JP2607604B2 - How to make clear honey - Google Patents
How to make clear honeyInfo
- Publication number
- JP2607604B2 JP2607604B2 JP63065990A JP6599088A JP2607604B2 JP 2607604 B2 JP2607604 B2 JP 2607604B2 JP 63065990 A JP63065990 A JP 63065990A JP 6599088 A JP6599088 A JP 6599088A JP 2607604 B2 JP2607604 B2 JP 2607604B2
- Authority
- JP
- Japan
- Prior art keywords
- honey
- brix
- membrane
- liquid
- make clear
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Description
【発明の詳細な説明】 〔産業上の利用分野〕 本発明は、蜂蜜が植物の花から採集、貯蔵した蜂蜜中
の糖類を殆ど損失させることなく、濁り成分や菌体を除
去して清澄な蜂蜜を得る方法に関する。DETAILED DESCRIPTION OF THE INVENTION [Industrial Application Field] The present invention relates to a method for removing turbid components and cells from honey with little loss of sugars in honey collected and stored from plant flowers. How to get honey.
蜂蜜が植物の花から採集、貯蔵した蜜、すなわち黄色
をおびた高粘性の濃厚液は大部分が糖分であるが、ポツ
リヌス菌等の菌体類の懸濁物質や蛋白質等を含有してお
り、外観的には濁った液である。かかる蜂蜜から得られ
る高糖度（高Brix）の液は、天然であるため食用あるい
は薬用として用いられているが、このまま使用すると問
題が生じる場合がある。例えば０歳児に起こるボツリヌ
ス症が最近問題となっている。ボツリヌス菌は毒素型の
代表的な菌であり、重症の場合呼吸困難や呼吸停止とな
る。またかかる液は懸濁しているため、特に薬用に用い
る場合抵抗感がある。Honey, which is collected and stored from plant flowers by honey, i.e., yellowish highly viscous concentrate is mostly sugar, but contains suspended substances and proteins of fungi such as Potulinum. It is a turbid liquid in appearance. A liquid having a high sugar content (high Brix) obtained from such honey is used for food or medicine because it is natural, but if used as it is, problems may occur. For example, botulism occurring in a 0-year-old child has recently become a problem. Clostridium botulinum is a typical toxin-type bacterium, and in severe cases, dyspnea or respiratory arrest. In addition, since such a liquid is suspended, there is a feeling of resistance particularly when used for medicinal purposes.
蜂蜜中の懸濁物質や高分子量の蛋白質を除去する方法
として、従来は蜂蜜を活性炭処理した後フィルターにか
けたり、イオン交換処理等が知られているが、これらの
方法では工程が複雑であるばかりでなく、効率良く上記
不純物を除去することはできなかった。Conventionally, as a method for removing suspended substances and high molecular weight proteins in honey, honey is treated with activated carbon and then filtered, or ion exchange treatment is known.However, these methods are only complicated. However, the impurities could not be efficiently removed.
本発明はかかる問題点を解決するためになされたもの
であって、二次おりの生じない清澄でかつ高糖度な蜂蜜
を効率的かつ経済的に得る方法に関するものである。The present invention has been made to solve such a problem, and relates to a method for efficiently and economically obtaining clear and high-sugar honey without secondary cage.
即ち本発明は、50〜70Brixの高濃度蜂蜜を、50℃以上
の液温で平均孔径0.1〜0.3μｍの多孔質平板状膜を装着
したプレートアンドフレーム型膜モジュールを用いて、
濾過することを特徴とする清澄蜂蜜の製造方法を提供す
る。That is, the present invention uses a plate-and-frame type membrane module equipped with a high-concentration honey of 50 to 70 Brix and a porous flat membrane having an average pore diameter of 0.1 to 0.3 μm at a liquid temperature of 50 ° C. or higher.
A method for producing a clarified honey, which is characterized by filtering.
本発明が適用される蜂蜜は、50〜70Brixの高濃度のも
のである。市販の蜂蜜の糖度は約90Brixであり、上記糖
度となるように薄めて処理する。糖度が50Brix未満の場
合は、清澄な蜂蜜が得られないので好ましくない。The honey to which the present invention is applied has a high concentration of 50 to 70 Brix. Commercially available honey has a sugar content of about 90 Brix, and is diluted to the above sugar content and processed. If the sugar content is less than 50 Brix, clear honey cannot be obtained, which is not preferable.
