適
用され、浸炭処理や浸炭・窒化処理等の表面硬化処理を
施して用いられる。その中でも代表的なものに歯車があ
り、近年自動車の軽量化および高出力化を増進するた
め、一層の高強度化が求められている。
2. Description of the Related Art Case hardening steel is applied to, for example, parts requiring high fatigue characteristics among mechanical parts such as automobiles and construction machines, and is used after being subjected to a surface hardening treatment such as carburizing treatment or carburizing / nitriding treatment. Can be Among them, a gear is a representative one. In recent years, in order to increase the weight and output of an automobile, a further increase in strength is required.

【0003】ところで歯車用鋼として実用化するに当た
っては、歯車としての高強度化を達成するため、曲げ疲
労特性やピッチング寿命、衝撃疲労特性も問題とされて
おり、このうち歯車の寿命は、特に曲げ疲労特性で律速
されることが多いところから、高強度肌焼鋼の適用(特
開平1−306545号)や浸炭後のショットピーニン
グ処理による表面硬質化処理(特開平1−306521
号)等によって曲げ疲労特性を高める方法が採用されて
きた。
By the way, in order to achieve high strength as a gear, practical use as a steel for a gear requires bending fatigue characteristics, pitting life, and impact fatigue characteristics. Among them, the life of a gear is particularly limited. Since the rate is often determined by the bending fatigue characteristics, application of high-strength case hardening steel (Japanese Patent Application Laid-Open No. 1-306545) and surface hardening treatment by shot peening after carburizing (Japanese Patent Application Laid-Open No. 1-306521)
No.) etc., a method of improving the bending fatigue characteristics has been adopted.

【0004】一方、肌焼鋼の高強度化が進んでくるにつ
れて、鋼中に存在する粗大介在物に起因する疲労寿命の
劣化が注目される様になり、例えば特開平2−2709
35号公報では、疲労特性に悪影響を及ぼす粗大な酸化
物系あるいは窒化物系の介在物を少なく抑えることによ
って疲労特性を高める技術も提案されている。しかしな
がら歯車等では、酸化物系介在物や窒化物系介在物の大
きさを規定するだけでは必ずしも満足のいく疲労特性は
得られず、酸化物系介在物と硫化物系介在物の存在形態
によっては疲労特性が著しく変わってくる。
[0004] On the other hand, as the strength of case hardening steel has increased, deterioration of fatigue life due to coarse inclusions present in the steel has become noticeable.
In Japanese Patent Publication No. 35, there is also proposed a technique for improving fatigue properties by suppressing a large amount of oxide-based or nitride-based inclusions that adversely affect fatigue properties. However, for gears, etc., simply specifying the size of oxide-based inclusions or nitride-based inclusions does not always provide satisfactory fatigue characteristics, and depends on the form of oxide-based inclusions and sulfide-based inclusions. Has a remarkable change in fatigue properties.

【0005】また実際の肌焼き部品では、例えばはす歯
歯車の様に鋼材の圧延方向に対して20〜40°程度の
傾斜方向に外力が作用することもあるため、縦目と横目
の両方に優れた疲労強度が要求される。特に横目の疲労
強度は、Al23 等の硬質な粒状介在物よりも、酸化
物系と硫化物系の複合介在物の方が顕著な影響を及ぼ
す。さらに歯車を製造する際には、熱間鍛造の後に超硬
旋削やホブ加工等により機械加工が施されるが、合金元
素の添加量を増大して素材強度を高めるにつれて鍛造後
あるいは焼ならし後の硬さは高くなってくるので、被削
性の問題が生じてくる。
[0005] In addition, in an actual case hardening part, an external force may act in an inclined direction of about 20 to 40 ° with respect to the rolling direction of steel, such as a helical gear, so that both vertical and horizontal eyes may be used. Excellent fatigue strength is required. In particular, the fatigue strength of the horizontal grain is more significantly affected by the oxide-based and sulfide-based composite inclusions than by hard granular inclusions such as Al 2 O 3 . Furthermore, when manufacturing gears, after forging, machining is performed by carbide turning, hobbing, etc., but after forging or normalizing as the amount of alloying elements is increased and the material strength is increased. Since the later hardness increases, the problem of machinability arises.

【0006】[0006]

【発明が解決しようとする課題】本発明は上記の様な事
情に着目してなされたものであって、その目的は、縦目
・横目両方向に優れた曲げ疲労特性を有すると共に、超
硬旋削やホブ加工等の被削性にも優れた肌焼鋼を提供し
ようとするものである。
SUMMARY OF THE INVENTION The present invention has been made in view of the above-mentioned circumstances, and an object thereof is to provide an excellent bending fatigue characteristic in both longitudinal and transverse directions, and to realize carbide turning. An object of the present invention is to provide a case hardened steel which is excellent in machinability such as hobbing and hobbing.

【0007】[0007]

【課題を解決するための手段】上記課題を解決すること
のできた本発明に係る肌焼鋼は、 C :0.10〜0.30% Mn:0.30〜2.0% Si:1.0%以下(0%を含む) S :0.003〜0.070% Al:0.01〜0.06% N :0.003〜0.03% O :0.002%以下(0%を含む) 残部:Feおよび不可避的不純物 の要件を満足する鋼材からなり、線状または棒状圧延材
の軸心を通る縦断面において、該軸心と平行で且つ該軸
心から 1/4・D(Dは圧延材の直径を表わす)離れた仮
想線を中心線として含む被検面積100mm2 中に存在
する、酸化物系と硫化物系からなる直径10μm以上の
複合介在物が20個以下であり、且つ上記と同一の被検
面積中に存在する直径3μm以上10μm未満の硫化物
系介在物が50個以上であるところに要旨を有してい
る。
The case hardening steel according to the present invention, which can solve the above problems, comprises: C: 0.10 to 0.30% Mn: 0.30 to 2.0% Si: 1. 0% or less (including 0%) S: 0.003 to 0.070% Al: 0.01 to 0.06% N: 0.003 to 0.03% O: 0.002% or less (0% The remainder: made of steel material that satisfies the requirements of Fe and inevitable impurities, and in a vertical section passing through the axis of the linear or rod-shaped rolled material, is parallel to the axis and 1/4 · D from the axis ( D represents the diameter of the rolled material) There are no more than 20 composite inclusions of 10 mm or more in diameter consisting of oxides and sulfides existing in a test area 100 mm 2 including the imaginary distant line as the center line. And sulfide-based inclusions having a diameter of 3 μm or more and less than 10 μm existing in the same test area as described above Has a gist where there are 50 or more.

