JP2023043656A - cosmetics - Google Patents
cosmetics Download PDFInfo
- Publication number
- JP2023043656A JP2023043656A JP2021151386A JP2021151386A JP2023043656A JP 2023043656 A JP2023043656 A JP 2023043656A JP 2021151386 A JP2021151386 A JP 2021151386A JP 2021151386 A JP2021151386 A JP 2021151386A JP 2023043656 A JP2023043656 A JP 2023043656A
- Authority
- JP
- Japan
- Prior art keywords
- cosmetic
- value
- mass
- skin
- pigments
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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- 239000002537 cosmetic Substances 0.000 title claims abstract description 58
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 claims description 20
- 239000000975 dye Substances 0.000 claims description 10
- 239000012860 organic pigment Substances 0.000 claims description 7
- 238000004040 coloring Methods 0.000 claims description 5
- 239000002994 raw material Substances 0.000 claims description 4
- -1 sericite Chemical compound 0.000 description 26
- 239000000843 powder Substances 0.000 description 21
- 239000000049 pigment Substances 0.000 description 17
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- 235000014113 dietary fatty acids Nutrition 0.000 description 10
- 239000000194 fatty acid Substances 0.000 description 10
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- 239000007787 solid Substances 0.000 description 10
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- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 6
- 239000004359 castor oil Substances 0.000 description 6
- 235000019438 castor oil Nutrition 0.000 description 6
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 6
- 239000003921 oil Substances 0.000 description 6
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- 239000004615 ingredient Substances 0.000 description 5
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- 239000001023 inorganic pigment Substances 0.000 description 2
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Landscapes
- Cosmetics (AREA)
Abstract
Description
本発明は、化粧料に関する。 The present invention relates to cosmetics.
ベースメークアップは、肌を美しく見せるためになされる化粧である。ベースメークアップ化粧料としては、ファンデーションの乗りを良くするための化粧下地や、肌色を整えるファンデーションや、シミやクマ等を目立たなくするコンシーラー等がある。
近年のベースメークには、肌色を整えたり、シミやソバカス等の肌の難点を隠したりするのみでなく、透明感のある自然な仕上がりが求められるようになっている。そのため、化粧料に含有させる粉体等の成分の改良が種々検討されている。例えば、肌において内部反射光量が高いと透明感が高まることに基づき、被覆成分の屈折率を調整した積層粉体を化粧料に含有させて、透明感のある仕上がりを演出することが提案されている(特許文献1)。
Base makeup is makeup applied to make the skin look beautiful. Base make-up cosmetics include a makeup base for improving the application of the foundation, a foundation for adjusting the skin color, and a concealer for making blemishes and dark circles inconspicuous.
In recent years, base makeup is required not only to adjust the skin color and hide skin defects such as blemishes and freckles, but also to provide a transparent and natural finish. Therefore, various studies have been made to improve components such as powders to be contained in cosmetics. For example, based on the fact that transparency increases when the amount of internally reflected light on the skin is high, it has been proposed to produce a finish with a sense of transparency by including in cosmetics a layered powder in which the refractive index of the coating component is adjusted. (Patent Document 1).
透明感のある自然な仕上がりを得ようとすると、シミやソバカス等を隠ぺいするカバー力が不十分となる場合がある。
また、透明感のある仕上がりを得るための化粧料の設計において、化粧料の色味に着目した例はない。
本発明は、カバー力がありながら化粧後の肌が透明感のある自然な仕上がりとなるメークアップ化粧料を提供することを課題とする。
When trying to obtain a transparent and natural finish, the covering power to hide stains, freckles, etc. may be insufficient.
Moreover, in the design of cosmetics for obtaining a finish with a sense of transparency, there is no example of paying attention to the color of the cosmetics.
An object of the present invention is to provide a make-up cosmetic that gives the skin after make-up a transparent and natural finish while having covering power.
本発明者らは、上記課題を解決すべく鋭意研究したところ、化粧料の外観色を青みがかった淡いピンク色とし、かつ所定の方法で測定されるコントラスト比が特定の範囲とすると、上記課題を解決できることに想到し、本発明を完成させた。 The inventors of the present invention have made intensive research to solve the above problems, and found that the above problems can be solved by making the appearance color of the cosmetic material pale pink with a bluish tinge and setting the contrast ratio measured by a predetermined method to a specific range. The present invention was completed after conceiving that the problem could be solved.
すなわち、本発明は以下の通りである。
[1]L*値が68以上、a*値が7.5~12.0、かつb*値が-0.5~2.0である色差を有し、
コントラスト比が0.38~0.65である、化粧料。
[2]少なくとも3種類の着色原料を含有する、[1]に記載の化粧料。
[3]少なくとも1種類の有機色素、染料又は酸化鉄を含有する、[1]又は[2]に記載の化粧料。
[4]ベースメークアップ化粧料である、[1]~[3]のいずれかに記載の化粧料。
[5]トーンアップ用である、[1]~[4]のいずれかに記載の化粧料。
That is, the present invention is as follows.
