JP2797987B2 - Infrared microscope - Google Patents

Infrared microscope

Info

Publication number
JP2797987B2
JP2797987B2 JP30235194A JP30235194A JP2797987B2 JP 2797987 B2 JP2797987 B2 JP 2797987B2 JP 30235194 A JP30235194 A JP 30235194A JP 30235194 A JP30235194 A JP 30235194A JP 2797987 B2 JP2797987 B2 JP 2797987B2
Authority
JP
Japan
Prior art keywords
aperture
image
light
mirror
sample
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP30235194A
Other languages
Japanese (ja)
Other versions
JPH08159966A (en
Inventor
伸朗 高木
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shimadzu Corp
Original Assignee
Shimadzu Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shimadzu Corp filed Critical Shimadzu Corp
Priority to JP30235194A priority Critical patent/JP2797987B2/en
Publication of JPH08159966A publication Critical patent/JPH08159966A/en
Application granted granted Critical
Publication of JP2797987B2 publication Critical patent/JP2797987B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Description

【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【0001】[0001]

【産業上の利用分野】本発明は、顕微赤外測定装置等に
用いられる赤外顕微鏡に関する。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to an infrared microscope used for a microscopic infrared measuring device and the like.

【0002】[0002]

【従来の技術】赤外顕微鏡による分析を行うにあたって
は、まず試料像を可視光で観察しながら試料中の分析領
域を決める。分析を行う場合、分析領域以外の光が測定
系に入らないようにマスキングをするため、可変のアパ
ーチャを使用して分析領域の光のみを検出器に送るよう
にしている。しかしながら、アパーチャでマスクされた
部分は見えなくなるために、マスクを介しての観察は視
野が狭いものとなり、分析領域を決める作業が困難であ
る。そこで、従来より用いられている赤外顕微鏡とし
て、たとえば本発明の発明者自身が既に出願した特願平
3−358486号において開示した図2に示すものが
ある。図において、Sは試料であり、1は可視光と赤外
光とを切り換えて照射する光源、2はコンデンサで光源
1からの光を試料Sに集光する。3は対物光学系であ
り、試料Sの像をアパーチャ9の位置に結像させる。ア
パーチャの開口の大きさは可変に構成され、分析領域の
大きさに応じて調整できるようにしている。試料Sを通
過した光は両面ミラー4、ミラー5、ハーフミラー6を
介して可視観察用光学系に送られる。光源8はアパーチ
ャ9の照明用光源で、光源8とレンズ光学系とにより両
面ミラー4を介して照明されたアパーチャ像がミラー
7、ハーフミラー6を介して可視観察用光学系に送ら
れ、可視観察用光学系においてアパーチャ9が試料像と
重畳して観察できるようにしている。両面ミラー4とミ
ラー7とは可動式で、必要に応じて光軸上に出入りされ
る。すなわち、可視観察時には光軸上に入り、赤外検出
時には光軸外に退く。
2. Description of the Related Art When performing analysis by an infrared microscope, first, an analysis area in a sample is determined while observing the sample image with visible light. When performing analysis, a variable aperture is used to send only the light in the analysis area to the detector in order to mask the light other than the analysis area from entering the measurement system. However, since the portion masked by the aperture becomes invisible, observation through the mask has a narrow field of view, and it is difficult to determine an analysis area. Therefore, as a conventional infrared microscope, there is an infrared microscope shown in FIG. 2 disclosed in Japanese Patent Application No. 3-358486 filed by the inventor of the present invention. In the figure, S is a sample, 1 is a light source for switching and irradiating visible light and infrared light, and 2 is a condenser for condensing light from the light source 1 on the sample S. An objective optical system 3 forms an image of the sample S at the position of the aperture 9. The size of the aperture of the aperture is variable and can be adjusted according to the size of the analysis area. The light that has passed through the sample S is sent to the visible observation optical system via the double-sided mirror 4, the mirror 5, and the half mirror 6. The light source 8 is an illumination light source for the aperture 9. The aperture image illuminated by the light source 8 and the lens optical system via the double-sided mirror 4 is sent to the visible observation optical system via the mirror 7 and the half mirror 6, and becomes visible. In the observation optical system, the aperture 9 can be observed while being superimposed on the sample image. The double-sided mirror 4 and the mirror 7 are movable, and are moved in and out of the optical axis as needed. That is, the light enters the optical axis during visible observation, and retreats off the optical axis during infrared detection.