【0008】上記本発明の肌焼鋼においては、更に他の
元素として他の元素としてNi:0.20〜4.5%、
Cr:0.20〜2.5%、Mo:0.05〜1.0
%、Cu:0.20〜1.0%よりなる群から選択され
る少なくとも一種、あるいは更に他の元素としてB:
0.0003〜0.0050%および/またはTi:
0.003〜0.05%、更にはV:0.03〜1.5
%および/またはNb:0.005〜1.5%、更には
Ca:0.0005〜0.01%、Pb:0.2%以下
(0%を含まない)、Te:0.1%以下(0%を含ま
ない)、Zr:0.1%以下(0%を含まない)よりな
る群から選択される少なくとも一種を含有させることに
よって、肌焼鋼としての特性を更に改質することができ
る。
[0008] In the case hardening steel of the present invention, Ni: 0.20 to 4.5% as another element.
Cr: 0.20 to 2.5%, Mo: 0.05 to 1.0
%, Cu: at least one selected from the group consisting of 0.20 to 1.0%, or B:
0.0003-0.0050% and / or Ti:
0.003 to 0.05%, further V: 0.03 to 1.5
% And / or Nb: 0.005 to 1.5%, Ca: 0.0005 to 0.01%, Pb: 0.2% or less (excluding 0%), Te: 0.1% or less (Not including 0%), Zr: 0.1% or less (not including 0%), by further containing at least one selected from the group consisting of: it can.

【0009】[0009]

【発明の実施の形態】まず、本発明で使用する鋼材の化
学成分を規定した理由について説明する。 C:0.10〜0.30% Cは、強化元素として芯部硬さを確保するのに欠くこと
のできない元素であり、少なくとも0.10%以上含有
させなければならない。しかし、0.30%を超えて過
多に含有させると靭性や被削性が悪くなるので、上限を
0.30%と定めた。Cのより好ましい含有量は0.1
0〜0.25%の範囲である。
DESCRIPTION OF THE PREFERRED EMBODIMENTS First, the reason for defining the chemical composition of the steel used in the present invention will be described. C: 0.10 to 0.30% C is an indispensable element for securing core hardness as a strengthening element, and must be contained at least 0.10% or more. However, if the content exceeds 0.30%, the toughness and machinability deteriorate, so the upper limit is set to 0.30%. A more preferred content of C is 0.1
The range is 0 to 0.25%.

【0010】Si:1.0%以下(0%を含む) Siは、溶製時に脱酸剤として有効に作用する他、強化
元素としても作用して芯部硬さの向上に寄与するが、多
過ぎると浸炭性を害すると共に粒界酸化を助長して曲げ
疲労特性にも悪影響を及ぼすので、多くとも1.0%以
下、好ましくは0.30%以下に抑えるべきである。
Si: 1.0% or less (including 0%) Si not only functions effectively as a deoxidizing agent at the time of melting, but also acts as a strengthening element and contributes to improvement of core hardness. If it is too large, it impairs carburizing properties and promotes grain boundary oxidation to adversely affect bending fatigue properties. Therefore, the content should be kept at most 1.0% or less, preferably 0.30% or less.

【0011】Mn:0.30〜2.0% Mnは溶製時に脱酸剤として有効に作用する他、焼入性
を高めて表層および芯部硬さを高め疲労強度の向上に寄
与する元素であり、それらの作用を有効に発揮させるに
は0.30%以上含有させなければならない。しかし、
多過ぎると素材が硬くなり過ぎて加工性や被削性が悪く
なるので2.0%以下に抑えるべきである。Mnのより
好ましい含有量は0.30〜1.6%の範囲である。
Mn: 0.30 to 2.0% Mn is an element which effectively acts as a deoxidizing agent at the time of melting, and also enhances hardenability to increase the hardness of the surface layer and the core and contributes to the improvement of fatigue strength. In order to exert their effects effectively, the content must be 0.30% or more. But,
If the content is too large, the material becomes too hard and the workability and machinability deteriorate, so the content should be suppressed to 2.0% or less. The more preferred content of Mn is in the range of 0.30 to 1.6%.

【0012】S:0.003〜0.070% Sは被削性向上成分として必要な元素であり、少なくと
も0.003%以上含有させなければならない。しかし
多量に含有させ過ぎると、硫化物系介在物および酸化物
系と硫化物系との粗大な複合介在物の生成量が多くなり
過ぎ、特に横目の曲げ疲労特性や衝撃特性に悪影響が現
われてくるので、0.070%以下、より好ましくは
0.035%以下に抑えるべきである。
S: 0.003 to 0.070% S is an element necessary as a machinability improving component, and must be contained at least 0.003% or more. However, if it is contained too much, the amount of sulfide inclusions and the formation of coarse composite inclusions of oxides and sulfides will be too large, and adversely affect the bending fatigue properties and impact properties of the cross-section in particular. Therefore, it should be suppressed to 0.070% or less, more preferably 0.035% or less.

【0013】Al:0.01〜0.06% Alも溶製時に脱酸成分として有効に作用し、複合介在
物の生成量を抑える作用を有する他、加熱処理時におけ
るオーステナイト結晶粒の成長を抑制して靭性を高める
作用も有しており、こうした作用は0.01%以上含有
させることによって有効に発揮される。しかし、それら
の作用は約0.06%で飽和し、それ以上になるとオー
ステナイト結晶粒を却って粗大化させ靭性を悪化させる
ので、0.06%以下に抑えなければならない。Alの
より好ましい含有量は0.015〜0.040%の範囲
である。
Al: 0.01 to 0.06% Al also effectively acts as a deoxidizing component at the time of smelting, has the effect of suppressing the amount of composite inclusions formed, and also suppresses the growth of austenite crystal grains during heat treatment. It also has the effect of suppressing and increasing the toughness, and such an effect is effectively exhibited by containing 0.01% or more. However, their effects saturate at about 0.06%, and above that, the austenite crystal grains are rather coarsened and the toughness is deteriorated, so they must be suppressed to 0.06% or less. The more preferred content of Al is in the range of 0.015 to 0.040%.

【0014】N:0.003〜0.03% Nは、上記Alと結合してAlNを生成しオーステナイ
ト結晶粒を微細化して靭性向上に寄与するが、0.00
3%以下ではこうした効果が期待できず、一方0.03
%を超えて過多に含有させると、鋳造時や熱間加工時に
割れを起こし易くなる。こうした利害得失を考えてNの
より好ましい含有量は0.003〜0.02%の範囲で
ある。
N: 0.003 to 0.03% N combines with Al to form AlN and refines austenite crystal grains and contributes to improvement in toughness.
Below 3%, such effects cannot be expected, while 0.03%
%, It is easy to cause cracking during casting or hot working. In view of such advantages and disadvantages, the more preferable content of N is in the range of 0.003 to 0.02%.

【0015】O:0.002%以下(0%を含む) OはAl23 やSiO2 等の酸化物系介在物の生成源
となり、疲労特性や切削加工時の超硬工具寿命に悪影響
を及ぼすと共に、複合介在物の核となる酸化物を粗大化
して該複合介在物のサイズを大きくし、特に横目の疲労
特性を劣化させるので、多くとも0.002%以下、よ
り好ましくは0.0015%以下に抑えるべきである。
O: 0.002% or less (including 0%) O becomes a source of oxide-based inclusions such as Al 2 O 3 and SiO 2 and adversely affects fatigue characteristics and the life of a cemented carbide tool during cutting. In addition, the oxides serving as nuclei of the composite inclusions are coarsened to increase the size of the composite inclusions, and particularly to degrade the fatigue characteristics of the grain, so that at most 0.002% or less, more preferably 0.1% or less. It should be kept below 0015%.

