JP2024020699A - Agricultural water surface application granular composition - Google Patents
Agricultural water surface application granular composition Download PDFInfo
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- JP2024020699A JP2024020699A JP2022123069A JP2022123069A JP2024020699A JP 2024020699 A JP2024020699 A JP 2024020699A JP 2022123069 A JP2022123069 A JP 2022123069A JP 2022123069 A JP2022123069 A JP 2022123069A JP 2024020699 A JP2024020699 A JP 2024020699A
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- JP
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- Prior art keywords
- methyl
- acid
- water surface
- active ingredient
- alkyl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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- 239000000203 mixture Substances 0.000 title claims abstract description 36
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 33
- 125000000217 alkyl group Chemical group 0.000 claims abstract description 32
- 239000012868 active agrochemical ingredient Substances 0.000 claims abstract description 14
- 239000004480 active ingredient Substances 0.000 claims description 40
- 230000002363 herbicidal effect Effects 0.000 claims description 30
- 229940100389 Sulfonylurea Drugs 0.000 claims description 11
- YROXIXLRRCOBKF-UHFFFAOYSA-N sulfonylurea Chemical class OC(=N)N=S(=O)=O YROXIXLRRCOBKF-UHFFFAOYSA-N 0.000 claims description 11
- KFSUCTRGHQKXSV-UHFFFAOYSA-N 5-(1h-pyrazol-5-yl)-1h-pyrazole Chemical class N1N=CC=C1C1=CC=NN1 KFSUCTRGHQKXSV-UHFFFAOYSA-N 0.000 claims description 6
- 241000196324 Embryophyta Species 0.000 claims description 3
- 238000000034 method Methods 0.000 claims description 2
- 241000607479 Yersinia pestis Species 0.000 claims 1
- 238000010586 diagram Methods 0.000 abstract 1
- -1 Ashram Chemical compound 0.000 description 142
- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 25
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 20
- 239000000194 fatty acid Substances 0.000 description 16
- 235000014113 dietary fatty acids Nutrition 0.000 description 15
- 229930195729 fatty acid Natural products 0.000 description 15
- 239000004094 surface-active agent Substances 0.000 description 13
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 12
- 239000003905 agrochemical Substances 0.000 description 11
- 238000009472 formulation Methods 0.000 description 11
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 11
- 229920002472 Starch Polymers 0.000 description 10
- 150000002148 esters Chemical class 0.000 description 10
- 229920000642 polymer Polymers 0.000 description 10
- 235000019698 starch Nutrition 0.000 description 10
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 8
- 229920001577 copolymer Polymers 0.000 description 8
- USIUVYZYUHIAEV-UHFFFAOYSA-N diphenyl ether Chemical compound C=1C=CC=CC=1OC1=CC=CC=C1 USIUVYZYUHIAEV-UHFFFAOYSA-N 0.000 description 8
- 150000003839 salts Chemical class 0.000 description 8
- 239000008107 starch Substances 0.000 description 8
- 229910019142 PO4 Inorganic materials 0.000 description 7
- 150000004665 fatty acids Chemical class 0.000 description 7
- 239000010452 phosphate Substances 0.000 description 7
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 6
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 6
- 239000002253 acid Substances 0.000 description 6
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 6
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 6
- 239000004927 clay Substances 0.000 description 6
- 239000000575 pesticide Substances 0.000 description 6
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 5
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 5
- 239000008187 granular material Substances 0.000 description 5
- 238000003860 storage Methods 0.000 description 5
- UFAPVJDEYHLLBG-UHFFFAOYSA-N 2-{2-chloro-4-(methylsulfonyl)-3-[(tetrahydrofuran-2-ylmethoxy)methyl]benzoyl}cyclohexane-1,3-dione Chemical compound ClC1=C(COCC2OCCC2)C(S(=O)(=O)C)=CC=C1C(=O)C1C(=O)CCCC1=O UFAPVJDEYHLLBG-UHFFFAOYSA-N 0.000 description 4
- 239000004375 Dextrin Substances 0.000 description 4
- 229920001353 Dextrin Polymers 0.000 description 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerol Natural products OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 4
- 240000007594 Oryza sativa Species 0.000 description 4
- 235000007164 Oryza sativa Nutrition 0.000 description 4
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 4
- BGNQYGRXEXDAIQ-UHFFFAOYSA-N Pyrazosulfuron-ethyl Chemical group C1=NN(C)C(S(=O)(=O)NC(=O)NC=2N=C(OC)C=C(OC)N=2)=C1C(=O)OCC BGNQYGRXEXDAIQ-UHFFFAOYSA-N 0.000 description 4
- 150000003973 alkyl amines Chemical class 0.000 description 4
- 235000013339 cereals Nutrition 0.000 description 4
- 238000000354 decomposition reaction Methods 0.000 description 4
- 235000019425 dextrin Nutrition 0.000 description 4
- 230000005484 gravity Effects 0.000 description 4
- PSZYNBSKGUBXEH-UHFFFAOYSA-N naphthalene-1-sulfonic acid Chemical compound C1=CC=C2C(S(=O)(=O)O)=CC=CC2=C1 PSZYNBSKGUBXEH-UHFFFAOYSA-N 0.000 description 4
- 239000002245 particle Substances 0.000 description 4
- BOTNYLSAWDQNEX-UHFFFAOYSA-N phenoxymethylbenzene Chemical compound C=1C=CC=CC=1COC1=CC=CC=C1 BOTNYLSAWDQNEX-UHFFFAOYSA-N 0.000 description 4
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 4
- 229920001451 polypropylene glycol Polymers 0.000 description 4
- 235000009566 rice Nutrition 0.000 description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 4
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 3
- 239000005472 Bensulfuron methyl Substances 0.000 description 3
- 239000005711 Benzoic acid Substances 0.000 description 3
- 239000005567 Imazosulfuron Substances 0.000 description 3
- NAGRVUXEKKZNHT-UHFFFAOYSA-N Imazosulfuron Chemical compound COC1=CC(OC)=NC(NC(=O)NS(=O)(=O)C=2N3C=CC=CC3=NC=2Cl)=N1 NAGRVUXEKKZNHT-UHFFFAOYSA-N 0.000 description 3
- 239000005578 Mesotrione Substances 0.000 description 3
- OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 3
- IHHMUBRVTJMLQO-UHFFFAOYSA-N Pyraclonil Chemical compound C#CCN(C)C1=C(C#N)C=NN1C1=NN(CCCC2)C2=C1Cl IHHMUBRVTJMLQO-UHFFFAOYSA-N 0.000 description 3
- 150000007513 acids Chemical class 0.000 description 3
- XMQFTWRPUQYINF-UHFFFAOYSA-N bensulfuron-methyl Chemical group COC(=O)C1=CC=CC=C1CS(=O)(=O)NC(=O)NC1=NC(OC)=CC(OC)=N1 XMQFTWRPUQYINF-UHFFFAOYSA-N 0.000 description 3
- 235000010233 benzoic acid Nutrition 0.000 description 3
- 150000001735 carboxylic acids Chemical class 0.000 description 3
- 239000007859 condensation product Substances 0.000 description 3
- 150000002170 ethers Chemical class 0.000 description 3
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 description 3
- 239000011976 maleic acid Substances 0.000 description 3
- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 description 3
- KPUREKXXPHOJQT-UHFFFAOYSA-N mesotrione Chemical compound [O-][N+](=O)C1=CC(S(=O)(=O)C)=CC=C1C(=O)C1C(=O)CCCC1=O KPUREKXXPHOJQT-UHFFFAOYSA-N 0.000 description 3
- 239000003921 oil Substances 0.000 description 3
- 229920002503 polyoxyethylene-polyoxypropylene Polymers 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- ZCVAOQKBXKSDMS-PVAVHDDUSA-N (+)-trans-(S)-allethrin Chemical compound CC1(C)[C@H](C=C(C)C)[C@H]1C(=O)O[C@@H]1C(C)=C(CC=C)C(=O)C1 ZCVAOQKBXKSDMS-PVAVHDDUSA-N 0.000 description 2
- ZFHGXWPMULPQSE-UKSCLKOJSA-N (Z)-(1R)-cis-tefluthrin Chemical compound FC1=C(F)C(C)=C(F)C(F)=C1COC(=O)[C@H]1C(C)(C)[C@H]1\C=C(/Cl)C(F)(F)F ZFHGXWPMULPQSE-UKSCLKOJSA-N 0.000 description 2
- PYCINWWWERDNKE-UHFFFAOYSA-N 1-(2-chloro-6-propylimidazo[1,2-b]pyridazin-3-yl)sulfonyl-3-(4,6-dimethoxypyrimidin-2-yl)urea Chemical compound N12N=C(CCC)C=CC2=NC(Cl)=C1S(=O)(=O)NC(=O)NC1=NC(OC)=CC(OC)=N1 PYCINWWWERDNKE-UHFFFAOYSA-N 0.000 description 2
- IXWKBUKANTXHJH-UHFFFAOYSA-N 1-[5-chloro-2-methyl-4-(5-methyl-5,6-dihydro-1,4,2-dioxazin-3-yl)pyrazol-3-yl]sulfonyl-3-(4,6-dimethoxypyrimidin-2-yl)urea Chemical compound COC1=CC(OC)=NC(NC(=O)NS(=O)(=O)C=2N(N=C(Cl)C=2C=2OC(C)CON=2)C)=N1 IXWKBUKANTXHJH-UHFFFAOYSA-N 0.000 description 2
- NFGXHKASABOEEW-UHFFFAOYSA-N 1-methylethyl 11-methoxy-3,7,11-trimethyl-2,4-dodecadienoate Chemical compound COC(C)(C)CCCC(C)CC=CC(C)=CC(=O)OC(C)C NFGXHKASABOEEW-UHFFFAOYSA-N 0.000 description 2
- JAHNSTQSQJOJLO-UHFFFAOYSA-N 2-(3-fluorophenyl)-1h-imidazole Chemical compound FC1=CC=CC(C=2NC=CN=2)=C1 JAHNSTQSQJOJLO-UHFFFAOYSA-N 0.000 description 2
- ZXVONLUNISGICL-UHFFFAOYSA-N 4,6-dinitro-o-cresol Chemical compound CC1=CC([N+]([O-])=O)=CC([N+]([O-])=O)=C1O ZXVONLUNISGICL-UHFFFAOYSA-N 0.000 description 2
- HGINCPLSRVDWNT-UHFFFAOYSA-N Acrolein Chemical compound C=CC=O HGINCPLSRVDWNT-UHFFFAOYSA-N 0.000 description 2
- 239000003666 Amidosulfuron Substances 0.000 description 2
- CTTHWASMBLQOFR-UHFFFAOYSA-N Amidosulfuron Chemical compound COC1=CC(OC)=NC(NC(=O)NS(=O)(=O)N(C)S(C)(=O)=O)=N1 CTTHWASMBLQOFR-UHFFFAOYSA-N 0.000 description 2
- 239000005469 Azimsulfuron Substances 0.000 description 2
- 244000063299 Bacillus subtilis Species 0.000 description 2
- 235000014469 Bacillus subtilis Nutrition 0.000 description 2
- 241000223679 Beauveria Species 0.000 description 2
- 239000005734 Benalaxyl Substances 0.000 description 2
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
- 239000005496 Chlorsulfuron Substances 0.000 description 2
- YVGGHNCTFXOJCH-UHFFFAOYSA-N DDT Chemical compound C1=CC(Cl)=CC=C1C(C(Cl)(Cl)Cl)C1=CC=C(Cl)C=C1 YVGGHNCTFXOJCH-UHFFFAOYSA-N 0.000 description 2
- UWVKRNOCDUPIDM-UHFFFAOYSA-N Ethoxysulfuron Chemical compound CCOC1=CC=CC=C1OS(=O)(=O)NC(=O)NC1=NC(OC)=CC(OC)=N1 UWVKRNOCDUPIDM-UHFFFAOYSA-N 0.000 description 2
- 239000005514 Flazasulfuron Substances 0.000 description 2
- HWATZEJQIXKWQS-UHFFFAOYSA-N Flazasulfuron Chemical compound COC1=CC(OC)=NC(NC(=O)NS(=O)(=O)C=2C(=CC=CN=2)C(F)(F)F)=N1 HWATZEJQIXKWQS-UHFFFAOYSA-N 0.000 description 2