[1] having a color difference with an L* value of 68 or more, an a* value of 7.5 to 12.0, and a b* value of −0.5 to 2.0;
A cosmetic having a contrast ratio of 0.38 to 0.65.
[2] The cosmetic according to [1], containing at least three coloring materials.
[3] The cosmetic according to [1] or [2], containing at least one kind of organic pigment, dye or iron oxide.
[4] The cosmetic according to any one of [1] to [3], which is a base makeup cosmetic.
[5] The cosmetic according to any one of [1] to [4], which is for tone-up.
本発明により、透明感があり自然な仕上がりと、カバー力とを両立して叶えるメークアップ化粧料が提供される。 ADVANTAGE OF THE INVENTION The present invention provides a makeup cosmetic that achieves both a clear and natural finish and good covering power.
以下、本発明の具体的な実施形態について説明する。
本発明の化粧料は、L*値が68以上、a*値が7.5~12.0、かつb*値が-0.5~2.0である色差を有し、コントラスト比が0.38~0.65である。
なお、本明細書における数値範囲には、「~」の前後の数値を含むものとする。
Specific embodiments of the present invention are described below.
The cosmetic of the present invention has a color difference with an L* value of 68 or more, an a* value of 7.5 to 12.0, and a b* value of −0.5 to 2.0, and a contrast ratio of 0. 0.38 to 0.65.
It should be noted that the numerical range in this specification includes numerical values before and after "-".
本明細書において、L*値、a*値、及びb*値は、CIE1976 L*a*b*の
色空間における値を指す。L*値は明度を表し、0(黒)~100(白)の範囲で表される。また、a*値及びb*値は色相と彩度を表し、-100~100の範囲で表される測定での値とする。
L*値、a*値、及びb*値は、通常、分光光度計で測定することができる。
As used herein, L* values, a* values, and b* values refer to values in the CIE 1976 L*a*b* color space. The L* value represents lightness and ranges from 0 (black) to 100 (white). The a* value and the b* value represent hue and saturation, and are measured values in the range of -100 to 100.
L* values, a* values, and b* values can usually be measured with a spectrophotometer.
本発明の化粧料において、L*値は68以上であり、好ましくは68.5以上、より好ましくは70以上である。また、L*値の上限は特に限定されないが、好ましくは80以下、より好ましくは76以下である。 In the cosmetic of the present invention, the L* value is 68 or more, preferably 68.5 or more, more preferably 70 or more. Although the upper limit of the L* value is not particularly limited, it is preferably 80 or less, more preferably 76 or less.
本発明の化粧料において、a*値は7.5以上であり、好ましくは8.0以上、より好ましくは9.0以上である。また、a*値は12.0以下であり、好ましくは11.5以下、より好ましくは10.5以下である。 In the cosmetic of the present invention, the a* value is 7.5 or more, preferably 8.0 or more, more preferably 9.0 or more. Also, the a* value is 12.0 or less, preferably 11.5 or less, more preferably 10.5 or less.
本発明の化粧料において、b*値は-0.5以上であり、好ましくは0.0以上、より好ましくは1.0以上である。また、b*値は2.0以下であり、好ましくは1.8以下、より好ましくは1.7以下である。 In the cosmetic of the present invention, the b* value is -0.5 or more, preferably 0.0 or more, more preferably 1.0 or more. Also, the b* value is 2.0 or less, preferably 1.8 or less, and more preferably 1.7 or less.
本明細書において、「コントラスト比」とは、化粧料を黒色及び白色の基板上にそれぞれ同厚さで塗布したときの各塗布膜の明度の比を指す。すなわち、黒色基板上の塗布膜の明度を白色基板上の塗布膜の明度で除してさらに100を乗じた値である。通常、この値が大きいほどカバー力(隠ぺい率)が高いとされる。 As used herein, the term "contrast ratio" refers to the brightness ratio of each coating film when the cosmetic is coated on a black substrate and a white substrate in the same thickness. That is, it is a value obtained by dividing the brightness of the coating film on the black substrate by the brightness of the coating film on the white substrate and multiplying the result by 100. Generally, the higher this value, the higher the covering power (hiding rate).
本発明の化粧料において、コントラスト比は0.38以上、0.65以下である。コントラスト比が0.38より低いと顔全体が暗い仕上がりとなり、0.65よりも高いと化粧が白浮きして顔全体が不自然な印象を与える仕上がりとなる。 The cosmetic of the present invention has a contrast ratio of 0.38 or more and 0.65 or less. If the contrast ratio is lower than 0.38, the entire face will have a dark finish, and if it is higher than 0.65, the makeup will appear white and the entire face will have an unnatural finish.