【0016】本発明に係る肌焼鋼の残部成分はFeおよ
び不可避的不純物であるが、必要により更に他の元素と
して下記の様な元素を適量含有させることによって、肌
焼鋼としての特性を一段と改善することが可能である。
The remaining components of the case hardening steel according to the present invention are Fe and unavoidable impurities. However, if necessary, the following elements may be added in appropriate amounts to further improve the properties of the case hardening steel. It is possible to improve.

【0017】Ni:0.20〜4.5%、Cr:0.2
0〜2.5%、Mo:0.05〜1.0%、Cu:0.
20〜1.0%よりなる群から選択される少なくとも一
種 これらの元素は、焼入れ性の向上に寄与する点で同効元
素であるといえるが、夫々の作用を詳述すると下記の通
りである。即ちCuは、良好な焼入れ性を確保すると共
に靭性の向上に有効に作用する元素であり、且つ耐食性
の向上にも有効に作用する。その効果は0.20%程度
以上含有させることによって有効に発揮される。しか
し、多過ぎると熱間割れを生じ易くなって熱間加工性を
害するので、1.0%以下、より好ましくは0.60%
以下に抑えるべきである。またNiは、浸炭部の焼入れ
性を確保して不完全焼入組織の生成を抑えると共に靭性
の向上に有効に作用する元素であり、こうした作用は
0.20%程度以上含有させることによって有効に発揮
されるが、その効果は4.5%で飽和するのでそれ以上
の添加は経済的に無駄である。Niのより好ましい含有
量は0.20〜2.0%の範囲である。
Ni: 0.20 to 4.5%, Cr: 0.2
0 to 2.5%, Mo: 0.05 to 1.0%, Cu: 0.
At least one element selected from the group consisting of 20% to 1.0% These elements can be said to be the same in that they contribute to the improvement of hardenability, and their actions are described in detail below. . That is, Cu is an element that secures good hardenability and effectively acts to improve toughness, and also effectively acts to improve corrosion resistance. The effect is effectively exhibited by containing about 0.20% or more. However, if the content is too large, hot cracking is likely to occur and hot workability is impaired, so that the content is 1.0% or less, more preferably 0.60%.
It should be kept below. Ni is an element that secures the hardenability of the carburized portion, suppresses the formation of an incompletely quenched structure, and effectively acts to improve the toughness. Such an effect is effectively achieved by containing about 0.20% or more. The effect is saturated, but the effect is saturated at 4.5%, so that further addition is economically useless. The more preferred content of Ni is in the range of 0.20 to 2.0%.

【0018】Crも、0.20%程度以上含有させるこ
とによって焼入れ性の向上に有効に作用するが、多過ぎ
ると浸炭を阻害するばかりでなく、炭化物の多量生成に
より該炭化物を起点とする亀裂の進展を助長し、曲げ疲
労特性や靭性に悪影響を及ぼすので、2.5%以下に抑
えるべきである。Crのより好ましい含有量は0.30
〜2.0%の範囲である。Moは、浸炭表層部で酸化物
を形成せずに固溶状態で存在し、浸炭層の焼入れ性を高
めて不完全焼入れ組織を低減し、更にはオーステナイト
結晶粒を微細化して曲げ疲労特性や靭性の向上に有効に
作用する元素であり、これらの作用は0.05%程度以
上含有させることによって有効に発揮される。しかし含
有量が多くなり過ぎると、被削性に悪影響が現われてく
るので1.0%以下に抑えなければならない。Moのよ
り好ましい含有量は0.05〜0.50%の範囲であ
る。
[0018] When Cr is also contained in an amount of about 0.20% or more, it effectively acts to improve the hardenability. However, if it is too much, it not only inhibits carburization, but also generates a large amount of carbides, thereby generating cracks originating from the carbides. Therefore, it should be suppressed to 2.5% or less because it promotes the development of the steel sheet and adversely affects the bending fatigue properties and toughness. The more preferred content of Cr is 0.30.
2.02.0%. Mo exists in a solid solution state without forming an oxide on the surface layer of the carburized layer, and enhances the hardenability of the carburized layer to reduce the incompletely quenched structure. It is an element that effectively acts on the improvement of toughness, and these actions are effectively exhibited by containing about 0.05% or more. However, if the content is too large, the machinability will be adversely affected, so it must be suppressed to 1.0% or less. The more preferred content of Mo is in the range of 0.05 to 0.50%.

【0019】V:0.03〜1.5%および/またはN
b:0.005〜1.5% これらの元素は、結晶粒を微細化して靭性向上に寄与
し、また浸炭もしくは浸炭窒化時に炭化物や炭窒化物を
析出させて表面硬さを高め曲げ疲労特性や耐ピッチング
性を高める作用を有する点で同効元素である。即ちVは
炭化物や炭窒化物を生成して結晶粒を微細化し靭性向上
に寄与する他、浸炭量を上げたり浸窒処理によって微細
な炭化物や炭窒化物を生成して焼戻し軟化抵抗を向上さ
せ、曲げ疲労特性や耐ピッチング性を高める作用を有し
ており、それらの効果は0.03%程度以上、好ましく
は0.2%以上含有させることによって有効に発揮され
る。しかしV含有量が多くなり過ぎると、芯部のA3
1 変態点が大幅に低下して芯部のγ化が不十分とな
り、焼きが入りにくくなって硬さ不足となるので、1.
5%以下、より好ましくは1.0%以下に抑えるべきで
ある。Nbも、Vと同様に炭化物や炭窒化物形成元素で
あり、結晶粒を微細化して靭性向上に寄与し、また表面
硬さの向上により曲げ疲労特性や耐ピッチング性の向上
に有効な元素であり、その効果は0.005%程度以
上、より好ましくは0.01%以上含有させることによ
って有効に発揮される。しかしその効果は1.5%で飽
和し、それ以上に添加しても経済的に不利益となるだけ
であるので、1.5%以下、より好ましくは1.0%以
下に抑えるべきである。
V: 0.03-1.5% and / or N
b: 0.005 to 1.5% These elements contribute to the improvement of toughness by refining the crystal grains, and also increase the surface hardness by precipitating carbides and carbonitrides during carburizing or carbonitriding to increase the bending fatigue properties. It is the same element in that it has an effect of improving the pitting resistance. That is, V generates carbides and carbonitrides to refine the crystal grains and contributes to the improvement of toughness, and also increases the amount of carburizing or generates fine carbides and carbonitrides by nitriding to improve tempering softening resistance. In addition, it has an effect of improving bending fatigue characteristics and pitting resistance, and these effects can be effectively exhibited by containing about 0.03% or more, preferably 0.2% or more. However, when the V content becomes too large, A 3 ,
The A 1 transformation point is greatly reduced, and the core is not sufficiently gamma-converted.
It should be kept below 5%, more preferably below 1.0%. Nb is also a carbide and carbonitride forming element, like V, and contributes to the improvement of toughness by refining crystal grains, and is an element effective for improving bending fatigue properties and pitting resistance by improving surface hardness. Yes, the effect is effectively exerted by containing about 0.005% or more, more preferably 0.01% or more. However, the effect saturates at 1.5%, and if added more than that, it is only economically disadvantageous. Therefore, the effect should be suppressed to 1.5% or less, more preferably 1.0% or less. .

