JP2022109855A - Milk solid-containing transparently bottled coffee beverage - Google Patents

Milk solid-containing transparently bottled coffee beverage Download PDF

Info

Publication number
JP2022109855A
JP2022109855A JP2021119301A JP2021119301A JP2022109855A JP 2022109855 A JP2022109855 A JP 2022109855A JP 2021119301 A JP2021119301 A JP 2021119301A JP 2021119301 A JP2021119301 A JP 2021119301A JP 2022109855 A JP2022109855 A JP 2022109855A
Authority
JP
Japan
Prior art keywords
milk
mass
coffee
flavor
fat
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP2021119301A
Other languages
Japanese (ja)
Inventor
康友 伊藤
Yasutomo Ito
太朗 矢野
Taro Yano
麻里 武藤
Mari Futo
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Suntory Holdings Ltd
Original Assignee
Suntory Holdings Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Suntory Holdings Ltd filed Critical Suntory Holdings Ltd
Publication of JP2022109855A publication Critical patent/JP2022109855A/en
Pending legal-status Critical Current

Links

Landscapes

  • Tea And Coffee (AREA)

Abstract

PROBLEM TO BE SOLVED: To provide a milk solid-containing transparently bottled coffee beverage that mitigates deterioration of a flavor caused by light radiation.
SOLUTION: A beverage contains 2.0-3.0 mass% of milk solids and 2.1-4.5 mass% of sucrose, where a mass ratio of non-fat milk solids/milk fat is adjusted to 1.4-3.0.
SELECTED DRAWING: None
COPYRIGHT: (C)2022,JPO&INPIT

Description

本発明は、乳固形分を含有する透明容器詰めコーヒー飲料に関する。特に本発明は、光照射による香味の劣化が低減された乳固形分含有透明容器詰めコーヒー飲料に関する。 TECHNICAL FIELD The present invention relates to a coffee beverage packed in a transparent container containing milk solids. In particular, the present invention relates to a milk solids-containing transparent container-packaged coffee beverage in which deterioration of flavor due to light irradiation is reduced.

コーヒー飲料は嗜好品として広く愛好されており、抽出したてのコーヒーだけでなく、缶や、PETボトル、紙容器等、幅広い飲料形態が展開されている。中でもPETボトルは、再栓可能であることから利便性が高く、近年販売数量も大きく伸びている。しかし、透明なPETボトルは光を透過させるため、コーヒー飲料に光が照射されることになり、他の飲料形態よりも香味の劣化等の品質面の問題を生じることがある。特に、乳成分を含有する飲料においては、光照射による香味の劣化が著しいことが知られている。これは、乳中に含まれるリボフラビンが光照射により励起され、乳成分であるタンパク質や脂質の酸化を促進し、その結果として香味の劣化が生じるためであると言われている。 Coffee beverages are widely loved as luxury goods, and not only freshly brewed coffee, but also in a wide range of beverage forms such as cans, PET bottles, and paper containers. Among them, PET bottles are highly convenient because they can be re-plugged, and their sales volume has been greatly increasing in recent years. However, since a transparent PET bottle allows light to pass through, the coffee beverage is exposed to light, which may cause quality problems such as deterioration of flavor, compared to other beverage types. In particular, it is known that the flavor of beverages containing milk components is remarkably deteriorated by light irradiation. It is said that this is because riboflavin contained in milk is excited by light irradiation and promotes oxidation of proteins and lipids, which are milk components, resulting in deterioration of flavor.

飲料における光照射による香味の劣化を抑制する技術として、乳含有酸性飲料では、アスコルビン酸、コレカルシフェロール及びフラボノールから選ばれた少なくとも2種以上を含有させることにより、リボフラビンの光の照射による励起を抑制して品質の劣化を防止する方法(特許文献1)が開示されており、また、乳飲料について、トコフェロールまたはその誘導体とアスコルビン酸またはその誘導体および/またはカロテノイドとから成る成分、もしくはそれらの成分とトレハロースを合わせた成分を含有させることで、光照射下での劣化を抑制し、保存安定性を向上させる方法(特許文献2)が開示されている。 As a technique for suppressing the deterioration of the flavor of beverages due to light irradiation, in milk-containing acidic beverages, at least two or more selected from ascorbic acid, cholecalciferol, and flavonol are added to reduce the excitation of riboflavin by light irradiation. A method for suppressing and preventing quality deterioration (Patent Document 1) is disclosed, and for milk beverages, a component consisting of tocopherol or a derivative thereof and ascorbic acid or a derivative thereof and / or a carotenoid, or components thereof and trehalose to suppress deterioration under light irradiation and improve storage stability (Patent Document 2).

また、乳成分由来の劣化臭に関して、特許文献3には、牛乳を含有するコーヒーや紅茶飲料をホットベンダーのような加温状態で保存した場合に発生する劣化臭の原因について検討したところ、乳脂肪由来の低中級脂肪酸、とくに炭素数10以下の脂肪酸が加温保存中に分解、遊離し、乳特有の劣化臭となることを発見したことが記載されている。また、特許文献4には、脂肪分が多い乳製品では、特にラジカル化された過酸化脂質が多く発生しやすいために、硫化化合物の発生量が多くなり加熱劣化臭が発生しやすいことが記載されている。 In addition, regarding the deterioration odor derived from milk components, Patent Document 3 describes the cause of the deterioration odor that occurs when coffee or tea beverages containing milk are stored in a heated state such as a hot vendor. It describes the discovery that fat-derived low-middle-class fatty acids, especially fatty acids with 10 or less carbon atoms, are decomposed and liberated during storage under heating, resulting in a degraded odor peculiar to milk. In addition, Patent Document 4 describes that dairy products with a high fat content are particularly likely to generate a large amount of radicalized lipid peroxide, so that the amount of sulfide compounds generated increases and the smell of heat deterioration tends to occur. It is

特開平3-272643号公報JP-A-3-272643 特開2002-78447号公報JP-A-2002-78447 特開平9-37713号公報JP-A-9-37713 特開2008-295335号公報JP 2008-295335 A

本発明者らは、コーヒー飲料において、乳固形分がある一定量以上含まれ、かつショ糖量が一定範囲内である場合に、光照射による香味の劣化が特に強く感じられることを見出した。本発明は、上記のような香味の劣化が強く感じられやすい条件を有し、かつ、透明容器に充填されることで光照射を受けやすい状態にある乳固形分含有コーヒー飲料において、光照射下での香味の劣化を低減し、保存時の香味劣化の少ないコーヒー飲料を提供することを課題とするものである。 The present inventors have found that when a coffee beverage contains a certain amount or more of milk solids and the amount of sucrose is within a certain range, the deterioration of flavor due to light irradiation is felt particularly strongly. The present invention provides a milk solids-containing coffee beverage that has the above-described conditions where the deterioration of the flavor is likely to be strongly felt, and is in a state where it is easily exposed to light irradiation by being filled in a transparent container. An object of the present invention is to provide a coffee beverage in which the deterioration of flavor during storage is reduced and the flavor is less deteriorated during storage.