また本発明においては、上記蜂蜜を50℃以上、好まし
くは50〜60℃の液温にて、後述の多孔質膜に接触させ
る。市販蜂蜜の粘度は、25℃で約1000cpにもなり、液温
を50℃以上とすることにより、数100cp以下、好ましく
は数cp〜100cpとすることができる。液温が50℃以下の
場合は、処理液の粘度が高すぎて好ましくない。In the present invention, the honey is brought into contact with a porous membrane described below at a liquid temperature of 50 ° C or higher, preferably 50 to 60 ° C. The viscosity of commercially available honey can be as high as about 1000 cp at 25 ° C., and can be set to several hundred cp or less, preferably several cp to 100 cp by setting the liquid temperature to 50 ° C. or more. When the liquid temperature is 50 ° C. or lower, the viscosity of the processing liquid is too high, which is not preferable.
本発明で用いられる多孔質膜は、平均孔径0.1〜0.3μ
ｍの微細孔構造を有する精密濾過膜である。平均孔径が
小さすぎると、蜂蜜中の糖分や香りが除去されて味が低
下するので好ましくない。The porous membrane used in the present invention has an average pore size of 0.1 to 0.3 μm.
It is a microfiltration membrane having a micropore structure of m. If the average pore size is too small, the sugar content and aroma in the honey are removed and the taste is lowered, which is not preferable.
一方平均孔径が大きすぎると、菌体等の懸濁物質や高
分子量の蛋白質等の不要物が濾過液側に透過してしま
い、得られた濾過液中に二次おりが発生して清澄な蜂蜜
が得られないので好ましくない。On the other hand, if the average pore size is too large, unnecessary substances such as suspended substances such as bacterial cells and high molecular weight proteins will permeate to the filtrate side, and a secondary cage will be generated in the obtained filtrate, resulting in a clear liquid. It is not preferable because honey cannot be obtained.
また膜厚は、通常50〜200μｍである。 The thickness is usually 50 to 200 μm.
多孔質膜の形態は平板状であるため、中空糸状膜に比
べて、高粘度の液でも濾過流束を大きくできるという利
点がある。本発明においては、この膜を装着したプレー
トアンドフレーム型膜モジュールを用いる。Since the form of the porous membrane is flat, there is an advantage that the filtration flux can be increased even with a liquid having a high viscosity, as compared with a hollow fiber membrane. In the present invention, a plate and frame type membrane module equipped with this membrane is used.
また膜材質としては、例えばポリテトラフルオロエチ
レン（PTFE）系、ポリエチレン系、ポリプロピレン系、
セルロースアセテート系、ポリスルホン系等の膜が挙げ
られる。特に液を高温で処理するため耐熱性を有するも
のが好ましい。As the film material, for example, polytetrafluoroethylene (PTFE), polyethylene, polypropylene,
Membranes of cellulose acetate type, polysulfone type and the like can be mentioned. In particular, since the liquid is processed at a high temperature, those having heat resistance are preferable.
また膜モジュールの濾過運転方式は、安定な濾過流束
を得るためクロスフロー方式（循環濾過方式）が好まし
く、循環時の線速度は通常0.5〜2m/sec、好ましくは0.5
〜1m/secとする。The filtration operation method of the membrane module is preferably a cross flow method (circulation filtration method) in order to obtain a stable filtration flux, and the linear velocity during circulation is usually 0.5 to 2 m / sec, preferably 0.5
11 m / sec.
また平均操作圧力は通常0.5〜4kgf/cm2、好ましくは
0.5〜2kgf/cm2である。The average operating pressure is usually 0.5 to 4 kgf / cm 2 , preferably
It is 0.5 to 2 kgf / cm 2 .
本発明は、特定の多孔質平板状膜を用いて特定条件下
で、高糖度の蜂蜜を濾過処理することにより、蜂蜜中の
糖分や香りを全く変化させることなく、清澄な蜂蜜を経
済的に得ることができる。得られた清澄蜂蜜はこのまま
使用してもよいし、さらに減圧濃縮によりBrixを90程度
になるまで濃縮することもできる。The present invention provides a process for filtering clear honey economically without any change in the sugar content and aroma in honey by filtering honey having a high sugar content under specific conditions using a specific porous flat membrane. Obtainable. The obtained clarified honey may be used as it is, or may be further concentrated under reduced pressure until Brix is reduced to about 90.
以下に本発明の実施例及び比較例を挙げるが、本発明
はこれに限定されるものではない。Hereinafter, examples and comparative examples of the present invention will be described, but the present invention is not limited thereto.