【0020】B:0.0003〜0.0050%および
/またはTi:0.003〜0.05% Bは、焼入れ性を高めると共に粒界強度を高めるのに有
効な元素であり、その効果は0.0003%程度以上、
より好ましくは0.0005%以上含有させることによ
って有効に発揮される。しかしそれらの効果は0.00
50%で飽和するので、それ以上の添加は無駄であり、
好ましくは0.0035%程度以下に抑えることが望ま
しい。またTiは、鋼の脱酸・脱窒に有効に作用する
他、B添加による焼入れ性向上効果を安定的かつ効果的
に発揮させる作用を有しており、こうした作用は0.0
03%以上含有させることによって有効に発揮される。
しかし、多過ぎるとTiN等の硬質介在物が多量生成し
て靭性や曲げ疲労特性を劣化させる傾向が生じてくるの
で、0.05%以下、より好ましくは0.04%以下に
抑えるのがよい。
B: 0.0003% to 0.0050% and / or Ti: 0.003% to 0.05% B is an element effective for increasing the hardenability and increasing the grain boundary strength. 0.0003% or more,
More preferably, it is effectively exhibited by containing 0.0005% or more. But their effect is 0.00
Since it saturates at 50%, further addition is useless,
Preferably, it is desirable to suppress the content to about 0.0035% or less. Further, Ti effectively acts on deoxidation and denitrification of steel, and also has an effect of stably and effectively exerting the effect of improving the hardenability by adding B. Such an effect is 0.0%.
Effectively exhibited by containing at least 03%.
However, if the content is too large, a large amount of hard inclusions such as TiN are generated, which tends to deteriorate toughness and bending fatigue properties. Therefore, the content is preferably suppressed to 0.05% or less, more preferably 0.04% or less. .

【0021】Ca:0.0005〜0.01%、Pb:
0.2%以下(0%を含まない)、Te:0.1%以下
(0%を含まない)、Zr:0.1%以下(0%を含ま
ない)よりなる群から選択される少なくとも一種 これらの元素は、いずれも被削性向上に寄与する点で同
効元素である。またCa,Te,Zrは、介在物を球状
化して異方性を改善する作用も有している。即ちCa
は、Mnと共に硫化物系介在物を生成し介在物を球状化
して異方性を改善し、且つ靭性や曲げ疲労特性を劣化さ
せずに被削性を高める作用を有しており、それらの効果
は0.0005%程度以上、より好ましくは0.000
8%以上含有させることによって有効に発揮される。し
かし多過ぎると、粗大なCaSや酸化物系介在物の周り
に硫化物系介在物が結びついた粗大な複合介在物が多量
生成して曲げ疲労特性を劣化させるので、0.01%以
下、より好ましくは0.005%以下に抑えるべきであ
る。Pbも被削性向上元素として有効に作用するが、多
過ぎると曲げ疲労特性やピッチング寿命を大幅に劣化さ
せるので、0.2%以下、より好ましくは0.1%以下
に抑えるべきである。
Ca: 0.0005-0.01%, Pb:
0.2% or less (excluding 0%), Te: 0.1% or less (excluding 0%), Zr: 0.1% or less (excluding 0%), at least selected from the group consisting of: Kind One of these elements is the same in that it contributes to improving machinability. In addition, Ca, Te, and Zr also have an effect of spheroidizing inclusions to improve anisotropy. That is, Ca
Has an effect of generating sulfide-based inclusions together with Mn, spheroidizing the inclusions, improving anisotropy, and enhancing machinability without deteriorating toughness or bending fatigue properties. The effect is about 0.0005% or more, more preferably 0.000%.
Effectively exhibited by containing at least 8%. However, if it is too large, a large amount of coarse composite inclusions in which sulfide-based inclusions are bound around coarse CaS or oxide-based inclusions and deteriorates the bending fatigue properties. Preferably, it should be suppressed to 0.005% or less. Pb also effectively acts as a machinability improving element, but if it is too much, the bending fatigue characteristics and the pitting life are significantly deteriorated. Therefore, it should be suppressed to 0.2% or less, more preferably 0.1% or less.

【0022】Teは、Mn−Teを形成してMnSの周
辺に共存し、熱間圧延時におけるMnSの変形を抑制し
てMnSの球状化を促し、鋼材の靭性や曲げ疲労特性を
劣化させずに被削性を高める作用を有しているが、0.
1%を超えると、非金属系介在物量の増大によって曲げ
疲労特性を却って悪化させるので、0.1%以下に抑え
なければならない。Zrも、熱間圧延時におけるMnS
の変形を抑えてMnSの球状化に寄与し異方性の改善に
有効に作用する他、靭性や曲げ疲労特性を劣化させずに
被削性を高める作用を有しているが、多過ぎるとZrO
2 等の非金属系介在物量が多くなって曲げ疲労特性を逆
に劣化させるので、0.1%以下に抑えなければならな
い。
Te forms Mn-Te and coexists around MnS, suppresses deformation of MnS during hot rolling, promotes spheroidization of MnS, and does not deteriorate the toughness and bending fatigue characteristics of steel. Has the effect of enhancing machinability,
If it exceeds 1%, the bending fatigue characteristics are rather deteriorated due to an increase in the amount of nonmetallic inclusions, so that it must be suppressed to 0.1% or less. Zr is also MnS during hot rolling.
In addition to contributing to the spheroidization of MnS by suppressing deformation and effectively acting to improve anisotropy, it also has the effect of increasing machinability without deteriorating toughness or bending fatigue properties, but too much ZrO
Since the amount of non-metallic inclusions such as 2 increases to deteriorate the bending fatigue properties in reverse, it must be suppressed to 0.1% or less.

【0023】次に、本発明で重要な構成要素となる介在
物の大きさ及び個数の限定理由について詳述する。本発
明の肌焼鋼は、前記成分組成の要件を満足する鋼材を線
状もしくは棒状に圧延した圧延材の、軸心を通る縦断面
において、該軸心と平行で且つ該軸心から1/4・D(D
は圧延材の直径を表わす)離れた仮想線を中心線として
含む被検面積100mm2 当たりに存在する介在物のう
ち、直径10μm以上の酸化物系と硫化物系との複合
介在物が20個以下であり、且つ直径3μm以上10
μm未満の硫化物系介在物が50個以上である点に大き
な特徴を有している。
Next, the reasons for limiting the size and number of inclusions, which are important components in the present invention, will be described in detail. The case hardened steel of the present invention is a rolled material obtained by rolling a steel material satisfying the requirements for the component composition into a wire or a rod, in a vertical cross section passing through the axis, being parallel to the axis and 1 / from the axis. 4 ・ D (D
Represents the diameter of the rolled material) Of the inclusions present per 100 mm 2 of the test area including the imaginary line as a center line, there are 20 composite inclusions of oxide and sulfide with a diameter of 10 μm or more. Or less, and a diameter of 3 μm or more and 10
A major feature is that there are 50 or more sulfide-based inclusions of less than μm.