本発明者らは、上記課題を解決するために鋭意検討した結果、乳固形分及びショ糖含有量をある一定量に制御した上で、無脂乳固形分/乳脂肪分の質量比を一定範囲内の値とすることで、光による香味の劣化が抑えられ、すっきりと飲みやすい味わいの乳固形分含有透明容器詰めコーヒー飲料が得られることを見出した。通常、特許文献3及び4に記載されるように、乳成分を含有する食品における劣化臭は、乳脂肪分の影響が大きいと言われている。これに対し、本発明者らは、乳固形分及びショ糖含有量をある一定範囲の量に制御したコーヒー飲料については、意外にも、無脂乳固形分/乳脂肪分の質量比を3.0以下とする、すなわち乳脂肪分の無脂乳固形分に対する配合割合を一定程度確保した方が、光照射による乳成分の香味の劣化が低減されることを見出した。 The present inventors have made intensive studies to solve the above problems, and found that after controlling the milk solids content and sucrose content to a certain amount, the mass ratio of non-fat milk solids / milk fat is constant It was found that by setting the value within the range, deterioration of the flavor due to light is suppressed, and a milk solids-containing transparent packaged coffee beverage with a refreshing and easy-to-drink taste can be obtained. Generally, as described in Patent Documents 3 and 4, it is said that milk fat content has a great influence on deterioration odors in foods containing milk components. On the other hand, the present inventors surprisingly found that the milk solids content and sucrose content were controlled within a certain range, and the mass ratio of non-fat milk solids / milk fat was 3. 0.0 or less, that is, by ensuring a certain ratio of milk fat to non-fat milk solids, deterioration of flavor of milk components due to light irradiation is reduced.

本発明は、これに限定されるものではないが、以下の態様を包含する。
[1]乳固形分を含有する透明容器詰めコーヒー飲料であって、
(a)乳固形分が2.0~3.0質量%であり、
(b)ショ糖を2.1~4.5質量%含み、
(c)無脂乳固形分/乳脂肪分(質量比)が1.4~3.0である、
上記コーヒー飲料。
[2](c)無脂乳固形分/乳脂肪分(質量比)が2.0~3.0である、[1]に記載の透明容器詰めコーヒー飲料。
[3](d)コーヒー固形分が0.5~1.2質量%である、[1]又は[2]に記載の透明容器詰めコーヒー飲料。
The present invention includes, but is not limited to, the following aspects.
[1] A coffee beverage packed in a transparent container containing milk solids,
(a) milk solids content is 2.0 to 3.0% by mass,
(b) contains 2.1 to 4.5% by mass of sucrose,
(c) non-fat milk solids/milk fat content (mass ratio) is 1.4 to 3.0,
Coffee drink above.
[2] The coffee beverage packed in a transparent container according to [1], wherein (c) non-fat milk solids/milk fat (mass ratio) is 2.0 to 3.0.
[3] (d) The coffee beverage packed in a transparent container according to [1] or [2], wherein the coffee solid content is 0.5 to 1.2% by mass.

本発明により、光照射による香味の劣化が抑えられ、すっきりと飲みやすい味わいの乳固形分含有コーヒー飲料を提供することが可能となる。また、本発明のコーヒー飲料は、光照射による香味の劣化が抑えられていることから、光照射を受けやすい状態であるPETボトルのような透明容器に充填して保管及び販売した場合でも、乳成分由来の不快な劣化香味が感じられにくいという利点がある。 According to the present invention, it is possible to provide a milk solids-containing coffee beverage with a refreshing and easy-to-drink taste, in which the deterioration of the flavor due to light irradiation is suppressed. In addition, since the deterioration of the flavor due to light irradiation is suppressed, the coffee beverage of the present invention can be stored and sold in a transparent container such as a PET bottle, which is easily exposed to light irradiation. There is an advantage that the unpleasant deteriorated flavor derived from the ingredients is hardly felt.

(コーヒー飲料)
本発明は、乳固形分が2.0~3.0質量%であり、ショ糖含有量が2.1~4.5質量%であり、無脂乳固形分/乳脂肪分の質量比が1.4~3.0である透明容器詰め乳固形分含有コーヒー飲料である。
(coffee drink)
The present invention has a milk solids content of 2.0 to 3.0% by mass, a sucrose content of 2.1 to 4.5% by mass, and a non-fat milk solids/milk fat mass ratio of It is a milk solids-containing coffee beverage packed in a transparent container with a ratio of 1.4 to 3.0.

本発明でいう「コーヒー飲料」とは、コーヒー分を原料として使用し、加熱殺菌処理がなされた飲料製品のことをいう。製品の種類は特に限定されないが、1977年に認定された「コーヒー飲料等の表示に関する公正競争規約」の定義である「コーヒー」、「コーヒー飲料」、及び「コーヒー入り清涼飲料」が主に挙げられる。また、コーヒー分を原料とした飲料においても、乳固形分が3.0質量%以上のものは「飲用乳の表示に関する公正競争規約」の適用を受け、「乳飲料」として取り扱われるが、これも、本発明におけるコーヒー飲料とする。ここで、コーヒー分とは、コーヒー豆由来の成分を含有するものをいい、例えば、コーヒー抽出液、即ち、焙煎、粉砕されたコーヒー豆を水や温水などを用いて抽出した溶液が挙げられる。また、コーヒー抽出液を濃縮したコーヒーエキス、コーヒー抽出液を乾燥したインスタントコーヒーなど、また、それらを水や温水などで適量に調整した溶液も、コーヒー分として挙げられる。 The term "coffee beverage" as used in the present invention refers to a beverage product that uses coffee as a raw material and is heat sterilized. The types of products are not particularly limited, but the main ones are “coffee,” “coffee beverages,” and “soft drinks containing coffee,” which are defined in the “Fair Competition Code Concerning Labeling of Coffee Beverages, etc.” approved in 1977. be done. In addition, coffee-based beverages with a milk solids content of 3.0% by mass or more are subject to the Fair Competition Code Concerning Labeling of Drinking Milk and are treated as "milk beverages." is also regarded as a coffee beverage in the present invention. Here, the coffee component refers to a substance containing components derived from coffee beans, and examples thereof include a coffee extract, that is, a solution obtained by extracting roasted and ground coffee beans using water, hot water, or the like. . In addition, coffee extracts obtained by concentrating coffee extracts, instant coffees obtained by drying coffee extracts, and solutions obtained by adjusting these with water or warm water in appropriate amounts are also included as coffee components.

本発明のコーヒー飲料に用いるコーヒー豆の栽培樹種は、特に限定されない。コーヒー豆の一般的な樹種としては、アラビカ種、ロブスタ種、リベリカ種などが挙げられる。これらをブレンドして用いてもよい。味わいがよい点から、アラビカ種を単独でまたはブレンドして用いることは好ましい。また、産地名も特に限定されず、例えば、モカ、ブラジ
ル、コロンビア、グアテマラ、ブルーマウンテン、コナ、マンデリン、キリマンジャロなどが挙げられるが、いずれでもよいし、これら以外のものであってもよい。コーヒー豆は1種でもよいし、複数種をブレンドして用いてもよい。コーヒー豆の焙煎方法に関して、焙煎温度や焙煎環境に特に制限はなく、通常の方法を採用できる。さらに、その焙煎コーヒー豆からの抽出方法についても何ら制限はなく、例えば焙煎コーヒー豆を粗挽き、中挽き、細挽き等に粉砕した粉砕物から水や温水(0~200℃)を用いて抽出する方法が挙げられる。抽出方法は、ドリップ式、サイフォン式、ボイリング式、ジェット式、連続式などを挙げることができ、いずれを用いてもよい。
The cultivar of coffee beans used for the coffee beverage of the present invention is not particularly limited. Common tree species of coffee beans include Arabica, Robusta, and Liberica. These may be blended and used. It is preferable to use Arabica alone or in a blend because of its good taste. Also, the name of the place of production is not particularly limited, and examples thereof include Mocha, Brazil, Colombia, Guatemala, Blue Mountain, Kona, Mandelin, and Kilimanjaro. One type of coffee beans may be used, or a plurality of types may be blended and used. Regarding the method of roasting coffee beans, there are no particular restrictions on the roasting temperature or the roasting environment, and ordinary methods can be used. Furthermore, there are no restrictions on the extraction method from the roasted coffee beans. a method of extracting Extraction methods include drip, siphon, boiling, jet, and continuous methods, and any of them may be used.

