JP2619835B2 - Hair rinse composition - Google Patents
Hair rinse compositionInfo
- Publication number
- JP2619835B2 JP2619835B2 JP32286788A JP32286788A JP2619835B2 JP 2619835 B2 JP2619835 B2 JP 2619835B2 JP 32286788 A JP32286788 A JP 32286788A JP 32286788 A JP32286788 A JP 32286788A JP 2619835 B2 JP2619835 B2 JP 2619835B2
- Authority
- JP
- Japan
- Prior art keywords
- hair
- weight
- present
- group
- rinse composition
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
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Description
【発明の詳細な説明】 〔産業上の利用分野〕 本発明は、ヘアーリンス剤に関し、更に詳しくは、毛
髪の腰のなさを大幅に改善するとともに、毛髪コンディ
ショニング効果及び乾燥後の毛髪のさらさら感に優れた
ヘアーリンス剤組成物に関する。Description: FIELD OF THE INVENTION The present invention relates to a hair rinsing agent, and more particularly to a hair rinsing agent, which significantly improves the limpness of the hair, as well as the hair conditioning effect and the dryness of the hair after drying. The present invention relates to a hair rinsing agent composition having excellent hair rinsing agent composition.
毛髪の汚れを除去するためにアニオン界面活性剤を主
成分とするシャンプーで洗髪すると、毛髪の汚れのほか
毛髪表面を保護している油分も当時に除去され、毛髪の
柔軟性が失なわれ、艶のないくし通りの悪い髪となり、
毛髪の損傷，枝毛，切毛が発生し易くなる。If you wash your hair with a shampoo containing an anionic surfactant as a main component to remove hair stains, oils that protect the hair surface as well as hair stains are also removed at that time, and the hair loses its flexibility. It becomes bad hair according to the dull comb,
Hair damage, split ends, and cuts are likely to occur.
これらの弊害を防ぐ目的で、カチオン界面活性剤であ
る第４級アンモニウム塩を有効成分とするヘアーリンス
剤が使用されている。しかし、いわゆる細くて腰のない
毛髪にこのような第４級アンモニウム塩を主要有効成分
とするヘアーリンス剤を適用すると、毛髪に過剰の柔軟
性を与え、更に乾燥後の毛髪が重くなるとともに毛髪の
腰がなくなる。その結果毛髪は、ふくよかさや、ボリュ
ーム感に欠けた猫毛状になりその後の毛髪処理（セット
性，ウェービング性）が悪化するという欠点を有してい
た。For the purpose of preventing these adverse effects, a hair rinse agent containing a quaternary ammonium salt as a cationic surfactant as an active ingredient has been used. However, when such a hair rinse agent containing a quaternary ammonium salt as a main active ingredient is applied to so-called thin and stiff hair, the hair becomes excessively flexible, the hair after drying becomes heavy and the hair becomes heavy. Loses his waist. As a result, the hair had a drawback that the hair became cat hair lacking in fullness and volume, and the subsequent hair treatment (setting properties and waving properties) deteriorated.
本発明は毛髪へ腰を付与するとともに、優れた毛髪コ
ンディショニング効果（柔軟性，しっとり感，なめらか
さ，くし通り性）及び乾燥後の毛髪の仕上がりの軽さ及
びさらさら感を有するヘアーリンス剤を提供することを
目的としている。The present invention provides a hair rinsing agent that imparts a stiffness to the hair, has excellent hair conditioning effects (flexibility, moist feeling, smoothness, combability), and has a light finish and a dry feeling after drying the hair. It is intended to be.
本発明は、 （Ａ） アルキル基が炭素数11〜21の直鎖又は分岐鎖で
ある、ビス（２−アルキル−Ｎ−ヒドロキシエチルイミ
ダゾリン）クロル酢酸錯体型両性界面活性剤0.5〜6.0重
量％と （Ｂ） カチオン性ポリマー0.1％〜3.0重量％と （Ｃ） 一般式 〔式中、R1はメチル基またはフェニル基（ただし、R1の
総数の90％以上はメチル基）,R2はメチル基または水酸
基を示す。またｎは900〜2500の整数を示す。〕 で表わされる高分子シリコーンの一種または二種以上0.
1〜6.0重量％とを含有するヘアーリンス剤組成物であ
る。The present invention relates to (A) a bis (2-alkyl-N-hydroxyethylimidazoline) chloroacetic acid complex-type amphoteric surfactant having an alkyl group of 11 to 21 carbon atoms in a linear or branched chain having 0.5 to 6.0% by weight. (B) 0.1% to 3.0% by weight of a cationic polymer and (C) a general formula [In the formula, R 1 represents a methyl group or a phenyl group (however, 90% or more of the total number of R 1 is a methyl group), and R 2 represents a methyl group or a hydroxyl group. N represents an integer of 900 to 2500. One or more of the polymeric silicones represented by
A hair rinse composition containing 1 to 6.0% by weight.