- FICWGWVVIRLNRB-UHFFFAOYSA-N Flucetosulfuron Chemical compound COCC(=O)OC(C(C)F)C1=NC=CC=C1S(=O)(=O)NC(=O)NC1=NC(OC)=CC(OC)=N1 FICWGWVVIRLNRB-UHFFFAOYSA-N 0.000 description 2
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- FMGZEUWROYGLAY-UHFFFAOYSA-N Halosulfuron-methyl Chemical group ClC1=NN(C)C(S(=O)(=O)NC(=O)NC=2N=C(OC)C=C(OC)N=2)=C1C(=O)OC FMGZEUWROYGLAY-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 description 2
- 239000005807 Metalaxyl Substances 0.000 description 2
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 description 2
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- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 2
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- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 description 2
- 150000001336 alkenes Chemical class 0.000 description 2
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- MAHPNPYYQAIOJN-UHFFFAOYSA-N azimsulfuron Chemical compound COC1=CC(OC)=NC(NC(=O)NS(=O)(=O)C=2N(N=CC=2C2=NN(C)N=N2)C)=N1 MAHPNPYYQAIOJN-UHFFFAOYSA-N 0.000 description 2
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- 239000001768 carboxy methyl cellulose Substances 0.000 description 2
- 239000000969 carrier Substances 0.000 description 2
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- 239000003795 chemical substances by application Substances 0.000 description 2
- NSWAMPCUPHPTTC-UHFFFAOYSA-N chlorimuron-ethyl Chemical group CCOC(=O)C1=CC=CC=C1S(=O)(=O)NC(=O)NC1=NC(Cl)=CC(OC)=N1 NSWAMPCUPHPTTC-UHFFFAOYSA-N 0.000 description 2
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- WQOXQRCZOLPYPM-UHFFFAOYSA-N dimethyl disulfide Chemical compound CSSC WQOXQRCZOLPYPM-UHFFFAOYSA-N 0.000 description 2
- FBOUIAKEJMZPQG-BLXFFLACSA-N diniconazole-M Chemical compound C1=NC=NN1/C([C@H](O)C(C)(C)C)=C/C1=CC=C(Cl)C=C1Cl FBOUIAKEJMZPQG-BLXFFLACSA-N 0.000 description 2
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- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 2
- KWIUHFFTVRNATP-UHFFFAOYSA-N glycine betaine Chemical compound C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 description 2
- 229940093915 gynecological organic acid Drugs 0.000 description 2
- RONFGUROBZGJKP-UHFFFAOYSA-N iminoctadine Chemical compound NC(N)=NCCCCCCCCNCCCCCCCCN=C(N)N RONFGUROBZGJKP-UHFFFAOYSA-N 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 230000000749 insecticidal effect Effects 0.000 description 2
- 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 2
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Abstract
【課題】農薬活性成分が安定な農業用水面施用粒状組成物を提供する。【解決手段】(a)農薬活性成分及び、水面拡展剤として(b)アルキルポリグリコシドを含有することを特徴とする農業用水面施用粒状組成物。【選択図】なしAn object of the present invention is to provide a granular composition for agricultural water surface application in which an agrochemical active ingredient is stable. SOLUTION: A granular composition for agricultural water surface application, characterized by containing (a) an agrochemical active ingredient and (b) an alkyl polyglycoside as a water surface spreader. [Selection diagram] None
Description
本発明は、農薬活性成分を長期間安定に保持でき、施用時に優れた水面拡展性を有する農薬粒剤に関するものである。 The present invention relates to agrochemical granules that can stably retain agrochemical active ingredients for a long period of time and have excellent water surface dispersibility when applied.
水稲用農薬製剤の剤型として、粒剤、フロアブル剤、水和剤、粉剤、乳剤等が知られている。近年においては、農薬散布の省力化として水田に浮遊させる農薬製剤の剤型が知られており、粒状組成物を直接水田に散布もしくはドローン等に搭載して散布する形態、水溶性フィルムで包装し投げ込む形態のように、水田に入らず畦畔から散布可能な農薬製剤が使用されている。 Granules, flowables, wettable powders, powders, emulsions, and the like are known as dosage forms of agrochemical formulations for paddy rice. In recent years, formulations of pesticide formulations that are suspended in rice fields have become known as labor-saving methods for spraying pesticides. Pesticide formulations are used, such as those that can be sprayed from the ridges without entering the rice fields.
農薬活性成分の中でもピラゾリルピラゾール誘導体、スルホニルウレア系除草活性成分及びトリケトン系除草活性成分は優れた除草活性を有することが知られており、これらを含有する農薬粒状組成物も数多く知られている。他方で除草活性成分の多くは、使用する条件によっては栽培植物に対する薬害が問題となる場合がある。例えば特許文献1ではこのような除草活性成分としてピラゾリルピラゾール誘導体であるピラクロニル及びシクロピラニルが挙げられ、両成分は実施例にも記載されている。また特許文献2ではこのような除草活性成分としてピラクロニルのほかスルホニルウレア系除草活性成分及びトリケトン系除草活性成分が挙げられ、実施例にはスルホニルウレア系除草活性成分であるベンスルフロンメチル、ピラゾスルフロンエチル及びハロスルフロン、並びに、トリケトン系除草活性成分であるベンゾビシクロン及びテフリルトリオンが記載されている。
一般に農薬活性成分が施用時に水田中で拡散せず局在することは薬害を助長する一因となるため、農薬粒状組成物は、施用時に優れた水面拡散性を有する必要がある。
Among pesticide active ingredients, pyrazolyl pyrazole derivatives, sulfonylurea herbicidal active ingredients, and triketone herbicidal active ingredients are known to have excellent herbicidal activity, and many granular pesticide compositions containing these are also known. On the other hand, many herbicidal active ingredients may pose a problem of phytotoxicity to cultivated plants depending on the conditions of use. For example, in Patent Document 1, pyraclonyl and cyclopyranyl, which are pyrazolyl pyrazole derivatives, are mentioned as such herbicidal active ingredients, and both ingredients are also described in Examples. Furthermore, in Patent Document 2, in addition to pyraclonil, sulfonylurea herbicidal active ingredients and triketone herbicidal active ingredients are mentioned as such herbicidal active ingredients, and examples include bensulfuron methyl, pyrazosulfuron ethyl, and pyrazosulfuronethyl, which are sulfonylurea herbicidal active ingredients. Halosulfuron and the triketone herbicidal active ingredients benzobiciclon and tefuryltrione are described.
Generally, when an agricultural chemical active ingredient is localized without being diffused in a paddy field during application, it is a factor that promotes phytotoxicity, so a granular agricultural chemical composition needs to have excellent water surface dispersibility during application.
他方、農薬活性成分の中でも特にスルホニルウレア系除草活性成分及びトリケトン系除草活性成分は保管中に製剤内で分解することが知られている。
例えば特許文献3ではスルホニルウレア系除草活性成分は加水分解が起こりやすく、製剤中において補助成分や他の有効成分との配合により経時的に不安定になることが記載されており、実施例にはイマゾスルフロンが記載されている。
さらに特許文献4ではトリケトン系除草活性成分を含む農薬粒剤において、特定の条件下で経時的に不安定になることが記載されており、実施例にはテフリルトリオン及びメソトリオンが記載されている。
したがって、スルホニルウレア系除草活性成分及び/又はトリケトン系除草活性成分を含有する農薬粒状組成物においては、副資材の選択に細心の注意を払う必要がある。
On the other hand, it is known that among agrochemical active ingredients, in particular, sulfonylurea herbicidal active ingredients and triketone herbicidal active ingredients decompose within the formulation during storage.
For example, Patent Document 3 describes that sulfonylurea herbicidal active ingredients are prone to hydrolysis and become unstable over time when mixed with auxiliary ingredients or other active ingredients in the formulation, and examples include imazosulfuron. is listed.
Furthermore, Patent Document 4 describes that pesticide granules containing triketone-based herbicidal active ingredients become unstable over time under certain conditions, and Examples include tefuryltrione and mesotrione. .
Therefore, in a granular agricultural chemical composition containing a sulfonylurea herbicidal active ingredient and/or a triketone herbicidal active ingredient, it is necessary to pay close attention to the selection of auxiliary materials.
水田に浮遊させる農薬製剤の剤型に主に用いられる水面拡展剤は、水面上で粒状組成物を局在化させずに、より広範囲に拡展させる剤である。
主に、アセチレン誘導体(例えば商品名オルフィンE1010;特許文献5参照)、アルキルアルコールのアルキレンオキサイド付加物(例えば商品名ノイゲンLF-60X;特許文献6参照)、アルカンジオール誘導体(例えば商品名ニューカルゲンTG-310;特許文献7参照)等が知られており、これらの水面拡展剤の使用は、優れた拡展性を付与するが、一部の農薬活性成分の分解を促進するという問題がある。
A water surface spreading agent, which is mainly used in the formulation of agricultural chemical formulations that are floated in rice fields, is an agent that spreads the granular composition over a wider area without localizing it on the water surface.
Mainly, acetylene derivatives (for example, trade name Olfine E1010; see Patent Document 5), alkylene oxide adducts of alkyl alcohols (for example, trade name Neugen LF-60X; see Patent Document 6), alkanediol derivatives (for example, trade name Nucalgen TG), -310; see Patent Document 7), and the use of these water surface spreaders provides excellent spreadability, but has the problem of accelerating the decomposition of some pesticide active ingredients. .
また、アルキルポリグリコシドは農薬製剤に使用されることがあり、スルホニルウレア系除草活性成分の分解を軽減する効果があることも知られている(例えば特許文献8、9、10及び11参照)。しかしながら、そのほとんどが水中に成分を分散させるための分散剤や物理的製剤安定性の向上を目的とした利用であり、水面拡展剤として使用すること
についてはこれまで開示されていなかった。
Furthermore, alkyl polyglycosides are sometimes used in agricultural chemical formulations, and are known to have the effect of reducing the decomposition of sulfonylurea herbicidal active ingredients (see, for example, Patent Documents 8, 9, 10, and 11). However, most of them are used as dispersants for dispersing components in water or to improve the stability of physical preparations, and their use as water surface spreaders has not been disclosed so far.
本発明は農薬活性成分を含有し、農薬活性成分を長期間安定に保持でき、かつ、施用時に優れた水面拡展性を有する農薬粒剤を提供することを課題とする。 An object of the present invention is to provide agrochemical granules that contain an agrochemical active ingredient, can stably retain the agrochemical active ingredient for a long period of time, and have excellent water surface dispersibility when applied.
本発明者らはこれらの課題を解決するべく鋭意研究を行った。その結果、(a)農薬活性成分を含有し、(b)アルキルポリグリコシドを水面拡展剤として使用することで前記の課題を解決し得ることを見出し、本発明の農薬粒状組成物を得るに至った。 The present inventors conducted extensive research to solve these problems. As a result, it was found that the above-mentioned problems could be solved by (a) containing an agrochemical active ingredient and (b) using an alkyl polyglycoside as a water surface extender, and in order to obtain the agrochemical granular composition of the present invention. It's arrived.
すなわち本発明は、次の〔1〕~〔5〕の通りである。
〔1〕(a)農薬活性成分及び、水面拡展剤として(b)アルキルポリグリコシドを含有することを特徴とする農業用水面施用粒状組成物。
That is, the present invention is as follows [1] to [5].
[1] A granular composition for agricultural water surface application, characterized by containing (a) an agrochemical active ingredient and (b) an alkyl polyglycoside as a water surface spreader.