【0024】上記の要件は、肌焼鋼の疲労特性に及ぼ
す介在物の影響について様々の角度から研究を重ねた結
果到達した要件であって、前述の如く縦目の疲労特性は
もとより横目の疲労特性についても満足のいく性能を確
保するには、非金属介在物のうち、特定サイズの酸化物
系と硫化物系との複合介在物の個数を制御することが重
要であり、その評価基準として、上記の様に、圧延材の
軸心を通る縦断面において、該軸心と平行で且つ該軸心
から 1/4・D離れた仮想線を中心線として含む被検面積
100mm2 中に存在する直径10μm以上の複合介在
物を20個以下に抑えてやれば、特に横目の疲労特性に
おいて優れた特性が安定して発揮される、と言う新たな
知見に基づいている。
The above requirement is a requirement reached as a result of repeated studies on the influence of inclusions on the fatigue characteristics of case hardened steel from various angles. It is important to control the number of composite inclusions of a specific size of oxide and sulfide among non-metallic inclusions in order to ensure satisfactory performance with respect to characteristics. As described above, in a longitudinal section passing through the axis of the rolled material, the area exists in a test area 100 mm 2 which includes, as a center line, an imaginary line parallel to the axis and 1/4 · D away from the axis. It is based on the new finding that, if the number of composite inclusions having a diameter of 10 μm or more is reduced to 20 or less, excellent characteristics, particularly in fatigue characteristics of the eyes, will be stably exhibited.

【0025】ちなみに図1は、後記実施例を含めて多く
の実験データの中から、上記被検面積100mm2 中に
存在する直径10μm以上の複合介在物の個数が、縦目
及び横目の疲労強度に与える影響を整理して示したグラ
フであり、この図からも明らかである様に、上記サイズ
の複合介在物個数が20個未満、とりわけ15個以下の
ものは優れた疲労強度を示しているのに対し、20個を
超えると該疲労強度が極端に悪くなることを確認するこ
とができる。
FIG. 1 shows that the number of composite inclusions having a diameter of 10 μm or more in the test area of 100 mm 2 was determined by the fatigue strength of the vertical and horizontal lines from among many experimental data including the examples described later. As is clear from this figure, the number of composite inclusions of the above-mentioned size is less than 20, especially 15 or less, showing excellent fatigue strength. On the other hand, it can be confirmed that when the number exceeds 20, the fatigue strength becomes extremely poor.

【0026】尚肌焼鋼においても、内部に存在する介在
物が疲労強度に悪影響を及ぼすこと自体は従来から知ら
れていたことであるが、それはあくまでも定性的且つ官
能的な傾向として確認されていたに止まり、様々の介在
物の内どの種の介在物が横目の疲労強度にどの程度悪影
響を及ぼすかといった具体的且つ定量的な傾向までも確
認されていた訳ではない。その結果として、前述の如く
従来の肌焼鋼では特に横目の疲労強度が不安定であり、
例えばはす歯車として実用化した時に疲労寿命不足がし
ばしば発生していたのであるが、本発明によれば、上記
の様に特定被検面積当たりに存在する特定サイズの複合
介在物の個数を評価基準とすることによって、縦目はも
とより横目においても安定して優れた疲労強度を示す肌
焼鋼を確実に得ることが可能となるのである。
It has been conventionally known that even in case hardened steel, the inclusions present therein have an adverse effect on the fatigue strength, but this has been confirmed as a qualitative and sensory tendency. However, no specific and quantitative tendency has been confirmed as to what kind of inclusions among various inclusions adversely affect the fatigue strength of the eyes. As a result, as described above, the conventional case-hardened steel has a particularly unstable fatigue strength at the side edges,
For example, when practically used as a helical gear, insufficient fatigue life often occurred, but according to the present invention, the number of composite inclusions of a specific size existing per specific test area as described above was evaluated. By using as a reference, it is possible to reliably obtain case hardened steel that exhibits excellent fatigue strength stably not only in the longitudinal direction but also in the lateral direction.

【0027】次に前記の要件は、横目の衝撃強度や曲
げ疲労強度を低下させることなく、被削性を高めて切削
工具寿命の延長を図るための要件として規定している。
即ち、まず被削性を向上させるには硫化物系介在物を多
くすることが望ましいが、該硫化物系介在物が直径10
μmを超える粗大なものでは、特に横目の衝撃強度や曲
げ疲労強度を著しく悪化させ、一方直径3μm未満の微
細な硫化物系介在物では、疲労強度等に与える悪影響は
少ないものの被削性の向上に殆ど寄与しない。ところ
が、直径が3μm以上10μm未満の範囲の硫化物系介
在物は、横目の衝撃強度や曲げ疲労強度に殆ど悪影響を
及ぼすことなく優れた被削性向上効果を発揮するという
新たな知見に基づくものである。但し、本発明で意図す
る様な優れた被削性向上効果を安定して発揮させるに
は、上記適正サイズの硫化物系介在物の絶対量も重要で
あり、該介在物量についても定量化すべく更に検討を重
ねた結果、上記で特定される被検面積100mm2 中に
上記適正サイズの硫化物系介在物が50個以上存在する
ものは、安定して良好な被削性を発揮することが確認さ
れた。
Next, the above requirements are defined as requirements for enhancing machinability and extending the life of the cutting tool without lowering the impact strength and bending fatigue strength of the cross section.
That is, to improve machinability, it is desirable to increase the number of sulfide-based inclusions.
Coarse ones exceeding μm significantly degrade the impact strength and bending fatigue strength, especially of grain, while fine sulfide-based inclusions less than 3 μm in diameter have little adverse effect on fatigue strength, but improve machinability. Hardly contributes to However, it is based on a new finding that sulfide-based inclusions having a diameter of 3 μm or more and less than 10 μm exhibit an excellent machinability improving effect with almost no adverse effect on the impact strength or bending fatigue strength of the grain. It is. However, in order to stably exert the excellent machinability improving effect as intended in the present invention, the absolute amount of the sulfide-based inclusion having the appropriate size is also important, and the amount of the inclusion is also quantified. As a result of further study, it was found that a specimen having the above-specified size of sulfide-based inclusions of 50 or more in the test area of 100 mm 2 specified above can stably exhibit good machinability. confirmed.

【0028】尚被削性向上の観点からすると、上記硫化
物系介在物の個数は多い程好ましいが、多くなり過ぎる
と、たとえ適正サイズの硫化物系介在物といえども衝撃
特性や疲労特性に悪影響を及ぼす様になるので、好まし
くは前記被検面積中の個数で250個程度以下に抑える
ことが望ましい。被削性と疲労特性等の物性の両面を考
慮してより好ましい個数は50〜250個の範囲である
(図2参照)。
From the viewpoint of improving machinability, the number of the sulfide-based inclusions is preferably as large as possible. However, if the number is too large, even if the sulfide-based inclusions have an appropriate size, the impact characteristics and the fatigue characteristics are not improved. Therefore, it is desirable that the number in the test area be suppressed to about 250 or less. A more preferable number is in the range of 50 to 250 in consideration of both machinability and physical properties such as fatigue characteristics (see FIG. 2).

【0029】かくして本発明によれば、鋼材の成分組成
を特定すると共に、特定断面を被検面とする特性サイズ
の複合酸化物および硫化物系介在物の個数を特定するこ
とによって、縦目および横目の衝撃特性や疲労特性と被
削性を共に満足する肌焼鋼を得ることが可能となる。
Thus, according to the present invention, by specifying the component composition of the steel material and specifying the number of complex oxide and sulfide-based inclusions of a characteristic size having a specific cross section as a surface to be inspected, It becomes possible to obtain a case hardened steel satisfying both the impact characteristics, fatigue characteristics and machinability of the horizontal grain.