(乳固形分)
本発明でいう「乳固形分」とは、無脂乳固形分と乳脂肪分の総量をいう。本発明の飲料に用いられる乳固形分は、飲料にミルク風味やミルク感を付与するために添加される乳原料由来の成分であり、その種類は特に制限されない。例えば、乳、全脂乳、脱脂乳、濃縮乳、脱脂濃縮乳、練乳、脱脂練乳、全脂粉乳、脱脂粉乳、生クリーム、バター、バターオイル、バターミルク、バターミルクパウダー、カゼイン、ホエー、チーズなどの乳原料由来の乳固形分が挙げられる。乳固形分の由来となる乳原料は、1種類であってもよく、2種類以上の混合物であってもよい。
(milk solids)
The term "milk solids" as used in the present invention means the total amount of non-fat milk solids and milk fat. The milk solids used in the beverage of the present invention are components derived from milk raw materials that are added to impart a milky flavor and milk feeling to the beverage, and the type thereof is not particularly limited. For example, milk, whole milk, skimmed milk, concentrated milk, skimmed concentrated milk, condensed milk, skimmed condensed milk, whole milk powder, skim milk powder, fresh cream, butter, butter oil, buttermilk, buttermilk powder, casein, whey, cheese Milk solids derived from dairy raw materials such as. The milk raw materials from which the milk solids are derived may be of one type or may be a mixture of two or more types.

本発明の乳固形分含有コーヒー飲料は、2.0質量%以上の乳固形分を含有する。乳固形分が少ないと光による香味の劣化という課題が顕在化しにくい。この点から、本発明が対象とするコーヒー飲料の乳固形分は、好ましくは2.1質量%以上であり、より好ましくは2.2質量%以上であり、さらに好ましくは2.3質量%以上である。また、飲料の嗜好性の観点からは、乳固形分は3.0質量%以下であり、好ましくは2.9質量%以下であり、さらに好ましくは2.8質量%以下である。乳固形分は、飲料中の乳成分を一般的な乾燥法(凍結乾燥、蒸発乾固等)を用いて乾燥させて水分を除いた後の乾固物の質量に相当する。 The milk solids-containing coffee beverage of the present invention contains 2.0% by mass or more of milk solids. If the milk solid content is low, the problem of deterioration of flavor due to light is less likely to emerge. From this point, the milk solids content of the coffee beverage targeted by the present invention is preferably 2.1% by mass or more, more preferably 2.2% by mass or more, and still more preferably 2.3% by mass or more. is. Moreover, from the viewpoint of palatability of the beverage, the milk solid content is 3.0% by mass or less, preferably 2.9% by mass or less, and more preferably 2.8% by mass or less. The milk solids content corresponds to the mass of the dried product after drying the milk component in the beverage using a general drying method (freeze-drying, evaporation to dryness, etc.) to remove water.

(ショ糖)
本発明の乳固形分含有コーヒー飲料は、2.1~4.5質量%のショ糖を含有する。本発明者らは、乳固形分含有コーヒー飲料において、乳固形分が2.0質量以上であり、ショ糖含有量が2.1~4.5質量%の範囲である場合に、光照射による香味の劣化の問題が生じやすくなることを見出した。また、この香味の劣化は、後述する無脂乳固形分/乳脂肪分の質量比を3.0以下とすることにより低減できることを見出した。
(sucrose)
The milk solids-containing coffee beverage of the present invention contains 2.1-4.5% by mass of sucrose. The present inventors found that in a milk solids-containing coffee beverage, when the milk solids content is 2.0 mass or more and the sucrose content is in the range of 2.1 to 4.5 mass%, by light irradiation It was found that the problem of deterioration of flavor tends to occur. In addition, the inventors have found that this deterioration in flavor can be reduced by setting the mass ratio of non-fat milk solids/milk fat to 3.0 or less.

本発明のコーヒー飲料中のショ糖含有量は、上述の通り、2.1~4.5質量%であるが、嗜好性の観点からは、2.3質量%以上が好ましく、2.5質量%以上がより好ましく、2.7質量%以上がさらに好ましい。ショ糖を配合することにより、乳固形分含有コーヒー飲料に甘味が付与され、味の厚みが増す。ショ糖含有量が4.5質量%以下の場合には、甘味、厚みが少ないことに伴って、乳固形分含有コーヒー飲料の光照射による香味の劣化という課題がより顕著となる。本発明の効果をより顕著に享受できる観点から、ショ糖含有量は4.3質量%以下が好ましく、4.1質量%以下がより好ましく、3.9質量%以下がさらに好ましい。ショ糖の含有量は、例えば後述する実施例に記載するように、高速液体クロマトグラフィーを用いて測定することが出来る。
(その他の甘味成分)
ブドウ糖は、加温殺菌や高温状態の保存によってpH低下による風味の変化を引き起こすことがあるから、本発明のコーヒー飲料は、嗜好性の観点からブドウ糖の配合量が少ないことが好ましい。具体的には0.50質量%以下が好ましく、0.30質量%以下がより好ましく、0.10質量%以下がさらに好ましく、0.05質量%以下がさらに好ましく、0.02質量%以下がさらに好ましい。また、ブドウ糖を配合しないことが最も好ましい。ブドウ糖の含有量は、例えば後述する実施例に記載するように、高速液体クロマト
グラフィーを用いて測定することが出来る。
コーヒー飲料に甘味を付与する手段として、糖類以外には、アセスルファムKやステビア抽出物などの高甘味度甘味料が挙げられる。これら高甘味度甘味料は、特有の苦みや雑味を有し、配合するとコーヒー飲料の味わいを損ねることがあるため、本発明のコーヒー飲料は、嗜好性の観点から、高甘味度甘味料の配合量が少ないことが好ましい。高甘味度甘味料の配合量は、0.01質量%以下が好ましく、0.008質量%以下がさらに好ましく、0.005質量%以下がさらに好ましい。また、高甘味度甘味料を配合しないことが最も好ましい。例えば、アセスルファムKの配合量は、0.01質量%以下が好ましく、0.008質量%以下がより好ましく、0.005質量%以下がさらに好ましい。また、アセスルファムKを配合しないことが最も好ましい。アセスルファムKの含有量は、例えば高速液体クロマトグラフィーにより測定することが出来る。ステビア抽出物の配合量は、0.001質量%以下が好ましく、0.0008質量%以下がより好ましく、0.0005質量%以下がさらに好ましく、0.0001質量%以下がさらに好ましく、0.00005質量%以下がさらに好ましい。また、ステビア抽出物を配合しないことが最も好ましい。
As described above, the sucrose content in the coffee beverage of the present invention is 2.1 to 4.5% by mass, but from the viewpoint of palatability, it is preferably 2.3% by mass or more, and 2.5% by mass. % or more is more preferable, and 2.7% by mass or more is even more preferable. By blending sucrose, sweetness is imparted to the milk solids-containing coffee beverage, and the depth of taste is increased. When the sucrose content is 4.5% by mass or less, the problem of deterioration of the flavor of the milk solids-containing coffee beverage due to light irradiation becomes more pronounced due to less sweetness and less thickness. The sucrose content is preferably 4.3% by mass or less, more preferably 4.1% by mass or less, and even more preferably 3.9% by mass or less, from the viewpoint of being able to enjoy the effects of the present invention more remarkably. The content of sucrose can be measured using high performance liquid chromatography, for example, as described in Examples below.
(Other sweetening ingredients)
Glucose may cause a change in flavor due to a decrease in pH due to heat sterilization or storage at high temperatures. Therefore, the coffee beverage of the present invention preferably contains a small amount of glucose from the viewpoint of palatability. Specifically, it is preferably 0.50% by mass or less, more preferably 0.30% by mass or less, still more preferably 0.10% by mass or less, further preferably 0.05% by mass or less, and 0.02% by mass or less. More preferred. Moreover, it is most preferable not to mix glucose. The glucose content can be measured using high performance liquid chromatography, for example, as described in the examples below.
In addition to sugars, high-intensity sweeteners such as acesulfame K and stevia extract can be used as a means of imparting sweetness to coffee beverages. These high-intensity sweeteners have a unique bitterness and unpleasant taste, and when blended, they may impair the taste of the coffee beverage. A small amount is preferred. The amount of the high-intensity sweetener is preferably 0.01% by mass or less, more preferably 0.008% by mass or less, and even more preferably 0.005% by mass or less. Moreover, it is most preferable not to mix a high-intensity sweetener. For example, the content of Acesulfame K is preferably 0.01% by mass or less, more preferably 0.008% by mass or less, and even more preferably 0.005% by mass or less. Moreover, it is most preferable not to mix acesulfame K. The content of acesulfame K can be measured, for example, by high performance liquid chromatography. The content of the stevia extract is preferably 0.001% by mass or less, more preferably 0.0008% by mass or less, even more preferably 0.0005% by mass or less, further preferably 0.0001% by mass or less, and 0.00005% by mass. % by mass or less is more preferable. Moreover, it is most preferable not to mix a stevia extract.