【0003】なお、光源10と、コンデンサ11と、切
り替えミラー12は上述の透過測定モードに代えて反射
観察モードにするときに使用するものである。切り替え
ミラー12は鏡面部分と切り欠き部分とがあるハーフミ
ラーであり、光源1の代わりに光源10から照明し、コ
ンデンサ11を介してミラー12の鏡面部分で反射さ
れ、対物光学系3で試料Sに集光される。試料Sからの
反射光は再び対物光学系を通り、切り替えミラー12の
切り欠き部分を通過して両面ミラー4、ミラー5、ハー
フミラー6を介して可視観察光学系に送られ、透過観察
モードと同様に観察ができるようにしている。
The light source 10, the condenser 11, and the switching mirror 12 are used when a reflection observation mode is set in place of the transmission measurement mode. The switching mirror 12 is a half mirror having a mirror surface portion and a notch portion, illuminates from the light source 10 instead of the light source 1, is reflected by the mirror surface portion of the mirror 12 via the condenser 11, and is sampled by the objective optical system 3. Is collected. The reflected light from the sample S passes through the objective optical system again, passes through the cutout portion of the switching mirror 12, is sent to the visible observation optical system via the double-sided mirror 4, the mirror 5, and the half mirror 6, and the transmission observation mode is set. Similarly, observation is made possible.

【0004】[0004]

【発明が解決しようとする課題】上記従来の装置では、
広い視野での観察ができるとともに、光源8により分析
領域のみを明るく照らし出すことができるので、視野全
体に対する測定部分の位置を識別することが容易に行え
る。しかしながら、この装置においては、アパーチャを
照らす光源8からの光を両面ミラー4を用いて導光する
ことから光源8からの光の光軸と赤外顕微鏡の光軸とを
合わせる必要があったが、この調整は熟練を要するもの
で困難な作業であった。また、光源自体の像がアパーチ
ャの像に重なって見えることがあり、試料像が見にくく
なった。
In the above-mentioned conventional apparatus,
Observation can be performed in a wide field of view, and only the analysis region can be brightly illuminated by the light source 8, so that the position of the measurement portion with respect to the entire field of view can be easily identified. However, in this device, since the light from the light source 8 that illuminates the aperture is guided using the double-sided mirror 4, it is necessary to match the optical axis of the light from the light source 8 with the optical axis of the infrared microscope. However, this adjustment required skill and was a difficult task. Further, the image of the light source itself sometimes overlaps with the image of the aperture, making it difficult to see the sample image.

【0005】本発明はこのような問題を解決し、特に光
軸合わせを必要とすることなく、分析領域を照らすこと
ができ、しかも光源像が重なって見えることのない赤外
顕微鏡を提供することを目的とする。
SUMMARY OF THE INVENTION The present invention has been made to solve the above problems, and to provide an infrared microscope capable of illuminating an analysis area without particularly requiring optical axis alignment, and in which light source images do not overlap. With the goal.

【0006】[0006]

【課題を解決するための手段】上記問題を解決するため
になされた本発明の赤外顕微鏡は、試料の分析領域を設
定する可変のアパーチャと、このアパーチャを照明する
手段を別途設け、アパーチャを通らない試料顕微鏡像と
アパーチャだけの像を可視観察用光学系に赤外測定時と
同じ位置関係となるよう合成して観察できるようにした
赤外顕微鏡において、前記アパーチャを照明する手段が
光源と、光源からの光を拡散光にする拡散板とからな
り、これらがアパーチャの光入射側に設けられ、拡散板
による拡散光によってアパーチャの入射側の面を照らす
とともに、試料顕微鏡像とアパーチャ像とのいずれかの
像の光路上にフィルタを設けたことを特徴とする。以
下、この顕微鏡がどのように作用するかを説明する。
In order to solve the above-mentioned problems, the infrared microscope according to the present invention is provided with a variable aperture for setting an analysis area of a sample, and a means for illuminating the aperture. In an infrared microscope in which a sample microscope image that does not pass through and an image of only the aperture are combined into a visible observation optical system so as to have the same positional relationship as that at the time of infrared measurement and can be observed, the means for illuminating the aperture includes a light source. And a diffusion plate that converts the light from the light source into diffused light.These are provided on the light incident side of the aperture.The diffused light from the diffuser illuminates the surface on the entrance side of the aperture, and a sample microscope image and an aperture image are formed. Wherein a filter is provided on the optical path of any of the images. Hereinafter, how this microscope works will be described.

