JP2022025772A - Robust drinking feel enhancing agent composed of dehydrorose oxide - Google Patents
Robust drinking feel enhancing agent composed of dehydrorose oxide Download PDFInfo
- Publication number
- JP2022025772A JP2022025772A JP2020128844A JP2020128844A JP2022025772A JP 2022025772 A JP2022025772 A JP 2022025772A JP 2020128844 A JP2020128844 A JP 2020128844A JP 2020128844 A JP2020128844 A JP 2020128844A JP 2022025772 A JP2022025772 A JP 2022025772A
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- JP
- Japan
- Prior art keywords
- beverage
- beverages
- drinking
- feeling
- dehydrorose
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 230000035622 drinking Effects 0.000 title claims abstract description 57
- 230000002708 enhancing effect Effects 0.000 title claims abstract description 17
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- 235000015197 apple juice Nutrition 0.000 claims abstract description 10
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 9
- 239000000203 mixture Substances 0.000 claims description 38
- 239000000796 flavoring agent Substances 0.000 claims description 33
- 235000019634 flavors Nutrition 0.000 claims description 33
- 235000013616 tea Nutrition 0.000 claims description 13
- 238000000034 method Methods 0.000 claims description 12
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- 235000019640 taste Nutrition 0.000 abstract description 11
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- 239000001069 triethyl citrate Substances 0.000 description 1
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Landscapes
- Tea And Coffee (AREA)
- Non-Alcoholic Beverages (AREA)
- Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)
Abstract
Description
本発明はデヒドロローズオキシドからなる飲みごたえ感増強剤および該飲みごたえ感増強剤を含有する飲みごたえ感増強用香料組成物もしくは飲みごたえ感が増強された飲料に関する。 The present invention relates to a mouthfeel-enhancing agent composed of dehydrorose oxide, a flavoring composition for enhancing the feeling of drinking, or a beverage having an enhanced feeling of drinking.
近年、消費者の多様化する嗜好、例えば、飲食品業界においては消費者の嗜好に合うおいしさや、天然感を有する香気・香味を有する飲食品へのニーズに応じるため様々な技術開発が求められている。 In recent years, various technological developments have been required to meet the diversifying tastes of consumers, for example, in the food and beverage industry, the taste that suits the tastes of consumers and the needs for foods and drinks that have a natural aroma and flavor. ing.
健康志向による低糖化や透明な飲料の流行など、飲料中に糖質をはじめとした固形分の配合を少なくした製品が増えてきている。これらの飲料では、カロリーの低減や、外観等を優先させるあまり、風味の点を犠牲にしているものが少なくない。この問題を解決するために種々の方法が開発されているが、いずれも十分ではない。 The number of products that contain less solids such as sugar in beverages is increasing due to health-conscious low sugar content and the popularity of transparent beverages. Many of these beverages sacrifice flavor because they give priority to reducing calories and appearance. Various methods have been developed to solve this problem, but none of them is sufficient.
飲料について評価するのに重要な要素として、「飲みごたえ感」がある。これは飲料が備える初期的な風味ではなく、飲料を飲んだ後に残る風味について示している。 An important factor in evaluating beverages is "feeling of drinking". This is not the initial flavor of the beverage, but the flavor that remains after drinking the beverage.
飲料の飲みごたえ感については、(Z)-3-ヘキセン-1-オール、インドール及び3-メチルノナン-2,4-ジオンを茶飲料に任意の割合で添加することにより、茶飲料の飲みごたえ感を増強する方法(特許文献1)、2,3-ジエチル-5-メチルピラジンと、2-メチルピラジン、3-エチル-2,5-ジメチルピラジン及び2,5-ジメチル-4-ヒドロキシ-3(2H)-フラノンからなる群から選ばれる1種以上の化合物を茶飲料に任意の割合で添加することにより、茶飲料の飲みごたえ感を増強する方法(特許文献2)、A)有機酸、B)イソアミルアルコールおよびC)イソ酪酸、カプロン酸および2-フェネチルアルコールから選ばれる1種以上を任意の割合で含有する、醸造酒様の飲みごたえが付与されたアルコール飲料(特許文献3)が開示されている。 Regarding the feeling of drinking of the beverage, by adding (Z) -3-hexen-1-ol, indole and 3-methylnonan-2,4-dione to the tea beverage in an arbitrary ratio, the feeling of drinking of the tea beverage (Patent Document 1), 2,3-diethyl-5-methylpyrazine, 2-methylpyrazine, 3-ethyl-2,5-dimethylpyrazine and 2,5-dimethyl-4-hydroxy-3 ( 2H) -A method of enhancing the drinkability of a tea beverage by adding one or more compounds selected from the group consisting of furanone to the tea beverage at an arbitrary ratio (Patent Document 2), A) Organic acid, B. ) Isoamyl alcohol and C) An alcoholic beverage having a brewed liquor-like texture and containing at least one selected from isobutyric acid, caproic acid and 2-phenethyl alcohol in an arbitrary ratio (Patent Document 3) is disclosed. ing.
