JP2022038173A - Oil-containing wastewater separator and its method - Google Patents

Oil-containing wastewater separator and its method Download PDF

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JP2022038173A
JP2022038173A JP2020142527A JP2020142527A JP2022038173A JP 2022038173 A JP2022038173 A JP 2022038173A JP 2020142527 A JP2020142527 A JP 2020142527A JP 2020142527 A JP2020142527 A JP 2020142527A JP 2022038173 A JP2022038173 A JP 2022038173A
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勇治 加藤
Yuji Kato
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Toenec Corp
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Abstract

To provide a separator that can achieve both improved treatment efficiency and space saving when separating oil-containing wastewater from oil-containing scum.SOLUTION: An ultrasonic vibrator 4 is installed in a storage tank 2 so that an upper surface 4a of the ultrasonic vibrator 4 has an inclination angle of 20 degrees with respect to a liquid surface of an oil-containing scum Scoil. This prevents oil-containing drainage water Woil (separated water) separated from the oil-containing scum Scoil from remaining on the top surface 4a. In other words, since the oil-impregnated scum Scoil is always present on the upper surface 4a of the ultrasonic transducer 4, it is possible to promote the separation of the oil-containing drainage Woil (separated water) and dust from the oil-containing scum Scoil due to the cavitation effect. Since the ultrasonic transducer 4 is only installed in the storage tank 2, the oil-containing drainage Woil (separated water) and dust can be separated from the oil-containing scum Scoil with a space-saving and simple structure.SELECTED DRAWING: Figure 1

Description

本発明は、含油スカムを減容化するための含油排水分離装置およびその方法に関する。 The present invention relates to an oil-impregnated wastewater separation device for reducing the volume of oil-containing scum and a method thereof.

特開2011-45846号公報(特許文献1)には、製鉄工場において発生する含油排水から分離された含油スカムを、目開きの異なる複数段の振動篩に掛けることで、当該含油スカムから水分(含油排水)を分離させて減容化を図る装置が記載されている。当該装置では、多くの薬剤や熱エネルギーを用いることなくスカムの減容化を図ることができる。 According to Japanese Patent Application Laid-Open No. 2011-45846 (Patent Document 1), an oil-impregnated scum separated from oil-impregnated wastewater generated in an iron-making factory is subjected to a multi-stage vibrating sieve having different openings to obtain moisture (patent-containing scum). A device for separating (oil-impregnated wastewater) to reduce the volume is described. With this device, it is possible to reduce the volume of scum without using a lot of chemicals and heat energy.

特開2011-45846号公報Japanese Unexamined Patent Publication No. 2011-45846

しかしながら、上述した公報に記載の含油排水分離装置は、複数段の振動篩を配置する必要があるため、広い設置スペースが必要となり、処理効率の向上と省スペース化との両立という点において、なお改良の余地がある。 However, since the oil-impregnated wastewater separation device described in the above-mentioned publication needs to arrange a plurality of vibrating sieves, a large installation space is required, and it is still possible to improve the treatment efficiency and save space. There is room for improvement.

本発明は、上記に鑑みてなされたものであり、含油スカムから含油排水を分離するに際し、処理効率の向上および省スペース化の両立に資する技術を提供することを主目的とする。 The present invention has been made in view of the above, and an object of the present invention is to provide a technique that contributes to both improvement of treatment efficiency and space saving when separating oil-containing wastewater from oil-containing scum.

本発明に係る含油排水分離装置の好ましい形態によれば、含油スカムを減容化するための含油排水分離装置が構成される。当該含油排水分離装置は、含油スカムを貯留可能な貯留槽と、振動子と、当該振動子に高周波電力を供給可能に当該振動子に電気的に接続された発振器と、を備えている。そして、振動子は、含油スカムの液面側を向く上面を有し、当該上面が含油スカムの液面に対して所定角度傾斜した状態で貯留槽内に配置される。 According to the preferred embodiment of the oil-containing wastewater separation device according to the present invention, the oil-containing wastewater separation device for reducing the volume of the oil-containing scum is configured. The oil-impregnated drainage separation device includes a storage tank capable of storing oil-impregnated scum, an oscillator, and an oscillator electrically connected to the oscillator so as to be able to supply high-frequency power to the oscillator. The oscillator has an upper surface facing the liquid surface side of the oil-containing scum, and is arranged in the storage tank with the upper surface inclined by a predetermined angle with respect to the liquid surface of the oil-containing scum.

本発明によれば、振動子が発生した超音波により含油スカム中に微細気泡を発生させ、音圧変化によって積極的にキャビテーションさせることができる。これにより、含油スカムに付着した微細気泡が消滅(崩壊)する際に発生する衝撃圧によって、含油スカムから水分(含油排水)やゴミなどを効果的に分離させることができる。なお、振動子の上面が含油スカムの液面に対して所定角度傾斜しているため、含油スカムから分離された水分(含油排水)が当該上面に留まることがない。即ち、振動子の上面に、常に含油スカムを存在させることができるため、キャビテーション効果による含油スカムからの水分(含油排水)やゴミの分離を促進することができる。また、振動子の上面を含油スカムの液面に対して所定角度傾斜させるのみであるため、省スペースかつ簡易な構造で含油スカムから水分(含油排水)やゴミを分離できる。 According to the present invention, fine bubbles can be generated in the oil-containing scum by the ultrasonic waves generated by the vibrator, and cavitation can be positively caused by the change in sound pressure. As a result, moisture (oil-containing drainage), dust, and the like can be effectively separated from the oil-containing scum by the impact pressure generated when the fine bubbles adhering to the oil-containing scum disappear (collapse). Since the upper surface of the oscillator is inclined at a predetermined angle with respect to the liquid surface of the oil-containing scum, the water (oil-containing drainage) separated from the oil-containing scum does not stay on the upper surface. That is, since the oil-impregnated scum can always be present on the upper surface of the oscillator, it is possible to promote the separation of water (oil-impregnated drainage) and dust from the oil-containing scum due to the cavitation effect. Further, since the upper surface of the oscillator is only tilted at a predetermined angle with respect to the liquid surface of the oil-containing scum, moisture (oil-containing drainage) and dust can be separated from the oil-containing scum with a space-saving and simple structure.

本発明に係る含油排水分離装置の更なる形態によれば、振動子の上面は、液面に対して15度以上25度以下、好ましくは約20度の傾斜角度を有している。 According to a further embodiment of the oil-impregnated drainage separation device according to the present invention, the upper surface of the oscillator has an inclination angle of 15 degrees or more and 25 degrees or less, preferably about 20 degrees with respect to the liquid surface.

本発明者は、鋭意研究の結果、振動子の上面の液面に対する傾斜角度が15度以上25度以下、好ましくは約20度のときに、含油スカムの削減率が高くなることを見出した。ここで、削減率とは、含油スカムから水分(含油排水)が除去されたことによる容積の低減率として規定され、具体的には、「貯留槽内における減容化前(処理前)の含油スカムの容積」から「貯留槽内における減容化後(処理後)の含油スカムの容積」を減じた値を「貯留槽内における減容化前(処理前)の含油スカムの容積」で除した後、100を乗じた値として規定される。この研究結果を踏まえて、本形態では、振動子の上面の液面に対する傾斜角度を、15度以上25度以下、好ましくは約20度とする構成とした。これにより、含油スカムの減容化をより促進することができる。 As a result of diligent research, the present inventor has found that the reduction rate of oil-containing scum becomes high when the inclination angle of the upper surface of the oscillator with respect to the liquid surface is 15 degrees or more and 25 degrees or less, preferably about 20 degrees. Here, the reduction rate is defined as the volume reduction rate due to the removal of water (oil-impregnated wastewater) from the oil-impregnated scum, and specifically, "oil-containing before volume reduction (before treatment) in the storage tank". The value obtained by subtracting the "volume of the oil-containing scum after volume reduction (after treatment) in the storage tank" from the "volume of scum" is divided by the "volume of oil-containing scum before volume reduction (before treatment) in the storage tank". After that, it is defined as a value multiplied by 100. Based on the results of this research, in this embodiment, the inclination angle of the upper surface of the vibrator with respect to the liquid surface is set to 15 degrees or more and 25 degrees or less, preferably about 20 degrees. Thereby, the volume reduction of the oil-containing scum can be further promoted.