〔2〕(a)農薬活性成分が除草活性成分である〔1〕に記載の農業用水面施用粒状組成物。 [2] (a) The granular composition for agricultural water surface application according to [1], wherein the agrochemical active ingredient is a herbicidal active ingredient.
〔3〕(a)除草活性成分がピラゾリルピラゾール誘導体及び/又はスルホニルウレア系除草活性成分及び/又はトリケトン系除草活性成分である〔2〕に記載の農業用水面施用粒状組成物。 [3] The granular composition for agricultural water surface application according to [2], wherein the herbicidal active ingredient (a) is a pyrazolyl pyrazole derivative and/or a sulfonylurea herbicidal active ingredient and/or a triketone herbicidal active ingredient.
〔4〕(b)アルキルポリグリコシドが0.1~20重量部である〔1〕~〔3〕に記載の農業用水面施用粒状組成物。 [4] The granular composition for agricultural water surface application according to [1] to [3], wherein the alkyl polyglycoside (b) is 0.1 to 20 parts by weight.
〔5〕(b)アルキルポリグリコシドが3~5重量部である〔4〕に記載の農業用水面施用粒状組成物。 [5] The granular composition for agricultural water surface application according to [4], wherein (b) the alkyl polyglycoside is 3 to 5 parts by weight.
本発明に用いられる農薬活性成分は、有害生物を防除する効果を有するものであればよく、例えば、除草活性成分、殺虫活性成分、殺菌活性成分等を挙げることができる。本発明の粒状組成物は、これらの一種または農薬活性成分の種類を超えて二種以上の農薬活性成分を含有することができる。以下に本発明に用いられる農薬活性成分を具体的に例示するが、これらに限定されるものではない。 The agrochemical active ingredient used in the present invention may be anything as long as it has the effect of controlling harmful organisms, and examples thereof include herbicidal active ingredients, insecticidal active ingredients, fungicidal active ingredients, and the like. The granular composition of the present invention may contain one or more types of agrochemical active ingredients. Specific examples of agricultural chemical active ingredients used in the present invention are shown below, but the invention is not limited thereto.
[除草活性成分]
3-{(イソプロピルスルホニル)メチル}-N-(5-メチル-1,3,4-オキサジアゾール-2-イル)-5-(トリフルオロメチル)-[1,2,4]トリアゾロ[4,3-a]ピリジン-8-カルボキサミド、アクロニフェン、アクロレイン、アザフェニジン、アシフルオルフェン、アジムスルフロン、アシュラム、アセトクロ-ル、アトラジン、アニロホス、アミカルバゾン、アミドスルフロン、アミトロール、アミノシクロピラクロル、アミノピラリド、アミプロホス・メチル、アメトリン、アラクロール、アロキシジム、イソウロン、イソキサクロルトール、イソキサフルトール、イソキサベン、イソプロツロン、イプフェンカルバゾン、イマザキン、イマザピク、イマザピル、イマザメタベンズ・メチル、イマザモックス、イマゾスルフロン、イマゼタピル、インダジフラム、インダノファン、エグリナジン・エチル、エスプロカルブ、エタメトスルフロン・メチル、エタルフルラリン、エチジムロン、エトキシスルフロン、エトキシフェン・エチル、エトフメセート、エトベンザニド、エピリフェナシル、エンドタール二ナトリウム塩、オキサジアゾン、オキサジアルギル、オキサジクロメホン、オキサスルフロン、オキシフルオルフェン、オリザリン、オルトスルファムロン、オルベンカルブ、カフェンストロール、カルフェントラゾン・エチル、カルブチレート、カルベタミド、キザロホップ・エチル、キザロホップ・P・エチル、キザロホップ・P・テフリル、キノクラミン、キンクロラック、キンメラック、クミルロン、クラシホス、グリホサート、グルホシネート、グルホシネート・P・ナトリウム塩、クレトジム、クロジナホップ・プロパルギル、クロピラリド、クロマゾン、クロメトキシフェン、クロメプロップ、クロランスラム・メチル、クロランベン、クロリダゾン、クロリムロン・エチル、クロルスルフロン、クロルタル・ジメチル、クロルチアミド、クロルフタリム、クロルフルレノール・メチル、クロルプロファム、クロルブロムロン、クロロクスロン、クロロトルロン、サフルフェナシル、シアナジン、シアナミド、ジウロン、ジエタチル・エチル、ジオキソピリトリオン、ジカンバ、シクロエート、シクロキシジム、ジクロスラム、シクロスルファムロン、シクロピラニル、シクロピリモレート、ジクロベニル、ジクロホップ・P・メチル、ジクロホップ・メチル、ジクロルプロップ、ジクロルプロップ-P、ジクワット、ジチオピル、シデュロン、ジニトラミン、シニドン・エチル、シノスルフロン、ジノテルブ、シハロホップ・ブチル、シピラスルオン、ジフェナミド、ジフェンゾコート、ジフルフェニカン、ジフルフェンゾピル、シマジン、ジメスルファゼット、ジメタクロール、ジメタメトリン、ジメテナミド、ジメテナミド・P、シメトリン、ジメピペレート、ジメフロン、シンメチリン、スエップ、スルコトリオン、スルフェントラゾン、スルホスルフロン、セトキシジム、ターバシル、ダイムロン、ダラポン、チアゾピル、チアフェナシル、チエンカルバゾン、チオカルバジル、チオベンカルブ、チジアジミン、チフェンスルフロン・メチル、デスメディファム、デスメトリン、テトフルピロリメト、テニルクロール、テブタム、テブチウロン、テプラロキシジム、テフリルトリオン、テルブチラジン、テルブトリン、テルブメトン、テンボトリオン、トプラメゾン、トラルコキシジム、トリアジフラム、トリアスルフロン、トリアファモン、トリアレート、トリエタジン、トリクロピル、トリクロピル-ブトティル、トリトスルフロン、トリピラスルホン、トリフルジムオキサジン、トリフルスルフロン・メチル、トリフルラリン、トリフロキシスルフロン、トリベニュロン・メチル、トルピラレート、ナプタラム、ナプロアニリド、ナプロパミド、ナプロパミド-M、ニコスルフロン、ネブロン、ノルフルラゾン、バーナレート、パラコート、ハルキシフェン-メチル、ハロキシホップ、ハロキシホップ・P、ハロキシホップ-エトティル、ハロスルフロン・メチル、ビクスロゾン、ピクロラム、ピコリナフェン、ビシクロピロン、ビスピリバック・ナトリウム塩、ピノキサデン、ビピラゾン、ビフェノックス、ピペロホス、ピラクロニル、ピラゾキシフェン、ピラゾスルフロン・エチル、ピラゾリネート、ビラナホス、ピラフルフェン・エチル、ピリダフォル、ピリチオバック・ナトリウム塩、ピリデート、ピリフタリド、ピリブチカルブ、ピリベンゾキシム、ピリミスルファン、ピリミノバック・メチル、ピロキサスルホン、ピロクススラム、フェニソファム、フェニュロン、フェノキサスルホン、フェノキサプロップ・P・エチル、フェンキノトリオン、フェンチアプロップ・エチル、フェントラザミド、フェンピラゾン、フェンメディファム、フォーラムスルフ
ロン、ブタクロール、ブタフェナシル、ブタミホス、ブチレート、ブテナクロール、ブトラリン、ブトロキシジム、フラザスルフロン、フラムプロップ、フラムプロップ・M、プリミスルフロン・メチル、フルアジホップ・ブチル、フルアジホップ・P・ブチル、フルアゾレート、フルオメツロン、フルオログリコフェン・エチル、フルカルバゾン・ナトリウム塩、フルクロラリン、フルセトスルフロン、フルチアセット・メチル、フルピリスルフロン・メチル、フルフェナセット、フルフェンピル・エチル、フルプロパネート、フルポキサム、フルミオキサジン、フルミクロラック・ペンチル、フルメツラム、フルリドン、フルルタモン、フルロキシピル、フルロクロリドン、プレチラクロール、プロカルバゾン・ナトリウム塩、プロジアミン、プロスルフロン、プロスルホカルブ、プロパキザホップ、プロパクロール、プロパジン、プロパニル、プロピザミド、プロピソクロール、プロピリスルフロン、プロファム、プロフルアゾール、プロポキシカルバゾン・ナトリウム塩、プロホキシジム、ブロマシル、ブロムピラゾン、プロメトリン、プロメトン、ブロモキシニル、ブロモフェノキシム、ブロモブチド、フロラスラム、フロルピラウキシフェンベンジル、ペトキサミド、ベナゾリン、ペノキススラム、ヘプタマロキシログルカン、ベフルブタミド、ベフルブタミド・M、ペブレート、ベンカルバゾン、ベンキトリオン、ペンジメタリン、ベンズフェンジゾン、ベンスリド、ベンスルフロン・メチル、ベンゾビシクロン、ベンゾフェナップ、ベンタゾン、ペンタノクロール、ペントキサゾン、ベンフルラリン、ベンフレセート、ホサミン、ホメサフェン、メコプロップ、メコプロップ・P・カリウム塩、メソスルフロン・メチル、メソトリオン、メタザクロール、メタゾスルフロン、メタベンズチアズロン、メタミトロン、メタミホップ、メチオゾリン、メチルダイムロン、メトキスロン、メトスラム、メトスルフロン・メチル、メトブロムロン、メトベンズロン、メトラクロール、メトリブジン、メフェナセット、モノスルフロン、モノスルフロン・メチル、モノリニュロン、モリネート、ヨードスルフロン・メチル、ラクトフェン、ランコトリオン・ナトリウム塩、リニュロン、リミソキサフェン、リムスルフロン、レナシル。
上記のうち好ましくはピラゾリルピラゾール誘導体、スルホニルウレア系及びトリケトン系除草活性成分であり、具体的には、ピラゾリルピラゾール誘導体として例えばピラクロニル、シクロピラニル、スルホニルウレア系除草活性成分として例えばアジムスルフロン、アミドスルフロン、イマゾスルフロン、エタメトスルフロンメチル、エトキシスルフロン、オキサスルフロン、オルトスルファムロン、クロリムロンエチル、クロルスルフロン、シクロスルファムロン、シノスルフロン、スルホスルフロン、チフェンスルフロンメチル、トリアスルフロン、トリトスルフロン、トリフルスルフロンメチル、トリフロキシスルフロン、トリベヌロンメチル、ニコスルフロン、ハロスルフロンメチル、ピラゾスルフロンエチル、フォーラムスルフロン、フラザスルフロン、プリミスルフロンメチル、フルセトスルフロン、フルピルスルフロンメチル、プロスルフロン、プロピリスルフロン、ベンスルフロンメチル、メソスルフロンメチル、メタゾスルフロン、メトスルフロンメチル、モノスルフロン、モノスルフロンメチル、ヨードスルフロンメチル、リムスルフロン、トリケトン系除草活性成分として例えばジオキソピリトリオン、スルコトリオン、テフリルトリオン、テンボトリオン、フェンキノトリオン、ベンキトリオン、ベンゾビシクロン、メソトリオン、ランコトリオンナトリウム塩等が挙げられる。
[Herbicidal active ingredient]
3-{(isopropylsulfonyl)methyl}-N-(5-methyl-1,3,4-oxadiazol-2-yl)-5-(trifluoromethyl)-[1,2,4]triazolo[4 , 3-a] Pyridine-8-carboxamide, aclonifen, acrolein, azafenidine, acifluorfen, azimsulfuron, Ashram, acetochlor, atrazine, anilophos, amicarbazone, amidosulfuron, amitrol, aminocyclopyrachlor, aminopyralid, amiprofos・Methyl, ametrine, alachlor, alloxydim, isouron, isoxachlortole, isoxaflutole, isoxaben, isoproturon, ipfencarbazone, imazaquin, imazapic, imazapyr, imazametabenz methyl, imazamox, imazosulfuron, imazethapyr, indaziflam, indanophane , eglinazine ethyl, esprocarb, etamethosulfuron methyl, etalfluralin, ethidimuron, ethoxysulfuron, ethoxyphen ethyl, ethofumesate, etobenzanide, epirifenacyl, endothal disodium salt, oxadiazone, oxadiargyl, oxadiclomefon, oxasulfuron, Oxyfluorfen, oryzalin, orthosulfamuron, orbencarb, cafenstrol, carfentrazone ethyl, carbutyrate, carbetamide, quizalofop ethyl, quizalofop P ethyl, quizalofop P tefuryl, quinocramine, quinclorac, quinmerac, cumiluron , Clacifos, glyphosate, glufosinate, glufosinate P sodium salt, clethodim, clodinafop propargyl, clopyralid, clomazone, clomethoxifen, clomeprop, chloranthula