本発明の（Ａ）成分であるビス（２−アルキル−Ｎ−
ヒドロキシエチルイミダゾリン）クロル酢酸錯体型両性
界面活性剤は、公知の物質である。Bis (2-alkyl-N-) as the component (A) of the present invention
The (hydroxyethylimidazoline) chloroacetic acid complex type amphoteric surfactant is a known substance.
（アルキル基は炭素数11〜21の直鎖又は分岐鎖であ
る。）例えば、ビス（ドデシル−Ｎ−ヒドロキシエチル
イミダゾリン）クロル酢酸錯体、ビス（テトラデシル−
Ｎ−ヒドロキシエチルイミダゾリン）クロル酢酸錯体，
ビス（ヘキサデシル−Ｎ−ヒドロキシエチルイミダゾリ
ン）クロル酢酸錯体，ビス（オクタデシル−Ｎ−ヒドロ
キシエチルイミダゾリン）クロル酢酸錯体，ビス（ドコ
シル−Ｎ−ヒドロキシエチルイミダゾリン）クロル酢酸
錯体などが挙げられ、特に好ましいものは、ビス（オク
タデシル−Ｎ−ヒドロキシエチルイミダゾリン）クロル
酢酸錯体である。(The alkyl group is a straight or branched chain having 11 to 21 carbon atoms.) For example, bis (dodecyl-N-hydroxyethylimidazoline) chloroacetic acid complex, bis (tetradecyl-
N-hydroxyethylimidazoline) chloroacetic acid complex,
Bis (hexadecyl-N-hydroxyethylimidazoline) chloroacetic acid complex, bis (octadecyl-N-hydroxyethylimidazoline) chloroacetic acid complex, bis (docosyl-N-hydroxyethylimidazoline) chloroacetic acid complex, and the like are particularly preferable. , Bis (octadecyl-N-hydroxyethylimidazoline) chloroacetic acid complex.
本発明のヘアーリンス剤組成物には、これらの両性界
面活性剤の一種または二種以上の混合物を総量を基準と
して、一般的には0.5〜6.0重量％（以下wt％と略記す
る）好ましくは、1.0〜4.0wt％配合される。配合量が0.
5wt％未満では、毛髪コンディショニング効果が不十分
となる傾向がみられ、6.0wt％を超えると毛髪にべたつ
きが生じ好ましくない。In the hair rinse composition of the present invention, one or a mixture of two or more of these amphoteric surfactants is generally used in an amount of 0.5 to 6.0% by weight (hereinafter abbreviated as wt%), preferably 0.5 to 6.0% by weight, based on the total amount. , 1.0 to 4.0 wt%. The blending amount is 0.
If the amount is less than 5% by weight, the hair conditioning effect tends to be insufficient. If the amount exceeds 6.0% by weight, the hair becomes sticky, which is not preferable.
本発明の（Ｂ）成分であるカチオン性ポリマーは、次
のものが例示される。The following are examples of the cationic polymer that is the component (B) of the present invention.
（ｉ）ビニルピロリドン／ジメチルアミノエチルメタク
レート共重合体とジメチルサルフェートからなるカチオ
ン化物（例えば、GAF社製ガフコート734及び755）。(I) A cationized product composed of a vinylpyrrolidone / dimethylaminoethyl methacrylate copolymer and dimethyl sulfate (for example, Guffcoat 734 and 755 manufactured by GAF).
（ii）グリシジルトリメチルアンモニウムクロリドとヒ
ドロキシエチルセルロースからなるカチオン化物（例え
ば、UCC社製 ポリマーJR 400）。(Ii) A cationized product composed of glycidyltrimethylammonium chloride and hydroxyethylcellulose (for example, polymer JR400 manufactured by UCC).
（iii）ジアリルジメチルアンモニウムクロリド／ヒド
ロキシエチルセルロースグラフト共重合体（例えば、NS
C社製 セルコートL200）。(Iii) diallyldimethylammonium chloride / hydroxyethylcellulose graft copolymer (for example, NS
Cell coat L200 manufactured by Company C).
（iv）ヒドロキシプロピルグアーの第４級アンモニウム
誘導体（例えば、MEYHALL社製 Jaguar Ｃ 13S）。(Iv) Quaternary ammonium derivatives of hydroxypropyl guar (eg, Jaguar C 13S manufactured by MEYHALL).