本発明に係る含油排水分離装置の更なる形態によれば、振動子は、上面のうち液面に最も近い部位と、液面と、の距離が5cm以上となるように貯留槽内に配置されている。 According to a further embodiment of the oil-impregnated drainage separation device according to the present invention, the oscillator is arranged in the storage tank so that the distance between the portion of the upper surface closest to the liquid level and the liquid level is 5 cm or more. ing.

本発明者は、鋭意研究の結果、振動子の上面と含油スカムの液面との間の距離が狭いと、含油スカムの液面の振動が激しくなり、超音波の効果で分離した含油スカムが瞬時に再混合されるといった現象が生じることを見出した。この研究結果を踏まえて、本形態では、振動子の上面と含油スカムの液面との距離を、5cm以上とする構成とした。これにより、含油スカムの減容効果が低減することを抑制することができる。 As a result of diligent research, the present inventor, as a result of diligent research, when the distance between the upper surface of the oscillator and the liquid surface of the oil-containing scum is narrow, the vibration of the liquid surface of the oil-containing scum becomes intense, and the oil-containing scum separated by the effect of ultrasonic waves is produced. We have found that a phenomenon such as instant remixing occurs. Based on the results of this research, in this embodiment, the distance between the upper surface of the oscillator and the liquid level of the oil-containing scum is set to 5 cm or more. As a result, it is possible to suppress the reduction of the volume reduction effect of the oil-containing scum.

本発明に係る含油排水分離装置の更なる形態によれば、貯留槽は、底面を有している。そして、振動子は、底面との間に空間を有する態様で貯留槽内に配置される。 According to a further embodiment of the oil-impregnated wastewater separation device according to the present invention, the storage tank has a bottom surface. Then, the oscillator is arranged in the storage tank so as to have a space between the oscillator and the bottom surface.

本形態によれば、含油スカムから分離された水分(含油排水)が振動子と底面との間の空間に流れ込み、対流効果によって含油スカムを振動子の上面側に移動させることができる。また、振動子が含油スカムから分離された水分(含油排水)に埋没してしまうことを良好に回避できる。これにより、キャビテーション効果による含油スカムからの水分(含油排水)やゴミの分離をより一層促進することができる。 According to this embodiment, the water (oil-impregnated drainage) separated from the oil-containing scum flows into the space between the vibrator and the bottom surface, and the oil-containing scum can be moved to the upper surface side of the vibrator by the convection effect. Further, it is possible to satisfactorily prevent the oscillator from being buried in the water (oil-impregnated drainage) separated from the oil-containing scum. This makes it possible to further promote the separation of water (oil-impregnated drainage) and dust from the oil-impregnated scum due to the cavitation effect.

本発明に係る含油排水分離装置の更なる形態によれば、含油スカムに出力される超音波周波数は、20kHz以上100kHz以下、好ましくは約40kHzである。 According to a further embodiment of the oil-impregnated wastewater separator according to the present invention, the ultrasonic frequency output to the oil-containing scum is 20 kHz or more and 100 kHz or less, preferably about 40 kHz.

本発明者は、鋭意研究の結果、特定の超音波周波数帯域において、含油スカムから水分(含油排水)やゴミを効果的に分離できることを見出した。この研究結果を踏まえて、本形態では、含油スカムに出力される超音波周波数を20kHz以上100kHz以下、好ましくは約40kHzとした。これにより、含油スカムから水分(含油排水)やゴミを効果的に分離することができる。 As a result of diligent research, the present inventor has found that water (oil-containing wastewater) and dust can be effectively separated from oil-containing scum in a specific ultrasonic frequency band. Based on the results of this research, in this embodiment, the ultrasonic frequency output to the oil-containing scum is set to 20 kHz or more and 100 kHz or less, preferably about 40 kHz. As a result, moisture (oil-impregnated drainage) and dust can be effectively separated from the oil-impregnated scum.

本発明に係る含油排水分離装置の更なる形態によれば、貯留槽に貯留される含油スカムは、20L以上30L以下、好ましくは30Lであり、高周波電力は、400W以上600W以下、好ましくは600Wである。即ち、発振器は、含油スカム1Lあたり20W以上30W以下、好ましくは20Wの高周波電力を振動子に供給する。 According to a further embodiment of the oil-impregnated wastewater separation device according to the present invention, the oil-containing scum stored in the storage tank is 20 L or more and 30 L or less, preferably 30 L, and the high-frequency power is 400 W or more and 600 W or less, preferably 600 W. be. That is, the oscillator supplies high frequency power of 20 W or more and 30 W or less, preferably 20 W, per 1 L of oil-containing scum to the oscillator.

本発明者は、鋭意研究の結果、振動子に供給する高周波電力の値と、処理する含油スカムの量と、に相関があることを見出した。出力を600Wより大きくすると、分離された水分(含油排水)の水質が低下する。一方、出力を400W未満にすると、処理時間が長くなってしまう。この研究結果を踏まえて、本形態では、含油スカムの量を20L以上30L以下、好ましくは30Lとし、振動子に供給する高周波電力を400W以上600W以下、好ましくは600Wとする構成とした。即ち、発振器によって、含油スカム1Lあたり20W以上30W以下、好ましくは20Wの高周波電力を振動子に供給する構成とした。これにより、含油スカムから水分(含油排水)やゴミをより効果的に分離することができる。 As a result of diligent research, the present inventor has found that there is a correlation between the value of high-frequency power supplied to the oscillator and the amount of oil-containing scum to be processed. When the output is made larger than 600 W, the water quality of the separated water (oil-containing wastewater) deteriorates. On the other hand, if the output is less than 400 W, the processing time becomes long. Based on the results of this research, in this embodiment, the amount of oil-containing scum is 20 L or more and 30 L or less, preferably 30 L, and the high-frequency power supplied to the vibrator is 400 W or more and 600 W or less, preferably 600 W. That is, the oscillator is configured to supply high frequency power of 20 W or more and 30 W or less, preferably 20 W per 1 L of oil-containing scum to the oscillator. This makes it possible to more effectively separate water (oil-impregnated drainage) and dust from the oil-impregnated scum.

本発明に係る含油排水分離装置の更なる形態によれば、含油スカムの温度を10℃以上40℃以下に調節可能な温度調節器をさらに備えている。 According to a further embodiment of the oil-impregnated wastewater separator according to the present invention, a temperature controller capable of adjusting the temperature of the oil-containing scum to 10 ° C. or higher and 40 ° C. or lower is further provided.

本発明者は、鋭意研究の結果、含油スカムの温度が低すぎると、含油スカムの粘度が高くなり、分離後(減容化後)の含油スカムを処理する際に目詰まりなどが発生してしまい、また、含油スカムの温度が高すぎると、分離効果は向上するが、濃縮された(減容化された)含油スカムや浮上油が超音波の効果で含油排水に溶けやすくなり、分離効果が低下してしまうことを見出した。この研究結果を踏まえて、本発明では、含油スカムの温度を10℃以上40℃以下に調節する構成とした。これにより、含油スカムから水分(含油排水)やゴミをより効果的に分離することができる。 As a result of diligent research, the present inventor found that if the temperature of the oil-containing scum is too low, the viscosity of the oil-containing scum becomes high, and clogging occurs when the oil-containing scum after separation (after volume reduction) is processed. If the temperature of the oil-containing scum is too high, the separation effect will be improved, but the concentrated (volume-reduced) oil-containing scum and floating oil will be more easily dissolved in the oil-containing wastewater due to the effect of ultrasonic waves, and the separation effect will be improved. Was found to decrease. Based on the results of this research, in the present invention, the temperature of the oil-containing scum is adjusted to 10 ° C. or higher and 40 ° C. or lower. This makes it possible to more effectively separate water (oil-impregnated drainage) and dust from the oil-impregnated scum.

本発明に係る含油排水分離方法の好ましい形態によれば、含油スカムを減容化するための含油排水分離方法が構成される。当該含油排水分離方法は、(a)貯留槽に含油スカムを貯留し、(b)含油スカムの液面に対して上面が所定角度傾斜した状態となるように振動子を貯留槽内に配置し、(c)振動子に高周波電力を供給する。 According to a preferred embodiment of the oil-containing wastewater separation method according to the present invention, an oil-containing wastewater separation method for reducing the volume of oil-containing scum is configured. In the oil-impregnated drainage separation method, (a) the oil-impregnated scum is stored in the storage tank, and (b) the vibrator is arranged in the storage tank so that the upper surface is inclined by a predetermined angle with respect to the liquid surface of the oil-impregnated scum. , (C) Supply high frequency power to the oscillator.

