JP2568839B2 - High durability sound absorbing insulation - Google Patents

High durability sound absorbing insulation

Info

Publication number
JP2568839B2
JP2568839B2 JP62077148A JP7714887A JP2568839B2 JP 2568839 B2 JP2568839 B2 JP 2568839B2 JP 62077148 A JP62077148 A JP 62077148A JP 7714887 A JP7714887 A JP 7714887A JP 2568839 B2 JP2568839 B2 JP 2568839B2
Authority
JP
Japan
Prior art keywords
fiber
silica
insulating material
alumina
highly durable
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
JP62077148A
Other languages
Japanese (ja)
Other versions
JPS63242978A (en
Inventor
敬一 阪下
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ibiden Co Ltd
Original Assignee
Ibiden Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ibiden Co Ltd filed Critical Ibiden Co Ltd
Priority to JP62077148A priority Critical patent/JP2568839B2/en
Publication of JPS63242978A publication Critical patent/JPS63242978A/en
Application granted granted Critical
Publication of JP2568839B2 publication Critical patent/JP2568839B2/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Landscapes

  • Exhaust Silencers (AREA)
  • Porous Artificial Stone Or Porous Ceramic Products (AREA)
  • Nonwoven Fabrics (AREA)
  • Soundproofing, Sound Blocking, And Sound Damping (AREA)

Description

【発明の詳細な説明】 [産業上の利用分野] 本発明は自動車エンジン排気音の消音装置に関するも
のである。
Description: TECHNICAL FIELD The present invention relates to a muffler for exhaust noise of an automobile engine.

[従来の技術及びその問題点] 従来自動車エンジン排気音のマフラーは、排気ガスが
通過する内管とそれを覆う金属容器からできている。
[Prior art and its problems] Conventionally, a muffler for exhaust sound of an automobile engine is made of an inner pipe through which exhaust gas passes and a metal container covering the inner pipe.

ところが、近年騒音に対する規制が一段と厳しくなり
つつあり、かつエンジンの高性能化や排気ガス触媒の効
率化の為、排気ガスの温度も上昇傾向にある。
However, in recent years, regulations on noise have become more stringent, and the temperature of exhaust gas has also been increasing due to higher performance of engines and more efficient exhaust gas catalysts.

この対策として金属容器内の形状を複雑化したり、金
属容器自体を大型化する事が実施されているが、排気抵
抗が増加する事や自動車部品のレイアウト上大型化には
限界がある為、近年金属容器内周壁にガラスウーム等吸
音材をパンチングメタル等で支持するマフラーが使用さ
れるようになった。
As a countermeasure, the shape inside the metal container has been complicated and the metal container itself has been increased in size. A muffler that supports a sound absorbing material such as glass worm with a punching metal or the like has been used on the inner peripheral wall of a metal container.

さらに吸音効果を向上させる為一つの排気管系の中で
エンジンと従来のマフラーの中間部にプリマフラーと呼
ばれるマフラーが使用されるようになった。
In order to further improve the sound absorbing effect, a muffler called a pre-muffler has been used in an exhaust pipe system between the engine and the conventional muffler.

しかしながら前記ガラスウールを内周壁に使用したプ
リマフラーにおいて、前記ガラスウールはその組成上の
理由から耐熱温度が500℃と低く、それ以上の温度(排
気熱)に長時間さらされると熱劣化及び熱収縮がおこ
り、車両の振動による繊維の粉化及び排気流による繊維
の飛散が著しく、マフラーの吸音特性を低下させる原因
となっていた。
However, in the pre-muffler using the glass wool for the inner peripheral wall, the heat resistance temperature of the glass wool is as low as 500 ° C. due to its composition. Shrinkage occurs, and the fibers of the fiber are powdered by the vibration of the vehicle, and the fibers are scattered by the exhaust gas flow, which causes the sound absorbing characteristics of the muffler to deteriorate.

[問題点を解決する為の手段及び作用] 本発明は上記従来技術の欠点を除去解決することを目
的とし、この目的を達成するための手段として特許請求
の範囲に記載した高耐久マフラーを提供するものであ
る。
[Means and Actions for Solving the Problems] An object of the present invention is to eliminate and solve the above-mentioned drawbacks of the prior art, and to provide a highly durable muffler described in the claims as means for achieving this object. Is what you do.