(無脂乳固形分/乳脂肪分)
本発明の乳含有コーヒー飲料の無脂乳固形分/乳脂肪分(質量比)は1.4~3.0である。本発明者らは、乳固形分含有コーヒー飲料において、乳固形分が2.0質量以上であり、ショ糖含有量が2.1~4.5質量%の範囲である場合に、光照射による香味の劣化の問題が生じやすくなることを見出し、また、この香味の劣化を、無脂乳固形分/乳脂肪分の質量比を3.0以下とすることにより低減できることを見出した。無脂乳固形分/乳脂肪分の質量比は、香味劣化の抑制の観点からは、2.9以下が好ましく、2.8以下がより好ましく、2.7以下がさらに好ましい。一方、乳脂肪分の割合が大きすぎると脂肪分特有のもたつきが発生し、飲料のすっきりとした味わいが失われるため、嗜好性の観点からは、上記質量比は、1.6以上が好ましく、1.8以上がより好ましく、2.0以上がさらに好ましく、2.2以上がさらに好ましく、2.4以上がさらに好ましく、2.5以上がさらに好ましい。通常、乳成分を含有する食品における劣化臭は、乳脂肪分の影響が大きいと言われているが、本発明者らは、意外にも、乳固形分及びショ糖含有量をある一定範囲の量に制御したコーヒー飲料については、無脂乳固形分/乳脂肪分の質量比を3.0以下とする、すなわち乳脂肪分の無脂乳固形分に対する配合割合を一定程度確保した方が、光照射による香味の劣化が低減されることを見出した。
(Non-fat milk solids/milk fat)
The non-fat milk solid content/milk fat content (mass ratio) of the milk-containing coffee beverage of the present invention is 1.4 to 3.0. The present inventors found that in a milk solids-containing coffee beverage, when the milk solids content is 2.0 mass or more and the sucrose content is in the range of 2.1 to 4.5 mass%, by light irradiation The present inventors have found that the problem of deterioration of flavor tends to occur, and that this deterioration of flavor can be reduced by setting the mass ratio of non-fat milk solids/milk fat to 3.0 or less. The mass ratio of non-fat milk solids/milk fat is preferably 2.9 or less, more preferably 2.8 or less, and even more preferably 2.7 or less, from the viewpoint of suppressing flavor deterioration. On the other hand, if the proportion of milk fat is too large, the sluggishness peculiar to the fat content occurs and the refreshing taste of the beverage is lost, so from the viewpoint of palatability, the mass ratio is preferably 1.6 or more. It is more preferably 1.8 or more, still more preferably 2.0 or more, still more preferably 2.2 or more, still more preferably 2.4 or more, and even more preferably 2.5 or more. Normally, it is said that the deterioration odor in foods containing milk components is greatly affected by the milk fat content, but surprisingly, the present inventors have found that the milk solid content and sucrose content are controlled within a certain range. For coffee beverages with a controlled amount, the mass ratio of non-fat milk solids / milk fat is 3.0 or less, that is, it is better to ensure a certain ratio of milk fat to non-fat milk solids. It was found that deterioration of flavor due to light irradiation is reduced.

(透明容器詰め飲料)
本発明の飲料は、透明容器に充填されてなる飲料である(本明細書中、透明容器詰め飲料とも称する)。透明容器詰め飲料は、内容物を目視でき消費者への安心感を与えることができる。ここで、本明細書において「透明容器」とは、容器に充填等された飲料を外部から視認できる容器を意味する。透明容器の概念には、容器の一部分においてその外部から内容物を視認できることも包含される。透明容器としては、例えば可視光700nmにおける透過率が40%以上、好ましくは50%以上となる透明領域を有する容器を挙げることができる。具体的には、透明プラスチックボトルやカップおよび透明ガラス瓶が例示でき、特に透明PETボトルが本発明で好適に用いられる。容器の色は限定されないが、無色のものが好ましい。容量も特に限定されないが、160~600mLが好ましく、250mL以上が好ましい。
(Beverages packed in transparent containers)
The beverage of the present invention is a beverage packed in a transparent container (also referred to herein as a transparent container-packed beverage). Beverages packed in transparent containers can give consumers a sense of security because the contents can be visually checked. Here, the term "transparent container" as used herein means a container in which the beverage filled in the container can be visually recognized from the outside. The concept of a transparent container also includes the ability to view the contents from the outside of a portion of the container. As the transparent container, for example, a container having a transparent region having a transmittance of 40% or more, preferably 50% or more at visible light of 700 nm can be used. Specifically, transparent plastic bottles, cups, and transparent glass bottles can be exemplified, and transparent PET bottles are particularly suitable for use in the present invention. Although the color of the container is not limited, it is preferably colorless. Although the volume is not particularly limited, 160 to 600 mL is preferable, and 250 mL or more is preferable.

また、透明容器は容器の一部または全部がフィルム等で覆われていてもよい。例えば、内容表示用のラベル・印刷部分は不透明あるいは半透明でそれ以外の部分が透明な容器や、意匠性を有する透明部分・不透明部分が複数箇所で異なるように組み合わされている容器、看視窓程度の大きさの透明部分のみを有する不透明容器など、内容物が視認できる透明部分が存在する限りにおいてその透明領域については限定されない。 Also, the transparent container may be partially or wholly covered with a film or the like. For example, labels for content display, containers where the printed part is opaque or semi-transparent and other parts are transparent, containers where transparent parts and opaque parts with design properties are combined in different ways in multiple places, The transparent region is not limited as long as there is a transparent portion through which the contents can be visually recognized, such as an opaque container having only a transparent portion with a window size.

本発明のコーヒー飲料は、加熱殺菌処理を経て得られる閉栓された透明容器詰め飲料である。加熱殺菌の条件は、例えば、食品衛生法に定められた条件と同等の効果が得られる方法を選択することができ、具体的には、60~150℃で1秒間~60分間とすることができる。容器として耐熱性容器(ガラス等)を使用する場合には、レトルト殺菌(110~140℃、1~数十分間)を行うこともできる。また、容器として非耐熱性容器(PETボトル等)を用いる場合は、例えば、調合液を予めプレート式熱交換器等で高温短時間殺菌(UHT殺菌:110~150℃、1~数十秒間)し、一定の温度まで冷却した後、容器に充填することができる。 The coffee beverage of the present invention is a beverage packed in a sealed transparent container obtained through heat sterilization. For the heat sterilization conditions, for example, a method that provides the same effect as the conditions stipulated in the Food Sanitation Law can be selected. Specifically, it can be 60 to 150 ° C. for 1 second to 60 minutes. can. When a heat-resistant container (glass, etc.) is used as the container, retort sterilization (110 to 140° C., 1 to several tens of minutes) can also be performed. In addition, when using a non-heat-resistant container (such as a PET bottle) as the container, for example, the prepared liquid is sterilized in advance with a plate-type heat exchanger or the like for a short time at high temperature (UHT sterilization: 110 to 150 ° C., 1 to several tens of seconds). and after cooling to a certain temperature, the container can be filled.