化粧料のL*値、a*値、及びb*値並びにコントラスト比を上記範囲とするには、化粧料含有成分、特に粉体や色素(粉体に包含される場合もある)等の種類や含有量を適宜調整すればよい。以下、調整例を挙げるが、本発明はこれらに限定されない。 In order to set the L* value, a* value, b* value, and contrast ratio of the cosmetic in the above ranges, the type of cosmetic-containing ingredients, particularly powders and pigments (which may be included in powders), etc. and content may be adjusted as appropriate. Adjustment examples will be given below, but the present invention is not limited to these.
L*値を所望の範囲とするためには、例えば顔料酸化チタン、酸化チタン等の白色顔料を用い、その含有量を好ましくは1~12質量%、より好ましくは3~10質量%、さらに好ましくは4~8質量%とすることによって調整してもよい。
このような範囲とすることで、化粧料を塗布した肌に自然な仕上がりを付与しやすくなる。白色顔料の含有量が多すぎるとL*値が大きくなりすぎる場合がある。また、白色顔料の含有量を多くしながらL*値を所定の範囲にまで下げようとすると、有色顔料の含有量を増やす必要が生じ、化粧料を塗布した際に色ムラが生じる場合がある。
In order to make the L* value in the desired range, for example, a white pigment such as pigment titanium oxide or titanium oxide is used, and the content thereof is preferably 1 to 12% by mass, more preferably 3 to 10% by mass, more preferably 3 to 10% by mass. may be adjusted to 4 to 8% by mass.
By setting it in such a range, it becomes easy to impart a natural finish to the skin to which the cosmetic is applied. If the white pigment content is too high, the L* value may become too large. In addition, when trying to lower the L* value to a predetermined range while increasing the content of the white pigment, it becomes necessary to increase the content of the colored pigment, which may cause color unevenness when the cosmetic is applied. .
また、L*値を所望の範囲とするためには、有機色素、染料、酸化鉄等の有色顔料を用い、その含有量を好ましくは0.001~1質量%、より好ましくは0.01~0.5質量%、さらに好ましくは0.01~0.1質量%とすることによって調整してもよい。 Further, in order to set the L* value to the desired range, organic pigments, dyes, colored pigments such as iron oxide are used, and the content thereof is preferably 0.001 to 1% by mass, more preferably 0.01 to 1% by mass. It may be adjusted to 0.5% by mass, more preferably 0.01 to 0.1% by mass.
また、L*値を所望の範囲とするためには、黒色粉体を用いないか、あるいは用いる場合はその含有量を好ましくは0.5質量%以下、より好ましくは0.2質量%以下、さら
に好ましくは0.1質量%以下とすることによって調整してもよい。有色顔料と黒色粉体とを組み合わせると、化粧料の外観がくすみ、透明感のある自然な仕上がりが得られにくい場合がある。
黒色粉体の例としては、黒酸化鉄、カーボンブラック、チタンブラック等があげられる。
Also, in order to make the L* value within the desired range, black powder is not used, or if it is used, the content is preferably 0.5% by mass or less, more preferably 0.2% by mass or less, More preferably, it may be adjusted to 0.1% by mass or less. When the colored pigment and the black powder are combined, the appearance of the cosmetic becomes dull and it may be difficult to obtain a transparent and natural finish.
Examples of black powder include black iron oxide, carbon black and titanium black.
a*値を所望の範囲とするためには、有機色素、染料、酸化鉄等の有色顔料を用い、その含有量を好ましくは0.001~1.0質量%、より好ましくは0.001~0.5質量%、さらに好ましくは0.01~0.5質量%とすることによって調整してもよい。 In order to set the a* value in the desired range, organic pigments, dyes, and colored pigments such as iron oxide are used, and the content thereof is preferably 0.001 to 1.0% by mass, more preferably 0.001 to 1.0% by mass. It may be adjusted to 0.5% by mass, more preferably 0.01 to 0.5% by mass.
b*値を所望の範囲とするためには、有機色素、染料、酸化鉄等の有色顔料を用い、その含有量を好ましくは0.001~1.0質量%、より好ましくは0.001~0.5質量%、さらに好ましくは0.01~0.5質量%とすることによって調整してもよい。 In order to set the b* value in the desired range, organic pigments, dyes, colored pigments such as iron oxide are used, and the content thereof is preferably 0.001 to 1.0% by mass, more preferably 0.001 to 1.0% by mass. It may be adjusted to 0.5% by mass, more preferably 0.01 to 0.5% by mass.
コントラスト比を所望の範囲とするためには、化粧料全体における粉体の総含有量を、好ましくは0.1~15質量%、より好ましくは2.0~10質量%、さらに好ましくは3~8質量%とすることによって調整してもよい。
また、コントラスト比を所望の範囲とするためには、化粧料に含有させる粉体の形状として板状のものを用いたり、大きさ(長径)が10~100nmの、微粒子金属酸化物(酸化チタン、酸化鉄等)や体質顔料(タルク等)を適当量用いることによって調整してもよい。
In order to bring the contrast ratio into the desired range, the total content of powder in the cosmetic is preferably 0.1 to 15% by mass, more preferably 2.0 to 10% by mass, more preferably 3 to 10% by mass. You may adjust by setting it as 8 mass %.