即ち、本発明は繊維径が1〜3μであるシリカ・アル
ミナ繊維と繊維径が5〜10μであるEガラス繊維を主原
料とするシート状物を、結合材を用いて所定の形状と
し、500℃以上の排気ガスが通過する部分に於いて長時
間使用しても吸音特性を失なわない高耐久吸音断熱材を
提供するものである。
That is, the present invention is a sheet-shaped material having silica-alumina fiber having a fiber diameter of 1 to 3 μm and E glass fiber having a fiber diameter of 5 to 10 μm as main raw materials, formed into a predetermined shape using a binder, and An object of the present invention is to provide a highly durable sound-absorbing heat-insulating material which does not lose its sound-absorbing properties even when used for a long time in a portion where exhaust gas of not less than ° C passes.

ところでシリカ・アルミナ繊維の繊維径を2〜3μと
したのは、一般的に低コストで入手可能であることと、
ガラスウール、ロックウール、アスベスト等に比較して
最高使用温度が1260℃と耐熱性に優れた繊維であること
である。(商品名:イビウール・バルク) また、Eガラス繊維の繊維径を5〜10μとしたのは、
繊維形が10μより太い繊維の集合体は絡みあった繊維同
志が互いにぶつかったとき互いの剛性が強く折れ易い
為、耐久性に劣ること、さらに10μより太い繊維は一般
に人間の皮膚に刺さり易く作業性が悪い為である。繊維
径を5μ以上としたのは、繊維形が5μより細い繊維は
シート状に加工した際嵩密度が高くなり、吸音率が減少
してしまうこと、一般的に低コストで入手可能なEガラ
ス繊維は繊維径が5μ以上である為である。
By the way, the reason why the fiber diameter of the silica-alumina fiber is set to 2-3 μ is that it is generally available at low cost,
The maximum service temperature is 1260 ° C. as compared with glass wool, rock wool, asbestos and the like, so that the fiber is excellent in heat resistance. (Product name: Ibi wool bulk) Also, the fiber diameter of E glass fiber was set to 5 to 10μ,
An aggregate of fibers with a fiber shape larger than 10μ is inferior in durability because the entangled fibers collide with each other because they have strong rigidity and are easily broken.Fibers larger than 10μ are generally easy to stick to human skin Because it is bad. The reason why the fiber diameter is set to 5 μ or more is that fibers having a fiber shape smaller than 5 μ have a high bulk density when processed into a sheet shape and a reduced sound absorption coefficient. This is because the fiber has a fiber diameter of 5 μ or more.

本発明においてシリカ・アルミナ繊維とEガラス繊維
の割合は、シリカ・アルミナ繊維を40〜60重量%とし、
残部がEガラス繊維からなり、その合計量が100重量%
としたのは、シリカ・アルミナ繊維とEガラス繊維の割
合は、シリカ・アルミナ繊維が60wt%より多いと、耐熱
性には優れるが、繊維径が約2〜3μと細くその繊維長
も製造上不均一かつ短かい為、排気ガスの流速が10m/se
cを越えると飛散してしまう。
In the present invention, the ratio of silica-alumina fiber and E glass fiber is 40-60% by weight of silica-alumina fiber,
The balance consists of E glass fiber, the total amount of which is 100% by weight.
The reason is that the ratio of silica-alumina fiber to E-glass fiber is excellent when the silica-alumina fiber is more than 60 wt%, but the heat resistance is excellent, but the fiber diameter is as small as about 2 to 3μ and the fiber length is too large for manufacturing. Exhaust gas flow rate of 10m / se due to unevenness and shortness
If it exceeds c, it will scatter.