（ｖ）ジメチルジアリルアンモニウム塩化物のホモポリ
マー又はジメチルジアリルアンモニウム塩化物／アクリ
ルアミドの共重合体（例えば、MERQ社製 マーコート
100及び550）。(V) A homopolymer of dimethyldiallylammonium chloride or a copolymer of dimethyldiallylammonium chloride / acrylamide (for example, Mercoat manufactured by Merq Co.)
100 and 550).
（vi）アクリルアミド／β−メタクリロイルオキシエチ
ルトリメチルアンモニウムメトサルフェート共重合体
（例えば、HERCULES社製 Reten 205）。(Vi) Acrylamide / β-methacryloyloxyethyltrimethylammonium methosulfate copolymer (for example, Reten 205 manufactured by HERCULES).
（vii）ビニルピロリドン／ビニルイミダゾールの第４
級カチオン重合体。（例えば、Basf社製 Luviquat FC
905）。(Vii) the fourth of vinylpyrrolidone / vinylimidazole
Grade cationic polymer. (For example, Basf Luviquat FC
905).
（viii）ポリエチレングリコール・エピクロルヒドリン
・ヤシ油アルキルアミン・ジプロピレントリアミン縮合
物（例えば、HENKEL社製 ポリコート H81）。(Viii) Polyethylene glycol / epichlorohydrin / coconut oil alkylamine / dipropylenetriamine condensate (for example, Polycoat H81 manufactured by HENKEL).
などが挙げられ、特に好ましいものは、グリシジルトリ
メチルアンモニウムクロリドとヒドロキシエチルセルロ
ースからなるカチオン化物及びジアリルジメチルアンモ
ニウムクロリド／ヒドロキシエチルセルロースグラフト
共重合体のようなカチオン性セルロースである。Particularly preferred are cationic products such as a cationized product composed of glycidyltrimethylammonium chloride and hydroxyethylcellulose and a diallyldimethylammonium chloride / hydroxyethylcellulose graft copolymer.
本発明のヘアーリンス剤組成物には、これらのカチオ
ン化ポリマーの一種または二種以上を総量を基準として
一般的には0.1〜3.0wt％，好ましくは0.1〜2.0wt％配合
される。配合量が0.1％未満では、毛髪へ腰を付与する
効果及び毛髪コンディショニング効果が不十分となる傾
向がみられ、3.0wt％を超えると、毛髪にべたつきと、
ガサガサした残存感が生じる傾向がある。The hair rinse composition of the present invention generally contains one or more of these cationized polymers in an amount of 0.1 to 3.0% by weight, preferably 0.1 to 2.0% by weight based on the total amount. If the amount is less than 0.1%, the effect of imparting waist to the hair and the effect of conditioning the hair tend to be insufficient.
There is a tendency for a loose feeling to remain.
本発明の（Ｃ）成分である高分子シリコーンは、次の
一般式 〔式中、R1はメチル基またはフェニル基（ただし、R1の
総数の90％以上はメチル基）,R2はメチル基または水酸
基を示す。またｎは900〜2500の整数を示す。〕 で表わされる高分子シリコーンの一種または二種以上の
混合物が適用される。The polymer silicone as the component (C) of the present invention has the following general formula: [In the formula, R 1 represents a methyl group or a phenyl group (however, 90% or more of the total number of R 1 is a methyl group), and R 2 represents a methyl group or a hydroxyl group. N represents an integer of 900 to 2500. One type or a mixture of two or more types of the high molecular silicone represented by the formula:
例えば、ジメチルポリシロキサン，メチルフェニルポ
リシロキサン，末端水酸基含有ジメチルポリシロキサ
ン，末端水酸基含有メチルフェニルポリシロキサンなど
が挙げられる。For example, dimethylpolysiloxane, methylphenylpolysiloxane, dimethylpolysiloxane having a terminal hydroxyl group, methylphenylpolysiloxane having a terminal hydroxyl group, and the like can be given.
式中のR1は総てメチル基かまたは一部がフェニル基で
あり、メチル基の割合は、R1の総数のうち90％以上であ
ることが必須である。R 1 in the formula is all methyl groups or a part thereof is a phenyl group, and the proportion of methyl groups is essential to be 90% or more of the total number of R 1 .