In addition, in order to set the contrast ratio within the desired range, the powder contained in the cosmetic may be plate-shaped, or fine particles of metal oxide (titanium oxide , iron oxide, etc.) or an extender (talc, etc.) may be used in an appropriate amount.
本発明の化粧料を肌に塗布すると、良好な透明感が付与される。透明感とは、くすみのない透き通ったように見える状態をいう。化粧肌に透明感があることにより、肌がトーンアップした演出が叶う。
また、通常は、肌の欠点をカバーしようとすると化粧膜の存在を感じさせる不自然な仕上がりになりやすいが、本発明の化粧料は、透明感のある自然な仕上がりとカバー力とを両立させることができる。
When the cosmetic composition of the present invention is applied to the skin, it imparts good transparency. Transparency refers to a state in which the material appears transparent without dullness. The transparency of the makeup skin makes it possible to create a tone-up effect on the skin.
In addition, usually, when trying to cover skin imperfections, it tends to result in an unnatural finish that makes one feel the presence of a cosmetic film. be able to.
本発明の化粧料の剤型は特に限定されず、パウダータイプ(粉末剤型)でも、オイルゲルタイプ、エマルジョンタイプ(乳化剤型)でも構わない。
また、本発明の化粧料の態様としては、通常はベースメーク化粧料であり、ファンデーション、フェイスパウダー、コンシーラー、チークカラー、アイカラー等が挙げられ、特に限定されない。
The dosage form of the cosmetic of the present invention is not particularly limited, and may be a powder type (powder dosage form), an oil gel type, or an emulsion type (emulsifier type).
In addition, the cosmetics of the present invention are usually base makeup cosmetics, and include foundations, face powders, concealers, cheek colors, eye colors, etc., and are not particularly limited.
本発明の化粧料は、定法により製造することができる。 The cosmetic of the present invention can be produced by a conventional method.
以下、本発明の化粧料に用いる原料について説明するが、特にこれらに限定されない。1)粉体
本発明の化粧料に使用し得る粉体は、水、油脂、界面活性剤、アルコール類、シリコーン類などの化粧料原料には溶解しない、有機或いは無機の固形物の総称を意味する。
粉体の具体例としては、カオリン、タルク、マイカ、セリサイト、チタンマイカ、積層樹脂小片(グリッター)、ホウケイ酸Ca/Al、チタンセリサイト、二酸化チタン、酸化鉄、酸化亜鉛、群青、紺青、赤色102号、赤色226号、黄色4号等の色素顔料、アルミニウムレーキ、シリカ、アルミナ、珪酸カルシウム、珪酸マグネシウム、炭酸カルシウム、炭酸マグネシウム、メチルシロキサン網状重合体、架橋型メチルポリシロキサン樹脂、アクリル酸アルキル樹脂類、ナイロン、シルク、セルロース或いはこれらの複合材料などが例示できる。
粉体の形状は、球状、不定形、多孔質状、中空状、繊維状、板状或いは塊状であってもよい。更に、その表面は、シリコーン被覆処理、金属石けん被覆処理、アシルアミノ酸塩
被覆処理など、通常知られている表面処理が為されていてもよい。
粉体は、化粧料において、1種のみ配合してもよく、2種以上を組み合わせて配合してもよい。
The raw materials used in the cosmetic composition of the present invention are described below, but are not particularly limited to these. 1) Powder The powder that can be used in the cosmetic of the present invention is a general term for organic or inorganic solids that are insoluble in cosmetic raw materials such as water, oils, surfactants, alcohols, and silicones. do.
Specific examples of powder include kaolin, talc, mica, sericite, titanium mica, laminated resin pieces (glitter), Ca/Al borosilicate, titanium sericite, titanium dioxide, iron oxide, zinc oxide, ultramarine blue, Prussian blue, Color pigments such as Red No. 102, Red No. 226, Yellow No. 4, aluminum lake, silica, alumina, calcium silicate, magnesium silicate, calcium carbonate, magnesium carbonate, methylsiloxane network polymer, crosslinked methylpolysiloxane resin, acrylic acid Examples include alkyl resins, nylon, silk, cellulose, and composite materials thereof.
The shape of the powder may be spherical, amorphous, porous, hollow, fibrous, plate-like or massive. Furthermore, the surface may be subjected to a generally known surface treatment such as silicone coating, metal soap coating, acylamino acid salt coating, and the like.
The powder may be used alone or in combination of two or more in the cosmetic.