【0030】本発明の肌焼鋼を用いて歯車等の部品を製
造する際には、常法に従って部品形状に加工した後、浸
炭もしくは浸炭・窒化処理(ガス、真空、プラズマ等に
よる浸炭もしくは浸炭・窒化)もしくは軟窒化処理を行
ない、必要によりショットピーニング加工等を行なっ
て、表面を硬質化すれば良い。
When manufacturing parts such as gears using the case hardened steel of the present invention, after processing into a part shape in accordance with a conventional method, carburizing or carburizing / nitriding (carburizing or carburizing by gas, vacuum, plasma, etc.) (Nitriding) or nitrocarburizing treatment and, if necessary, shot peening or the like to harden the surface.

【0031】[0031]

【実施例】次に実施例を挙げて本発明の構成および作用
効果をより具体的に説明するが、本発明はもとより下記
実施例によって制限を受けるものではなく、前後記の趣
旨に適合し得る範囲で変更を加えて実施することも勿論
可能であり、それらはいずれも本発明の技術的範囲に含
まれる。
EXAMPLES Next, the structure and operation and effect of the present invention will be described more specifically with reference to examples. However, the present invention is not limited to the following examples, and can be adapted to the spirit of the preceding and following examples. Of course, the present invention can be implemented with modifications within the scope, and all of them are included in the technical scope of the present invention.

【0032】実施例1 表1に示す成分組成の鋼材を使用し、鋳造時の冷却速度
を変化させて複合介在物等の大きさと量を変えるため、
本発明例では150kg真空溶解炉を用いて溶製してか
ら鋳造し、次いで直径65mmの丸棒に鍛造し、また比
較例では7トンのインゴットに鋳造した後直径65mm
の丸棒に圧延した。
Example 1 A steel material having the composition shown in Table 1 was used, and the size and amount of composite inclusions were changed by changing the cooling rate during casting.
In the example of the present invention, it was melted and cast using a 150 kg vacuum melting furnace, and then forged into a round bar having a diameter of 65 mm.
Rolled into round bars.

【0033】[0033]

【表1】 [Table 1]

【0034】その後、各丸棒中の非金属介在物を調べる
ため、図3に示す如く、各丸棒の軸心を含む縦断面にお
いて、該軸心と平行で且つ該軸心から直径(縦断面の
幅)65mmの1/4・D離れた仮想線を中心線として
含む位置から幅20mm×30mmのサンプルを切り出
し、EPMAを用いて該断面に存在する非金属介在物の
組成、大きさ、個数を調べた。測定は、連続自動運転で
倍率は400倍とし、被検面積100mm2 当たりに存
在する全ての非金属介在物の組成と大きさ及び個数を測
定し、そのうち平均粒径[(長径+短径)/2]が10
μm以上の酸化物系と硫化物系の複合介在物の個数を求
めた。その結果、10μm以上の複合介在物の個数は、
本発明例では11個、比較例では28個であることが確
認された。
Thereafter, in order to examine the non-metallic inclusions in each round bar, as shown in FIG. 3, in a longitudinal section including the axis of each round bar, the diameter (vertical section) is parallel to the axis and from the axis. (Width of the surface) A sample having a width of 20 mm × 30 mm is cut out from a position including a virtual line 1/4 · D apart from 65 mm as a center line, and the composition, size, The number was checked. The measurement was performed in a continuous automatic operation at a magnification of 400 times, and the composition, size, and number of all nonmetallic inclusions existing per 100 mm 2 of the test area were measured, and the average particle diameter [(major axis + minor axis) was obtained. / 2] is 10
The number of oxide-based and sulfide-based composite inclusions of μm or more was determined. As a result, the number of composite inclusions of 10 μm or more is
It was confirmed that the number was 11 in the present invention and 28 in the comparative example.

【0035】また、直径65mmの各鍛造・圧延材に、
1200℃×2時間→空冷の溶体化処理と、900℃×
2時間→空冷の焼ならし処理を施した後、図4に示す如
く各丸棒の中心部から圧延方向に垂直な横目のサンプル
を切り出し、図5に示す寸法形状の平滑小野式回転曲げ
疲労試験片を作製した。各試験片の両端は摩擦接合し、
仕上げ加工を施した。その後、図6に示す条件で浸炭焼
入れ、焼戻し処理を行なった後回転曲げ疲労試験を行な
った。
For each forged / rolled material having a diameter of 65 mm,
1200 ° C x 2 hours → solution treatment with air cooling and 900 ° C x
After 2 hours of air-cooling normalizing treatment, a sample of a cross section perpendicular to the rolling direction was cut out from the center of each round bar as shown in FIG. 4, and a smooth Ono-type rotary bending fatigue having the dimensions and shape shown in FIG. Test pieces were prepared. Both ends of each specimen were friction bonded,
Finished. Thereafter, carburizing and quenching and tempering were performed under the conditions shown in FIG. 6, and then a rotating bending fatigue test was performed.

【0036】図7は、上記で得た介在物測定結果と回転
曲げ疲労試験結果の関係を示したグラフであり、このグ
ラフからも明らかである様に、10μm以上の複合介在
物の個数が20個以下である本発明例は、同個数が20
個を超える比較例に比べて横目の曲げ疲労強度が格段に
優れており、且つそのバラツキも少ないことが分かる。
FIG. 7 is a graph showing the relationship between the results of inclusion measurement obtained above and the results of a rotary bending fatigue test. As is clear from this graph, the number of composite inclusions having a size of 10 μm or more was 20 μm. In the present invention example in which the number is
It can be seen that the bending fatigue strength of the side grain is remarkably excellent and the variation is small as compared with the comparative examples exceeding the number.

【0037】実施例2 表2に示す化学成分の鋼材を溶製し、下記の方法で鋳
造、鍛造(または圧延)を行なった。即ち、鋼No.1
〜14,16〜18,20〜23は150kg真空溶解
炉、No.24は10kgの真空炉で溶製し、鋼No.
15は大気炉で溶製した後、直径65mmの丸棒に鍛造
し、また鋼No.19は7トンのインゴットで鋳造して
から直径65mmの丸棒に圧延した。
Example 2 A steel material having the chemical composition shown in Table 2 was melted and cast and forged (or rolled) by the following methods. That is, steel No. 1
Nos. To 14, 16 to 18, and 20 to 23 are 150 kg vacuum melting furnaces. No. 24 was melted in a 10 kg vacuum furnace.
No. 15 was melted in an atmospheric furnace and then forged into a round bar having a diameter of 65 mm. 19 was cast with a 7-ton ingot and then rolled into a round bar having a diameter of 65 mm.