(コーヒー固形分)
本発明のコーヒー飲料におけるコーヒー分の含有量は、「コーヒー固形分」として表される。本発明において「コーヒー固形分」とは、コーヒー分を一般的な乾燥法(凍結乾燥、蒸発乾固など)を用いて乾燥させて水分を除いた後の、乾固物の質量のことをいう。すなわち、コーヒー飲料におけるコーヒー固形分は、コーヒー飲料に含まれ得る可溶性固形分のうち、乳分、甘味成分、pH調整剤、香料等のコーヒー豆に由来しない成分を除いた固形分に相当する。また、コーヒー飲料の原料の1つ(コーヒー分)として用いられ得るコーヒー抽出液中のコーヒー固形分は、コーヒー抽出液のBrix(%)に相当すると考えることができ、当該Brixは、糖度計(糖用屈折計)を用いて測定することができる。
(Coffee solids)
The coffee content in the coffee beverage of the present invention is expressed as "coffee solids". In the present invention, "coffee solid content" refers to the mass of the dry matter after drying the coffee content using a general drying method (freeze drying, evaporation to dryness, etc.) to remove water. . That is, the coffee solids content in the coffee beverage corresponds to the solid content of the soluble solids content that can be contained in the coffee beverage, excluding components not derived from coffee beans such as milk, sweeteners, pH adjusters, and flavorings. In addition, the coffee solids content in the coffee extract that can be used as one of the raw materials of the coffee beverage (coffee content) can be considered to correspond to the Brix (%) of the coffee extract, and the Brix is the saccharimeter ( Refractometer for sugar) can be used for measurement.

本発明のコーヒー飲料におけるコーヒー固形分は0.5~1.2重量%である。嗜好性の観点から、コーヒー固形分は好ましくは0.6質量%以上、より好ましくは0.7質量%以上、さらに好ましくは0.8質量%以上である。コーヒー飲料の光照射による香味劣化は、コーヒー分と乳固形分が相まって発生するが、乳固形分の方がコーヒー分よりも香味劣化に対する寄与度は大きい。そのため、コーヒー固形分が少ない方が、光照射による劣化香味という課題が顕在化しやすい。本発明の効果をより顕著に享受できる観点からは、コーヒー固形分は好ましくは1.1質量%以下、より好ましくは1.0質量%以下、さらに好ましくは0.9質量%以下である。 The coffee solids content in the coffee beverage of the present invention is 0.5-1.2% by weight. From the viewpoint of palatability, the coffee solids content is preferably 0.6% by mass or more, more preferably 0.7% by mass or more, and even more preferably 0.8% by mass or more. Flavor deterioration of coffee beverages due to light irradiation occurs due to the combination of the coffee content and the milk solid content, but the milk solid content contributes more to the flavor deterioration than the coffee content. Therefore, when the solid content of coffee is low, the problem of degraded flavor due to light irradiation tends to become apparent. From the viewpoint of being able to enjoy the effects of the present invention more remarkably, the coffee solids content is preferably 1.1% by mass or less, more preferably 1.0% by mass or less, and even more preferably 0.9% by mass or less.

(その他の成分)
本発明のコーヒー飲料は、乳化剤を含んでいてもよい。乳化剤の例としては、ショ糖脂肪酸エステル、グリセリン脂肪酸エステル、レシチン、リゾレシチン、ソルビタン脂肪酸エステル、ポリグリセリン脂肪酸エステル等、公知の乳化剤を挙げることができる。中でもショ糖脂肪酸エステルを好ましく選択することができる。
コーヒー飲料には、乳脂肪の代替としてヤシ油、パーム油、ヒマワリ油などの植物油脂が使用されることがあるが、植物油脂特有の香りがコーヒー飲料に付与されてしまい、味わいを損ねる可能性があるため、本発明のコーヒー飲料は、植物油脂の含有量は少ないほうが望ましい。具体的には2.0質量%以下が好ましく、1.5質量%以下がより好ましく、1.0質量%以下がさらに好ましく、0.5質量%以下がさらに好ましく、0.3質量%以下がさらに好ましい。また、植物油脂を配合しないことが最も好ましい。
(other ingredients)
The coffee beverage of the present invention may contain emulsifiers. Examples of emulsifiers include known emulsifiers such as sucrose fatty acid esters, glycerin fatty acid esters, lecithin, lysolecithin, sorbitan fatty acid esters and polyglycerin fatty acid esters. Among them, sucrose fatty acid ester can be preferably selected.
Vegetable oils such as coconut oil, palm oil, and sunflower oil are sometimes used in coffee beverages as a substitute for milk fat, but the aroma peculiar to vegetable oils and fats is imparted to coffee beverages, which may impair the taste. Therefore, it is desirable that the coffee beverage of the present invention contains as little vegetable oil as possible. Specifically, it is preferably 2.0% by mass or less, more preferably 1.5% by mass or less, still more preferably 1.0% by mass or less, further preferably 0.5% by mass or less, and 0.3% by mass or less. More preferred. Moreover, it is most preferable not to mix vegetable oil.

本発明のコーヒー飲料は、乳固形分を含んでいるため、pHが酸性領域になると、乳中の主要たんぱく質であるカゼインが凝集、沈殿する。したがって、凝集及び沈殿の抑制のためには、本発明に係る飲料のpH(20℃)は好ましくは5.0~8.0であり、より好ましくは5.5~8.0であり、より好ましくは5.8~7.5である。pHをこの範囲にするために、コーヒー飲料に一般的に用いることができるpH調整剤を配合してもよい。pH調整剤の例としては、これに限定されないが、重曹が挙げられる。また、酸味料は配合しないことが好ましい。ここで、本明細書におけるpHとは、液状飲料100mLを300mLのビーカーに量り取り、20℃に温度調整をしてpHメータにより測定する
値をいう。
Since the coffee beverage of the present invention contains milk solids, casein, which is a major protein in milk, aggregates and precipitates when the pH reaches an acidic range. Therefore, in order to suppress aggregation and precipitation, the pH (20 ° C.) of the beverage according to the present invention is preferably 5.0 to 8.0, more preferably 5.5 to 8.0, and more It is preferably 5.8 to 7.5. In order to adjust the pH to this range, a pH adjuster generally used in coffee beverages may be blended. Examples of pH adjusting agents include, but are not limited to, baking soda. Moreover, it is preferable not to mix an acidulant. Here, the pH as used herein refers to a value measured by measuring 100 mL of a liquid beverage in a 300 mL beaker, adjusting the temperature to 20° C., and measuring with a pH meter.

これら成分の他、本発明の効果に影響を及ぼさない範囲で、香料、酸化防止剤等を添加することができる。 In addition to these components, fragrances, antioxidants, and the like can be added as long as they do not affect the effects of the present invention.