methyl, chloramben, chloridazone, chlorimuron ethyl, chlorsulfuron, chlortal dimethyl, Chlorthiamide, chlorphthalim, chlorflurenol methyl, chlorpropham, chlorbromulon, chloroxuron, chlorotoluron, saflufenacil, cyanazine, cyanamide, diuron, diethythyl ethyl, dioxopyritrone, dicamba, cycloate, cycloxydim, diclosulam, cyclosulfame Ron, cyclopyranyl, cyclopyrimoleate, dichlobenil, diclofop-P-methyl, diclofop-methyl, dichlorprop, dichlorprop-P, diquat, dithiopyr, ciduron, dinitramine, cinidon ethyl, sinosulfuron, dinoterb, cyhalofop butyl , cipirasluone, diphenamide, difenzocort, diflufenican, diflufenzopyr, simazine, dimesulfazet, dimethaclor, dimethamethrine, dimethenamide, dimethenamide P, simetrine, dimepiperate, dimefron, synmethyline, swep, sulcotrione, sulfentrazone, sulfonate Sulfuron, Setoxydim, Terbacil, Daimeron, Darapon, Thiazopyr, Thiafenacil, Thiencarbazone, Thiocarbasil, Thiobencarb, Thidiazimine, Thifensulfuron Methyl, Desmedipham, Desmetrin, Tetoflupyrrolimeth, Tenilchlor, Tebutam, Tebutiuron, Tepraloxydim, Tefuryltrione, terbuthylazine, terbutryn, terbumetone, tembotrione, topramezone, tralkoxydim, triaziflam, triasulfuron, triafamone, trialate, trietadine, triclopyr, triclopyr-butotyl, tritosulfuron, tripyrasulfone, trifluzimoxazine, triflusulfuron. Methyl, trifluralin, trifloxysulfuron, tribenuron methyl, tolpyrate, naptalam, naproanilide, napropamide, napropamide-M, nicosulfuron, neblon, norflurazone, vernalate, paraquat, haloxifene-methyl, haloxyfop, haloxyfop-P, haloxyfop- Ethotil, halosulfuron methyl, bixlozone, picloram, picolinafen, bicyclopyrone, bispyribac sodium salt, pinoxaden, bipyrazone, bifenox, piperofos, pyraclonil, pyrazoxifene, pyrazosulfuron ethyl, pyrazolinate, viranafos, pyraflufen ethyl, pyridafol, pyrithiobac sodium salt, pyridate, pyrifthalide, pyributicarb, pyribenzoxime, pyrimisulfan, pyriminobac methyl, pyroxasulfone, piroxsulam, fenisofam, fenuron, fenoxasulfone, fenoxaprop P-ethyl, fenquinotrione, fenthiaprop ethyl, Fentrazamide, fenpyrazone, phenmedipham, forumsulfuron, butachlor, butafenacil, butamifos, butyrate, butenachlor, butraline, butroxydim, flazasulfuron, flamprop, flamprop M, primisulfuron methyl, fluazifop butyl, fluazifop P-butyl, fluazolate, fluometuron, fluoroglycofen ethyl, flucarbazone sodium salt, fluchloralin, flucetosulfuron, fluthiacet methyl, flupyrisulfuron methyl, flufenacet, flufenpyr ethyl, flupropanate, flupoxam, flumioxazin, flumicolac pentyl, flumetulam, fluridone, flurutamon, fluroxypyr, flurochloridone, pretilachlor, procarbazone sodium salt, prodiamine, prosulfuron, prosulfocarb, propaquizafop, propachlor, propazine, propanil, propyzamide , propisochlor, propyrisulfuron, profam, profluazole, propoxycarbazone sodium salt, propoxydim, bromacil, brompyrazone, promethrin, promethone, bromoxynil, bromophenoxime, bromobutide, florasulam, florpyrauxifenbenzyl, petoxamide, Benazoline, Penoxsulam, Heptamaloxyloglucan, Beflubutamide, Beflubutamide M, Pebrate, Bencarbazone, Benchytrione, Pendimethalin, Benzfendizone, Bensuride, Bensulfuron Methyl, Benzobicicone, Benzofenap, Bentazone, Pentanochlor, Pentoxazone, benfluralin, benfuresate, fosamine, fomesafen, mecoprop, mecoprop P potassium salt, mesosulfuron methyl, mesotrione, metazachlor, metazosulfuron, metabenzthiazuron, metamitrone, metamifop, methiozoline, methyldimeron, metoxuron, metsulam, metsulfuron Methyl, metobromulon, metobenzuron, metolachlor, metribuzin, mefenacet, monosulfuron, monosulfuron methyl, monolinuron, molinate, iodosulfuron methyl, lactofen, lankotrione sodium salt, linuron, rimisoxafen, rimsulfuron, renacil.
Among the above, preferred are pyrazolyl pyrazole derivatives, sulfonylurea-based herbicidal active ingredients, and triketone-based herbicidal active ingredients. Specifically, pyrazolyl pyrazole derivatives such as pyraclonyl, cyclopyranyl, and sulfonylurea-based herbicidal active ingredients such as azimsulfuron, amidosulfuron, imazosulfuron, Etamethosulfuron methyl, ethoxysulfuron, oxasulfuron, orthosulfamuron, chlorimuron ethyl, chlorsulfuron, cyclosulfamuron, sinosulfuron, sulfosulfuron, thifensulfuron methyl, trisulfuron, tritosulfuron, triflusulfuron methyl, trifloxysulfuron, tribenuron methyl, nicosulfuron, halosulfuron methyl, pyrazosulfuron ethyl, forum sulfuron, flazasulfuron, primisulfuron methyl, flucetosulfuron, flupyrsulfuron methyl, Prosulfuron, propyrisulfuron, bensulfuron methyl, mesosulfuron methyl, metazosulfuron, metsulfuron methyl, monosulfuron, monosulfuron methyl, iodosulfuron methyl, rimsulfuron, triketone herbicidal active ingredients such as dioxopyritrione, sulcotrione, Examples include tefuryltrione, tembotrione, fenquinotrone, benchytrione, benzobiciclone, mesotrione, and lankotrione sodium salt.
[殺虫活性成分]
アクリナトリン、アザジラクチン、アザメチホス、アシノナピル、アジンホス・エチル、アジンホス・メチル、アセキノシル、アセタミプリド、アセトプロール、アセフェート、アゾシクロチン、アバメクチン、アフィドピロペン、アミドフルメット、アミトラズ、アラニカルブ、アルジカルブ、アルドキシカルブ、アレスリン、イサゾホス、イサミドホス、イソカルボホス、イソキサチオン、イソシクロセラム、イソフェンホス・メチル、イソプロカルブ、イベルメクチン、イミシアホス、イミダクロプリド、イミプロトリン、インドキサカルブ、エスフェンバレレート、エチオフェンカルブ、エチオン、エチプロール、エチレンジブロミド、エトキサゾール、エトフェンプロックス、エトプロホス、エトリ
ムホス、エマメクチンベンゾエート、エンドスルファン、エンペントリン、オキサゾスルフィル、オキサミル、オキシジメトン・メチル、オキシデプロホス、オメトエート、カズサホス、カッパ-テフルトリン、カッパ-ビフェントリン、カランジン、カルタップ、カルバリル、カルボスルファン、カルボフラン、ガンマ-BHC、キシリルカルブ、キナルホス、キノプレン、キノメチオネート、クマホス、クリオライト、クロチアニジン、クロフェンテジン、クロマフェノジド、クロラントラニリプロール、クロルエトキシホス、クロルデン、クロルピクリン、クロルピリホス、クロルピリホス・メチル、クロルフェナピル、クロルフェンビンホス、クロルフルアズロン、クロルメホス、シアノホス、ジアフェンチウロン、ジアミダホス、シアントラニリプロール、ジエノクロル、シエノピラフェン、ジオキサベンゾホス、ジオフェノラン、シクラニリプロール、ジクロトホス、ジクロフェンチオン、シクロプロトリン、ジクロルボス、ジクロロメゾチアッツ、1,3‐ジクロロプロペン、ジコホル、ジシクラニル、ジスルホトン、ジノテフラン、ジノブトン、シハロトリン、シフェノトリン、シフルトリン、ジフルベンズロン、シフルメトフェン、ジフロビダジン、シプロフラニリド、シヘキサチン、シペルメトリン、ジメチルビンホス、ジメフルスリン、ジメトエート、シラフルオフェン、シロマジン、ジンプロピリダズ、スピドキサマト、スピネトラム、スピノサド、スピロジクロフェン、スピロテトラマト、スピロメシフェン、スピロピジオン、スルコフロン・ナトリウム塩、スルフルラミド、スルホキサフロル、スルホテップ、ダイアジノン、チアクロプリド、チアメトキサム、チオキサザフェン、チオジカルブ、チオシクラム、チオスルタップ、チオナジン、チオファノックス、チオメトン、チクロピラゾフロル、テトラクロラントラニリプロール、テトラクロルビンホス、テトラジホン、テトラニリプロール、テトラメチルフルスリン、テトラメトリン、テブピリムホス、テブフェノジド、テブフェンピラド、テフルトリン、テフルベンズロン、デメトン・S・メチル、テメホス、デルタメトリン、テルブホス、トラロメトリン、トランスフルトリン、トリアザメート、トリアゾホス、トリクロルホン、トリフルムロン、トリフルメゾピリム、トリメタカルブ、トルフェンピラド、ナレッド、ニコフルプロール、ニテンピラム、ノバルロン、ノビフルムロン、バーティシリウム レカニ、ハイドロプレン、パスツーリアペネトランス胞子、バミドチオン、パラチオン、パラチオン・メチル、ハルフェンプロックス、ハロフェノジド、ビオアレスリン、ビオアレスリンS-シクロペンテニル、ビオレスメトリン、ビストリフルロン、ヒドラメチルノン、ビフェナゼート、ビフェントリン、ピフルブミド、ピペロニルブトキシド、ピメトロジン、ピラクロホス、ピラフルプロール、ピリダフェンチオン、ピリダベン、ピリダリル、ピリフルキナゾン、ピリプロール、ピリプロキシフェン、ピリミカルブ、ピリミジフェン、ピリミノストロビン、ピリミホス・メチル、ピレトリン、ファムフル、フィプロニル、フェナザキン、フェナミホス、フェニトロチオン、フェノキシカルブ、フェノチオカルブ、フェノトリン、フェノブカルブ、フェンチオン、フェントエート、フェンバレレート、フェンピロキシメート、フェンブタンチン・オキシド、フェンプロパトリン、フォノホス、フッ化スルフリル、ブトカルボキシム、ブトキシカルボキシム、ブプロフェジン、フラチオカルブ、プラレトリン、フルアクリピリム、フルアズロン、フルエンスルホン、フルオロ酢酸ナトリウム塩、フルシクロクスロン、フルシトリネート、フルスルファミド、フルバリネート、フルピラジフロン、フルピラゾホス、フルピリミン、フルフィプロール、フルフェネリム、フルフェノキシストロビン、フルフェノクスロン、フルヘキサフォン、フルベンジアミド、フルペンチオフェノックス、フルメトリン、プロトリフェンブト、プロチオホス、フロニカミド、プロパホス、プロパルギット、プロフェノホス、ブロフラニリド、プロフルトリン、プロペタムホス、プロポキスル、フロメトキン、ブロモプロピレート、ヘキサチアゾクス、ヘキサフルムロン、ペキロマイセス・テヌイペス、ペキロマイセス・フモソロセウス、ヘプタフルスリン、ヘプテノホス、ペルメトリン、ベンクロチアズ、ベンズピリモキサン、ベンスルタップ、ベンゾキシメート、ベンダイオカルブ、ベンフラカルブ、ボーベリア・テネーラ、ボーベリア・バッシアーナ、ボーベリア・ブロンニアティ、ホキシム、ホサロン、ホスチアゼート、ホスチエタン、ホスファミドン、ホスメット、ポリナクチン複合体、ホルメタネート、ホレート、マラチオン、ミルベメクチン、メカルバム、