本発明の化粧料は、少なくとも3種類の着色原料を含有することが好ましい。ここで着色原料は、有機色素、染料、無機顔料、天然色素、高分子粉体等を指す。本発明の化粧料は、少なくとも1種類の有機色素、染料又は酸化鉄を含有することがより好ましい。
有機色素としては、アゾ系顔料、インジゴ系顔料、フタロシアニン系顔料等が挙げられ、具体的には赤色227号、赤色226号、赤色201号等が挙げられるが特に限定されない。
染料としては、アゾ系染料、キサンテン系染料、キノリン系染料等が挙げられ、具体的には青色1号、コンジョウ、グンジョウ等が挙げられるが特に限定されない。
無機顔料としては、赤酸化鉄、黄酸化鉄、雲母チタン等が挙げられるが特に限定されない。
天然色素としては、動植物由来又は微生物由来の、カロチノイド系色素、フラボノイド系色素等が挙げられ、具体的にはシコニン、クチナシ、コチニール色素等が挙げられるが特に限定されない。
高分子粉体としては、積層高分子粉体(ラメ)等が挙げられるが特に限定されない。
The cosmetic of the present invention preferably contains at least three coloring materials. Here, the coloring raw materials refer to organic pigments, dyes, inorganic pigments, natural pigments, polymer powders, and the like. More preferably, the cosmetic of the present invention contains at least one kind of organic pigment, dye or iron oxide.
Examples of organic dyes include azo pigments, indigo pigments, and phthalocyanine pigments. Specific examples include Red No. 227, Red No. 226, and Red No. 201, but are not particularly limited.
Examples of dyes include azo dyes, xanthene dyes, quinoline dyes, and specific examples include Blue No. 1, konjou, and gunjou, but are not particularly limited.
Examples of inorganic pigments include, but are not limited to, red iron oxide, yellow iron oxide, mica titanium, and the like.
Examples of natural pigments include carotenoid pigments and flavonoid pigments derived from animals and plants or microorganisms, and specific examples include shikonin, gardenia, and cochineal pigments, but are not particularly limited.
Examples of the polymer powder include laminated polymer powder (lame) and the like, but are not particularly limited.
2)油性成分
本発明の化粧料は、油性成分を含んでもよい。
油性成分の具体例としては、例えば、マカデミアナッツ油、アボガド油、トウモロコシ油、オリーブ油、ナタネ油、ゴマ油、ヒマシ油、サフラワー油、綿実油、ホホバ油、ヤシ油、パーム油、液状ラノリン等の動植物油;流動パラフィン、スクワラン、プリスタン等の炭化水素油;オレイン酸、イソステアリン酸等の液状脂肪酸;イソステアリルアルコール、オクチルドデカノール等の液状高級アルコール;イソオクタン酸セチル、ミリスチン酸イソプロピル、イソステアリン酸ヘキシルデシル、アジピン酸ジイソプロピル、セバチン酸ジ-2-エチルヘキシル、乳酸セチル、リンゴ酸ジイソステアリル、ジ-2-エチルヘキサン酸エチレングリコール、ジカプリン酸ネオペンチルグリコール、ジ-2-ヘプチルウンデカン酸グリセリン、トリ-2-エチルヘキサン酸グリセリン、エチルヘキサン酸セチル、トリ-2-エチルヘキサン酸トリメチロールプロパン、トリイソステアリン酸トリメチロールプロパン、テトラ-2-エチルヘキサン酸ペンタンエリトリット、グリセリルトリイソステアレート、グリセリルトリイソオクタネート等の合成エステル油;ジメチルポリシロキサン、メチルフェニルポリシロキサン、ジフェニルポリシロキサン等の鎖状ポリシロキサン;オクタメチルシクロテトラシロキサン、デカメチルシクロペンタシロキサン、ドデカメチルシクロヘキサンシロキサン等の環状ポリシロキサン;アミノ変性ポリシロキサン、ポリエーテル変性ポリシロキサン、アルキル変性ポリシロキサン、フッ素変性ポリシロキサン等の変性ポリシロキサン等のシリコーン油;が挙げられる。但し、後述する特定の界面活性剤群に属するものは、油性成分として取り扱わないものとする。
2) Oily component The cosmetic of the present invention may contain an oily component.
Specific examples of oily components include animal and plant oils such as macadamia nut oil, avocado oil, corn oil, olive oil, rapeseed oil, sesame oil, castor oil, safflower oil, cottonseed oil, jojoba oil, coconut oil, palm oil, and liquid lanolin. Hydrocarbon oils such as liquid paraffin, squalane, and pristane; Liquid fatty acids such as oleic acid and isostearic acid; Liquid higher alcohols such as isostearyl alcohol and octyldodecanol; Cetyl isooctanoate, isopropyl myristate, hexyldecyl isostearate, and adipine diisopropyl acid, di-2-ethylhexyl sebacate, cetyl lactate, diisostearyl malate, ethylene glycol di-2-ethylhexanoate, neopentyl glycol dicaprate, glyceryl di-2-heptylundecanoate, tri-2-ethyl Glyceryl hexanoate, cetyl ethylhexanoate, trimethylolpropane tri-2-ethylhexanoate, trimethylolpropane triisostearate, pentane erythritol tetra-2-ethylhexanoate, glyceryl triisostearate, glyceryl triisooctanate, etc. Synthetic ester oils of dimethylpolysiloxane, methylphenylpolysiloxane, diphenylpolysiloxane and other chain polysiloxanes; octamethylcyclotetrasiloxane, decamethylcyclopentasiloxane, dodecamethylcyclohexanesiloxane and other cyclic polysiloxanes; amino-modified polysiloxane , polyether-modified polysiloxane, alkyl-modified polysiloxane, and modified polysiloxane such as fluorine-modified polysiloxane. However, those belonging to the specific group of surfactants described later shall not be treated as oily components.