以下、実験例を示して本発明の詳細を具体的に説明するが、本発明はこれに限定されるものではない。また、本明細書において、特に記載しない限り、数値範囲はその端点を含むものとして記載される。また、飲料中のショ糖及びブドウ糖濃度は、以下の方法で測定できる。
(ショ糖及びブドウ糖濃度の測定)
飲料中のショ糖濃度及びブドウ糖濃度は、HPLC糖分析装置(LC-20AD株式会社 島津製作所社製)を以下の条件で操作し、検量線法により定量することで測定することができる。
・カラム:Inertsil NH2,φ3mm×150mm[ジーエルサイエンス株式会社]
・カラム温度:室温
・移動相:アセトニトリル:水=8:2
・流量:0.7ml/min
・注入量:5μL
・検出:示差屈折計 RID-10A[株式会社 島津製作所]
EXAMPLES The present invention will be specifically described below with reference to experimental examples, but the present invention is not limited thereto. Also, in this specification, unless otherwise stated, numerical ranges are described as including their endpoints. Moreover, the sucrose and glucose concentrations in the beverage can be measured by the following methods.
(Measurement of sucrose and glucose concentration)
The sucrose concentration and glucose concentration in the beverage can be measured by operating an HPLC sugar analyzer (LC-20AD, manufactured by Shimadzu Corporation) under the following conditions and quantifying by the calibration curve method.
・Column: Inertsil NH2, φ3mm×150mm [GL Sciences Co., Ltd.]
・Column temperature: room temperature ・Mobile phase: acetonitrile: water = 8:2
・Flow rate: 0.7ml/min
・Injection volume: 5 μL
・Detection: Differential refractometer RID-10A [Shimadzu Corporation]

実験1:コーヒー飲料の製造と評価
コーヒー濃縮エキス(Brix51%)を使用し、水、ショ糖、生クリーム、脱脂粉乳、及び重曹を添加して表1に示されるショ糖含有量、乳固形分、及び無脂乳固形分/乳脂肪分の質量比を有するコーヒー飲料を調製した。得られたコーヒー飲料を65℃に昇温し、高圧ホモジナイザーにて20MPaの圧力で均質化後、加熱殺菌処理(120~125℃、5~15分)し、透明PETボトル容器に充填して、乳固形分を含有する透明容器詰めコーヒー飲料とした(サンプル1-1~1-4)。また、缶に充填したサンプルも製造し、対照飲料とした。殺菌後の飲料のpH(20℃)は6.7~7.0であった。また、コーヒー固形分は0.6質量%であった。
Experiment 1: Production and Evaluation of Coffee Beverage Using concentrated coffee extract (Brix 51%), water, sucrose, fresh cream, skim milk powder, and baking soda were added, and the sucrose content and milk solids shown in Table 1 were obtained. , and a non-fat milk solids/milkfat mass ratio. The resulting coffee beverage is heated to 65° C., homogenized with a high pressure homogenizer at a pressure of 20 MPa, heat sterilized (120 to 125° C., 5 to 15 minutes), and filled into a transparent PET bottle container. Coffee beverages packed in transparent containers containing milk solids were prepared (Samples 1-1 to 1-4). A canned sample was also produced to serve as a control beverage. The pH of the beverage after sterilization (20°C) was 6.7-7.0. Also, the coffee solid content was 0.6% by mass.

得られた透明容器詰め飲料を光照射(35,000ルクス、25℃、48時間)し、その香味を評価した。評価は、光照射しなかった缶入り飲料を基準とし、光照射による香味劣化の強弱を、基準と比較した相対評価として3段階評価(〇:光照射していない基準と同等であり香味劣化がない、△:基準に比べるとやや香味劣化があるが許容できる範囲である、×:基準に比べると強い香味劣化があり飲料製品として許容できない)で行った。なお、評価は専門パネル5名が光照射による香味劣化の強弱について各自で評価した後、パネル全員で協議して決定した。 The obtained beverage packaged in a transparent container was irradiated with light (35,000 lux, 25°C, 48 hours), and its flavor was evaluated. Evaluation is based on canned beverages that have not been irradiated with light, and the intensity of flavor deterioration due to light irradiation is evaluated in three stages as a relative evaluation compared with the standard (○: equivalent to the standard without light irradiation, and flavor deterioration is Δ: The flavor is slightly deteriorated compared to the standard, but within an acceptable range. ×: The flavor is strongly deteriorated compared to the standard, and is not acceptable as a beverage product. The evaluation was determined by discussion among all the panel members after each of the five expert panel members individually evaluated the degree of flavor deterioration due to light irradiation.

結果を表1に示す。無脂乳固形分/乳脂肪分の質量比が3.5であり、乳固形分を2.0質量%以上の濃度で含有するコーヒー飲料は、光照射による強い劣化香味、具体的には、後味に残るチーズ様の香味が知覚された。 Table 1 shows the results. A coffee beverage having a non-fat milk solids/milk fat mass ratio of 3.5 and containing milk solids at a concentration of 2.0% by mass or more has a strong deteriorated flavor due to light irradiation, specifically, A lingering cheese-like flavor was perceived.

Figure 2022109855000001
Figure 2022109855000001

実験2:コーヒー飲料の製造と評価
コーヒー濃縮エキス(Brix51%)を使用し、水、ショ糖、生クリーム、脱脂粉乳、重曹を添加して表2に示されるショ糖含有量、乳固形分、及び無脂乳固形分/乳脂肪分の質量比を有するコーヒー飲料を調製した。得られたコーヒー飲料を65℃に昇温し、高圧ホモジナイザーにて20MPaの圧力で均質化後、加熱殺菌処理(120~125℃、5~15分)し、透明PETボトル容器に充填して、乳固形分含有透明容器詰めコーヒー飲料とした(サンプル2-1~2-4)。殺菌後の飲料のpH(20℃)は6.4~6.5であった。また、コーヒー固形分は0.6質量%であった。
Experiment 2: Production and Evaluation of Coffee Beverage Using concentrated coffee extract (Brix 51%), adding water, sucrose, fresh cream, skim milk powder, and baking soda, the sucrose content, milk solids, and a non-fat milk solids/milkfat mass ratio. The resulting coffee beverage is heated to 65° C., homogenized with a high pressure homogenizer at a pressure of 20 MPa, heat sterilized (120 to 125° C., 5 to 15 minutes), and filled into a transparent PET bottle container. Coffee beverages packed in transparent containers containing milk solids were prepared (Samples 2-1 to 2-4). The pH of the beverage after sterilization (20° C.) was 6.4-6.5. Also, the coffee solid content was 0.6% by mass.

得られた透明容器詰め飲料2-1~2-4を光照射(35,000ルクス、25℃、48時間)した。また、サンプル2-1については透明PETボトルに充填した後に光照射を行わないものも用意した。2-1~2-4の光照射ありと、2-1の光照射なしを用い、それぞれの香味を専門パネル4名が評価した。先ず、事前にパネルがサンプル2-1の光照射なしとありの2種類のサンプルを飲用し、光照射による劣化香味(後味に残るチーズ様の香味)についてディスカッションをし、共通認識を持つようにした。その後、各サンプルについて、以下の評価基準に基づいて各パネルが評価し、その平均点を採用した。 The obtained beverages 2-1 to 2-4 packed in transparent containers were irradiated with light (35,000 lux, 25° C., 48 hours). In addition, as for sample 2-1, a transparent PET bottle was filled and then not irradiated with light. Using 2-1 to 2-4 with light irradiation and 2-1 without light irradiation, each flavor was evaluated by four expert panels. First, the panel drank two types of sample 2-1, one without light irradiation and the other with light irradiation, and discussed the deterioration flavor (cheese-like flavor that remains in the aftertaste) due to light irradiation in advance, so as to have a common understanding. did. After that, each sample was evaluated by each panel based on the following evaluation criteria, and the average score was adopted.