またシリカ・アルミナ繊維は40wt%より少ないと、排
気ガスの流速に対しては耐久性があるが、排気ガスの温
度が600℃より高くなると、Eガラス繊維の熱劣化の影
響が大きく、マフラーの振動によりEガラス繊維が折
れ、そのために飛散してしまう。
If the silica / alumina fiber content is less than 40 wt%, it is durable against the exhaust gas flow rate, but if the exhaust gas temperature is higher than 600 ° C, the thermal deterioration of the E glass fiber will have a large effect, The E glass fiber breaks due to the vibration and is scattered.

また、本発明において、一般的に用いられるラテック
スエマルジョン等の有機結合材、シリカゾル等の無機結
合から選択されるいずれか少なくとも1種を10重量%以
下としたのは、有機結合材が10重量%よりも多いと、成
形体中において見かけ嵩密度の小さい有機結合材の占有
する体積部分が増え、Eガラス繊維、シリカ・アルミナ
繊維の繊維同士の絡みが少なくなり、耐久性に悪影響を
及ぼすためであり、また無機結合材が10重量%より多い
と、前記繊維同士の結び付きが強すぎ、振動等に対する
耐久性が著しく劣化してしまいためである。
Further, in the present invention, at least one selected from organic binders such as latex emulsions and inorganic binders such as silica sol is generally used in an amount of 10% by weight or less. If it is larger than the above, the volume occupied by the organic binder having a small apparent bulk density in the molded body increases, and the entanglement between the E glass fiber and the silica-alumina fiber decreases, which adversely affects the durability. Also, if the amount of the inorganic binder is more than 10% by weight, the binding between the fibers is too strong, and the durability against vibration and the like is significantly deteriorated.

本発明を実施例により説明する。 The present invention will be described with reference to examples.

[実施例] シリカ50wt%アルミナ50wt%平均繊維径2.3μからな
るセラミックファイバーバルク(商品名イビウール・バ
ルク)50%と、あらかじめ繊維長が70mmになるように切
断加工した平均繊維径7μのEガラス繊維50%を乾式解
繊機にて混綿した後集綿しニードルパンチング処理を行
い、厚み5mm、嵩密度1.0g/cm3のシートに成形した高耐
久吸音断熱材に、固形分濃度を10%に希釈したSBR系ラ
テックスを含浸させ、外径100mmのパイプに嵩密度が変
化しないように巻きつけた後乾燥し、肉厚5mmの筒状耐
久断熱材を成形した。
[Example] 50% of silica 50% of alumina 50% of ceramic fiber bulk (trade name: ibiwool bulk) having an average fiber diameter of 2.3μ and E glass having an average fiber diameter of 7μ previously cut so that the fiber length becomes 70mm. 50% fibers make cotton was needle-punched current after the cotton mixing by a dry fiberizer, thickness 5 mm, the high durability acoustic insulation material molded into a sheet having a bulk density of 1.0 g / cm 3, a solid content of 10% The diluted SBR-based latex was impregnated, wound around a pipe having an outer diameter of 100 mm without changing the bulk density, and then dried to form a 5 mm-thick cylindrical durable heat insulating material.

さらに、開口率30%、穴径4mm、肉厚1mm、外径100mm
の筒状パンチングメタルの外側に前記筒状高耐久断熱材
を嵌装し、さらに肉厚1mm、外径110mmの金属性パイプを
嵌装した後、筒状パンチングメタルの両端に、中心に直
径50m/mの穴をあけたドーナツ状のパンチングメタル
(開口率30%穴径4mm、肉厚1mm、外径100mm)を全周溶
接する。
In addition, aperture ratio 30%, hole diameter 4mm, wall thickness 1mm, outer diameter 100mm
After fitting the cylindrical highly durable heat insulating material outside the cylindrical punching metal, and further fitting a metal pipe having a thickness of 1 mm and an outer diameter of 110 mm, the diameter of the center is 50 m at both ends of the cylindrical punching metal. Donut-shaped perforated metal (hole diameter 30%, hole diameter 4mm, wall thickness 1mm, outer diameter 100mm) with / m holes is welded all around.