しかしながら、これらの発明は、茶飲料やアルコール飲料といった、特定の飲料において飲みごたえ感の付与または増強についての効果を謳ったものにすぎず、一般的かつ様々な飲料について効果を示したものではない。 However, these inventions merely claim the effect of imparting or enhancing the feeling of drinking in a specific beverage such as a tea beverage or an alcoholic beverage, and do not show the effect on general and various beverages. ..
2-(2-メチル-1-プロペニル)-4-メチレンテトラヒドロピラン(以下デヒドロローズオキシドと記す)は、香料化合物として有用なローズオキシドの合成原料として開示されている(特許文献4、特許文献5、特許文献6)。また、デヒドロローズオキシドそれ自体の有用な合成方法が開示されている(特許文献7)。さらに、デヒドロローズオキシドが香料化合物として有用であることが開示されている(特許文献8、特許文献9)。
しかしながら、デヒドロローズオキシドが飲料の飲みごたえ感を増強することについては記載されていない。
2- (2-Methyl-1-propenyl) -4-methylenetetrahydropyran (hereinafter referred to as dehydrorose oxide) is disclosed as a synthetic raw material for rose oxide useful as a fragrance compound (Patent Documents 4 and 5). , Patent Document 6). Further, a useful method for synthesizing dehydrorose oxide itself is disclosed (Patent Document 7). Further, it is disclosed that dehydrorose oxide is useful as a fragrance compound (Patent Documents 8 and 9).
However, it is not described that dehydrorose oxide enhances the drinkability of beverages.
本発明の目的は、飲料の飲みごたえ感増強剤ならびに、飲料の飲みごたえ感増強方法を提供することにある。 An object of the present invention is to provide an agent for enhancing the feeling of drinking of a beverage and a method for enhancing the feeling of drinking of a beverage.
本発明者らは、上記の課題を解決するために鋭意研究を行ってきた結果、デヒドロローズオキシドが飲料、特に炭酸飲料、ビールテイスト飲料、ニアウォーター飲料、りんご果汁飲料、紅茶飲料またはコーヒー飲料の飲みごたえ感を増強することを見いだし、本発明を完成するに至った。 As a result of diligent research to solve the above problems, the present inventors have found that dehydrorose oxide is used in beverages, especially carbonated beverages, beer-taste beverages, near water beverages, apple juice beverages, tea beverages or coffee beverages. We have found that it enhances the feeling of drinking, and have completed the present invention.
かくして、本発明は
(1)デヒドロローズオキシドからなる飲料の飲みごたえ感増強剤。
(2)(1)に記載の飲料が、炭酸飲料、ビールテイスト飲料、ニアウォーター飲料、りんご果汁飲料、紅茶飲料またはコーヒー飲料から選択される飲みごたえ感増強剤。
(3)(1)または(2)から選択される飲みごたえ感増強剤を、香料組成物中に0.5ppb~10%の濃度含有する飲みごたえ感増強用香料組成物。
(4)(1)または(2)から選択される飲みごたえ感増強剤を飲料中に0.05ppt~10ppmの濃度含有する飲料。
(5)(1)または(2)から選択される飲みごたえ感増強剤を飲料中に0.05ppt~10ppmの濃度添加する飲料の飲みごたえ感増強方法。
を提供する。
Thus, the present invention is (1) an agent for enhancing the feeling of drinking of a beverage composed of dehydrorose oxide.
(2) The beverage according to (1) is a drinkability enhancer selected from carbonated beverages, beer-taste beverages, near water beverages, apple juice beverages, tea beverages or coffee beverages.
(3) A flavoring composition for enhancing the feeling of drinking, which contains the agent for enhancing the feeling of drinking selected from (1) or (2) at a concentration of 0.5 ppb to 10% in the flavor composition.
(4) A beverage containing a drinkability enhancer selected from (1) or (2) at a concentration of 0.05 ppt to 10 ppm in the beverage.
(5) A method for enhancing the drinkability by adding a drinkability enhancer selected from (1) or (2) to the beverage at a concentration of 0.05 ppt to 10 ppm.
I will provide a.