【0007】[0007]

【作用】本発明の赤外顕微鏡では、アパーチャを照らす
ための光源からの光は拡散板により反射され、拡散光と
なってアパーチャ全体を均一に照らす。このため、アパ
ーチャ照明手段の光軸調整は不要となる。また、光源の
像がアパーチャの像と重なることもない。さらに、フィ
ルタにより試料顕微鏡像とアパーチャ像との識別を色の
違いで行えるので明瞭に識別できる。
In the infrared microscope according to the present invention, the light from the light source for illuminating the aperture is reflected by the diffusion plate and becomes a diffused light to uniformly illuminate the entire aperture. Therefore, the optical axis adjustment of the aperture illuminating means becomes unnecessary. Further, the image of the light source does not overlap with the image of the aperture. Furthermore, the sample microscope image and the aperture image can be distinguished by the difference in color by the filter, so that they can be clearly distinguished.

【0008】[0008]

【実施例】以下、本発明の実施例を図を用いて説明す
る。図1は本発明の一実施例を示す赤外顕微鏡の構成図
であり、特に示さないものは従来例と同じ符号を付ける
ことにより説明を省略する。
DESCRIPTION OF THE PREFERRED EMBODIMENTS Embodiments of the present invention will be described below with reference to the drawings. FIG. 1 is a configuration diagram of an infrared microscope showing one embodiment of the present invention. Unless otherwise indicated, the same reference numerals as those in the conventional example are used to omit the description.

【0009】図において、14は対物光学系側の面が鏡
面であるミラーであり、その裏側には光を乱反射する拡
散板15が貼りつけられ、光源8からの光が拡散板15
により乱反射されるようにしてある。そして、拡散板に
よる拡散光がアパーチャ9の入射側面全体を均一に照明
するようになっている。また、図1に示すように2つの
光路のいずれかに試料顕微鏡像とアパーチャ像とを明瞭
に識別するためのフィルタFを設ける。
In FIG. 1, reference numeral 14 denotes a mirror whose surface on the objective optical system side is a mirror surface, and a diffusion plate 15 for irregularly reflecting light is adhered to the back of the mirror.
Scattered light. The light diffused by the diffusion plate uniformly illuminates the entire incident side surface of the aperture 9. Also, as shown in FIG. 1, a filter F for clearly distinguishing the sample microscope image from the aperture image is provided in one of the two optical paths.

【0010】以上のような構成の赤外顕微鏡によれば、
試料顕微鏡像がミラー14、ミラー5、ハーフミラー6
を介して可視観察用光学系に送られるとともに、アパー
チャだけの像がミラー7、ハーフミラー6を介して可視
観察用光学系に送られ、これらが重畳された像が観察さ
れる。この像は、広い視野の顕微鏡像と、開口部のみが
明るいアパーチャ9の像とが重ね合わされたものであ
り、観察者には広い視野の試料像の中で赤外スペクトル
を測定する部分であるアパーチャ9の開口部が明瞭に識
別できる。
According to the infrared microscope configured as described above,
Sample microscope images are mirror 14, mirror 5, half mirror 6.
Is transmitted to the optical system for visible observation via the optical system, and the image of only the aperture is transmitted to the optical system for visible observation via the mirror 7 and the half mirror 6, and an image in which these are superimposed is observed. This image is obtained by superimposing a microscope image of a wide field of view and an image of the aperture 9 having only a bright opening, and is a portion for measuring the infrared spectrum in the sample image of the wide field of view for the observer. The opening of the aperture 9 can be clearly identified.

【0011】特に、フィルタFにより顕微鏡像とアパー
チャ像とが色で識別されているのでアパーチャ9の開口
部が明瞭に識別できる。
In particular, since the microscope image and the aperture image are distinguished by color by the filter F, the opening of the aperture 9 can be clearly distinguished.

【0012】本実施例では拡散板15をミラー14の裏
側に張り付けたものとしたが、ミラー14とは別に拡散
板を取り付けるようにしてもよい。拡散板15は、光を
乱反射する機能を有するものであればよく、たとえばつ
や消し塗装したものやサンディングしたものでもよい。
In this embodiment, the diffusion plate 15 is attached to the back side of the mirror 14, but a diffusion plate may be attached separately from the mirror 14. The diffusion plate 15 may have any function of irregularly reflecting light, and may be, for example, a matte-painted one or a sanded one.