メスルフェンホス、メソプレン、メソミル、メタフルミゾン、メタミドホス、メタム、メチオカルブ、メチダチオン、メチルイソチオシアネート、メチルブロマイド、メトキシクロル、メトキシフェノジド、メトトリン、メトフルトリン、メトプレン、メトルカルブ、メビンホス、メペルフルスリン、モナクロスポリウム・フィマトパガム、モノクロトホス、モムフルオロスリン、リトルアA、リトルアB、リン化アルミニウム、リン化亜鉛、リン化水素、ルフェヌロン、レスカルレ、レスメトリン、レピメクチン、ロテノン、酸化フェンブタスズ、石灰窒素、硫酸ニコチン、(Z)-11-テトラデセニル=アセタート、(Z)-11-ヘキサデセナール、(Z)-11-ヘキサデセニル=アセタート、(Z)-9,12-テトラデカジエニル=アセタート、(Z)-9-テトラデセン-1-オール、(Z,E)-9,11-テトラデカジエニル=アセタート、(Z,E)-9,12-テトラデカジエニル=アセタート、バシルス・ポピリエ、バシルス・ズブチリス、バシルス・スフェリカス、バシルス・チューリンゲンシス・亜種・アイザワイ、バシルス・チューリンゲンシス・亜種・イスラエレンシス、バシルス・チューリンゲンシス・亜種・クルスターキ、バシルス・チューリンゲンシス・亜種・テネブリオニス、DCIP(ビス‐(2-クロロ‐1-メチルエチル)エーテル)、DDT(1,1,1-トリクロロ‐2,2-ビス(4-クロロフェニル)エタン)、DEP(ジメチル-2,2,2-トリクロロ‐1-ヒドロキシエチルホスホネート)、DNOC(4,6-ジニトロ-o-クレゾール)、DSP(O,O-ジエチル-O-[4-(ジメチルスルファモイル)フェニル]-ホスホロチオネート)、EPN(O-エチル-O-4-(ニトロフェニル)フェニルホスホノチオエート)、核多角体病ウイルス包埋体。
[Insecticidal active ingredient]
Acrinathrine, azadirachtin, azamethyphos, acinonapyr, azinphos ethyl, azinphos methyl, acequinocyl, acetamiprid, acetoprol, acephate, azocyclotine, abamectin, afidopyropene, amidoflumet, amitraz, aranicarb, aldicarb, aldoxycarb, allethrin, isazofos, isamidophos, isocarbofos, isoxathion, isocycloceram, isofenphos methyl, isoprocarb, ivermectin, imisiafos, imidacloprid, imiprothrin, indoxacarb, efenvalerate, ethiofencarb, ethion, ethiprole, ethylene dibromide, etoxazole, etofenprox, ethoprofos, etrimfos, Emamectin benzoate, endosulfan, empenthrin, oxazosulfil, oxamyl, oxydimeton methyl, oxydeprofos, omethoate, cassafos, kappa-tefluthrin, kappa-bifenthrin, calandin, cartap, carbaryl, carbosulfan, carbofuran, gamma-BHC , xylylcarb, quinalphos, quinoprene, quinomethionate, coumafos, cryolite, clothianidin, clofentedine, chromafenozide, chlorantraniliprole, chlorethoxyphos, chlordane, chlorpicrin, chlorpyrifos, chlorpyrifos methyl, chlorfenapyr, chlorfenvinphos, chlor fluazuron, chlormephos, cyanophos, diafenthiuron, diamidaphos, cyantraniliprole, dienochlor, cyenopyrafen, dioxabenzophos, diphenolan, cyclaniliprole, dicrotophos, diclofenthione, cycloprothrin, dichlorvos, dichloromesothiaz , 1,3-dichloropropene, dicofol, dicyclanil, disulfoton, dinotefuran, dibutone, cyhalothrin, cyphenothrin, cyfluthrin, diflubenzuron, cyflumetofen, diflobidazine, ciprofuranilide, cyhexatin, cypermethrin, dimethylvinphos, dimefluthrin, dimethoate, silafluofen, cyromazine, Zinpropyridaz, spidoxamato, spinetoram, spinosad, spirodiclofen, spirotetramat, spiromesifen, spiropidione, sulcofuron sodium salt, sulfuramide, sulfoxaflor, sulfotep, diazinon, thiacloprid, thiamethoxam, thioxazafene, thiodicarb, thiocyclam, thiosultap, thionazine, thio Fanox, Thiometone, Ticlopyrazoflor, Tetrachlorantraniliprole, Tetrachlorvinphos, Tetradifon, Tetraniliprole, Tetramethylfluthrin, Tetramethrin, Tebupirimphos, Tebufenozide, Tebufenpyrad, Tefluthrin, Teflubenzuron, Demeton S. Methyl , temefos, deltamethrin, terbufos, tralomethrin, transfluthrin, triazamate, triazophos, trichlorfon, triflumuron, triflumezopyrim, trimetacarb, tolfenpyrad, naled, nicofluprole, nitenpyram, novaluron, noviflumuron, verticillium lecani, hydroprene, pas Turiapenetrans spores, vamidothion, parathion, parathion methyl, halfenprox, halofenozide, bioallethrin, bioallethrin S-cyclopentenyl, bioresmethrin, bistrifluron, hydramethylnon, bifenazate, bifenthrin, pyflubumide, piperonyl butoxide, pymetrozine, Pyraclofos, pyrafluprole, pyridafenthione, pyridaben, pyridalyl, pyrifluquinazone, pyriprole, pyriproxyfen, pirimicarb, pyrimidifen, pyriminostrobin, pirimiphos methyl, pyrethrin, famflu, fipronil, fenazaquin, fenamiphos, fenitrothion, phenoxycarb, phenothiocarb, Phenothrin, fenobucarb, fenthion, fentoate, fenvalerate, fenpyroximate, fenbutantine oxide, fenpropathrin, phonophos, sulfuryl fluoride, butocarboxime, butoxycarboxime, buprofezin, furathiocarb, pralethrin, fluacrypyrim, fluazuron, fluensulfone, Fluoroacetic acid sodium salt, flucycloxuron, flucitrinate, flusulfamide, fluvalinate, flupyradifurone, flupyrazophos, flupyrimine, flufiprole, flufenerim, flufenoxystrobin, flufenoxuron, fluhexaphone, flubendiamide, flupenthiopher Nox, Flumethrin, Protrifenbut, Prothiofos, Flonicamid, Propafos, Propargite, Profenofos, Broflanilide, Profluthrin, Propetamfos, Propoxur, Flometoquine, Bromopropylate, Hexathiazox, Hexaflumuron, Pechiromyces tenuipes, Pechiromyces fumosoroseus, Heptafluthrin , heptenophos, permethrin, bencrothiaz, benzpyrimoxane, bensultap, benzoximate, bendiocarb, benfuracarb, Beauveria tenera, Beauveria bassiana, Beauveria bronniati, Phoxim, Phosaron, Fosthiazate, Fosthiethane, Phosphamidon, Phosmet, Polynactin complex body, formanate, phorate, malathion, milbemectin, mecarbam,
Mesulfenphos, methoprene, methomyl, metaflumizone, methamidophos, metam, methiocarb, methidathion, methyl isothiocyanate, methyl bromide, methoxychlor, methoxyfenozide, methotrine, metofluthrin, methoprene, metolcarb, mevinfos, meperfluthrin, Monacrosporium phymatopagam, monocrotophos, momfluoro Surin, Littleua A, Littleua B, aluminum phosphide, zinc phosphide, hydrogen phosphide, lufenuron, rescalle, resmethrin, lepimectin, rotenone, fenbutastin oxide, lime nitrogen, nicotine sulfate, (Z)-11-tetradecenyl acetate, ( Z)-11-hexadecenal, (Z)-11-hexadecenyl acetate, (Z)-9,12-tetradecadienyl acetate, (Z)-9-tetradecen-1-ol, (Z,E)- 9,11-tetradecadienyl acetate, (Z,E)-9,12-tetradecadienyl acetate, Bacillus popilliae, Bacillus subtilis, Bacillus sphaericus, Bacillus thuringiensis subsp. aizawai, Bacillus thuringiensis subsp. israelensis, Bacillus thuringiensis subsp. kurstaki, Bacillus thuringiensis subsp. tenebrionis, DCIP (bis-(2-chloro-1-methylethyl) ether), DDT (1,1,1-trichloro-2,2-bis(4-chlorophenyl)ethane), DEP (dimethyl-2,2,2-trichloro-1-hydroxyethylphosphonate), DNOC (4,6-dinitro-o -cresol), DSP (O,O-diethyl-O-[4-(dimethylsulfamoyl)phenyl]-phosphorothioate), EPN (O-ethyl-O-4-(nitrophenyl)phenylphosphonothioate) ), nuclear polyhedrosis virus-embedded body.