本発明によれば、振動子が発生した超音波により含油スカム中に微細気泡を発生させ、音圧変化によって積極的にキャビテーションさせることができる。これにより、含油スカムに付着した微細気泡が消滅(崩壊)する際に発生する衝撃圧によって、含油スカムから水分(含油排水)やゴミなどを効果的に分離させることができる。なお、振動子の上面が含油スカムの液面に対して所定角度傾斜しているため、含油スカムから分離された水分(含油排水)が当該上面に留まることがない。即ち、振動子の上面に、常に含油スカムを存在させることができるため、キャビテーション効果による含油スカムからの水分(含油排水)やゴミの分離を促進することができる。また、振動子の上面を含油スカムの液面に対して所定角度傾斜させるのみであるため、省スペースかつ簡易な構造で含油スカムから水分(含油排水)やゴミを分離できる。 According to the present invention, fine bubbles can be generated in the oil-containing scum by the ultrasonic waves generated by the vibrator, and cavitation can be positively caused by the change in sound pressure. As a result, moisture (oil-containing drainage), dust, and the like can be effectively separated from the oil-containing scum by the impact pressure generated when the fine bubbles adhering to the oil-containing scum disappear (collapse). Since the upper surface of the oscillator is inclined at a predetermined angle with respect to the liquid surface of the oil-containing scum, the water (oil-containing drainage) separated from the oil-containing scum does not stay on the upper surface. That is, since the oil-impregnated scum can always be present on the upper surface of the oscillator, it is possible to promote the separation of water (oil-impregnated drainage) and dust from the oil-containing scum due to the cavitation effect. Further, since the upper surface of the oscillator is only tilted at a predetermined angle with respect to the liquid surface of the oil-containing scum, moisture (oil-containing drainage) and dust can be separated from the oil-containing scum with a space-saving and simple structure.

本発明に係る含油排水分離方法の更なる形態によれば、ステップ(b)は、上面を液面に対して15度以上25度以下、好ましくは約20度の傾斜角となるように振動子を貯留槽内に配置するステップを含んでいる。 According to a further embodiment of the oil-impregnated wastewater separation method according to the present invention, in step (b), the vibrator is set so that the upper surface has an inclination angle of 15 degrees or more and 25 degrees or less, preferably about 20 degrees with respect to the liquid surface. Includes the step of placing the in a reservoir.

本発明者は、鋭意研究の結果、振動子の上面の液面に対する傾斜角度が15度以上25度以下、好ましくは約20度のときに、含油スカムの削減率が高くなることを見出した。ここで、削減率とは、「貯留槽内における減容化前(処理前)の含油スカムの容積」から「貯留槽内における減容化後(処理後)の含油スカムの容積」を減じた値を「貯留槽内における減容化前(処理前)の含油スカムの容積」で除した後、100を乗じた値として規定される。この研究結果を踏まえて、本形態では、振動子の上面の液面に対する傾斜角度を、15度以上25度以下、好ましくは約20度とする構成とした。これにより、含油スカムの減容化をより促進することができる。 As a result of diligent research, the present inventor has found that the reduction rate of oil-containing scum becomes high when the inclination angle of the upper surface of the oscillator with respect to the liquid surface is 15 degrees or more and 25 degrees or less, preferably about 20 degrees. Here, the reduction rate is obtained by subtracting "the volume of the oil-containing scum after the volume reduction (after the treatment) in the storage tank" from "the volume of the oil-containing scum before the volume reduction (before the treatment) in the storage tank". The value is defined as a value multiplied by 100 after dividing by "volume of oil-containing scum before volume reduction (before treatment) in the storage tank". Based on the results of this research, in this embodiment, the inclination angle of the upper surface of the vibrator with respect to the liquid surface is set to 15 degrees or more and 25 degrees or less, preferably about 20 degrees. Thereby, the volume reduction of the oil-containing scum can be further promoted.

本発明に係る含油排水分離方法の更なる形態によれば、ステップ(b)は、上面のうち液面に最も近い部位と、液面と、の距離が5cm以上となるように振動子を貯留槽に配置するステップを含んでいる。 According to a further embodiment of the oil-impregnated wastewater separation method according to the present invention, in step (b), the oscillator is stored so that the distance between the portion of the upper surface closest to the liquid surface and the liquid surface is 5 cm or more. Includes steps to place in the tank.

本発明者は、鋭意研究の結果、振動子の上面と含油スカムの液面との間の距離が狭いと、含油スカムの液面の振動が激しくなり、超音波の効果で分離した含油スカムが瞬時に再混合されるといった現象が生じることを見出した。この研究結果を踏まえて、本形態では、振動子の上面と含油スカムの液面との距離を、5cm以上とする構成とした。これにより、含油スカムの減容効果が低減することを抑制することができる。 As a result of diligent research, the present inventor, as a result of diligent research, when the distance between the upper surface of the oscillator and the liquid surface of the oil-containing scum is narrow, the vibration of the liquid surface of the oil-containing scum becomes intense, and the oil-containing scum separated by the effect of ultrasonic waves is produced. We have found that a phenomenon such as instant remixing occurs. Based on the results of this research, in this embodiment, the distance between the upper surface of the oscillator and the liquid level of the oil-containing scum is set to 5 cm or more. As a result, it is possible to suppress the reduction of the volume reduction effect of the oil-containing scum.

本発明に係る含油排水分離方法の更なる形態によれば、ステップ(b)は、振動子と、貯留槽の底面と、の間に空間を有する態様で振動子を貯留槽内に配置するステップを含んでいる。 According to a further embodiment of the oil-impregnated wastewater separation method according to the present invention, step (b) is a step of arranging the vibrator in the storage tank in such a manner that a space is provided between the vibrator and the bottom surface of the storage tank. Includes.

本形態によれば、含油スカムから分離された水分(含油排水)が振動子と底面との間の空間に流れ込み、対流効果によって含油スカムを振動子の上面側に移動させることができる。また、振動子が含油スカムから分離された水分(含油排水)に埋没してしまうことを良好に回避できる。これにより、キャビテーション効果による含油スカムからの水分(含油排水)やゴミの分離をより一層促進することができる。 According to this embodiment, the water (oil-impregnated drainage) separated from the oil-containing scum flows into the space between the vibrator and the bottom surface, and the oil-containing scum can be moved to the upper surface side of the vibrator by the convection effect. Further, it is possible to satisfactorily prevent the oscillator from being buried in the water (oil-impregnated drainage) separated from the oil-containing scum. This makes it possible to further promote the separation of water (oil-impregnated drainage) and dust from the oil-impregnated scum due to the cavitation effect.

本発明によれば、含油スカムから含油排水を分離するに際し、処理効率の向上および省スペース化の両立を図ることができる。 According to the present invention, when separating the oil-containing wastewater from the oil-containing scum, it is possible to improve the treatment efficiency and save space at the same time.

本発明の実施の形態に係る含油排水分離装置1の構成の概略を示す構成図である。It is a block diagram which shows the outline of the structure of the oil-impregnated drainage separation device 1 which concerns on embodiment of this invention. 含油スカムScoilの量と,含油スカムScoilの削減率および含油排水Woil(分離水)中の油の量と,の関係についての実験結果を示した説明図である。It is explanatory drawing which showed the experimental result about the relationship between the amount of oil-containing scum school, the reduction rate of oil-containing scum school, and the amount of oil in oil-containing drainage school (separated water). 含油スカムScoilに出力される超音波周波数と削減率との関係についての実験結果を示した説明図である。It is explanatory drawing which showed the experimental result about the relationship between the ultrasonic frequency and reduction rate output to the oil-impregnated scum school. 超音波発振器8の出力と削減率との関係についての実験結果を示した説明図である。It is explanatory drawing which showed the experimental result about the relationship between the output of an ultrasonic oscillator 8 and the reduction rate. 含油スカムScoilの液面に対する超音波振動子4の上面4aの傾斜角度と変化率との関係についての実験結果を示した説明図である。It is explanatory drawing which showed the experimental result about the relationship between the inclination angle of the upper surface 4a of the ultrasonic vibrator 4 with respect to the liquid surface of oil-containing scum school, and the rate of change. 変形例の含油排水分離装置1Aの構成の概略を示す構成図である。It is a block diagram which shows the outline of the structure of the oil-impregnated drainage separation device 1A of a modification. 変形例の含油排水分離装置1Bの構成の概略を示す構成図である。It is a block diagram which shows the outline of the structure of the oil-impregnated drainage separation device 1B of a modification.