さらに、前記ドーナツ状のパンチングメタルの外側
に、前記シート状に成形した厚み5mmの高耐久吸音断熱
材を内径50mm、外径110mにより打ち抜き加工したものを
装着しさらに、厚み1mm、内径50mm、外径110mmの鋼板を
あて、金属性パイプの端部に前周溶接をおこない、外径
110mm、全長200mmの高耐久吸音断熱機とし、両端の開口
部に厚み1mm、外径50mm、長さ20mmのパイプを差し込み
外側から全周溶接した第1図に示される試験体を製作し
た。
Furthermore, on the outside of the donut-shaped punching metal, a 5 mm-thick highly durable sound-absorbing heat-insulating material formed into a sheet shape and punched with an inner diameter of 50 mm and an outer diameter of 110 m is attached. Apply a steel plate with a diameter of 110 mm, weld the front circumference to the end of the metal pipe,
A highly durable sound-absorbing heat insulator having a length of 110 mm and a total length of 200 mm, a pipe having a thickness of 1 mm, an outer diameter of 50 mm, and a length of 20 mm was inserted into openings at both ends, and a test piece shown in FIG.

前記試験体の片側の開口部に外径45mmのスピーカーを
あて、反射側の開口部に於いて、「リオンオクターブ・
バンドアナライザー」を用いて吸音率を測定した後、第
2図に示される耐久性試験機に装着し、温度800℃、流
速25m/sec、振動数2930cpm、振幅1.5mm、振動加速度7
G、の条件で720時間テストした後、再度吸音率を測定し
た結果を第1表に示す。
A speaker having an outer diameter of 45 mm was placed on one side of the opening of the test piece, and "Rion Octave /
After measuring the sound absorption coefficient using the “Band Analyzer”, it was attached to the durability tester shown in FIG. 2, and the temperature was 800 ° C., the flow velocity was 25 m / sec, the frequency was 2930 cpm, the amplitude was 1.5 mm, and the vibration acceleration was 7
After a 720-hour test under the conditions of G, the sound absorption coefficient was measured again, and the results are shown in Table 1.

(比較例1) 吸音材を使用せず、実施例1と同様の耐久性試験を行
った結果を第1表に示す。
(Comparative Example 1) The results of a durability test performed in the same manner as in Example 1 without using any sound absorbing material are shown in Table 1.

((比較例2) シリカ50%のアルミナ50%平均繊維径2.3μからなる
セラミックファイバーバルク80%と平均繊維径8μのE
ガラス繊維20%を用いて、実施例1と同様の耐久性試験
を行った結果は第1表に示すとおりである。
((Comparative Example 2) 50% silica, 50% alumina, 80% ceramic fiber bulk with an average fiber diameter of 2.3μ and E with an average fiber diameter of 8μ
The results of a durability test performed in the same manner as in Example 1 using 20% of glass fibers are as shown in Table 1.

(比較例3) シリカ50%アルミナ50%平均繊維2.3μからなるセラ
ミックファイバーバルク20%と平均繊維径8μのEガラ
ス繊維80%を用いて、実施例1と同様の耐久性試験を行
った結果は第1表に示すとおりである。
(Comparative Example 3) The same durability test as in Example 1 was performed using 20% ceramic fiber bulk consisting of 50% silica and 50% alumina and 2.3% average fiber and 80% E glass fiber having an average fiber diameter of 8μ. Is as shown in Table 1.

(比較例4) シリカ50%アルミナ50%平均繊維径2.3μからなるセ
ラミックファイバーバルク50%と平均繊維径20μのEガ
ラス繊維50%を用いて、実施例1と同様の耐久性試験を
行った結果は第1表に示すとおりである。
(Comparative Example 4) A durability test similar to that of Example 1 was performed using 50% of ceramic fiber bulk having 50% silica and 50% alumina and 50% ceramic fiber bulk having an average fiber diameter of 2.3μ and E glass fiber having an average fiber diameter of 20μ. The results are as shown in Table 1.

(発明の効果) 比較例1及び3及び4にくらべ、吸音特性に優れる。(Effects of the Invention) Compared with Comparative Examples 1, 3 and 4, the sound absorbing properties are excellent.

比較例2及び3及び4にくらべ、吸音特性の経時変化
が少ない。
Compared to Comparative Examples 2, 3 and 4, the change over time in the sound absorption characteristics is small.