[殺菌活性成分]
アザコナゾール、アシベンゾラル・S・メチル、アゾキシストロビン、アニラジン、アミスルブロム、アミノピリフェン、アメトクトラジン、アルジモルフ、イソチアニル、イソピラザム、イソフェタミド、イソフルシプラム、イソプロチオラン、イプコナゾール、イプフルフェノキン、イプロジオン、イプロバリカルブ、イプロベンホス、イマザリル、イミノクタジンアルベシル酸塩、イミノクタジン酢酸塩、イミベンコナゾール、インピルフルキサム、エジフェンホス、エタコナゾ-ル、エタボキサム、エチリモル、エトキシキン、エトリジアゾール、エネストロブリン、エノキサストロビン、エポキシコナゾール、オーガニックオイル、オキサジキシル、オキサジニラゾール、オキサチアピプロリ、オキシカルボキシン、オキシキノリン銅、オキシテトラサイクリン、オキスポコナゾールフマル酸塩、オキソリニック酸、オクタン酸銅、オクチリノン、オフラセ、オリサストロビン、オルソフェニルフェノール、カスガマイシン、カプタホール、カルプロパミド、カルベンダジム、カルボキシン、カルボネ、キノキシフェン、キノメチオネート、キャプタン、キンコナゾール、キントゼン、グアザチン、クフラネブ、クモキシストロビン、クレソキシム・メチル、クロジラコン、クロゾリネート、クロロインコナジド、クロロタロニル、クロロネブ、シアゾファミド、ジエトフェンカルブ、ジクロシメット、ジクロフルアニド、ジクロメジン、ジクロラン、ジクロロフェン、ジチアノン、ジニコナゾール、ジニコナゾール・M、ジネブ、ジノカップ、ジピメチトロン、ジフェニルアミン、ジフェノコナゾール、シフルフェナミド、ジフルメトリム、シプロコナゾール、シプロジニル、シメコナゾール、ジメチリモル、ジメチルジスルフィド、ジメトモルフ、シモキサニル、ジモキシストロビン、ジラム、シルチオファム、ストレプトマイシン、スピロキサミン、セダキサン、ゾキサミド、ダゾメット、チアジニル、チアベンダゾール、チウラム、チオファネート、チオファネート・メチル、チフルザミド、テクナゼン、テクロフタラム、テトラコナゾール、デバカルブ、テブコナゾール、テブフロキン、テルビナフィン、ドジン、ドデモルフ、トリアジメノール、トリアジメホン、トリアゾキシド、トリクラミド、トリクロピリカルブ、トリシクラゾール、トリチコナゾール、トリデモルフ、トリフルミゾール、トリフロキシストロビン、トリホリン、トリルフルアニド、トルクロホス・メチル、トルニファニド、トルプロカルブ、ナーバム、ナタマイシン、ナフティフィン、ニトラピリン、ニトロタル・イソプロピル、ヌアリモル、ノニルフェノールスルホン酸銅、バチルス・ズ
ブチリス、バリダマイシン、バリフェナレート、ピカルブトラゾックス、ビキサフェン、ピコキシストロビン、ビテルタノール、ビナパクリル、ビフェニル、ピペラリン、ヒメキサゾール、ピラオキシストロビン、ピラクロストロビン、ピラジフルミド、ピラゾホス、ピラプロポイン、ピラメトストロビン、ピリオフェノン、ピリソキサゾール、ピリダクロメチル、ピリフェノックス、ピリブチカルブ、ピリメタニル、ピロキロン、ビンクロゾリン、ファーバム、ファモキサドン、フェナジンオキシド、フェナミドン、フェナミンストロビン、フェナリモル、フェノキサニル、フェリムゾン、フェンピクロニル、フェンピラザミン、フェンブコナゾール、フェンフラム、フェンプロピジン、フェンプロピモルフ、フェンヘキサミド、フォルペット、フサライド、ブピリメート、フベリダゾール、ブラストサイジン-S、フラメトピル、フララキシル、フランカルボン酸、フルアジナム、フルインダピル、フルオキサストロビン、フルオキサピプロリン、フルオキシチオコナゾール、フルオピコリド、フルオピモミド、フルオピラム、フルオルイミド、フルキサピロキサド、フルキンコナゾール、フルコナゾール、フルコナゾール・シス、フルジオキソニル、フルシラゾール、フルスルファミド、フルチアニル、フルトラニル、フルトリアホール、フルフェノキサジアザム、フルフェノキシストロビン、フルベネテラム、フルメトベル、フルモルフ、プロキナジド、プロクロラズ、プロシミドン、プロチオカルブ、プロチオコナゾール、ブロノポール、プロパモカルブ塩酸塩、プロピコナゾール、プロピネブ、プロベナゾール、ブロムコナゾール、フロリルピコキサミド、ヘキサコナゾール、ベナラキシル、ベナラキシル・M、ベノダニル、ベノミル、ペフラゾエート、ペンコナゾール、ペンシクロン、ベンゾビンジフルピル、ベンチアゾール、ベンチアバリカルブ・イソプロピル、ペンチオピラド、ペンフルフェン、ボスカリド、ホセチル、ポリオキシン、ポリカーバメート、ボルドー液、マンコゼブ、マンジプロパミド、マンデストロビン、マンネブ、ミクロブタニル、ミネラルオイル、ミルディオマイシン、メタスルホカルブ、メタム、メタラキシル、メタラキシル・M、メタリルピコキサミド、メチラム、メチルテトラプロール、メトコナゾール、メトミノストロビン、メトラフェノン、メパニピリム、メプチルジノカップ、メプロニル、ヨードカルブ、ラミナリン、亜リン酸および塩、塩基性塩化銅、銀、酸化第一銅、水酸化第二銅、炭酸水素カリウム、炭酸水素ナトリウム、硫黄、硫酸オキシキノリン、硫酸銅。
[Bactericidal active ingredient]
Azaconazole, acibenzolar S. methyl, azoxystrobin, anilazine, amisulbrome, aminopyrifene, ametoctrazine, aldimorph, isotianil, isopyrazam, isofetamide, isoflucipram, isoprothiolane, ipconazole, ipflufenoquine, iprodione, iprovaricarb, iprobenfos, Imazalil, iminoctadine albesylate, iminoctadine acetate, imibenconazole, impirfluxam, edifenphos, etaconazole, ethaboxam, ethyrimol, ethoxyquin, etridiazole, enestrobulin, enoxastrobin, epoxiconazole, organic oil, Oxadixyl, oxazinirazole, oxathiapiproli, oxycarboxine, copper oxyquinoline, oxytetracycline, oxpoconazole fumarate, oxolinic acid, copper octoate, octylinone, ofrace, orysastrobin, orthophenylphenol, kasugamycin, captafol, carpropamide, carbendazim, carboxin, carbonone, quinoxyphene, quinomethionate, captan, quinconazole, quintozene, guazatine, cufraneb, cumoxystrobin, cresoxime methyl, cloziracone, clozolinate, chloroinconazide, chlorothalonil, chloroneb, cyazofamid, Dietofencarb, diclocymet, dichlofluanid, diclomedine, dichlorane, dichlorophene, dithianone, diniconazole, diniconazole M, zineb, dinocap, dipimethitron, diphenylamine, difenoconazole, cyflufenamide, diflumetrim, cyproconazole, cyprodinil, simeconazole, dimethylimole, dimethyl disulfide, Dimethomorph, cymoxanil, dimoxystrobin, ziram, silthiopham, streptomycin, spiroxamine, sedaxane, zoxamide, dazomet, thiazinil, thiabendazole, thiuram, thiophanate, thiophanate methyl, thifluzamide, tecnazen, tecloftalam, tetraconazole, debacarb, tebuconazole, tebufloquine , terbinafine, dodine, dodemorph, triadimenol, triadimefon, triazoxide, triclamide, triclopiricarb, tricyclazole, triticonazole, tridemorph, triflumizole, trifloxystrobin, triforine, tolylfluanid, tolclofos methyl, tolnifanide, tolprocarb, nabam, natamycin, naftifine, nitrapyrin, nitrotal isopropyl, nuarimol, copper nonylphenol sulfonate, Bacillus subtilis, validamycin, variphenarate, picarbutrazox, bixaphene, picoxystrobin, bitertanol, binapacryl, biphenyl, piperaline, hymexazole, pyraoxystrobin, pyraclostrobin, pyradiflumide, pyrazophos, pyrapropoine, pyramethostrobin, piriophenone, pyrisoxazole, pyridacromethyl, pyrifenox, pyributicarb, pyrimethanil, pyroquilone, vinclozolin, furbam, famoxadone, phenazine oxide, Fenamidone, phenaminestrobin, fenarimol, fenoxanil, felimzone, fenpiclonil, fenpyrazamine, fenbuconazole, fenflam, fenpropidine, fenpropimorph, fenhexamide, folpet, fusaride, bupirimate, fuberidazole, blasticidin-S, flametopyr , furalaxyl, furocarboxylic acid, fluazinam, fluindapyr, fluoxastrobin, fluoxapiproline, fluoxythioconazole, fluopicolide, fluopimomide, fluopyram, fluorimide, fluxapiroxad, fluquinconazole, fluconazole, fluconazole cis, fludioxonil, flusilazole, flusulfamide, flutianil, flutolanil, flutriafor, flufenoxadiazam, flufenoxystrobin, fluveneteram, flumethover, flumorph, proquinazide, prochloraz, procymidone, prothiocarb, prothioconazole, bronopol, propamocarb hydrochloride, propico Nazole, propineb, probenazole, bromconazole, florylpicoxamide, hexaconazole, benalaxyl, benalaxyl M, benodanil, benomyl, pefurazoate, penconazole, pencycurone, benzobine diflupyr, bentiazole, bentiavaricarb isopropyl , penthiopyrad, penflufen, boscalid, fosetyl, polyoxine, polycarbamate, Bordeaux liquid, mancozeb, mandipropamide, mandestrobin, maneb, myclobutanil, mineral oil, mildiomycin, methasulfocarb, metham, metalaxyl, metalaxyl M, methallylpico Xamide, Methiram, Methyltetraprole, Metconazole, Metominostrobin, Metraphenone, Mepanipirim, Meptyldinocap, Mepronil, Iodocarb, Laminarin, Phosphite and Salts, Basic Copper Chloride, Silver, Cuprous Oxide, Hydroxide Cupric, potassium bicarbonate, sodium bicarbonate, sulfur, oxyquinoline sulfate, copper sulfate.
本発明に用いられるアルキルポリグリコシドは、具体的には、例えば、いずれも商品名として、ニューカルゲン4000-G(竹本油脂製)、マイドール10(花王製)、マイドール12(花王製)、AG6202(ライオンアグゾ製)、アグニークPG8105(コグニス製)、アグニークPG8107-G(コグニス製)、アグニークPG264-G(コグニス製)などが挙げられる。 Specifically, the alkyl polyglycosides used in the present invention include, for example, New Calgen 4000-G (manufactured by Takemoto Yushi), Mydol 10 (manufactured by Kao), Mydol 12 (manufactured by Kao), Examples include AG6202 (manufactured by Lion Agzo), Agnique PG8105 (manufactured by Cognis), Agnique PG8107-G (manufactured by Cognis), and Agnique PG264-G (manufactured by Cognis).
アルキルポリグリコシドの農薬組成物中の配合割合は適宜選択できるが、通常0.1から40重量部、好ましくは0.1から20重量部、さらに好ましくは3から5重量部である。 The proportion of the alkyl polyglycoside in the agrochemical composition can be selected as appropriate, but is usually 0.1 to 40 parts by weight, preferably 0.1 to 20 parts by weight, and more preferably 3 to 5 parts by weight.
本発明の組成物の見掛け比重は通常1未満、好ましくは0.01~0.8、さらに好ましくは0.1~0.6である。
なお見掛け比重については農薬公定法に則り試験を行った。以下に概要を示す。
1)内径50mmの100mlの金属製円筒容器の上に80メッシュの篩を置き、これに試料を入れ、刷毛で軽くはたき落として容器を満たす。
2)ただちにスライドグラスを用いて余剰分を擦り落し、内容物の重量(A)を精秤する。
3)内容物の重量(A)から次式より見掛け比重を算出する。
The apparent specific gravity of the composition of the present invention is usually less than 1, preferably from 0.01 to 0.8, more preferably from 0.1 to 0.6.
The apparent specific gravity was tested in accordance with the Official Agricultural Chemicals Law. An overview is shown below.
1) Place an 80 mesh sieve on top of a 100 ml metal cylindrical container with an inner diameter of 50 mm, pour the sample into the sieve, and gently brush it off with a brush to fill the container.
2) Immediately scrape off the excess using a slide glass and accurately weigh the contents (A).
3) Calculate the apparent specific gravity from the weight (A) of the contents using the following formula.
[数1]
見掛け比重=A(g)/100(ml)
[Number 1]
Apparent specific gravity = A (g) / 100 (ml)
本発明の組成物の粒度は通常0.5mm~3.0mmの範囲に80%以上であり、好ましくは0.5mm~1.7mmの範囲に80%以上である。
なお粒度については農薬公定法の則り試験を行った。以下に概要を示す。
1)篩の目開きの小から大の順に受け皿の上に積み重ね、その際上部の篩上に試料50gを入れ、蓋をする。
2)振とう回数250~300rpm、打数130~105tpmのロータップ型篩い分け器に取り付け、10分間篩い分けを行う。
3)それぞれの篩を離し、各篩に残留した試料の重量(B)を精秤し、次式より粒度分布の重量百分率を算出する。
The particle size of the composition of the present invention is usually 80% or more in the range of 0.5 mm to 3.0 mm, preferably 80% or more in the range of 0.5 mm to 1.7 mm.
The particle size was tested in accordance with the Official Pesticide Law. An overview is shown below.
1) Stack the sieves on a saucer in the order of their openings from small to large, then place 50 g of the sample on the top sieve and cover with a lid.
2) Attach to a low-tap type sieve with a shaking frequency of 250 to 300 rpm and a stroke number of 130 to 105 tpm, and sieve for 10 minutes.
3) Separate each sieve, accurately weigh the weight (B) of the sample remaining on each sieve, and calculate the weight percentage of the particle size distribution using the following formula.