次に、本発明を実施するための最良の形態を実施例を用いて説明する。 Next, the best mode for carrying out the present invention will be described with reference to examples.

本実施の形態に係る含油排水分離装置1は、図1に示すように、含油スカムを貯留可能な貯留槽2と、当該貯留槽2内に配置された超音波振動子4と、当該超音波振動子4を載置可能に貯留槽2内に配置された載置台6と、超音波振動子4に高周波電力を供給可能に当該超音波振動子4に電力ラインLを介して電気的に接続された超音波発振器8と、貯留槽2内の含油スカムの温度調節を行う温度調節器30と、を備えている。 As shown in FIG. 1, the oil-impregnated drainage separation device 1 according to the present embodiment includes a storage tank 2 capable of storing oil-containing scum, an ultrasonic vibrator 4 arranged in the storage tank 2, and the ultrasonic wave. The mounting table 6 arranged in the storage tank 2 so that the vibrator 4 can be mounted and the ultrasonic vibrator 4 can be electrically connected to the ultrasonic vibrator 4 via the power line L so that high-frequency power can be supplied. It is provided with the ultrasonic oscillator 8 and the temperature controller 30 for controlling the temperature of the oil-containing scum in the storage tank 2.

貯留槽2は、図1に示すように、底壁2aが先細りの形状を有している。換言すれば、底壁2aは、中央に向かうほど深さが深くなる形状を有しているということができる。当該底壁2aの約中央には、バルブ付き吐出配管10が接続されている。即ち、バルブ付き吐出配管10は、貯留槽2の最も深さが深い箇所に接続されている。また、貯留槽2の側壁2bには、バルブ付き吐出配管12が接続されている。バルブ付き吐出配管12は、側壁2bのうち底壁2a寄りの位置、好ましくは底壁2aに隣接して配置されている。貯留槽2には、油水分離槽90からポンプPによって汲み上げられた含油スカムScoilがホースHを介して供給される。なお、油水分離槽90は、例えば金属加工工場内で発生した廃液や排水を浮上油Foil、含油スカムScoil、含油排水Woil、および、スラッジSlgに分離する装置である。 As shown in FIG. 1, the storage tank 2 has a tapered bottom wall 2a. In other words, it can be said that the bottom wall 2a has a shape that becomes deeper toward the center. A discharge pipe 10 with a valve is connected to about the center of the bottom wall 2a. That is, the discharge pipe 10 with a valve is connected to the deepest part of the storage tank 2. Further, a discharge pipe 12 with a valve is connected to the side wall 2b of the storage tank 2. The discharge pipe 12 with a valve is arranged at a position closer to the bottom wall 2a in the side wall 2b, preferably adjacent to the bottom wall 2a. An oil-containing scum school pumped from the oil-water separation tank 90 by the pump P is supplied to the storage tank 2 via the hose H. The oil-water separation tank 90 is a device that separates waste liquid and wastewater generated in a metal processing factory into floating oil foil, oil-containing scum school, oil-containing drainage Woil, and sludge slg.

超音波振動子4は、例えば、圧電セラミックスにより構成されており、交流電圧を付加することにより伸縮する性質を有している。即ち、超音波振動子4は、電気エネルギーを機械エネルギーに変換する、より具体的には、超音波発振器8より供給される高周波電力を機械振動に変換して超音波を発生する。本実施の形態では、超音波振動子4として、貯留槽2内に沈める投込型振動子を用いる構成とした。なお、超音波振動子4は、約直方体形状を有している。 The ultrasonic vibrator 4 is made of, for example, piezoelectric ceramics, and has a property of expanding and contracting by applying an AC voltage. That is, the ultrasonic transducer 4 converts electrical energy into mechanical energy, more specifically, converts high frequency power supplied from the ultrasonic oscillator 8 into mechanical vibration to generate ultrasonic waves. In the present embodiment, as the ultrasonic vibrator 4, an immersion type vibrator that is submerged in the storage tank 2 is used. The ultrasonic transducer 4 has a rectangular parallelepiped shape.

載置台6は、図1に示すように、所定の高さを有する格子状の台として構成されており、貯留槽2の上縁部に引っ掛けることにより当該貯留槽2に設置可能とされている。また、載置台6は、超音波振動子4を載置可能な載置面6aを有している。当該載置面6aは、貯留槽2に貯留される含油スカムScoilの液面に対して約20度の傾斜角度を有している。当該載置面6aに超音波振動子4が載置されることによって、超音波振動子4の上面4aも貯留槽2に貯留される含油スカムScoilの液面に対して約20度の傾斜角度を有する。また、載置台6の高さは、載置面6aに載置された超音波振動子4の上面4aのうち含油スカムScoilの液面に最も近い部位と、当該含油スカムScoilの液面と、の距離が5cm以上となるように設定されている。なお、超音波振動子4が載置台6の載置面6aに載置されるため、超音波振動子4と貯留槽2の底壁2aとの間には、所定の空間Rが構成される。なお、本実施の形態では、載置台6を格子状の台としたが、超音波振動子4の上面4aが貯留槽2に貯留される含油スカムScoilの液面に対して傾斜角度を有した状態で超音波振動子4を載置できれば如何なる構造であっても良いことは言うまでもない。 As shown in FIG. 1, the mounting table 6 is configured as a grid-like table having a predetermined height, and can be installed in the storage tank 2 by hooking it on the upper edge of the storage tank 2. .. Further, the mounting table 6 has a mounting surface 6a on which the ultrasonic vibrator 4 can be mounted. The mounting surface 6a has an inclination angle of about 20 degrees with respect to the liquid surface of the oil-containing scum Scoil stored in the storage tank 2. By mounting the ultrasonic vibrator 4 on the mounting surface 6a, the upper surface 4a of the ultrasonic vibrator 4 also has an inclination angle of about 20 degrees with respect to the liquid surface of the oil-containing scum school stored in the storage tank 2. Have. The height of the mounting table 6 is the portion of the upper surface 4a of the ultrasonic transducer 4 mounted on the mounting surface 6a that is closest to the liquid level of the oil-containing scum school, and the liquid level of the oil-containing scum school. The distance is set to be 5 cm or more. Since the ultrasonic vibrator 4 is mounted on the mounting surface 6a of the mounting table 6, a predetermined space R is formed between the ultrasonic vibrator 4 and the bottom wall 2a of the storage tank 2. .. In the present embodiment, the mounting table 6 is a grid-like table, but the upper surface 4a of the ultrasonic vibrator 4 has an inclination angle with respect to the liquid level of the oil-containing scum Scoil stored in the storage tank 2. Needless to say, any structure may be used as long as the ultrasonic vibrator 4 can be placed in the state.

温度調節器30は、図示しないヒーターと、当該ヒーターに通電する電流を断続可能な開閉器(図示せず)と、貯留槽2に貯留される含油スカムScoilの温度を測定する温度センサ(図示せず)と、温度センサによって測定された温度に基づいて開閉器を制御する制御装置(図示せず)と、を有している。制御装置は、測定された温度と、貯留槽2に貯留される含油スカムScoilの温度と、を比較して、含油スカムScoilの温度が所望の温度を維持するように開閉器を制御する。 The temperature controller 30 includes a heater (not shown), a switch (not shown) capable of intermittently energizing the heater, and a temperature sensor (not shown) for measuring the temperature of the oil-impregnated scum Scoil stored in the storage tank 2. It has a control device (not shown) that controls the switch based on the temperature measured by the temperature sensor. The control device compares the measured temperature with the temperature of the oil-impregnated scum Scoil stored in the storage tank 2 and controls the switch so that the temperature of the oil-impregnated scum Scoil maintains a desired temperature.