【0038】[0038]

【表2】 [Table 2]

【0039】その後、各丸棒中の非金属介在物を調べる
ため、図3に示した如く、各丸棒の軸心を含む縦断面に
おいて、該軸心から1/4 ・D離れた仮想線を中心線とし
て含む位置から幅20mm×30mmのサンプルを切り
出し、前記実施例1と同様にしてEPMAにより該断面
に存在する非金属介在物の組成、大きさ、個数を調べ
た。測定は、連続自動運転で倍率は400倍とし、被検
面積100mm2 当たりに存在する全ての非金属介在物
の組成と大きさ及び個数を測定し、そのうち平均粒径
[(長径+短径)/2]が10μm以上の酸化物系と硫
化物系の複合介在物の個数、および平均粒径が3μm以
上10μm未満の硫化物系介在物の個数を求めた。
Thereafter, in order to examine non-metallic inclusions in each round bar, as shown in FIG. 3, in a vertical section including the axis of each round bar, an imaginary line 1 / 4.D away from the axis is shown. A sample having a width of 20 mm × 30 mm was cut out from a position including as a center line, and the composition, size, and number of nonmetallic inclusions present in the cross section were examined by EPMA in the same manner as in Example 1. The measurement was performed in a continuous automatic operation at a magnification of 400 times, and the composition, size, and number of all nonmetallic inclusions existing per 100 mm 2 of the test area were measured, and the average particle diameter [(major axis + minor axis) was obtained. / 2] is 10 μm or more, and the number of oxide- and sulfide-based composite inclusions and the number of sulfide-based inclusions having an average particle diameter of 3 μm or more and less than 10 μm were determined.

【0040】また、直径65mmの各鍛造・圧延材を、
前記実施例1と同様にして1200℃×2時間→空冷の
溶体化処理と、900℃×2時間→空冷の焼ならし処理
を施した後、図4に示した様に各丸棒の中心部から圧延
方向に垂直な横目のサンプルを、また各丸棒の軸心から
1/4 ・D離れた位置から圧延方向に平行に縦目のサンプ
ルを切り出し、平滑小野式回転曲げ疲労試験片を作製し
た。横目の試験片については、試験片の両端を摩擦接合
し、仕上げ加工を施した。その後、図6に示した条件で
浸炭焼入れ、焼戻し処理を行なった後回転曲げ疲労試験
を行なった。
Each forged / rolled material having a diameter of 65 mm is
After performing a solution treatment of 1200 ° C. × 2 hours → air cooling and a normalizing process of 900 ° C. × 2 hours → air cooling in the same manner as in Example 1, as shown in FIG. From the center of each round bar.
A longitudinal sample was cut out from a position 1 / 4.D away in parallel with the rolling direction to produce a smooth Ono-type rotating bending fatigue test piece. Regarding the test piece on the side, the both ends of the test piece were friction-welded and finished. Thereafter, carburizing and quenching and tempering were performed under the conditions shown in FIG. 6, and then a rotary bending fatigue test was performed.

【0041】介在物測定結果および曲げ疲労試験結果を
表3に示す。尚、回転曲げ疲労試験結果は、107 回の
疲労強度で比較した。また、溶体化処理および焼ならし
処理を施した各丸棒について、表4に示す条件で切削試
験を行ない、その結果を表3に併記した。
Table 3 shows the results of inclusion measurement and bending fatigue test. The rotational bending fatigue test results were compared with the fatigue strength of 10 7 times. Further, a cutting test was performed on each of the round bars subjected to the solution treatment and the normalizing process under the conditions shown in Table 4, and the results are also shown in Table 3.

【0042】[0042]

【表3】 [Table 3]

【0043】[0043]

【表4】 [Table 4]

【0044】表3,4より次の様に考えることができ
る。鋼No.1〜11は、本発明の規定要件を全て満足
する実施例であり、鋼材の成分組成が適正であり、しか
も10μmの複合介在物の個数が10個以下で且つ3μ
m以上10μm未満の硫化物系介在物が50個以上存在
しているため、曲げ疲労強度および被削性(超硬工具寿
命)いのいずれにおいても優れた結果が得られている。
From Tables 3 and 4, it can be considered as follows. Steel No. Examples 1 to 11 satisfy all of the requirements of the present invention. The composition of the steel material is appropriate, and the number of 10 μm composite inclusions is 10 or less and 3 μm.
Since there are 50 or more sulfide-based inclusions of m or more and less than 10 μm, excellent results are obtained in both bending fatigue strength and machinability (hard tool life).

【0045】これに対し鋼No.12〜24は、本発明
で規定するいずれかの要件を欠く比較例であり、下記の
如く疲労強度あるいは被削性(超硬工具寿命)のいずれ
かに問題がある。
On the other hand, steel No. Nos. 12 to 24 are comparative examples lacking any of the requirements specified in the present invention, and have a problem in either fatigue strength or machinability (carbide tool life) as described below.

【0046】鋼No.12は、鋼材の炭素量が多過ぎる
ため焼ならし後の硬さが高くなり過ぎ、被削性が悪くて
超硬工具寿命が短い。鋼No.13は、鋼材の炭素量が
不足するため芯部硬さが低く、縦目および横目の曲げ疲
労強度が低い。鋼No.14は、鋼材のS含有量が多過
ぎるため粗大な複合介在物の個数が多くなり過ぎ、横目
の曲げ疲労強度が低い。
Steel No. In No. 12, the hardness after normalizing is too high because the carbon content of the steel material is too large, the machinability is poor, and the life of the carbide tool is short. Steel No. Sample No. 13 has a low core hardness due to an insufficient carbon content of the steel material, and has low bending fatigue strength in longitudinal and transverse directions. Steel No. In No. 14, since the S content of the steel material is too large, the number of the coarse composite inclusions becomes too large, and the bending fatigue strength of the side grain is low.

【0047】鋼No.15は、鋼材の酸素量が多過ぎる
ため酸化物系介在物のサイズが大きくなって粗大な複合
介在物個数が多くなり、縦目および横目の曲げ疲労強度
が低い。鋼No.16,17は、鋼材中のSi量あるい
はCr量が多過ぎるため表層の浸炭が阻害され、縦目お
よび横目の曲げ疲労強度が低くなっている。
Steel No. In No. 15, since the amount of oxygen in the steel material is too large, the size of the oxide-based inclusions increases, the number of coarse composite inclusions increases, and the bending fatigue strength in the longitudinal and transverse directions is low. Steel No. In Nos. 16 and 17, since the amount of Si or Cr in the steel material is too large, the carburization of the surface layer is inhibited, and the bending fatigue strength in the longitudinal and transverse directions is low.

【0048】鋼No.18は、鋼材中のCa量が多過ぎ
るため粗大な複合介在物個数が多くなり、縦目および横
目の曲げ疲労強度が低下している。鋼No.19は、鋼
材中のS含有量が不足すると共に鋳造速度も遅いため硫
化物系介在物の個数が不足し、被削性が悪くなって満足
のいく超硬工具寿命が得られない。
Steel No. In No. 18, since the amount of Ca in the steel material was too large, the number of coarse composite inclusions increased, and the bending fatigue strength of the longitudinal and transverse eyes decreased. Steel No. In No. 19, since the S content in the steel material is insufficient and the casting speed is low, the number of sulfide-based inclusions is insufficient, and the machinability is deteriorated, so that a satisfactory carbide tool life cannot be obtained.