また、剤型によっては、油性成分として固形脂及び/又は半固形脂を用いてもよい。ここで、固形脂には半固形脂も含まれる。なお、固形とは25℃で流動性がないものをいい、半固形とは1気圧、20℃で応力の存在しない環境では殆ど変形しないが、若干の応力(10~100g/cm2程度)がかかると変形するものをいう。また、融点が50℃以上のものがより好ましい。
固形脂及び/又は半固形脂としては、植物由来のものとして、カルナウバロウ、モクロウ、キャンデリラロウ、コメヌカロウ、シアバター、アフリカマンゴバター等が挙げられ、動物由来のものとして、ミツロウ、シェラックロウ、イボタロウ等が挙げられ、石油由来のものとして、パラフィンワックス、マイクロクリスタリンワックス等の精製ワックスが挙げられ、鉱物由来のものとしてオゾケライト、セレシン、モンタンワックス等の精製
ワックスが挙げられる。
In addition, solid fat and/or semi-solid fat may be used as the oily component depending on the dosage form. Here, semi-solid fat is also included in solid fat. The term “solid” refers to those that have no fluidity at 25°C, and “semi-solid” means that they are hardly deformed under stress-free conditions at 1 atm and 20°C, but some stress (approximately 10 to 100 g/cm 2 ) is applied. It is said to deform when applied. Further, those having a melting point of 50° C. or higher are more preferable.
Solid fats and/or semi-solid fats include plant-derived ones such as carnauba wax, Japanese wax, candelilla wax, rice bran wax, shea butter, and African mango butter, and animal-derived ones such as beeswax, shellac wax, and ivory wax. Petroleum-derived waxes include refined waxes such as paraffin wax and microcrystalline wax, and mineral-derived waxes include refined waxes such as ozokerite, ceresin and montan wax.
また、剤型によっては、前述の固形脂や半固形脂に加えて又は替えて、油性ゲル化剤を含有することも好ましい。
ここで油性ゲル化剤とは、油剤等の油性成分と相溶性のあるゲル化剤をいい、特に限定されないが、12-ヒドロキシステアリン酸、パルミチン酸デキストリン、(パルミチン酸/オクタン酸)デキストリン、ジブチルラウロイルグルタミド、ジメチコンクロスポリマー等を例示できる。
Moreover, depending on the dosage form, it is also preferable to contain an oily gelling agent in addition to or in place of the above-mentioned solid fat or semi-solid fat.
Here, the oily gelling agent refers to a gelling agent that is compatible with oily components such as oil agents, and is not particularly limited. Examples include lauroyl glutamide and dimethicone crosspolymer.
3)その他成分
本発明の化粧料には、通常固形化粧料に使用される成分を広く配合することが可能である。
例えば、有効成分としては、美白成分、抗炎症成分、植物エキス等が挙げられる。
また、界面活性剤としては、脂肪酸セッケン(ラウリン酸ナトリウム、パルミチン酸ナトリウム等)、ラウリル硫酸カリウム、アルキル硫酸トリエタノールアミンエーテル等のアニオン界面活性剤類;
塩化ステアリルトリメチルアンモニウム、塩化ベンザルコニウム、ラウリルアミンオキサイド等のカチオン界面活性剤類;
ベタイン系界面活性剤(アルキルベタイン、アミドベタイン、スルホベタイン等)、イミダゾリン系両性界面活性剤(2-ココイル-2-イミダゾリニウムヒドロキサイド-1-カルボキシエチロキシ2ナトリウム塩等)、アシルメチルタウリン等の両性界面活性剤類;
ソルビタン脂肪酸エステル類(ソルビタンモノステアレート、セスキオレイン酸ソルビタン等) 、グリセリン脂肪酸類(モノステアリン酸グリセリン等)、プロピレングリコ
ール脂肪酸エステル類(モノステアリン酸プロピレングリコール等)、硬化ヒマシ油誘導体、グリセリンアルキルエーテル、POEソルビタン脂肪酸エステル類(POEソルビタンモノオレエート、モノステアリン酸ポリオキシエチレンソルビタン等)、POEソルビット脂肪酸エステル類(POE-ソルビットモノラウレート等)、POEグリセリン脂肪酸エステル類(POE-グリセリンモノイソステアレート等)、POE脂肪酸エステル類(ポリエチレングリコールモノオレート、POEジステアレート等)、POEアルキルエーテル類(POE2-オクチルドデシルエーテル等)、POEアルキルフェニルエーテル類(POEノニルフェニルエーテル等)、プルロニック(登録商標)型類、POE・POPアルキルエーテル類(POE・POP2-デシルテトラデシルエーテル等)、テトロニック類、POEヒマシ油・硬化ヒマシ油誘導体(POEヒマシ油、POE硬化ヒマシ油等)、ショ糖脂肪酸エステル、アルキルグルコシド等の非イオン界面活性剤類;等が挙げられる。
3) Other Ingredients The cosmetic of the present invention can contain a wide range of ingredients that are commonly used in solid cosmetics.