本発明のヘアーリンス剤組成物には、これらの高分子
シリコーンの一種または二種以上の混合物を総量を基準
として0.1〜6.0wt％、好ましくは0.3〜5.0wt％配合され
る。配合量が0.1wt％未満では、乾燥後のさらさら感に
良好な結果が得られず、6.0wt％を超えると毛髪にべた
つきが生じ好ましくない。The hair rinse composition of the present invention is blended with 0.1 to 6.0% by weight, preferably 0.3 to 5.0% by weight, based on the total amount, of one or a mixture of two or more of these polymeric silicones. If the amount is less than 0.1% by weight, good results cannot be obtained for the dry feeling after drying, and if it exceeds 6.0% by weight, the hair becomes sticky, which is not preferable.
一方、本発明で使用する高分子シリコーンの平均重合
度（ｎ）は900〜2500であり、好ましくは1000〜2000で
ある。On the other hand, the average polymerization degree (n) of the high molecular silicone used in the present invention is from 900 to 2500, preferably from 1,000 to 2,000.
平均重合度が900に満たないものは効果がなく、平均
重合度が2500を超えるものを使用すると、連用した場合
なめらかさ，くし通り性が悪いので好ましくない。Those having an average degree of polymerization of less than 900 have no effect, and those having an average degree of polymerization of more than 2500 are not preferred because smoothness and combability are poor when used continuously.
本発明のヘアーリンス剤組成物は、上述した３成分を
必須の構成成分とするが、当該組成物には、本発明の目
的を達成できる範囲で他の成分を適宜配合することがで
きる。The hair rinse composition of the present invention contains the above-mentioned three components as essential components, but other components can be appropriately added to the composition as long as the object of the present invention can be achieved.
即ち、ワセリン，スクワラン，低沸点イソパラフィ
ン，流動パラフィン等の炭化水素，イソプロピルミリス
テート，イソプロピルパルミテート等のエステル油，ツ
バキ油，オリーブ油，アボガド油等の植物油，低沸点シ
リコーン，環状シリコーン等のシリコン油，ポリグリセ
リン脂肪酸エステル，ポリオキシエチレンソルビタンモ
ノラウレート等の非イオン性界面活性剤，メチルセルロ
ース，ヒドロキシエチルセルロース，カチオン化セルロ
ース等のセルロース誘導体，エチレングリコール，プロ
ピレングリコール，グリセリン等の保湿剤，ポリペプチ
ド，その他殺菌剤，着色剤，香料などが挙げられこれら
の一種または二種以上を配合することができる。That is, hydrocarbons such as petrolatum, squalane, low-boiling isoparaffin, and liquid paraffin; ester oils such as isopropyl myristate and isopropyl palmitate; vegetable oils such as camellia oil, olive oil and avocado oil; silicone oils such as low-boiling silicone and cyclic silicone Nonionic surfactants such as polyglycerol fatty acid esters, polyoxyethylene sorbitan monolaurate, cellulose derivatives such as methylcellulose, hydroxyethylcellulose, cationized cellulose, humectants such as ethylene glycol, propylene glycol, glycerin, polypeptides, In addition, a bactericide, a coloring agent, a fragrance and the like can be mentioned, and one or more of these can be blended.
次に実施例を挙げ本発明を説明するが、本発明はこれ
ら実施例に限定されるものではない。Next, the present invention will be described with reference to examples, but the present invention is not limited to these examples.
なお、本実施例中で用いた試験方法は、下記のとおり
である。The test method used in this example is as follows.
（毛髪の腰のつよさ及び毛髪コンディショニング効果，
乾燥後の毛髪の仕上がりの軽さ及びさらさら感試験） 細くて、腰のない髪質を訴える女性20名のパネラーに
て各例を一週間連用後、「髪の腰のつよさ」，「髪の柔
軟性」，「髪のしっとり感」，「髪のなめらかさ」，
「くし通り性」，乾燥後の毛髪の仕上がりの軽さ及びさ
らさら感を官能的に比較し、下記基準で評価を行なっ
た。(Hair stiffness and hair conditioning effect,
Test of lightness and smoothness of the finished hair after drying) After continuous use of each example for one week by a panel of 20 women who complain of thin and waistless hair quality, "Hairiness of hair", "Hair Flexibility, hair moistness, hair smoothness,
The "comb passability", the lightness of the finished hair after drying, and the feeling of dryness were sensuously compared and evaluated according to the following criteria.
◎ ： 良いと答えた人が 18人以上の場合 ○ ： 〃 が 14〜17人の場合 △ ： 〃 が ８〜13人の場合 × ： 〃 が ７人以下の場合 実施例 １〜3,比較例１〜３ 第一表の上段に示す配合組成のヘアーリンス剤を通常
の方法で調整し、上記試験を行い第一表の下段にその結
果を示した。◎: 18 or more people answered good ○: 〃 14 to 17 people △: ８ 8 to 13 people ×: 以下 7 or less Examples 1-3, Comparative Examples 1-3 A hair rinse agent having the composition shown in the upper row of Table 1 was prepared by an ordinary method, and the above test was performed. The results are shown in the lower row of Table 1.