実施例 平均孔径0.2μｍの多孔質平板状膜（PTFE製，日東電
工社製：商品名NTF−5202）を装着したプレートアンド
フレーム型モジュール（膜面積0.38m2）を用いて、蜂蜜
（Brix;50）を、平均圧力0.7kgf/cm2、液温60℃、線速
0.5m/secの条件下で、濃縮倍率10倍（蜂蜜回収率90％）
となるように処理した。その濾過液性状の分析結果を表
に示す。Example Using a plate and frame type module (membrane area 0.38 m 2 ) equipped with a porous plate-like membrane (PTFE, manufactured by Nitto Denko Corporation; trade name: NTF-5202) having an average pore diameter of 0.2 μm, honey (Brix; 50), average pressure 0.7kgf / cm 2 , liquid temperature 60 ℃, linear velocity
Under the condition of 0.5m / sec, concentration ratio 10 times (Honey recovery rate 90%)
It processed so that it might become. The analysis results of the properties of the filtrate are shown in the table.
濾過流束は初期が42/m2・ｈ、最終時（濃縮倍率10
倍、蜂蜜回収率90％）で15/m2・ｈ、平均で25/m2・
ｈであった。The filtration flux was 42 / m 2 · h at the beginning and at the end (concentration factor 10
Double, honey recovery rate 90%) 15 / m 2 · h, average 25 / m 2 ·
h.
比較例 30Brixの蜂蜜を用いた以外は実施例と同様にして処理
した。その濾過液性状の分析結果を表に示す。Comparative Example A treatment was performed in the same manner as in Example except that 30 Brix honey was used. The analysis results of the properties of the filtrate are shown in the table.
濾過流束は初期が75/m2・ｈ、最終時（濃縮倍率10
倍、回収率90％）で25/m2・ｈ、平均で38/m2・ｈで
あった。The initial filtration flux was 75 / m 2 · h and the final
(Recovery rate: 90%) was 25 / m 2 · h, and the average was 38 / m 2 · h.
Claims (1)
温で平均孔径0.1〜0.3μｍの多孔質平板状膜を搭載した
プレートアンドフレーム型膜モジュールを用いて、濾過
することを特徴とする清澄蜂蜜の製造方法。1. A high-concentration honey of 50 to 70 Brix is filtered at a liquid temperature of 50 ° C. or higher using a plate and frame type membrane module equipped with a porous flat membrane having an average pore diameter of 0.1 to 0.3 μm. Characteristic method of producing clear honey.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP63065990A JP2607604B2 (en) | 1988-03-18 | 1988-03-18 | How to make clear honey |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP63065990A JP2607604B2 (en) | 1988-03-18 | 1988-03-18 | How to make clear honey |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPH01240156A JPH01240156A (en) | 1989-09-25 |
| JP2607604B2 true JP2607604B2 (en) | 1997-05-07 |
Family
ID=13302956
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP63065990A Expired - Lifetime JP2607604B2 (en) | 1988-03-18 | 1988-03-18 | How to make clear honey |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JP2607604B2 (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2294929A1 (en) | 2009-09-14 | 2011-03-16 | Apinov | Method for treating honey to obtain liquid, clear honey |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH01296948A (en) * | 1988-05-26 | 1989-11-30 | Sumitomo Bakelite Co Ltd | Purification of honey and purified honey |
| CN109170740A (en) * | 2018-08-22 | 2019-01-11 | 江苏润邦食品有限公司 | A kind of sphere adsorption purifying type honey defecation method and adsorption cleaning sphere |
| CN109170741A (en) * | 2018-08-22 | 2019-01-11 | 江苏润邦食品有限公司 | A kind of stirring-type honey defecation method and adsorption cleaning sphere |
| CN109259165A (en) * | 2018-11-15 | 2019-01-25 | 贵州超记蜂蜜商贸有限公司 | A kind of preparation method for clarifying honey |
| EP3794959A1 (en) | 2019-09-23 | 2021-03-24 | Universitatea Stefan cel Mare Suceava - Romania | Method and process for preventing honey crystallization |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH01157347A (en) * | 1987-12-12 | 1989-06-20 | Riyuuhoudou Seiyaku Kk | Production of undenatured and sterile honey |
-
1988
- 1988-03-18 JP JP63065990A patent/JP2607604B2/en not_active Expired - Lifetime
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2294929A1 (en) | 2009-09-14 | 2011-03-16 | Apinov | Method for treating honey to obtain liquid, clear honey |
| WO2011030020A1 (en) | 2009-09-14 | 2011-03-17 | Apinov | Method for treating honey in order to obtain a clear liquid honey |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH01240156A (en) | 1989-09-25 |
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