[数2]
粒度(%)=B(g)/50(g)×100
[Number 2]
Particle size (%) = B (g) / 50 (g) x 100
また、本発明の組成物は、更に各種補助剤を含有させることができる。使用できる補助剤としては、界面活性剤、結合剤、酸および固体担体等があり、その例を以下に示すが、これらに限定されるものではない Moreover, the composition of the present invention can further contain various auxiliary agents. Examples of adjuvants that can be used include, but are not limited to, surfactants, binders, acids, and solid carriers.
界面活性剤としては、以下の(A)、(B)、(C)、(D)及び(E)が挙げられる。 Examples of the surfactant include the following (A), (B), (C), (D) and (E).
(A)ノニオン性界面活性剤:
(A‐1)ポリエチレングリコール型界面活性剤:例えば、ポリオキシエチレンアルキル(C8~18)エーテル、アルキルナフトールのエチレンオキサイド付加物、ポリオキシエチレン(モノまたはジ)アルキル(C8~12)フェニルエーテル、ポリオキシエチレン(モノまたはジ)アルキル(C8~12)フェニルエーテルのホルマリン縮合物、ポリオキシエチレン(モノ、ジまたはトリ)フェニルフェニルエーテル、ポリオキシエチレン(モノ、ジまたはトリ)ベンジルフェニルエーテル、ポリオキシプロピレン(モノ、ジまたはトリ)ベンジルフェニルエーテル、ポリオキシエチレン(モノ、ジまたはトリ)スチリルフェニルエーテル、ポリオキシプロピレン(モノ、ジまたはトリ)スチリルフェニルエーテル、ポリオキシエチレン(モノ、ジまたはトリ)スチリルフェニルエーテルのポリマー、アルキル(C8~18)ポリオキシエチレンポリオキシプロピレンブロックポリマーエーテル、アルキル(C8~12)フェニルポリオキシエチレンポリオキシプロピレンブロックポリマーエーテル、ポリオキシエチレンビスフェニルエーテル、ポリオキシエチレン樹脂酸エステル、ポリオキシエチレン脂肪酸(C8~18)モノエステル、ポリオキシエチレン脂肪酸(C8~18)ジエステル、ポリオキシエチレンソルビタン脂肪酸(C8~18)エステル、グリセロール脂肪酸エステルエチレンオキサイド付加物、ヒマシ油エチレンオキサイド付加物、硬化ヒマシ油エチレンオキサイド付加物、アルキル(C8~18)アミンエチレンオキサイド付加物および脂肪酸(C8~18)アミドエチレンオキサイド付加物等が挙げられる。
(A‐2)多価アルコール型界面活性剤:例えば、グリセロール脂肪酸エステル、ポリグリセリン脂肪酸エステル、ペンタエリスリトール脂肪酸エステル、ソルビトール脂肪酸(C8~18)エステル、ソルビタン脂肪酸(C8~18)エステル、ショ糖脂肪酸エステル、多価アルコールアルキルエーテル及び脂肪酸アルカノールアミド等が挙げられる。
(A) Nonionic surfactant:
(A-1) Polyethylene glycol type surfactant: For example, polyoxyethylene alkyl (C 8-18 ) ether, ethylene oxide adduct of alkylnaphthol, polyoxyethylene (mono- or di)alkyl (C 8-12 ) phenyl Ether, formalin condensate of polyoxyethylene (mono- or di-)alkyl (C 8-12 ) phenyl ether, polyoxyethylene (mono-, di- or tri) phenyl phenyl ether, polyoxyethylene (mono-, di- or tri) benzylphenyl Ether, polyoxypropylene (mono, di or tri)benzylphenyl ether, polyoxyethylene (mono, di or tri)styrylphenyl ether, polyoxypropylene (mono, di or tri)styrylphenyl ether, polyoxyethylene (mono, di or tri)styrylphenyl ether, Polymers of di- or tri)styrylphenyl ethers, alkyl (C 8-18 ) polyoxyethylene polyoxypropylene block polymer ethers, alkyl (C 8-12 ) phenyl polyoxyethylene polyoxypropylene block polymer ethers, polyoxyethylene bisphenyl Ether, polyoxyethylene resin acid ester, polyoxyethylene fatty acid (C 8-18 ) monoester, polyoxyethylene fatty acid (C 8-18 ) diester, polyoxyethylene sorbitan fatty acid (C 8-18 ) ester, glycerol fatty acid ester Examples include ethylene oxide adducts, castor oil ethylene oxide adducts, hydrogenated castor oil ethylene oxide adducts, alkyl (C 8-18 ) amine ethylene oxide adducts, and fatty acid (C 8-18 ) amide ethylene oxide adducts.
(A-2) Polyhydric alcohol type surfactant: For example, glycerol fatty acid ester, polyglycerin fatty acid ester, pentaerythritol fatty acid ester, sorbitol fatty acid (C 8-18 ) ester, sorbitan fatty acid (C 8-18 ) ester, Examples include sugar fatty acid esters, polyhydric alcohol alkyl ethers, and fatty acid alkanolamides.
(B)アニオン性界面活性剤:
(B‐1)カルボン酸型界面活性剤:例えば、ポリアクリル酸、ポリメタアクリル酸、ポリマレイン酸、ポリ無水マレイン酸、マレイン酸または無水マレイン酸とオレフィン(例えばイソブチレンおよびジイソブチレン等)との共重合物、アクリル酸とイタコン酸の共重合物、メタアクリル酸とイタコン酸の共重合物、マレイン酸または無水マレイン酸と
スチレンの共重合物、アクリル酸とメタアクリル酸の共重合物、アクリル酸とアクリル酸メチルエステルとの共重合物、アクリル酸と酢酸ビニルとの共重合物、アクリル酸とマレイン酸または無水マレイン酸の共重合物、N-メチル-脂肪酸(C8~18)サルコシネート、樹脂酸および脂肪酸(C8~18)等のカルボン酸、並びにそれらカルボン酸の塩が挙げられる。
(B‐2)硫酸エステル型界面活性剤:例えば、アルキル(C8~18)硫酸エステル、ポリオキシエチレンアルキル(C8~18)エーテル硫酸エステル、ポリオキシエチレン(モノまたはジ)アルキル(C8~12)フェニルエーテル硫酸エステル、ポリオキシエチレン(モノまたはジ)アルキル(C8~12)フェニルエーテルのポリマーの硫酸エステル、ポリオキシエチレン(モノ、ジまたはトリ)フェニルフェニルエーテル硫酸エステル、ポリオキシエチレン(モノ、ジまたはトリ)ベンジルフェニルエーテル硫酸エステル、ポリオキシエチレン(モノ、ジまたはトリ)スチリルフェニルエーテル硫酸エステル、ポリオキシエチレン(モノ、ジまたはトリ)スチリルフェニルエーテルのポリマーの硫酸エステル、ポリオキシエチレンポリオキシプロピレンブロックポリマーの硫酸エステル、硫酸化油、硫酸化脂肪酸エステル、硫酸化脂肪酸および硫酸化オレフィン等の硫酸エステル、並びにそれら硫酸エステルの塩が挙げられる。
(B‐3)スルホン酸型界面活性剤:例えば、リグニンスルホン酸、パラフィン(C8~22)スルホン酸、アルキル(C8~12)ベンゼンスルホン酸、アルキル(C8~12)ベンゼンスルホン酸のホルマリン縮合物、クレゾールスルホン酸のホルマリン縮合物、α-オレフィン(C8~16)スルホン酸、ポリオキシエチレン(モノまたはジ)アルキル(C8~12)フェニルエーテルスルホン酸、ナフタレンスルホン酸、(モノまたはジ)アルキル(C1~6)ナフタレンスルホン酸、ナフタレンスルホン酸のホルマリン縮合物、(モノまたはジ)アルキル(C1~6)ナフタレンスルホン酸のホルマリン縮合物、クレオソート油スルホン酸のホルマリン縮合物、アルキル(C8~12)ジフェニルエーテルジスルホン酸、イゲポンT(商品名)、ポリスチレンスルホン酸及びスチレンスルホン酸とメタアクリル酸の共重合物等のスルホン酸、並びにそれらスルホン酸の塩が挙げられる。
(B‐4)燐酸エステル型界面活性剤:例えば、アルキル(C8~12)燐酸エステ
ル、ポリオキシエチレンアルキル(C8~18)エーテル燐酸エステル、ポリオキシエチレン(モノまたはジ)アルキル(C8~12)フェニルエーテル燐酸エステル、ポリオキシエチレン(モノ、ジまたはトリ)アルキル(C8~12)フェニルエーテルのポリマーの燐酸エステル、ポリオキシエチレン(モノ、ジまたはトリ)フェニルフェニルエーテル燐酸エステル、ポリオキシエチレン(モノ、ジまたはトリ)ベンジルフェニルエーテル燐酸エステル、ポリオキシエチレン(モノ、ジまたはトリ)スチリルフェニルエーテル燐酸エステル、ポリオキシエチレン(モノ、ジまたはトリ)スチリルフェニルエーテルのポリマーの燐酸エステル、ポリオキシエチレンポリオキシプロピレンブロックポリマーの燐酸エステル、ホスファチジルコリン、ホスファチジルエタノールイミン及び縮合燐酸(例えばトリポリリン酸等)等の燐酸エステル、並びにそれら燐酸エステルの塩が挙げられる。
上記の(B‐1)~(B‐4)における塩としては、アルカリ金属(リチウム、ナトリウムおよびカリウム等)、アルカリ土類金属(カルシウムおよびマグネシウム等)、アンモニウムおよび各種アミン(例えばアルキルアミン、シクロアルキルアミン及びアルカノールアミン等)等が挙げられる。
(B) Anionic surfactant:
(B-1) Carboxylic acid type surfactant: For example, a combination of polyacrylic acid, polymethacrylic acid, polymaleic acid, polymaleic anhydride, maleic acid or maleic anhydride with an olefin (such as isobutylene and diisobutylene). Polymers, copolymers of acrylic acid and itaconic acid, copolymers of methacrylic acid and itaconic acid, copolymers of maleic acid or maleic anhydride and styrene, copolymers of acrylic acid and methacrylic acid, acrylic acid Copolymers of acrylic acid and methyl acrylate, copolymers of acrylic acid and vinyl acetate, copolymers of acrylic acid and maleic acid or maleic anhydride, N-methyl-fatty acid (C 8-18 ) sarcosinate, resins Examples include carboxylic acids such as acids and fatty acids (C 8-18 ), and salts of these carboxylic acids.
(B-2) Sulfate ester type surfactant: For example, alkyl (C 8-18 ) sulfate, polyoxyethylene alkyl (C 8-18 ) ether sulfate, polyoxyethylene (mono- or di)alkyl (C 8 ) ~12 ) Phenyl ether sulfate, polyoxyethylene (mono- or di)alkyl ( C8-12 ) polymer sulfate of phenyl ether, polyoxyethylene (mono-, di- or tri) phenyl phenyl ether sulfate, polyoxyethylene (mono, di or tri)benzylphenyl ether sulfate, polyoxyethylene (mono, di or tri)styrylphenyl ether sulfate, sulfate of polymers of polyoxyethylene (mono, di or tri)styrylphenyl ether, polyoxy Sulfuric esters such as sulfuric esters of ethylene polyoxypropylene block polymers, sulfated oils, sulfated fatty acid esters, sulfated fatty acids and sulfated olefins, and salts of these sulfuric esters can be mentioned.
(B-3) Sulfonic acid type surfactant: For example, lignin sulfonic acid, paraffin (C 8-22 ) sulfonic acid, alkyl (C 8-12 ) benzenesulfonic acid, alkyl (C 8-12 ) benzenesulfonic acid. Formalin condensate, formalin condensate of cresol sulfonic acid, α-olefin (C 8-16 ) sulfonic acid, polyoxyethylene (mono- or di)alkyl (C 8-12 ) phenyl ether sulfonic acid, naphthalene sulfonic acid, (mono- or di)alkyl (C 8-12 ) phenyl ether sulfonic acid, or di)alkyl (C 1-6 ) naphthalene sulfonic acid, formalin condensation product of naphthalene sulfonic acid, formalin condensation product of (mono- or di)alkyl (C 1-6 ) naphthalene sulfonic acid, formalin condensation product of creosote oil sulfonic acid. Examples include sulfonic acids such as alkyl (C 8-12 ) diphenyl ether disulfonic acid, Igepon T (trade name), polystyrene sulfonic acid, and a copolymer of styrene sulfonic acid and methacrylic acid, and salts of these sulfonic acids.