次に、こうして構成された本発明の実施の形態に係る含油排水分離装置1の動作について説明する。まず、貯留槽2内に載置台6および超音波振動子4を配置した状態で、貯留槽2内の含油スカムScoilの量が約30Lとなるまで、油水分離槽90から含油スカムScoilを貯留槽2内に供給する。このとき、超音波振動子4の上面4aは、含油スカムScoilの液面に対して約20度の傾斜角度を有している。また、超音波振動子4の上面のうち含油スカムScoilの液面に最も近い部位と、当該含油スカムScoilの液面と、の距離が5cm以上となるように設定されている。さらに、超音波振動子4と貯留槽2の底壁2aとの間には、所定の空間Rが構成されている。 Next, the operation of the oil-impregnated wastewater separation device 1 according to the embodiment of the present invention thus configured will be described. First, in a state where the mounting table 6 and the ultrasonic transducer 4 are arranged in the storage tank 2, the oil-containing scum Scoil is stored in the storage tank from the oil-water separation tank 90 until the amount of the oil-containing scum Scoil in the storage tank 2 becomes about 30 L. Supply within 2. At this time, the upper surface 4a of the ultrasonic transducer 4 has an inclination angle of about 20 degrees with respect to the liquid surface of the oil-containing scum school. Further, the distance between the portion of the upper surface of the ultrasonic transducer 4 closest to the liquid level of the oil-containing scum school and the liquid level of the oil-containing scum school is set to be 5 cm or more. Further, a predetermined space R is formed between the ultrasonic vibrator 4 and the bottom wall 2a of the storage tank 2.

続いて、温度調節器30によって、含油スカムScoilの温度を10℃以上40℃以下に設定し、当該状態で、超音波発振器8から超音波振動子4に高周波電力を供給する。ここで、本実施の形態では、超音波発振器8から超音波振動子4に供給される高周波電力は、出力600Wに設定すると共に(即ち、超音波発振器8が、含油スカムScoil1Lあたり20Wの高周波電力を超音波振動子4に供給する構成)、含油スカムScoilに出力される超音波周波数が40kHzとなるように設定する構成とした。 Subsequently, the temperature of the oil-containing scum school is set to 10 ° C. or higher and 40 ° C. or lower by the temperature controller 30, and high-frequency power is supplied from the ultrasonic oscillator 8 to the ultrasonic oscillator 4 in this state. Here, in the present embodiment, the high frequency power supplied from the ultrasonic oscillator 8 to the ultrasonic oscillator 4 is set to an output of 600 W (that is, the ultrasonic oscillator 8 has a high frequency power of 20 W per 1 L of oil-containing scum Scoil. The configuration is such that the ultrasonic frequency output to the oil-impregnated scum Scoil is set to 40 kHz.

こうして貯留槽2内の含油スカムScoilに超音波振動を与えると、含油スカムScoilから含油排水Woil(分離水)が分離され、比較的比重の小さい含油スカムScoilが貯留槽2の上方に移動すると共に、比較的比重の大きい含油排水Woil(分離水)が貯留槽2の下方(底)に移動する。ここで、含油スカムScoilからの含油排水Woil(分離水)の分離は、以下のメカニズムによって行われる。即ち、含油スカムScoilに超音波振動を作用させることで、含油スカムScoil中に微細気泡を発生させ、音圧変化によって積極的にキャビテーションさせることができ、これにより、含油スカムScoilに付着した微細気泡が消滅(崩壊)する際に発生する衝撃圧によって、含油スカムScoilから含油排水Woil(分離水)やゴミなどが効果的に分離されるのである。 When ultrasonic vibration is applied to the oil-containing scum school in the storage tank 2 in this way, the oil-impregnated drainage Wheel (separated water) is separated from the oil-containing scum school, and the oil-containing scum school having a relatively low specific density moves above the storage tank 2 and at the same time. The oil-impregnated wastewater (separated water) having a relatively large specific gravity moves to the lower side (bottom) of the storage tank 2. Here, the separation of the oil-impregnated wastewater (separated water) from the oil-impregnated scum School is performed by the following mechanism. That is, by applying ultrasonic vibration to the oil-containing scum school, fine bubbles can be generated in the oil-containing scum school and cavitation can be positively caused by the change in sound pressure, whereby the fine bubbles attached to the oil-containing scum school can be positively cavitated. The impact pressure generated when the school disappears (collapses) effectively separates the oil-impregnated drainage school (separated water) and dust from the oil-containing scum school.

なお、超音波振動子4の上面4aが含油スカムScoilの液面に対して20度の傾斜角度を有しているため、含油スカムScoilから分離された含油排水Woil(分離水)が当該上面4aに留まることがない。即ち、超音波振動子4の上面4aに、常に含油スカムScoilを存在させることができる。また、当該上面4aを流下した含油排水Woil(分離水)は、超音波振動子4と貯留槽2の底壁2aとの間の空間Rに流れ込み、対流効果によって当該空間Rに存在している含油スカムScoilを貯留槽2の上方に移動させることができる。さらに、超音波振動子4が載置台によってかさ上げされているため、超音波振動子4が含油スカムScoilから分離された含油排水Woil(分離水)に埋没してしまうことを良好に回避できる。これにより、キャビテーション効果による含油スカムScoilからの含油排水Woil(分離水)やゴミの分離を促進することができる。 Since the upper surface 4a of the ultrasonic transducer 4 has an inclination angle of 20 degrees with respect to the liquid surface of the oil-containing scum school, the oil-containing drainage wall (separated water) separated from the oil-containing scum school is the upper surface 4a. Never stay in. That is, the oil-containing scum school can always be present on the upper surface 4a of the ultrasonic transducer 4. Further, the oil-impregnated drainage Woil (separated water) flowing down the upper surface 4a flows into the space R between the ultrasonic vibrator 4 and the bottom wall 2a of the storage tank 2, and exists in the space R due to the convection effect. The oil-impregnated scum Scoil can be moved above the storage tank 2. Further, since the ultrasonic vibrator 4 is raised by the mounting table, it is possible to satisfactorily prevent the ultrasonic vibrator 4 from being buried in the oil-containing drainage wall (separated water) separated from the oil-containing scum school. This makes it possible to promote the separation of oil-impregnated drainage Woil (separated water) and dust from the oil-impregnated scum School due to the cavitation effect.

なお、超音波振動子4の上面のうち含油スカムScoilの液面に最も近い部位と、当該含油スカムScoilの液面と、の距離が5cm以上となるように設定されているため、含油スカムScoilの液面付近での激しい振動の発生を防止できる。これにより、含油スカムScoilの減容化効果が低減することを抑制できる。 Since the distance between the portion of the upper surface of the ultrasonic transducer 4 closest to the liquid level of the oil-containing scum Scoil and the liquid level of the oil-containing scum Scoil is set to be 5 cm or more, the oil-containing scum Scoil is set. It is possible to prevent the occurrence of violent vibration near the liquid level. As a result, it is possible to suppress the reduction of the volume reducing effect of the oil-containing scum school.

また、含油スカムScoilの量を30Lに設定すると共に、含油スカムScoilの油温を10℃以上40℃以下に設定し、さらに、含油スカムScoilに出力される超音波周波数を40kHzに設定すると共に、超音波発振器8の出力を600Wとしたため、含油スカムScoilから含油排水(分離水)やゴミの分離をより一層効果的に促進することができる。 Further, the amount of the oil-containing scum school is set to 30 L, the oil temperature of the oil-containing scum school is set to 10 ° C. or higher and 40 ° C. or lower, and the ultrasonic frequency output to the oil-containing scum school is set to 40 kHz. Since the output of the ultrasonic oscillator 8 is 600 W, it is possible to more effectively promote the oil-containing drainage (separated water) and the separation of dust from the oil-containing scum school.

こうして貯留槽2内で含油スカムScoilから含油排水Woil(分離水)を分離した後、バルブ付き吐出配管10を開状態とすることによって、含油排水(分離水)を排出することができ、また、バルブ付き吐出配管12を開状態とすることによって、減容化された含油スカムScoilを排出することができる。 After separating the oil-impregnated drainage Wheel (separated water) from the oil-impregnated scum School in the storage tank 2 in this way, the oil-containing drainage (separated water) can be discharged by opening the discharge pipe 10 with a valve. By opening the discharge pipe 12 with a valve, the volume-reduced oil-containing scum school can be discharged.