前記の理由により自動車のエキゾーストパイプに於い
て、マフラーを500℃以上の排気温度の高い場所に設置
できるようになり、高い吸音効果を長期間維持し続ける
ことが可能となった。
For the above-mentioned reason, in the exhaust pipe of the automobile, the muffler can be installed at a place where the exhaust temperature is higher than 500 ° C., and the high sound absorbing effect can be maintained for a long time.

【図面の簡単な説明】[Brief description of the drawings]

第1図は本発明の高耐久吸音断熱材を実際プリマフラー
に用いられる形状としたモデルの縦断面図である。第2
図は耐久性試験装置を示す経路図である。 符号の説明 1……金属容器、2……パンチングメタル、3……高耐
久吸音断熱材、4……吸気管、5……排気管、11……バ
ーナー、12……熱交換器、13……電磁弁、14……試験
体、15……振動機、16……周波数交換機、17……圧力
計、18……熱伝対、19……温度指示計、20……温度記録
計、21……風速計、22……耐振ゴム、23……レギュレー
ター。
FIG. 1 is a longitudinal sectional view of a model in which the highly durable sound-absorbing heat-insulating material of the present invention has a shape used in an actual pre-muffler. Second
The figure is a route diagram showing the durability test apparatus. DESCRIPTION OF SYMBOLS 1 ... Metal container, 2 ... Punched metal, 3 ... Highly durable sound absorbing heat insulating material, 4 ... Intake pipe, 5 ... Exhaust pipe, 11 ... Burner, 12 ... Heat exchanger, 13 ... … Solenoid valve, 14… Test piece, 15… Vibrator, 16… Frequency exchanger, 17… Pressure gauge, 18… Thermocouple, 19… Temperature indicator, 20… Temperature recorder, 21 …… Anemometer, 22… Vibration-proof rubber, 23 …… Regulator.

Claims (5)

(57)【特許請求の範囲】(57) [Claims] 【請求項1】平均繊維径1〜3μであるシリカ・アルミ
ナ繊維と、平均繊維径が5〜10μであるEガラス繊維か
らなる混綿繊維90重量%以上と、一般的に用いられるラ
テックスエマルジョン等の有機結合材、シリカゾル等の
無機結合材から選択されるいずれか少なくとも1種を10
重量%以下使用して所定の形状に成形したことを特徴と
する自動車エンジンのプリマフラー用高耐久吸音断熱
材。
1. A silica-alumina fiber having an average fiber diameter of 1 to 3 .mu.m, a blended fiber made of E glass fiber having an average fiber diameter of 5 to 10 .mu. At least one selected from organic binders and inorganic binders such as silica sol
A highly durable sound-absorbing heat insulating material for an automotive engine pre-muffler, wherein the heat insulating material is formed into a predetermined shape using less than 10% by weight.
【請求項2】前記シリカ・アルミナ繊維は、アルミナ45
〜95重量%で残部がシリカからなることを特徴とする特
許請求の範囲第1項記載の項耐久吸音断熱材。
2. The method according to claim 1, wherein the silica-alumina fiber comprises alumina 45.
2. The durable sound absorbing and heat insulating material according to claim 1, wherein the balance is from 95 to 95% by weight of silica.
【請求項3】前記高耐久吸音断熱材は常法の乾式で作ら
れた不織布を切断加工等によって成形するか、湿式の抄
造成形法で成形する事を特徴とする特許請求の範囲第1
項〜第2項記載の高耐久吸音断熱材。
3. The highly durable sound-absorbing heat-insulating material is formed by cutting a nonwoven fabric made by an ordinary dry method by cutting or by a wet papermaking method.
Item 3. A highly durable sound-absorbing heat-insulating material according to item 2 or 3.
【請求項4】前記プリマフラーは自動車のエキゾースト
パイプに連らなる、500℃以上の排気ガスが通過する部
分に位置することを特徴とする特許請求の範囲第1項〜
第3項記載の高耐久吸音断熱材。
4. The exhaust system according to claim 1, wherein said pre-muffler is located at a portion connected to an exhaust pipe of an automobile and through which exhaust gas of 500 ° C. or more passes.
4. A highly durable sound absorbing and heat insulating material according to claim 3.
【請求項5】前記シリカ・アルミナ繊維とEガラス繊維
の混綿繊維は、シリカ・アルミナ繊維が40〜60重量%か
らなり残部がEガラス繊維からなりその合計量が100重
量%となることを特徴とする特許請求の範囲第1項〜第
4項記載の高耐久吸音断熱材。
5. The mixed fiber of silica / alumina fiber and E glass fiber is characterized in that the silica / alumina fiber is 40 to 60% by weight, the balance is E glass fiber, and the total amount is 100% by weight. The highly durable sound absorbing and heat insulating material according to any one of claims 1 to 4, wherein
JP62077148A 1987-03-30 1987-03-30 High durability sound absorbing insulation Expired - Lifetime JP2568839B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP62077148A JP2568839B2 (en) 1987-03-30 1987-03-30 High durability sound absorbing insulation