(B-4) Phosphate ester type surfactant: For example, alkyl (C 8-12 ) phosphate ester, polyoxyethylene alkyl (C 8-18 ) ether phosphate, polyoxyethylene (mono- or di)alkyl (C 8 ) ~12 ) Phenyl ether phosphate ester, polyoxyethylene (mono, di or tri) alkyl (C 8-12 ) phenyl ether polymer phosphate ester, polyoxyethylene (mono, di or tri) phenyl phenyl ether phosphate ester, polyoxyethylene (mono, di or tri) phenyl phenyl ether phosphate ester, oxyethylene (mono, di or tri)benzylphenyl ether phosphate, polyoxyethylene (mono, di or tri)styrylphenyl ether phosphate, phosphoric ester of polymers of polyoxyethylene (mono, di or tri)styrylphenyl ether, Examples include phosphoric esters of polyoxyethylene polyoxypropylene block polymers, phosphoric esters such as phosphatidylcholine, phosphatidylethanolimine, condensed phosphoric acid (eg, tripolyphosphoric acid, etc.), and salts of these phosphoric esters.
Examples of the salts in (B-1) to (B-4) above include alkali metals (lithium, sodium, potassium, etc.), alkaline earth metals (calcium, magnesium, etc.), ammonium, and various amines (such as alkylamines, cyclo alkylamines, alkanolamines, etc.).
(C)カチオン性界面活性剤:
例えば、アルキルアミン、アルキル4級アンモニウム塩、アルキルアミンのエチレンオキサイド付加物及びアルキル4級アンモニウム塩のエチレンオキサイド付加物等が挙げられる。
(C) Cationic surfactant:
Examples include alkyl amines, alkyl quaternary ammonium salts, ethylene oxide adducts of alkyl amines, and ethylene oxide adducts of alkyl quaternary ammonium salts.
(D)両性界面活性剤:
例えば、ベタイン型界面活性剤及びアミノ酸型界面活性剤等が挙げられる。
(D) Amphoteric surfactant:
Examples include betaine type surfactants and amino acid type surfactants.
(E)その他の界面活性剤:
例えば、シリコーン系界面活性剤及びフッ素系界面活性剤等が挙げられる。
(E) Other surfactants:
Examples include silicone surfactants and fluorine surfactants.
結合剤としては、例えばデキストリン(焙焼デキストリンおよび酵素変性デキストリ
ン等)、酸分解澱粉、酸化澱粉、アルファー化澱粉、エーテル化澱粉(カルボキシメチル澱粉、ヒドロキシアルキル澱粉及びカチオン澱粉等)、エステル化澱粉(酢酸澱粉及びリン酸澱粉等)、架橋澱粉及びグラフト化澱粉等の加工澱粉、例えばアルギン酸ナトリウム、アラビアガム、ゼラチン、トラガントガム、ローカストビーンガム及びカゼイン等の天然物質、例えばカルボキシメチルセルロースナトリウム塩、ヒドロキシエチルセルロース、ヒドロキシプロピルセルロース、ヒドロキシプロピルメチルセルロース、メチルセルロース、エチルセルロース及びアセチルセルロース等のセルロース誘導体、並びに例えばポリビニルメチルエーテル、ポリエチレングリコール、ポリプロピレングリコール、ポリエチレンポリプロピレンブロック共重合体、ポリビニルアルコール、部分けん化酢酸ビニルとビニルエーテルの共重合体、ポリビニルピロリドン、ポリビニルピロリドンと酢酸ビニルの共重合物及びポリアクリルアミド等のその他の高分子が挙げられる。
Examples of binders include dextrin (roasted dextrin, enzyme-modified dextrin, etc.), acid-decomposed starch, oxidized starch, pregelatinized starch, etherified starch (carboxymethyl starch, hydroxyalkyl starch, cationic starch, etc.), esterified starch ( starch acetate and starch phosphate), modified starches such as cross-linked starches and grafted starches, natural substances such as sodium alginate, gum arabic, gelatin, gum tragacanth, locust bean gum and casein, such as sodium carboxymethyl cellulose, hydroxyethyl cellulose, Cellulose derivatives such as hydroxypropyl cellulose, hydroxypropyl methyl cellulose, methyl cellulose, ethyl cellulose and acetyl cellulose, and for example polyvinyl methyl ether, polyethylene glycol, polypropylene glycol, polyethylene polypropylene block copolymers, polyvinyl alcohol, copolymers of partially saponified vinyl acetate and vinyl ether. Examples include other polymers such as polyvinylpyrrolidone, polyvinylpyrrolidone and vinyl acetate copolymers, and polyacrylamide.
酸としては、例えば有機酸や無機酸が挙げられる。有機酸の好ましい例としては、アスコルビン酸及びエリソルビン酸などのラクトン、酢酸、ソルビン酸、コハク酸、フマル酸、オレイン酸、クエン酸、酒石酸、リンゴ酸及び安息香酸などのカルボン酸であり、好ましくはクエン酸である。また無機酸としては、塩酸、燐酸、硫酸、亜硫酸及び重亜硫酸などが挙げられる。 Examples of acids include organic acids and inorganic acids. Preferred examples of organic acids are lactones such as ascorbic acid and erythorbic acid, carboxylic acids such as acetic acid, sorbic acid, succinic acid, fumaric acid, oleic acid, citric acid, tartaric acid, malic acid and benzoic acid, preferably It is citric acid. Examples of inorganic acids include hydrochloric acid, phosphoric acid, sulfuric acid, sulfite, and bisulfite.
固体担体としては、例えば石英、方解石、海泡石、ドロマイト、チョーク、カオリナイト、パイロフィライト、セリサイト、ハロサイト、メタハロサイト、木節粘土、蛙目粘土、陶石、ジークライト、アロフェン、シラス、きら、タルク、ベントナイト、活性白土、酸性白土、軽石、アタパルジャイト、ゼオライト及び珪藻土等の天然鉱物質、例えば焼成クレー、パーライト、シラスバルーン、バーミキュライト、アタパルガスクレー及び焼成珪藻土等の天然鉱物質の焼成品、例えば炭酸マグネシウム、炭酸カルシウム、硫酸アンモニウム、硫酸ナトリウム、硫酸マグネシウム、リン酸水素二アンモニウム、リン酸二水素アンモニウム及び塩化カリウム等の無機塩類、例えばブドウ糖、果糖、しょ糖及び乳糖などの糖類、例えば澱粉、粉末セルロース及びデキストリン等の多糖類、例えば尿素、尿素誘導体、安息香酸及び安息香酸の塩等の有機物、例えば木粉、コルク粉、トウモロコシ穂軸、クルミ殻及びタバコ茎等の植物類、フライアッシュ、ホワイトカーボン、プラスチック中空体、ガラス質中空体並びに肥料等が挙げられる。 Examples of solid carriers include quartz, calcite, sepiolite, dolomite, chalk, kaolinite, pyrophyllite, sericite, hallosite, metahallosite, kibushi clay, frog's eye clay, potter's stone, ziecrite, and allophane. , shirasu, kira, talc, bentonite, activated clay, acid clay, pumice, attapulgite, zeolite and diatomaceous earth, natural minerals such as calcined clay, perlite, shirasu balloon, vermiculite, attapulgus clay and calcined diatomaceous earth. Inorganic salts such as magnesium carbonate, calcium carbonate, ammonium sulfate, sodium sulfate, magnesium sulfate, diammonium hydrogen phosphate, ammonium dihydrogen phosphate and potassium chloride, sugars such as glucose, fructose, sucrose and lactose. , polysaccharides such as starch, powdered cellulose and dextrins, organic substances such as urea, urea derivatives, benzoic acid and salts of benzoic acid, plants such as wood flour, cork flour, corn cobs, walnut shells and tobacco stalks. , fly ash, white carbon, plastic hollow bodies, vitreous hollow bodies, and fertilizers.
次に実施例を挙げて本発明をさらに詳細に説明するが、本発明はこれらに限定されるものではない。 EXAMPLES Next, the present invention will be explained in more detail with reference to Examples, but the present invention is not limited thereto.
[実施例1]
ピラクロニル5重量部、リグニンスルホン酸ナトリウム5重量部、カルボキシメチルセルロースナトリウム10重量部、コルク30重量部、クレー45重量部を混合し、ニューカルゲン4000G(商品名)5重量部を適量の水に溶解した水溶液を加えて混練後、1.5mmの細孔を開けたプレートから押し出し造粒した。得られた造粒物を80℃の温風で乾燥し実施例1の粒状製剤を得た。
[Example 1]
5 parts by weight of pyraclonil, 5 parts by weight of sodium ligninsulfonate, 10 parts by weight of sodium carboxymethyl cellulose, 30 parts by weight of cork, and 45 parts by weight of clay were mixed, and 5 parts by weight of Nucalgen 4000G (trade name) was dissolved in an appropriate amount of water. After adding the aqueous solution and kneading, the mixture was extruded through a plate with 1.5 mm pores and granulated. The obtained granules were dried with warm air at 80°C to obtain the granular preparation of Example 1.
[実施例2~44]
実施例1の各成分を下記表1~4に記載の成分及び配合量に変更した以外は、実施例1と同様にし、粒状製剤を得た。
[Examples 2 to 44]
A granular preparation was obtained in the same manner as in Example 1, except that each component in Example 1 was changed to the components and amounts listed in Tables 1 to 4 below.
[試験例1]
長期加温条件における成分安定性試験:実施例1~44で得た製剤各100gをアルミ袋に入れ、入り口をヒートシールで密封した。これを50℃条件下に1ヶ月保存し保存後の有効成分を分析し、保存前の分析値との差を保存前の分析値で除し分解率を求めた。結果は下表1~4に示す。
[Test Example 1]
Component stability test under long-term heating conditions: 100 g of each of the formulations obtained in Examples 1 to 44 was placed in an aluminum bag, and the entrance was sealed with a heat seal. This was stored under 50°C conditions for one month, and the active ingredients after storage were analyzed.The difference between the analysis value before storage and the analysis value before storage was divided by the analysis value before storage to determine the decomposition rate. The results are shown in Tables 1 to 4 below.
[試験例2]
水面拡散性評価試験:7.5m×0.4mの水槽に水道水を入れ水深5cmの水槽を調製する。水槽端に実施例1~44で得た製剤各5gを処理し、製剤の水面拡散性を評価した。評価方法は以下の通りである。結果は下表1~4に示す。
[Test Example 2]
Water surface diffusivity evaluation test: Fill a 7.5 m x 0.4 m water tank with tap water and prepare a water tank with a water depth of 5 cm. 5 g of each of the formulations obtained in Examples 1 to 44 was placed at the end of the water tank, and the water surface diffusivity of the formulations was evaluated. The evaluation method is as follows. The results are shown in Tables 1 to 4 below.
〈水面拡散性〉
◎:粒の到達距離が7m以上
○:粒の到達距離が6m以上
△:粒の到達距離が5m以上
×:粒の到達距離が5m未満
<Water surface diffusivity>
◎: Grain reach distance is 7 m or more ○: Grain reach distance is 6 m or more △: Grain reach distance is 5 m or more ×: Grain reach distance is less than 5 m
上記の実施例1~44において何れも拡散性は良好であり、有効成分の分解が軽微であった。 In all of the above Examples 1 to 44, the diffusibility was good, and the decomposition of the active ingredient was slight.
本発明の組成物は、農業用製剤として有用である。 The compositions of the present invention are useful as agricultural formulations.
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