【0049】[0049]

【発明の効果】本発明は以上の様に構成されており、鋼
材の化学成分を特定すると共に、特定断面を被検面とす
る特性サイズの複合介在物および硫化物系介在物の個数
を特定することによって、縦目および横目の衝撃特性や
疲労特性と被削性を共に満足する肌焼鋼を提供し得るこ
とになった。
The present invention is configured as described above, and specifies the chemical composition of the steel material and specifies the number of composite inclusions and sulfide-based inclusions of a characteristic size having a specific cross section as a test surface. By doing so, it is possible to provide a case hardened steel that satisfies both the impact characteristics, fatigue characteristics, and machinability of vertical and horizontal eyes.

【図面の簡単な説明】[Brief description of the drawings]

【図1】複合介在物(10μm以上)の個数と曲げ疲労
強度の関係を示すグラフである。
FIG. 1 is a graph showing the relationship between the number of composite inclusions (10 μm or more) and bending fatigue strength.

【図2】硫化物系介在物(3〜10μm)の個数と超硬
工具寿命および曲げ疲労強度の関係を示すグラフであ
る。
FIG. 2 is a graph showing the relationship between the number of sulfide-based inclusions (3 to 10 μm) and the life of a carbide tool and the bending fatigue strength.

【図3】介在物観察の試料採取位置を示す説明図であ
る。
FIG. 3 is an explanatory view showing a sampling position for observing inclusions.

【図4】曲げ疲労試験片の採取位置を示す説明図であ
る。
FIG. 4 is an explanatory view showing a sampling position of a bending fatigue test piece.

【図5】曲げ疲労試験片の寸法形状を示す図である。FIG. 5 is a view showing the dimensions and shape of a bending fatigue test piece.

【図6】浸炭焼入処理のヒートパターンを示す図であ
る。
FIG. 6 is a diagram showing a heat pattern of a carburizing and quenching process.

【図7】介在物測定結果と回転曲げ疲労試験結果の関係
を示したグラフである。
FIG. 7 is a graph showing the relationship between inclusion measurement results and rotational bending fatigue test results.

フロントページの続き (56)参考文献 特開 平4−350113(JP,A) 特開 平6−299287(JP,A)Continuation of the front page (56) References JP-A-4-350113 (JP, A) JP-A-6-299287 (JP, A)

Claims (5)

(57)【特許請求の範囲】(57) [Claims] 【請求項1】C :0.10〜0.30%(以下、特記
しない限り質量%を意味する) Mn:0.30〜2.0% Si:1.0%以下(0%を含む) S :0.003〜0.070% Al:0.01〜0.06% N :0.003〜0.03% O :0.002%以下(0%を含む) 残部:Feおよび不可避的不純物 の要件を満足する鋼材からなり、線状または棒状圧延材
の軸心を通る縦断面において、該軸心と平行で且つ該軸
心から 1/4・D(Dは圧延材の直径を表わす)離れた仮
想線を中心線として含む被検面積100mm2 中に存在
する、酸化物系と硫化物系からなる直径10μm以上の
複合介在物が20個以下であり、且つ上記と同一の被検
面積中に存在する直径3μm以上10μm未満の硫化物
系介在物が50個以上であることを特徴とする疲労特性
および被削性に優れた肌焼鋼。
1. C: 0.10 to 0.30% (hereinafter, mass% unless otherwise specified) Mn: 0.30 to 2.0% Si: 1.0% or less (including 0%) S: 0.003 to 0.070% Al: 0.01 to 0.06% N: 0.003 to 0.03% O: 0.002% or less (including 0%) Balance: Fe and inevitable impurities In a longitudinal section passing through the axis of a linear or rod-shaped rolled material, which is parallel to the axis and 1 / 4.D from the axis (D represents the diameter of the rolled material) No more than 20 composite inclusions of 10 μm or more in diameter consisting of oxides and sulfides are present in the test area 100 mm 2 including the imaginary line as a center line, and the same test area as described above. Characterized in that there are 50 or more sulfide-based inclusions with a diameter of 3 µm or more and less than 10 µm Fatigue properties and machinability in excellent hardened steel to.
【請求項2】 鋼材が、他の元素としてNi:0.20
〜4.5%、Cr:0.20〜2.5%、Mo:0.0
5〜1.0%、Cu:0.20〜1.0%よりなる群か
ら選択される少なくとも一種を含有するものである請求
項1に記載の肌焼鋼。
2. The steel material contains Ni: 0.20 as another element.
-4.5%, Cr: 0.20-2.5%, Mo: 0.0
The case hardening steel according to claim 1, which contains at least one selected from the group consisting of 5 to 1.0% and Cu: 0.20 to 1.0%.
【請求項3】 鋼材が、更に他の元素としてB:0.0
003〜0.0050%および/またはTi:0.00
3〜0.05%を含有するものである請求項1または2
に記載の肌焼鋼。
3. The steel material further contains B: 0.0 as another element.
003 to 0.0050% and / or Ti: 0.00
3. The composition according to claim 1, which contains 3 to 0.05%.
Case hardening steel according to the above.
【請求項4】 鋼材が、更に他の元素としてV:0.0
3〜1.5%および/またはNb:0.005〜1.5
%を含有するものである請求項1〜3のいずれかに記載
の肌焼鋼。
4. The steel material further comprises V: 0.0 as another element.
3 to 1.5% and / or Nb: 0.005 to 1.5
%. The case hardened steel according to any one of claims 1 to 3, which contains%.
【請求項5】 鋼材が、他の元素として、Ca:0.0
005〜0.01%、Pb:0.2%以下(0%を含ま
ない)、Te:0.1%以下(0%を含まない)、Z
r:0.1%以下(0%を含まない)よりなる群から選
択される少なくとも一種を含有するものである請求項1
〜4のいずれかに記載の肌焼鋼。
5. The steel according to claim 1, wherein the other element is Ca: 0.0
005 to 0.01%, Pb: 0.2% or less (excluding 0%), Te: 0.1% or less (excluding 0%), Z
r: containing at least one selected from the group consisting of 0.1% or less (excluding 0%).
5. The case hardened steel according to any one of items 1 to 4.
JP7337257A 1995-12-25 1995-12-25 Case hardened steel with excellent fatigue properties and machinability Expired - Lifetime JP2989766B2 (en)

Priority Applications (1)

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Application Number Priority Date Filing Date Title
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Publication Number Publication Date
JPH09176784A JPH09176784A (en) 1997-07-08
JP2989766B2 true JP2989766B2 (en) 1999-12-13

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7384488B2 (en) * 2003-09-18 2008-06-10 Mahindra & Mahindra Ltd Method for producing gears and/or shaft components with superior bending fatigue strength and pitting fatigue life from conventional alloy steels
JP4193998B1 (en) 2007-06-28 2008-12-10 株式会社神戸製鋼所 Machine structural steel excellent in machinability and manufacturing method thereof
CN109440007B (en) * 2018-11-27 2020-09-01 唐山不锈钢有限责任公司 Thin-gauge high-performance ultrahigh-strength semi-hard steel strip and production method thereof

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JPH0791579B2 (en) * 1991-05-28 1995-10-04 新日本製鐵株式会社 Method for manufacturing case-hardening steel in which crystal grains do not coarsen during carburizing heat treatment
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