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP62077148A JP2568839B2 (en) 1987-03-30 1987-03-30 High durability sound absorbing insulation

Publications (2)

Publication Number Publication Date
JPS63242978A JPS63242978A (en) 1988-10-07
JP2568839B2 true JP2568839B2 (en) 1997-01-08

Family

ID=13625710

Family Applications (1)

Application Number Title Priority Date Filing Date
JP62077148A Expired - Lifetime JP2568839B2 (en) 1987-03-30 1987-03-30 High durability sound absorbing insulation

Country Status (1)

Country Link
JP (1) JP2568839B2 (en)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2003089953A (en) * 2001-09-14 2003-03-28 Nippon Glass Fiber Kogyo Kk Heat-resistant glass fiber mat and method of producing the same
WO2007054697A1 (en) * 2005-11-10 2007-05-18 The Morgan Crucible Company Plc High temperature resistant fibres
JP2010096171A (en) * 2008-04-30 2010-04-30 Ibiden Co Ltd Mat material, method for manufacturing mat material, muffler, and method for manufacturing muffler
KR20090117969A (en) * 2008-04-30 2009-11-17 이비덴 가부시키가이샤 Mat materials, method for producing mat materials, silencer and method for producing silencer
EP3971154A4 (en) * 2019-05-14 2023-01-25 Nichias Corporation Porous material

Also Published As

Publication number Publication date
JPS63242978A (en) 1988-10-07

Similar Documents

Publication Publication Date Title
US2834425A (en) Exhaust muffler
EP0161692B1 (en) Sound-absorbing device for use as muffler for exhaust gas from an internal combustion engine
JPH09144986A (en) Noise absorbing duct structure
GB2262947A (en) Sound absorbing fibrous materials
JP2568839B2 (en) High durability sound absorbing insulation
US4529060A (en) Absorption muffler for gas-dynamic pressure-wave machines
US4137993A (en) Insulated exhaust system component
US4598791A (en) Exhaust silencer
WO2020217862A1 (en) Noise reduction structure for exhaust pipes
JPH04203308A (en) Silencer of internal combustion engine
JP2018161778A (en) Sound absorber and vehicle component
JPH11101121A (en) Muffler for internal combustion engine
WO2020217863A1 (en) Inorganic-fiber containing mat and noise reduction structure for exhaust pipe
JP2004138057A (en) Exhaust construction of internal combustion engine, and method for manufacturing the same
JPH01211608A (en) Heat resistant sound absorbing material
JP6670914B1 (en) Sound absorbing material
JPS622261Y2 (en)
JPS639610A (en) High durability muffler
JPH08286673A (en) Sound absorbing duct structure
JPH076377B2 (en) Silencer for internal combustion engine
US3746114A (en) Sound attenuating structure
JP2798759B2 (en) Silencer
JP3302497B2 (en) Three-dimensional soundproof and heat insulating plate
JPH08260939A (en) Muffler
JPH09228822A (en) Muffler of internal combustion engine

Legal Events

Date Code Title Description
R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

EXPY Cancellation because of completion of term
FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20071003

Year of fee payment: 11