For example, active ingredients include whitening ingredients, anti-inflammatory ingredients, plant extracts, and the like.
Examples of surfactants include anionic surfactants such as fatty acid soaps (sodium laurate, sodium palmitate, etc.), potassium lauryl sulfate, and alkyl sulfate triethanolamine ether;
cationic surfactants such as stearyltrimethylammonium chloride, benzalkonium chloride, laurylamine oxide;
Betaine-based surfactants (alkylbetaine, amidobetaine, sulfobetaine, etc.), imidazoline-based amphoteric surfactants (2-cocoyl-2-imidazolinium hydroxide-1-carboxyethyloxy disodium salt, etc.), acylmethyl taurine Amphoteric surfactants such as;
Sorbitan fatty acid esters (sorbitan monostearate, sorbitan sesquioleate, etc.), glycerin fatty acids (glyceryl monostearate, etc.), propylene glycol fatty acid esters (propylene glycol monostearate, etc.), hydrogenated castor oil derivatives, glycerin alkyl ether , POE sorbitan fatty acid esters (POE sorbitan monooleate, polyoxyethylene sorbitan monostearate, etc.), POE sorbit fatty acid esters (POE-sorbit monolaurate, etc.), POE glycerin fatty acid esters (POE-glycerin monoisostea rate, etc.), POE fatty acid esters (polyethylene glycol monooleate, POE distearate, etc.), POE alkyl ethers (POE 2-octyldodecyl ether, etc.), POE alkylphenyl ethers (POE nonylphenyl ether, etc.), Pluronic (registered trademark) types, POE/POP alkyl ethers (POE/POP 2-decyltetradecyl ether, etc.), tetronics, POE castor oil/hydrogenated castor oil derivatives (POE castor oil, POE hydrogenated castor oil, etc.), sucrose fatty acid esters, nonionic surfactants such as alkyl glucoside;
多価アルコールとしては、ポリエチレングリコール、グリセリン、1,3-ブチレングリコール、エリスリトール、ソルビトール、キシリトール、マルチトール、プロピレングリコール、ジプロピレングリコール、ジグリセリン、イソプレングリコール、1,2-ペンタンジオール、2,4-ヘキシレングリコール、1,2-ヘキサンジオール、1,2-オクタンジオール等が挙げられる。 Polyhydric alcohols include polyethylene glycol, glycerin, 1,3-butylene glycol, erythritol, sorbitol, xylitol, maltitol, propylene glycol, dipropylene glycol, diglycerin, isoprene glycol, 1,2-pentanediol, 2,4 -hexylene glycol, 1,2-hexanediol, 1,2-octanediol and the like.
増粘剤としては、グアガム、クインスシード、カラギーナン、ガラクタン、アラビアガム、ペクチン、マンナン、デンプン、キサンタンガム、カードラン、メチルセルロース、ヒドロキシエチルセルロース、カルボキシメチルセルロース、メチルヒドロキシプロピルセルロース、コンドロイチン硫酸、デルマタン硫酸、グリコーゲン、ヘパラン硫酸、ヒアルロン酸、ヒアルロン酸ナトリウム、トラガントガム、ケラタン硫酸、コンドロイチン、ムコイチン硫酸、ヒドロキシエチルグアガム、カルボキシメチルグアガム、デキストラン、ケラト硫酸、ローカストビーンガム、サクシノグルカン、カロニン酸,キチン、キトサ
ン、カルボキシメチルキチン、寒天、ポリビニルアルコール、ポリビニルピロリドン、カルボキシビニルポリマー、アルキル変性カルボキシビニルポリマー、ポリアクリル酸ナトリウム、ポリエチレングリコール、ベントナイト等が挙げられる。
Thickeners include guar gum, quince seed, carrageenan, galactan, gum arabic, pectin, mannan, starch, xanthan gum, curdlan, methylcellulose, hydroxyethylcellulose, carboxymethylcellulose, methylhydroxypropylcellulose, chondroitin sulfate, dermatan sulfate, glycogen, Heparan sulfate, hyaluronic acid, sodium hyaluronate, tragacanth gum, keratan sulfate, chondroitin, mucoitin sulfate, hydroxyethyl guar gum, carboxymethyl guar gum, dextran, kerato sulfate, locust bean gum, succinoglucan, caroninic acid, chitin, chitosan, carboxymethyl Chitin, agar, polyvinyl alcohol, polyvinylpyrrolidone, carboxyvinyl polymer, alkyl-modified carboxyvinyl polymer, sodium polyacrylate, polyethylene glycol, bentonite and the like.