本発明のデヒドロローズオキシドは、飲料、特に炭酸飲料、ビールテイスト飲料、ニアウォーター飲料、りんご果汁飲料、紅茶飲料またはコーヒー飲料に一定量添加することにより、飲料の飲みごたえ感を増強し、また、飲料へ後半の厚味のある味を増強する効果を有し、消費者の嗜好に合うバラエティーに富んだ飲料を提供することが可能となる。 The dehydrorose oxide of the present invention enhances the drinkability of beverages by adding a certain amount to beverages, particularly carbonated beverages, beer-taste beverages, near water beverages, apple juice beverages, tea beverages or coffee beverages. It has the effect of enhancing the thick taste of the latter half of the beverage, and makes it possible to provide a wide variety of beverages that meet the tastes of consumers.
以下、本発明について更に詳細に説明する。 Hereinafter, the present invention will be described in more detail.
本発明において、%、ppm、ppb、pptの値は特に断りのない限り、それぞれ質量対質量の値を示す。 In the present invention, the values of%, ppm, ppb, and ppt indicate the values of mass vs. mass, respectively, unless otherwise specified.
本発明に記載の以下の式(1)に示される、デヒドロローズオキシドは、上述の特許文献7に記載する方法、すなわち、イソプレノールおよびプレナールを任意の触媒を用いて調製することができる。 The dehydrorose oxide represented by the following formula (1) described in the present invention can be prepared by the method described in the above-mentioned Patent Document 7, that is, isoprenol and plenal using any catalyst.
本発明において「飲料の飲みごたえ感」とは、飲料を飲んだ時の飲用後に感じる風味であり、特に厚味、呈味を示し、飲用した充実感を想起させるものである。 In the present invention, the "drinking feeling of a beverage" is a flavor felt after drinking when a beverage is drunk, and particularly shows a thick taste and a taste, and reminds us of a fulfilling feeling of drinking.
本発明において「厚味」とは、飲料中に感じられる味が、飲料全体に広がることを意味する。 In the present invention, the "thick taste" means that the taste felt in the beverage spreads throughout the beverage.
本発明のデヒドロローズオキシドは、そのまま飲料に添加することにより、飲料の飲みごたえ感を増強することができるが、他の成分と混合して香料組成物を調製し、該香料組成物を用いて飲料の飲みごたえ感を増強することもできる。該香料組成物のデヒドロローズオキシドと共に含有し得る他の香料成分としては、各種の合成香料、天然香料、天然精油、動植物エキスなどを挙げることができる。 The dehydrorose oxide of the present invention can be added to a beverage as it is to enhance the drinkability of the beverage. However, a flavor composition is prepared by mixing with other components, and the flavor composition is used. It is also possible to enhance the feeling of drinking of the beverage. Other fragrance components that can be contained together with the dehydrorose oxide of the fragrance composition include various synthetic fragrances, natural fragrances, natural essential oils, animal and plant extracts and the like.
上記の合成香料として、例えば、炭化水素化合物としてα-ピネン、β-ピネン、ミルセン、カンフェン、リモネンなどのモノテルペン、バレンセン、セドレン、カリオフィレン、ロンギフォレンなどのセスキテルペン、1,3,5-ウンデカトリエンなどが挙げられる。 As the above synthetic fragrances, for example, as hydrocarbon compounds, monoterpenes such as α-pinene, β-pinene, myrcene, camphene and limonene, sesquiterpenes such as valencene, cedrene, cariophyllene and longifolene, 1,3,5-undeca Trien and the like can be mentioned.
アルコール化合物としてプロパノール、ブタノール、ペンタノール、ヘキサノール、オクタノール、2-ブタノール、3-メチルブタノールなどの直鎖・飽和アルカノール、プレノール、(Z)-3-ヘキセン-1-オール、(E)-2-ヘキセン-1-オール、2,6-ノナジエノールなどの直鎖・不飽和アルコール、リナロール、ゲラニオール、ターピネオール、シトロネロール、テトラヒドロミルセノール、ファルネソール、ネロリドール、セドロールなどのテルペンアルコール、ベンジルアルコール、フェニルエチルアルコールなどの芳香族アルコールが挙げられる。 As alcohol compounds, linear / saturated alkanols such as propanol, butanol, pentanol, hexanol, octanol, 2-butanol, 3-methylbutanol, plenol, (Z) -3-hexene-1-ol, (E) -2- Linear / unsaturated alcohols such as hexen-1-ol and 2,6-nonazienol, terpenal alcohols such as linalool, geraniol, tarpineol, citronellol, tetrahydromilsenol, farnesol, nerolidol and sedrol, benzyl alcohol and phenylethyl alcohol. Aromatic alcohols such as.