図2は、含油スカムScoilの量と,含油スカムScoilの削減率および含油排水Woil(分離水)中の油の量と,の関係についての実験結果を示した説明図であり、図3は、含油スカムScoilに出力される超音波周波数と削減率との関係についての実験結果を示した説明図であり、図4は、超音波発振器8の出力と削減率との関係についての実験結果を示した説明図であり、図5は、含油スカムScoilの液面に対する超音波振動子4の上面4aの傾斜角度と変化率との関係についての実験結果を示した説明図である。 FIG. 2 is an explanatory diagram showing the experimental results regarding the relationship between the amount of oil-containing scum spill, the reduction rate of oil-containing scum spill, and the amount of oil in the oil-containing drainage wall (separated water), and FIG. 3 is an explanatory diagram. It is explanatory drawing which showed the experimental result about the relationship between the ultrasonic frequency and reduction rate output to the oil-impregnated scum Scoil, and FIG. 4 shows the experimental result about the relationship between the output and reduction rate of an ultrasonic oscillator 8. FIG. 5 is an explanatory diagram showing the experimental results regarding the relationship between the tilt angle and the rate of change of the upper surface 4a of the ultrasonic transducer 4 with respect to the liquid surface of the oil-containing scum Scoil.

含油スカムScoilの量と含油スカムScoilの削減率との関係は、図2に示すように、含油スカムScoilの量が増加するのに伴って削減率は減少する傾向を示す。ここで、削減率とは、含油スカムScoilから含油排水Woil(分離水)が除去されたことによる容積の低減率として規定され、具体的には、「貯留槽2内における減容化前(処理前)の含油スカムの容積」から「貯留槽2内における減容化後(処理後)の含油スカムの容積」を減じた値を「貯留槽2内における減容化前(処理前)の含油スカムの容積」で除した後、100を乗じた値として規定される。ここで、含油排水Woil(分離水)中の油の量(ノルマルヘキサン抽出物質量、以下、「n-Hex」という。単位は、<mg/L>)は、数値が大きいほど含油排水Woil(分離水)中に多くの油が溶け込んでいることを示し、水質が悪化することを意味する。なお、含油スカムScoilの量が45Lの場合に、削減率およびn-Hexともに最も小さい値を示しているが、処理効果が不安定であり、かつ、処理時間が長く掛かるという結果となった。以上の結果より、本実施の形態では、含油スカムScoilの量は、20L以上30L以下、好ましくは30Lとした。 As shown in FIG. 2, the relationship between the amount of oil-containing scum Scoil and the reduction rate of oil-containing scum Scoil shows that the reduction rate tends to decrease as the amount of oil-containing scum Scoil increases. Here, the reduction rate is defined as the volume reduction rate due to the removal of the oil-impregnated wastewater Wheel (separated water) from the oil-impregnated scum School. Specifically, "Before volume reduction (treatment in the storage tank 2)". The value obtained by subtracting the "volume of the oil-impregnated scum after volume reduction (after treatment) in the storage tank 2" from the "volume of the oil-impregnated scum in the previous)" is the value obtained by subtracting the "volume before volume reduction (before treatment) in the storage tank 2". It is defined as a value multiplied by 100 after dividing by "volume of scum". Here, the amount of oil in the oil-impregnated wastewater (separated water) (normal hexane extract substance amount, hereinafter referred to as "n-Hex". The unit is <mg / L>). It indicates that a lot of oil is dissolved in the separated water), which means that the water quality deteriorates. When the amount of oil-containing scum school was 45 L, both the reduction rate and n-Hex showed the smallest values, but the result was that the treatment effect was unstable and the treatment time was long. From the above results, in the present embodiment, the amount of oil-containing scum school was set to 20 L or more and 30 L or less, preferably 30 L.

含油スカムScoilに出力される超音波周波数と削減率との関係は、図3に示すように、40kHz付近において最も高い削減率を示す結果となった。当該結果より、本実施の形態では、含油スカムScoilに出力される超音波周波数は、20kHz以上100kHz以下、好ましくは約40kHzとした。 As shown in FIG. 3, the relationship between the ultrasonic frequency output to the oil-containing scum school and the reduction rate showed the highest reduction rate in the vicinity of 40 kHz. From the above results, in the present embodiment, the ultrasonic frequency output to the oil-containing scum school is set to 20 kHz or more and 100 kHz or less, preferably about 40 kHz.

超音波発振器8の出力と削減率との関係は、図4に示すように、出力が600Wのときに最も大きい削減率を示す結果となった。出力を600Wより大きくすると、分離された含油排水Woil(分離水)の水質が低下し、出力を400W未満にすると、処理時間が長くなってしまう。以上の結果より、本実施の形態では、超音波発振器8の出力は、400W以上600W以下、好ましくは600Wとした。即ち、超音波発振器8が、含油スカムScoil1Lあたり20W以上30W以下、好ましくは20Wの高周波電力を超音波振動子4に供給する構成である。なお、含油スカムScoilに出力される超音波周波数を40kHzおよび超音波発振器8の出力を600Wに設定した場合、削減率は平均で39%を示した。 As shown in FIG. 4, the relationship between the output of the ultrasonic oscillator 8 and the reduction rate shows the largest reduction rate when the output is 600 W. If the output is larger than 600 W, the water quality of the separated oil-impregnated wastewater (separated water) deteriorates, and if the output is less than 400 W, the treatment time becomes long. From the above results, in the present embodiment, the output of the ultrasonic oscillator 8 is 400 W or more and 600 W or less, preferably 600 W. That is, the ultrasonic oscillator 8 is configured to supply high frequency power of 20 W or more and 30 W or less, preferably 20 W, to the ultrasonic oscillator 4 per 1 L of oil-impregnated scoil. When the ultrasonic frequency output to the oil-containing scum school was set to 40 kHz and the output of the ultrasonic oscillator 8 was set to 600 W, the reduction rate was 39% on average.

含油スカムScoilの液面に対する超音波振動子4の上面4aの傾斜角度と変化率との関係は、図5に示すように、傾斜角度が約17.5度において変化率が最も大きい値を示す結果となった。ここで、変化率とは、含油スカムScoilの液面に対する超音波振動子4の上面4aの傾斜角度が0度のときを1としたときの削減率の増減割合として規定される。以上の結果より、本実施の形態では、含油スカムScoilの液面に対する超音波振動子4の上面4aの傾斜角度は、15度以上25度以下、好ましくは約20度とした。 As shown in FIG. 5, the relationship between the tilt angle of the upper surface 4a of the ultrasonic transducer 4 and the rate of change with respect to the liquid surface of the oil-containing scum school shows the value with the largest rate of change when the tilt angle is about 17.5 degrees. The result was. Here, the rate of change is defined as the rate of increase / decrease in the reduction rate when the inclination angle of the upper surface 4a of the ultrasonic transducer 4 with respect to the liquid surface of the oil-impregnated scum School is 0 degree. From the above results, in the present embodiment, the inclination angle of the upper surface 4a of the ultrasonic vibrator 4 with respect to the liquid surface of the oil-containing scum school is set to 15 degrees or more and 25 degrees or less, preferably about 20 degrees.

以上、説明した本実施の形態に係る本発明の含油排水分離装置1によれば、超音波振動子4の上面4aが、含油スカムScoilの液面に対して20度の傾斜角度を有するように、超音波振動子4を貯留槽2に設置するのみであるため、省スペースかつ簡易な構造で含油スカムScoilから含油排水Woil(分離水)やゴミを分離できる。しかも、上面4aが含油スカムScoilの液面に対して傾斜しているため、含油スカムScoilから分離された含油排水Woil(分離水)が上面4aに滞留することがない。即ち、超音波振動子4の上面4aには、常に含油スカムScoilが存在することになるため、キャビテーション効果による含油スカムScoilからの含油排水Woil(分離水)やゴミの分離を促進することができる。この結果、低コストで含油スカムScoilの減容化を実現し得ると共に産廃排出量の削減も図ることができるため、産廃処理費用の削減に寄与することができる。 According to the oil-impregnated drainage separation device 1 of the present invention according to the above-described embodiment, the upper surface 4a of the ultrasonic vibrator 4 has an inclination angle of 20 degrees with respect to the liquid surface of the oil-containing scum school. Since the ultrasonic vibrator 4 is only installed in the storage tank 2, the oil-containing drainage wall (separated water) and dust can be separated from the oil-containing scum school with a space-saving and simple structure. Moreover, since the upper surface 4a is inclined with respect to the liquid surface of the oil-containing scum school, the oil-containing drainage wall (separated water) separated from the oil-containing scum school does not stay on the upper surface 4a. That is, since the oil-impregnated scum school is always present on the upper surface 4a of the ultrasonic transducer 4, it is possible to promote the separation of the oil-containing drainage Woil (separated water) and dust from the oil-containing scum school due to the cavitation effect. .. As a result, the volume of the oil-containing scum school can be reduced at low cost, and the amount of industrial waste discharged can be reduced, which can contribute to the reduction of the industrial waste treatment cost.