紫外線吸収剤としては、パラアミノ安息香酸系紫外線吸収剤、アントラニル酸系紫外線吸収剤、サリチル酸系紫外線吸収剤、桂皮酸系紫外線吸収剤、ベンゾフェノン系紫外線吸収剤、糖系紫外線吸収剤、2-(2'-ヒドロキシ-5'-t-オクチルフェニル)ベンゾ
トリアゾール、4-メトキシ-4'-t-ブチルジベンゾイルメタン等の紫外線吸収剤類
、等が挙げられる。
Examples of UV absorbers include para-aminobenzoic acid UV absorbers, anthranilic acid UV absorbers, salicylic acid UV absorbers, cinnamic acid UV absorbers, benzophenone UV absorbers, sugar UV absorbers, 2-(2 UV absorbers such as '-hydroxy-5'-t-octylphenyl)benzotriazole, 4-methoxy-4'-t-butyldibenzoylmethane, and the like.
以下、実施例により、本発明をより詳細に説明するが、本発明の技術的範囲が例示された実施例のみに限定されることはない。 Hereinafter, the present invention will be described in more detail with reference to examples, but the technical scope of the present invention is not limited only to the illustrated examples.
<化粧料の調製>
表1に示す処方にしたがって、油中水剤型の化粧料を作製した。主に白色顔料(酸化チタン、酸化鉄)でL*値及びコントラスト比を、着色原料(青色1号、赤色227号)でa*値及びb*値を調整した。
具体的には、粉体成分を油剤成分に加えて分散混合して混合物を得た。
得られた化粧料をシャーレに厚さ1cm充填し、ハンディ分光測色計(コニカミノルタ社製、CM―600d)を用いて測色した。
また、以下の手順でコントラスト比を測定した。具体的には、得られた化粧料を隠ぺい率試験紙(「JIS K 5101-4 顔料試験方法 第4部:隠ぺい力-隠ぺい率試験紙法」に記載されるもの)にドクターブレード0.5ミルの厚さで塗布し、25℃、湿度40%で30分間静置した。その後、分光測色計を用いて、隠ぺい率試験紙の黒色部上及び白色部上の塗布膜色の各明度を測定し、黒色部上の塗布膜の明度を白色基板上の塗布膜の明度で除してさらに100を乗じて算出した値をコントラスト比とした。
<Preparation of cosmetics>
A water-in-oil type cosmetic was prepared according to the formulation shown in Table 1. The L* value and contrast ratio were adjusted mainly with white pigments (titanium oxide and iron oxide), and the a* value and b* value were adjusted with coloring materials (Blue No. 1 and Red No. 227).
Specifically, the powder component was added to the oil component and dispersed and mixed to obtain a mixture.
The obtained cosmetic was filled in a petri dish with a thickness of 1 cm, and the color was measured using a handy spectrophotometer (manufactured by Konica Minolta, CM-600d).
Also, the contrast ratio was measured by the following procedure. Specifically, the obtained cosmetic was applied to a hiding rate test paper (described in "JIS K 5101-4 Pigment Test Method Part 4: Hiding power-Hiding rate test paper method"). It was coated with a mil thickness and allowed to stand at 25° C. and 40% humidity for 30 minutes. After that, using a spectrophotometer, measure the brightness of each coating film color on the black part and the white part of the opacity test paper, and measure the brightness of the coating film on the black part with the brightness of the coating film on the white substrate. The contrast ratio was calculated by dividing by 100 and then multiplying by 100.
また、各化粧料を手の甲に100mgずつ均一に塗布して得た化粧膜について、熟練の評価者が以下の基準で評価した。
◎:肌全体が明るく感じ、全体の色味が均一になり、透明感があり、ツヤがある。
〇:肌全体が明るく感じ、全体の色味が均一であるが、透明感がやや足りない。
△:肌全体が明るく感じるが不自然な色味である、又は肌全体が暗くなるが全体の色味が均一である。
×:肌全体が暗くなり、不自然な色味
結果を表1~2に示す。
In addition, the cosmetic film obtained by uniformly applying 100 mg of each cosmetic to the back of the hand was evaluated by an experienced evaluator according to the following criteria.
⊚: The skin as a whole feels bright, the overall color is uniform, and the skin has transparency and gloss.
◯: The skin as a whole feels bright, and the overall color tone is uniform, but the transparency is slightly insufficient.
Δ: The whole skin feels bright but the color is unnatural, or the whole skin becomes dark but the overall color is uniform.
x: The skin as a whole becomes darker, giving an unnatural tint. The results are shown in Tables 1 and 2.
Claims (5)
コントラスト比が0.38~0.65である、化粧料。 having a color difference with an L* value of 68 or more, an a* value of 7.5 to 12.0, and a b* value of −0.5 to 2.0;
A cosmetic having a contrast ratio of 0.38 to 0.65.
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