【0013】[0013]

【発明の効果】以上のように、本願発明によればアパー
チャの照明を拡散板による拡散光を用いることとしたの
で、集光レンズなどの光学系や光軸調整機構を必要とせ
ず、調整作業が不要となるとともにコストダウンとな
り、また光源自体の像が現れないので、試料像を明瞭に
観察することができる。
As described above, according to the present invention, since the aperture is illuminated by the diffused light from the diffusion plate, the optical system such as a condenser lens and the optical axis adjustment mechanism are not required, and the adjustment work is performed. Is unnecessary, the cost is reduced, and the image of the light source itself does not appear, so that the sample image can be clearly observed.

【図面の簡単な説明】[Brief description of the drawings]

【図1】本発明の一実施例である赤外顕微鏡の構成図。FIG. 1 is a configuration diagram of an infrared microscope according to an embodiment of the present invention.

【図2】従来からの赤外顕微鏡の構成図。FIG. 2 is a configuration diagram of a conventional infrared microscope.

【符号の説明】[Explanation of symbols]

1:光源 3:対物光学系 5、7、14:ミラー 6:ハーフミラー 8:光源 15:拡散板 F:フィルタ 1: light source 3: objective optical system 5, 7, 14: mirror 6: half mirror 8: light source 15: diffuser F: filter

───────────────────────────────────────────────────── フロントページの続き (58)調査した分野(Int.Cl.6,DB名) G01N 21/00 - 21/01 G01N 21/17 - 21/61 G02B 21/00 - 21/36 G02B 23/00 - 23/26──────────────────────────────────────────────────続 き Continued on the front page (58) Field surveyed (Int. Cl. 6 , DB name) G01N 21/00-21/01 G01N 21/17-21/61 G02B 21/00-21/36 G02B 23 / 00-23/26

Claims (1)

(57)【特許請求の範囲】(57) [Claims] 【請求項1】試料の分析領域を設定する可変のアパーチ
ャと、このアパーチャを照明する手段を別途設け、アパ
ーチャを通らない試料顕微鏡像とアパーチャだけの像を
可視観察用光学系に赤外測定時と同じ位置関係となるよ
う合成して観察できるようにした赤外顕微鏡において、 前記アパーチャを照明する手段が光源と、光源からの光
を拡散光にする拡散板とからなり、これらがアパーチャ
の光入射側に設けられ、拡散板による拡散光によってア
パーチャの入射側の面を照らすとともに、試料顕微鏡像
とアパーチャ像とのいずれかの像の光路上にフィルタを
設けたことを特徴とする赤外顕微鏡。
1. A variable aperture for setting an analysis area of a sample and a means for illuminating the aperture are separately provided, and a sample microscope image which does not pass through the aperture and an image of only the aperture are measured by an optical system for visible observation when infrared measurement is performed. In the infrared microscope which can be synthesized and observed so as to have the same positional relationship as described above, the means for illuminating the aperture comprises a light source and a diffusion plate for diffusing light from the light source, and these are the light of the aperture. An infrared microscope, which is provided on the incident side, illuminates the surface on the incident side of the aperture with diffused light from the diffusion plate, and has a filter on the optical path of one of the sample microscope image and the aperture image. .
JP30235194A 1994-12-06 1994-12-06 Infrared microscope Expired - Fee Related JP2797987B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP30235194A JP2797987B2 (en) 1994-12-06 1994-12-06 Infrared microscope

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP30235194A JP2797987B2 (en) 1994-12-06 1994-12-06 Infrared microscope

Publications (2)

Publication Number Publication Date
JPH08159966A JPH08159966A (en) 1996-06-21
JP2797987B2 true JP2797987B2 (en) 1998-09-17

Family

ID=17907874

Family Applications (1)

Application Number Title Priority Date Filing Date
JP30235194A Expired - Fee Related JP2797987B2 (en) 1994-12-06 1994-12-06 Infrared microscope

Country Status (1)

Country Link
JP (1) JP2797987B2 (en)

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0776747B2 (en) * 1989-11-03 1995-08-16 株式会社堀場製作所 Microspectrophotometer
JP2528145Y2 (en) * 1990-12-25 1997-03-05 日本分光株式会社 Microscopic infrared spectrum measurement device
JPH0630708U (en) * 1991-02-01 1994-04-22 株式会社ニコン Telescope for surveying instrument
JP2575981B2 (en) * 1991-12-28 1997-01-29 株式会社島津製作所 Infrared microscope
JPH05307691A (en) * 1992-04-28 1993-11-19 Matsushita Electric Works Ltd Dimming type smoke detector
JPH0618410A (en) * 1992-06-30 1994-01-25 Shimadzu Corp Infrared micromeasuring device

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