また、本実施の形態に係る本発明の含油排水分離装置1によれば、超音波振動子4と、貯留槽2の底壁2aとの間に空間Rが存在するため、上面4aを流下した含油排水Woil(分離水)が、当該空間Rに流れ込み、対流効果によって当該空間Rに滞留している含油スカムScoilを貯留槽2の上方に移動させることができる。これにより、キャビテーション効果による含油スカムScoilからの含油排水Woil(分離水)やゴミの分離を促進することができる。 Further, according to the oil-impregnated drainage separation device 1 of the present invention according to the present embodiment, since the space R exists between the ultrasonic vibrator 4 and the bottom wall 2a of the storage tank 2, the upper surface 4a flows down. The oil-impregnated drainage wall (separated water) flows into the space R, and the oil-containing scum school staying in the space R can be moved above the storage tank 2 due to the convection effect. This makes it possible to promote the separation of oil-impregnated drainage Woil (separated water) and dust from the oil-impregnated scum School due to the cavitation effect.

さらに、本実施の形態に係る本発明の含油排水分離装置1によれば、超音波振動子4の上面のうち含油スカムScoilの液面に最も近い部位と、当該含油スカムScoilの液面と、の距離が5cm以上となるように設定するため、含油スカムScoilの液面に激しい振動が生じることを防止できる。これにより、含油スカムScoilの減容化効果が低減することを抑制することができる。 Further, according to the oil-impregnated drainage separation device 1 of the present invention according to the present embodiment, the portion of the upper surface of the ultrasonic transducer 4 closest to the liquid level of the oil-containing scum school, the liquid level of the oil-containing scum school, and the liquid level of the oil-containing scum school. Since the distance is set to be 5 cm or more, it is possible to prevent violent vibration from occurring on the liquid surface of the oil-containing scum school. As a result, it is possible to suppress the reduction of the volume reducing effect of the oil-containing scum school.

また、本実施の形態に係る本発明の含油排水分離装置1によれば、含油スカムScoilの量を30Lに設定すると共に、含油スカムScoilの温度を10℃以上40℃以下に設定し、さらに、含油スカムScoilに出力される超音波周波数を40kHzに設定すると共に、超音波発振器8の出力を600Wとしたため、含油スカムScoilの粘度が高くなることにより、減容化後の含油スカムScoilの処理が困難になるといった不都合や、減容化後の含油スカムScoilや浮上油が超音波の効果で含油排水Woilに溶け込み分離効果が低下してしまうといった不都合、あるいは、分離された含油排水(分離水)の水質が悪化するといった不都合を抑制できる。これにより、含油スカムScoilから含油排水Woil(分離水)やゴミをより効果的に分離することができる。 Further, according to the oil-containing drainage separation device 1 of the present invention according to the present embodiment, the amount of the oil-containing scum school is set to 30 L, the temperature of the oil-containing scum school is set to 10 ° C. or higher and 40 ° C. or lower, and further. Since the ultrasonic frequency output to the oil-containing scum school is set to 40 kHz and the output of the ultrasonic oscillator 8 is 600 W, the viscosity of the oil-containing scum school increases, so that the oil-containing scum school can be treated after volume reduction. Inconveniences such as difficulty, inconvenience that the oil-containing scum school and floating oil after volume reduction dissolve in the oil-containing drainage school due to the effect of ultrasonic waves, or the separation effect is reduced, or the separated oil-containing drainage (separated water) It is possible to suppress inconveniences such as deterioration of water quality. This makes it possible to more effectively separate the oil-impregnated wastewater (separated water) and dust from the oil-impregnated scum school.

本実施の形態では、超音波振動子4は載置台6の載置面6aに載置することで、上面4aを含油スカムScoilの液面に対して約20度傾斜させると共に、超音波振動子4と貯留槽2の底壁2aとの間に空間Rを設ける構成としたが、これに限らない。例えば、図6に示す変形例の含油排水分離装置1Aに例示するように、超音波振動子4の一端を持ち上げることにより、上面4aを含油スカムScoilの液面に対して約20度傾斜させると共に、超音波振動子4と貯留槽2の底壁2aとの間に空間Rを設ける構成としても良い。 In the present embodiment, the ultrasonic vibrator 4 is placed on the mounting surface 6a of the mounting table 6 so that the upper surface 4a is tilted by about 20 degrees with respect to the liquid surface of the oil-containing scum school and the ultrasonic vibrator is used. A space R is provided between the 4 and the bottom wall 2a of the storage tank 2, but the present invention is not limited to this. For example, as illustrated in the oil-impregnated drainage separation device 1A of the modified example shown in FIG. 6, by lifting one end of the ultrasonic vibrator 4, the upper surface 4a is tilted by about 20 degrees with respect to the liquid surface of the oil-containing scum Scoil. A space R may be provided between the ultrasonic vibrator 4 and the bottom wall 2a of the storage tank 2.

本実施の形態では、超音波振動子4の上面4aを含油スカムScoilの液面に対して約20度傾斜させたが、15度以上25度以下であれば如何なる傾斜角度であっても良い。 In the present embodiment, the upper surface 4a of the ultrasonic transducer 4 is tilted by about 20 degrees with respect to the liquid surface of the oil-containing scum school, but any tilt angle may be used as long as it is 15 degrees or more and 25 degrees or less.

本実施の形態では、貯留槽2には30Lの含油スカムScoilを貯留すると共に、超音波発振器8から超音波振動子4に供給される高周波電力を600Wとしたが、これに限らない。例えば、貯留槽2には20L以上30L以下の含油スカムScoilを貯留すると共に、超音波振動子4に400W以上600W以下の高周波電力を供給する構成、即ち、超音波発振器8が、含油スカムScoil1Lあたり20W以上30W以下の高周波電力を超音波振動子4に供給する構成としても良い。 In the present embodiment, 30 L of oil-containing scum school is stored in the storage tank 2, and the high-frequency power supplied from the ultrasonic oscillator 8 to the ultrasonic oscillator 4 is 600 W, but the present invention is not limited to this. For example, the storage tank 2 stores 20 L or more and 30 L or less of oil-impregnated scoil, and the ultrasonic oscillator 4 is supplied with high-frequency power of 400 W or more and 600 W or less. A configuration may be used in which high-frequency power of 20 W or more and 30 W or less is supplied to the ultrasonic vibrator 4.

本実施の形態では、含油スカムScoilに出力される超音波周波数を40kHzとしたが、20kHz以上100kHz以下であれば如何なる周波数であっても良い。 In the present embodiment, the ultrasonic frequency output to the oil-impregnated scum School is 40 kHz, but any frequency may be used as long as it is 20 kHz or more and 100 kHz or less.

本実施の形態では、超音波振動子4の上面4aを含油スカムScoilの液面に対して傾斜させたが、これに限らない。例えば、図7に例示する変形例の含油排水分離装置1Bに示すように、超音波振動子4の上面4aを含油スカムScoilの液面に対して傾斜させることなく、載置台6Bによって超音波振動子4をかさ上げした状態で載置する構成としても構わない。 In the present embodiment, the upper surface 4a of the ultrasonic vibrator 4 is tilted with respect to the liquid surface of the oil-containing scum school, but the present invention is not limited to this. For example, as shown in the oil-impregnated drainage separation device 1B of the modified example illustrated in FIG. 7, the ultrasonic vibration is caused by the mounting table 6B without inclining the upper surface 4a of the ultrasonic transducer 4 with respect to the liquid surface of the oil-containing scum school. The child 4 may be placed in a raised state.

本実施の形態では、専用のヒーターによって含油スカムScoilを加熱する構成としたが、これに限らない。専用のヒーターに替えて、含油スカムScoilに熱伝達可能な位置に配置された機器、例えば、超音波振動子4などから生じる熱によって含油スカムScoilを加熱する構成としても良い。 In the present embodiment, the oil-containing scum school is heated by a dedicated heater, but the present invention is not limited to this. Instead of the dedicated heater, the oil-containing scum school may be heated by the heat generated from a device arranged at a position where heat can be transferred to the oil-containing scum school, for example, the ultrasonic vibrator 4.