<評価基準>
4:サンプル2-1の光照射なしと同等であり、劣化香味を感じない
3:サンプル2-1の光照射なしに比べるとかすかに劣化香味が感じられるが、劣化香味の程度は弱い
2:サンプル2-1の光照射なしと比べて明らかに劣化香味があるが、サンプル2-1の光照射ありと比べると劣化香味は弱い
1:サンプル2-1の光照射ありと同等かそれ以上の劣化香味を感じる。
<Evaluation Criteria>
4: Equivalent to sample 2-1 without light irradiation, no deteriorated flavor 3: Compared to sample 2-1 without light irradiation, slightly deteriorated flavor is felt, but the degree of deteriorated flavor is weak 2: Compared to sample 2-1 without light irradiation, there is clearly a deteriorated flavor, but compared to sample 2-1 with light irradiation, the deteriorated flavor is weaker 1: equal to or greater than sample 2-1 with light irradiation I feel a deteriorated flavor.

評価結果を表2に示す。コーヒー飲料に含まれる乳固形分を3.0質量%に固定した場合、無脂乳固形分/乳脂肪分が3.0以下であると、無脂乳固形分/乳脂肪分が3.5である場合に比べて、光照射による劣化香味が抑制された。サンプル2-4については、劣化香味は抑制されていたが、脂肪特有のもたつきを感じ、飲みづらいという評価をしたパネルがいたことから、無脂乳固形分/乳脂肪分の下限値は1.4程度が好ましいことが示唆された。 Table 2 shows the evaluation results. When the milk solids content contained in the coffee beverage is fixed at 3.0% by mass, if the non-fat milk solids / milk fat content is 3.0 or less, the non-fat milk solids / milk fat content is 3.5 The deteriorated flavor due to light irradiation was suppressed compared to the case of . Regarding Sample 2-4, although the deteriorated flavor was suppressed, there was a panel who evaluated that it felt sticky and difficult to drink, so the lower limit of non-fat milk solids / milk fat was 1. It was suggested that about 4 is preferable.

Figure 2022109855000002
Figure 2022109855000002

実験3:コーヒー飲料の製造と評価
実験2と同様の手順、条件で、表3の通りとなるようにコーヒー飲料を調製し、光照射をした透明PET容器詰めサンプル3-1~3-3を作成した。サンプル3-1については透明PET容器に充填した後に光照射を行わないものも用意した。透明PET容器詰めコーヒー飲料のpH(20℃)は6.4~6.5、コーヒー固形分は0.6質量%であった。サンプル3-1の光照射なしとありの2種類のサンプルを評価基準として用いた以外は実験2と同様にして光照射による劣化香味の評価を行った。
Experiment 3: Production and evaluation of coffee beverage Coffee beverages were prepared as shown in Table 3 using the same procedure and conditions as in Experiment 2, and transparent PET container-packed samples 3-1 to 3-3 were irradiated with light. Created. As for sample 3-1, a sample was also prepared in which light irradiation was not performed after filling the transparent PET container. The transparent PET-packaged coffee beverage had a pH (20° C.) of 6.4 to 6.5 and a solid coffee content of 0.6% by mass. The deteriorated flavor due to light irradiation was evaluated in the same manner as in Experiment 2, except that two types of sample 3-1, one without light irradiation and one with light irradiation, were used as evaluation criteria.

<評価基準>
4:サンプル3-1の光照射なしと同等であり、劣化香味を感じない
3:サンプル3-1の光照射なしに比べるとかすかに劣化香味が感じられるが、劣化香味の程度は弱い
2:サンプル3-1の光照射なしと比べて明らかに劣化香味があるが、サンプル3-1の光照射ありと比べると劣化香味は弱い
1:サンプル3-1の光照射ありと同等かそれ以上の劣化香味を感じる。
<Evaluation Criteria>
4: Equivalent to sample 3-1 without light irradiation, no deteriorated flavor 3: Compared to sample 3-1 without light irradiation, slightly deteriorated flavor is felt, but the degree of deteriorated flavor is weak 2: Compared to sample 3-1 without light irradiation, there is clearly a deteriorated flavor, but compared to sample 3-1 with light irradiation, the deteriorated flavor is weaker 1: equal to or greater than sample 3-1 with light irradiation I feel a deteriorated flavor.

評価結果を表3に示す。コーヒー飲料に含まれる乳固形分を2.0質量%に固定した場合も、実験2の乳固形分を3.0質量%に固定した場合と同様に、無脂乳固形分/乳脂肪分が3.0以下のときに、無脂乳固形分/乳脂肪分が3.5である場合に比べて、光照射による劣化香味が抑制された。 Table 3 shows the evaluation results. Even when the milk solids content contained in the coffee beverage is fixed at 2.0% by mass, similarly to the case where the milk solids content in Experiment 2 is fixed at 3.0% by mass, the non-fat milk solids / milk fat content is When the non-fat milk solids/milk fat ratio was 3.0 or less, deterioration of flavor due to light irradiation was suppressed compared to the case where the non-fat milk solids/milk fat ratio was 3.5.

Figure 2022109855000003
Figure 2022109855000003

実験4:コーヒー飲料の製造と評価
実験2と同様の手順、条件で、表4の通りとなるようにコーヒー飲料を調製し、光照射をした透明PET容器詰めサンプル4-1~4-3を作成した。サンプル4-1については透明PET容器に充填した後に光照射を行わないものも用意した。透明PET容器詰めコーヒー飲料のpH(20℃)は6.4~6.5、コーヒー固形分は0.6質量%であった。サンプル4-1の光照射なしとありの2種類のサンプルを評価基準として用いた以外は実験2と同様にして光照射による劣化香味の評価を行った。
Experiment 4: Production and Evaluation of Coffee Beverage Coffee beverages were prepared as shown in Table 4 using the same procedure and conditions as Experiment 2, and transparent PET container-packed samples 4-1 to 4-3 were irradiated with light. Created. As for sample 4-1, a sample was also prepared in which the light irradiation was not carried out after filling the transparent PET container. The transparent PET-packaged coffee beverage had a pH (20° C.) of 6.4 to 6.5 and a solid coffee content of 0.6% by mass. The deteriorated flavor due to light irradiation was evaluated in the same manner as in Experiment 2, except that two types of sample 4-1, one without light irradiation and one with light irradiation, were used as evaluation criteria.

<評価基準>
4:サンプル4-1の光照射なしと同等であり、劣化香味を感じない
3:サンプル4-1の光照射なしに比べるとかすかに劣化香味が感じられるが、劣化香味の程度は弱い
2:サンプル4-1の光照射なしと比べて明らかに劣化香味があるが、サンプル4-1の光照射ありと比べると劣化香味は弱い
1:サンプル4-1の光照射ありと同等かそれ以上の劣化香味を感じる。
<Evaluation Criteria>
4: Equivalent to sample 4-1 without light irradiation, no deteriorated flavor 3: slightly deteriorated flavor compared to sample 4-1 without light irradiation, but the degree of deteriorated flavor is weak 2: Compared to sample 4-1 without light irradiation, there is clearly a deteriorated flavor, but compared to sample 4-1 with light irradiation, the deteriorated flavor is weaker 1: equal to or greater than sample 4-1 with light irradiation I feel a deteriorated flavor.

評価結果を表4に示す。コーヒー飲料に含まれる乳固形分を2.5質量%に固定した場合も、実験2の乳固形分を3.0質量%に固定した場合や実験3の乳固形分を2.0質量%に固定した場合と同様に、無脂乳固形分/乳脂肪分が3.0以下のときに、無脂乳固形分/乳脂肪分が3.5である場合に比べて、光照射による劣化香味が抑制された。 Table 4 shows the evaluation results. Even when the milk solids content in the coffee beverage is fixed at 2.5% by mass, when the milk solids content in Experiment 2 is fixed at 3.0% by mass, or when the milk solids content in Experiment 3 is fixed at 2.0% by mass As in the case of fixing, when the non-fat milk solids / milk fat content is 3.0 or less, compared to the case where the non-fat milk solids / milk fat content is 3.5, the deteriorated flavor due to light irradiation was suppressed.