実施例 ４〜7,比較例４〜９ 第二表の上段に示す配合組成のヘアーリンス剤を通常
の方法で調製し、上記試験を行い第二表の下段にその結
果を示した。 Examples 4 to 7, Comparative Examples 4 to 9 Hair rinse agents having the composition shown in the upper part of the second table were prepared by a usual method, and the above test was conducted. The results are shown in the lower part of the second table.
〔特性〕 実施例１〜７より明らかなように、本発明のヘアーリ
ンス剤組成物は、いずれも優れた性能を示していた。 [Characteristics] As is clear from Examples 1 to 7, all of the hair rinse composition of the present invention showed excellent performance.
一方、必須成分であるビス（２−アルキル−Ｎ−ヒド
ロキシエチルイミダゾリン）クロル酢酸錯体型両性界面
活性剤，カチオン性ポリマー，第４級アンモニウム塩の
どれかを欠いた場合（比較例１〜３）又は、これらの配
合量および高分子シリコーンの平均重合度（ｎ）が本発
明の範囲外の場合（比較例４〜９）はいずれも劣った性
能を示し本発明の目的を達成できなかった。On the other hand, when any of bis (2-alkyl-N-hydroxyethylimidazoline) chloroacetic acid complex type amphoteric surfactant, cationic polymer, and quaternary ammonium salt, which are essential components, is missing (Comparative Examples 1 to 3) Alternatively, when the amounts of these components and the average degree of polymerization (n) of the high molecular silicone were out of the range of the present invention (Comparative Examples 4 to 9), all of them exhibited inferior performance and could not achieve the object of the present invention.
以上記載のごとく、本発明は毛髪に腰を付与するとと
にも毛髪コンディショニング効果（柔軟性，しっとり
感，なめらかさ，くし通り性）並びに乾燥後の毛髪の仕
上がりの軽さ及びさらさら感に優れ、連用しても髪を傷
めない有用なるヘアーリンス剤組成物を提供することは
明らかである。As described above, the present invention imparts a waist to the hair and is excellent in hair conditioning effects (flexibility, moist feeling, smoothness, combability) and lightness and smoothness of the finished hair after drying, It is apparent that the present invention provides a useful hair rinse composition which does not damage the hair even if it is used continuously.
Claims (1)
は分岐鎖である、ビス（２−アルキル−Ｎ−ヒドロキシ
エチルイミダゾリン）クロル酢酸錯体型両性界面活性剤
0.5〜6.0重量％と （Ｂ）カチオン性ポリマー0.1〜3.0重量％と （Ｃ）一般式 〔式中、R1はメチル基またはフェニル基（ただし、R1の
総数の90％以上はメチル基）,R2はメチル基または水酸
基を示す。またｎは900〜2500の整数を示す。〕 で表わされる高分子シリコーンの一種または二種以上0.
1〜6.0重量％とを含有することを特徴とするヘアーリン
ス剤組成物。1. A bis (2-alkyl-N-hydroxyethylimidazoline) chloroacetic acid complex type amphoteric surfactant wherein (A) the alkyl group is a straight or branched chain having 11 to 21 carbon atoms.
0.5-6.0% by weight and (B) 0.1-3.0% by weight of cationic polymer (C) [In the formula, R 1 represents a methyl group or a phenyl group (however, 90% or more of the total number of R 1 is a methyl group), and R 2 represents a methyl group or a hydroxyl group. N represents an integer of 900 to 2500. One or more of the polymeric silicones represented by
A hair rinse composition comprising 1 to 6.0% by weight.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP32286788A JP2619835B2 (en) | 1988-12-20 | 1988-12-20 | Hair rinse composition |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP32286788A JP2619835B2 (en) | 1988-12-20 | 1988-12-20 | Hair rinse composition |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPH02167215A JPH02167215A (en) | 1990-06-27 |
| JP2619835B2 true JP2619835B2 (en) | 1997-06-11 |
Family
ID=18148498
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP32286788A Expired - Lifetime JP2619835B2 (en) | 1988-12-20 | 1988-12-20 | Hair rinse composition |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JP2619835B2 (en) |
-
1988
- 1988-12-20 JP JP32286788A patent/JP2619835B2/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| JPH02167215A (en) | 1990-06-27 |
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