本実施の形態では、温度調節器30は、ヒーターと、開閉器と、温度センサと、制御装置と、を有し、含油スカムScoilの温度が所望の温度を維持するように開閉器を制御する構成としたが、これに限らない。例えば、温度調節器30は、冷却器と、当該冷却器に通電する電流を断続可能な第2開閉器と、をさらに有し、含油スカムScoilの温度が所望の温度を維持するように開閉器および第2開閉器を制御する構成としても良い。 In the present embodiment, the temperature controller 30 includes a heater, a switch, a temperature sensor, and a control device, and controls the switch so that the temperature of the oil-containing scum school maintains a desired temperature. The configuration is limited to this. For example, the temperature controller 30 further includes a cooler and a second switch capable of interrupting the current that energizes the cooler, so that the temperature of the oil-containing scum school is maintained at a desired temperature. And it may be configured to control the second switch.

本実施の形態は、本発明を実施するための形態の一例を示すものである。したがって、本発明は、本実施形態の構成に限定されるものではない。 The present embodiment shows an example of the embodiment for carrying out the present invention. Therefore, the present invention is not limited to the configuration of the present embodiment.

1 含油排水分離装置(含油排水分離装置)
1A 含油排水分離装置(含油排水分離装置)
1B 含油排水分離装置(含油排水分離装置)
2 貯留槽(貯留槽)
2a 底壁(底面)
2b 側壁
4 超音波振動子(振動子)
4a 上面(上面)
6 載置台
6B 載置台
6a 載置面
8 超音波発振器(発振器)
10 バルブ付き吐出配管
12 バルブ付き吐出配管
90 油水分離槽
30 温度調節器(温度調節器)
L 電力ライン
Scoil 含油スカム(含油スカム)
H ホース
P ポンプ
Foil 浮上油
Woil 含油排水
Slg スラッジ
R 空間
1 Oil-impregnated drainage separator (oil-impregnated drainage separator)
1A Oil-impregnated drainage separator (oil-impregnated drainage separator)
1B Oil-impregnated drainage separator (oil-impregnated drainage separator)
2 Storage tank (storage tank)
2a Bottom wall (bottom)
2b Side wall 4 Ultrasonic oscillator (oscillator)
4a Top surface (top surface)
6 Mounting table 6B Mounting table 6a Mounting surface 8 Ultrasonic oscillator (oscillator)
10 Discharge pipe with valve 12 Discharge pipe with valve 90 Oil-water separation tank 30 Temperature controller (Temperature controller)
L Power line School Oil-impregnated scum (oil-impregnated scum)
H Hose P Pump Foil Floating Oil Wheel Oil-Containing Drainage Slg Sludge R Space

Claims (12)

含油スカムを減容化するための含油排水分離装置であって、
前記含油スカムを貯留可能な貯留槽と、
前記含油スカムの液面側を向く上面を有し、該上面が前記液面に対して所定角度傾斜した状態で前記貯留槽内に配置される振動子と、
該振動子に高周波電力を供給可能に該振動子に電気的に接続された発振器と、
を備える含油排水分離装置。
An oil-impregnated wastewater separation device for reducing the volume of oil-impregnated scum.
A storage tank capable of storing the oil-impregnated scum and
An oscillator having an upper surface facing the liquid surface side of the oil-impregnated scum and being arranged in the storage tank with the upper surface tilted by a predetermined angle with respect to the liquid surface.
An oscillator electrically connected to the oscillator that can supply high frequency power to the oscillator,
An oil-impregnated drainage separator equipped with.
前記上面は、前記液面に対して15度以上25度以下、好ましくは約20度の傾斜角度を有している
請求項1に記載の含油排水分離装置。
The oil-impregnated wastewater separation device according to claim 1, wherein the upper surface has an inclination angle of 15 degrees or more and 25 degrees or less, preferably about 20 degrees with respect to the liquid surface.
前記振動子は、前記上面のうち前記液面に最も近い部位と、前記液面と、の距離が5cm以上となるよう前記貯留槽内に配置されている
請求項1または2に記載の含油排水分離装置。
The oil-containing drainage according to claim 1 or 2, wherein the oscillator is arranged in the storage tank so that the distance between the portion of the upper surface closest to the liquid level and the liquid level is 5 cm or more. Separator.
前記貯留槽は、底面を有しており、
前記振動子は、前記底面との間に空間を有する態様で前記貯留槽内に配置される
請求項1ないし3のいずれか1項に記載の含油排水分離装置。
The storage tank has a bottom surface and has a bottom surface.
The oil-impregnated drainage separation device according to any one of claims 1 to 3, wherein the oscillator is arranged in the storage tank so as to have a space between the oscillator and the bottom surface.
前記含油スカムに出力される超音波周波数は、20kHz以上100kHz以下、好ましくは約40kHzである
請求項1ないし4のいずれか1項に記載の含油排水分離装置。
The oil-impregnated wastewater separation device according to any one of claims 1 to 4, wherein the ultrasonic frequency output to the oil-impregnated scum is 20 kHz or more and 100 kHz or less, preferably about 40 kHz.
前記貯留槽に貯留される前記含油スカムは、20L以上30L以下、好ましくは30Lであり、
前記高周波電力は、400W以上600W以下、好ましくは600Wである
請求項1ないし5のいずれか1項に記載の含油排水分離装置。
The oil-containing scum stored in the storage tank is 20 L or more and 30 L or less, preferably 30 L.
The oil-impregnated wastewater separation device according to any one of claims 1 to 5, wherein the high-frequency power is 400 W or more and 600 W or less, preferably 600 W.
前記発振器は、前記含油スカム1Lあたり20W以上30W以下、好ましくは20Wの前記高周波電力を前記振動子に供給する
請求項1ないし6のいずれか1項に記載の含油排水分離装置。
The oil-impregnated drainage separation device according to any one of claims 1 to 6, wherein the oscillator supplies the high-frequency power of 20 W or more and 30 W or less, preferably 20 W per 1 L of the oil-impregnated scum to the oscillator.
前記含油スカムの温度を10℃以上40℃以下に調節可能な温度調節器をさらに備える
請求項1ないし7のいずれか1項に記載の含油排水分離装置。
The oil-impregnated wastewater separation device according to any one of claims 1 to 7, further comprising a temperature controller capable of adjusting the temperature of the oil-impregnated scum to 10 ° C. or higher and 40 ° C. or lower.
含油スカムを減容化するための含油排水分離方法であって、
(a)貯留槽に前記含油スカムを貯留し、
(b)前記含油スカムの液面に対して上面が所定角度傾斜した状態となるよう振動子を前記貯留槽内に配置し、
(c)前記振動子に高周波電力を供給する
含油排水分離方法。
It is an oil-impregnated wastewater separation method for reducing the volume of oil-impregnated scum.
(A) The oil-impregnated scum is stored in a storage tank, and the oil-impregnated scum is stored.
(B) The oscillator is arranged in the storage tank so that the upper surface is inclined by a predetermined angle with respect to the liquid level of the oil-impregnated scum.
(C) An oil-containing wastewater separation method for supplying high-frequency power to the oscillator.
前記ステップ(b)は、前記上面を前記液面に対して15度以上25度以下、好ましくは約20度の傾斜角となるように前記振動子を前記貯留槽内に配置するステップを含んでいる
請求項9に記載の含油排水分離方法。
The step (b) includes a step of arranging the oscillator in the storage tank so that the upper surface has an inclination angle of 15 degrees or more and 25 degrees or less, preferably about 20 degrees with respect to the liquid surface. The oil-impregnated wastewater separation method according to claim 9.
前記ステップ(b)は、前記上面のうち前記液面に最も近い部位と、前記液面と、の距離が5cm以上となるよう振動子を前記貯留槽に配置するステップを含んでいる
請求項9または10に記載の含油排水分離方法。
9. The step (b) includes a step of arranging the oscillator in the storage tank so that the distance between the portion of the upper surface closest to the liquid level and the liquid level is 5 cm or more. Alternatively, the oil-impregnated wastewater separation method according to 10.
前記ステップ(b)は、前記振動子と、前記貯留槽の底面と、の間に空間を有する態様で前記振動子を前記貯留槽内に配置するステップを含んでいる
請求項9ないし11のいずれか1項に記載の含油排水分離方法。
9. The oil-impregnated wastewater separation method according to item 1.
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