Figure 2022109855000004
Figure 2022109855000004

実験5:コーヒー飲料の製造と評価
コーヒー抽出液、水、ショ糖、牛乳を含む乳原料、pH調整剤、及び乳化剤等を用い、表5に記載のショ糖含有量、乳固形分、無脂乳固形分/乳脂肪分の比、及びコーヒー固形分を有する透明PETボトル容器詰め乳固形分含有コーヒー飲料サンプルを製造した。サンプル5-1と5-2について、ブドウ糖の含有量を上記方法で測定したところ、0.02質量%以下であった。サンプル5-1と5-2のそれぞれについて、光照射(35,000ルクス、25℃、48時間)なしとありのサンプルを用意した。専門パネル4名にて、サンプル5-1の光照射なしとありの劣化香味を評価した。同様に、サンプル5-2の光照射なしとありの劣化香味も評価した。サンプル5-1の光照射なしとありの劣化香味の差と、サンプル5-2の光照射なしとありの劣化香味の差を各専門パネルがそれぞれ比べたところ、4名ともサンプル5-2の方が、劣化香味の差が小さいという評価となった。
Experiment 5: Production and evaluation of coffee beverage Using coffee extract, water, sucrose, milk raw materials including milk, pH adjuster, emulsifier, etc., sucrose content, milk solids, non-fat Milk solids/milkfat ratios and milk solids containing coffee beverage samples packaged in clear PET bottles with coffee solids were produced. The glucose content of samples 5-1 and 5-2 was measured by the above method and found to be 0.02% by mass or less. Samples 5-1 and 5-2 were prepared without and with light irradiation (35,000 lux, 25° C., 48 hours), respectively. Four expert panels evaluated the deteriorated flavor of Sample 5-1 with and without light irradiation. Similarly, the deteriorated flavor of sample 5-2 with and without light irradiation was also evaluated. When each specialized panel compared the difference in the deteriorated flavor of Sample 5-1 with and without light irradiation and the difference in the deteriorated flavor of Sample 5-2 with and without light irradiation, all four panelists compared Sample 5-2. It was evaluated that the difference in the deteriorated flavor was small.

Figure 2022109855000005
Figure 2022109855000005

Claims (3)

乳固形分を含有する透明容器詰めコーヒー飲料であって、
(a)乳固形分が2.0~3.0質量%であり、
(b)ショ糖を2.1~4.5質量%含み、
(c)無脂乳固形分/乳脂肪分(質量比)が1.4~3.0である、
上記コーヒー飲料。
A coffee beverage packed in a transparent container containing milk solids,
(a) milk solids content is 2.0 to 3.0% by mass,
(b) contains 2.1 to 4.5% by mass of sucrose,
(c) non-fat milk solids/milk fat content (mass ratio) is 1.4 to 3.0,
Coffee drink above.
(c)無脂乳固形分/乳脂肪分(質量比)が2.0~3.0である、請求項1に記載の透明容器詰めコーヒー飲料。 2. The coffee beverage packed in a transparent container according to claim 1, wherein (c) non-fat milk solids/milk fat (mass ratio) is 2.0 to 3.0. (d)コーヒー固形分が0.5~1.2質量%である、請求項1又は2に記載の透明容器詰めコーヒー飲料。 (d) The coffee beverage packed in a transparent container according to claim 1 or 2, wherein the coffee solid content is 0.5 to 1.2% by mass.
JP2021119301A 2021-01-15 2021-07-20 Milk solid-containing transparently bottled coffee beverage Pending JP2022109855A (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2021004859 2021-01-15
JP2021004859 2021-01-15
JP2021017616A JP6918260B1 (en) 2021-01-15 2021-02-05 Coffee beverage in a transparent container containing milk solids

Related Parent Applications (1)

Application Number Title Priority Date Filing Date
JP2021017616A Division JP6918260B1 (en) 2021-01-15 2021-02-05 Coffee beverage in a transparent container containing milk solids

Publications (1)

Publication Number Publication Date
JP2022109855A true JP2022109855A (en) 2022-07-28

Family

ID=77172705

Family Applications (2)

Application Number Title Priority Date Filing Date
JP2021017616A Active JP6918260B1 (en) 2021-01-15 2021-02-05 Coffee beverage in a transparent container containing milk solids
JP2021119301A Pending JP2022109855A (en) 2021-01-15 2021-07-20 Milk solid-containing transparently bottled coffee beverage

Family Applications Before (1)

Application Number Title Priority Date Filing Date
JP2021017616A Active JP6918260B1 (en) 2021-01-15 2021-02-05 Coffee beverage in a transparent container containing milk solids

Country Status (1)

Country Link
JP (2) JP6918260B1 (en)

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010104324A (en) * 2008-10-31 2010-05-13 Asahi Kasei Chemicals Corp Crystalline cellulose conjugated product suitable for milk beverage
JP5255419B2 (en) * 2008-12-10 2013-08-07 旭化成ケミカルズ株式会社 Crystalline cellulose composites as milk beverage stabilizers
JP5539748B2 (en) * 2010-02-12 2014-07-02 旭化成ケミカルズ株式会社 Crystalline cellulose composite
SG10201601476XA (en) * 2011-03-11 2016-03-30 Meiji Co Ltd Photodegradation resistant beverage
JP5881301B2 (en) * 2011-03-18 2016-03-09 サントリー食品インターナショナル株式会社 Bottled milk coffee drink
JP5189195B2 (en) * 2011-09-06 2013-04-24 キリンビバレッジ株式会社 Milk-containing coffee
JP6397616B2 (en) * 2013-11-07 2018-09-26 ユーシーシー上島珈琲株式会社 Coffee with milk that reproduces the latte flavor
JP6566593B1 (en) * 2018-12-26 2019-08-28 森永乳業株式会社 Beverage and method for producing the same

Also Published As

Publication number Publication date
JP2022109837A (en) 2022-07-28
JP6918260B1 (en) 2021-08-11

Similar Documents

Publication Publication Date Title
CN110621165B (en) Packaged coffee beverage containing furfuryl methyl sulfide
AU2009287839B2 (en) Milk composition and milk-added beverage, both having lower whey protein content
CA2829744A1 (en) Photodegradation resistant beverage
JP2021119762A (en) Beverage and method of suppressing milky smell of beverage
JP6584750B2 (en) Containerized coffee beverage
JP6556975B1 (en) Container drink
JP2022115178A (en) Coffee beverage
JP6329551B2 (en) Milk coffee drink with low coffee fat content
JP6392966B1 (en) Containerized coffee beverages containing furfuryl methyl sulfide
JP6771411B2 (en) Concentrated coffee beverage in a container
JP6918260B1 (en) Coffee beverage in a transparent container containing milk solids
JP5647744B1 (en) Coffee beverage containing containerized milk and method for producing the same, method for stabilizing properties of coffee beverage containing containerized milk, and method for suppressing stickiness
JP2017163864A (en) Packaged concentrated coffee beverage
JP6316599B2 (en) Bottled milk coffee drink
JP7174733B2 (en) Dairy-containing beverage
JP6584749B2 (en) Containerized coffee beverage
JP7186087B2 (en) Method for producing packaged milk-containing green tea beverage
WO2016006603A1 (en) Lactose-containing coffee beverage
JP2008086210A (en) Method for producing packaged coffee beverage
JP2024059196A (en) Coffee beverage
AU2023258713A1 (en) BLACK COFFEE BEVERAGE CONTAINING γ-AMINOBUTYRIC ACID
JP2024129412A (en) Coffee drinks
JP6385801B2 (en) Packaged beverages containing milk and plant extracts
TW202245608A (en) Coffee beverage and manufacturing method thereof
JP2022013878A (en) Bottled milk coffee beverage, bottled milk coffee beverage production method and aggregate suppression method in bottled milk coffee beverage