アルデヒド化合物としてアセトアルデヒド、ブタナール、ペンタナール、ヘキサナール、オクタナール、デカナールなどの直鎖・飽和アルデヒド、(Z)-3-ヘキセナール、(E)-2-ヘキセナール、2,4-オクタジエナールなどの直鎖・不飽和アルデヒド、シトロネラール、シトラールなどのテルペンアルデヒド、ベンズアルデヒド、シンナミルアルデヒド、バニリン、エチルバニリン、ヘリオトロピンなどの芳香族アルデヒドが挙げられる。 As aldehyde compounds, straight chain / saturated aldehydes such as acetaldehyde, butanal, pentanal, hexanal, octanal, and decanal, linear chain such as (Z) -3-hexenal, (E) -2-hexenal, and 2,4-octadienal. Examples include unsaturated aldehydes, terpenaldehydes such as citroneral and citral, aromatic aldehydes such as benzaldehyde, cinnamylaldehyde, vanillin, ethyl vanillin and heliotropin.
ケトン化合物として2-ヘプタノン、2-ウンデカノン、1-オクテン-3-オンなどの直鎖・飽和および不飽和ケトン、アセトイン、ジアセチル、2,3-ペンタジオン、マルトール、エチルマルトール、シクロテン、2,5-ジメチル-4-ヒドロキシ-3(2H)-フラノンなどの直鎖および環状ジケトンおよびヒドロキシケトン、カルボン、メントン、ヌートカトンなどのテルペンケトン、α-イオノン、β-イオノン、β-ダマセノンなどのテルペン分解物に由来するケトン、ラズベリーケトンなどの芳香族ケトンが挙げられる。 Linear / saturated and unsaturated ketones such as 2-heptanone, 2-undecanone, 1-octen-3-one, acetoin, diacetyl, 2,3-pentadione, maltor, ethylmaltor, cycloten, 2,5- as ketone compounds For linear and cyclic diketones such as dimethyl-4-hydroxy-3 (2H) -furanone and terpene ketones such as hydroxyketones, carboxylics, menthone and nutcatons, and terpene decomposition products such as α-ionone, β-ionone and β-damasenone. Examples thereof include aromatic ketones such as derived ketones and raspberry ketones.
フラン・エーテル化合物としてフルフリルアルコール、フルフラール、ローズオキシド、リナロールオキシド、メントフラン、テアスピランなどの環状エーテル類が挙げられる。 Examples of the furan ether compound include cyclic ethers such as furfuryl alcohol, furfural, rose oxide, linalool oxide, mentofran, and theaspirane.
エステル化合物として酢酸エチル、酢酸ブチル、酢酸アミル、酢酸イソアミル、酢酸ヘキシル、酢酸オクチルなどの脂肪族アルコールの酢酸エステル、酢酸リナリル、酢酸ゲラニル、酢酸ラバンジュリルなどのテルペンアルコール酢酸エステル、ギ酸エチル、ギ酸イソアミル、酪酸エチル、吉草酸エチル、吉草酸アミル、ヘキサン酸エチル、オクタン酸エチルなどの脂肪酸と低級アルコールエステル、酪酸ゲラニル、酪酸ネリル、イソ吉草酸ゲラニル、イソ吉草酸ネリル、ヘキサン酸ゲラニル、オクタン酸リナリルなどの脂肪酸とテルペンアルコールのエステル、酢酸ベンジル、酢酸フェニルエチル、酢酸ジメチルベンジルカルビニル、酢酸スチラリル、イソ酪酸フェニルエチル、イソ吉草酸シンナミル、サリチル酸メチルなどの芳香族エステルが挙げられる。 As ester compounds, acetates of aliphatic alcohols such as ethyl acetate, butyl acetate, amyl acetate, isoamyl acetate, hexyl acetate, octyl acetate, terpene alcohol acetates such as linaryl acetate, geranyl acetate, lavandryl acetate, ethyl formate, isoamyl formate, Acetic acid and lower alcohol esters such as ethyl butyrate, ethyl valerate, amyl valerate, ethyl hexanoate, ethyl octanate, geranyl butyrate, neryl butyrate, geranyl isovalerate, neryl isovalerate, geranyl hexane, linaryl octanate, etc. Examples thereof include aromatic esters such as esters of fatty acids and terpene alcohols, benzyl acetate, phenylethyl acetate, dimethylbenzyl carvinyl acetate, styralyl acetate, phenylethyl isobutyrate, cinnamyl isovalerate, and methyl salicylate.
ラクトン化合物としてγ-デカラクトン、γ-ウンデカラクトン、γ-ドデカラクトン、δ-デカラクトン、δ-ウンデカラクトン、δ-ドデカラクトンなどの飽和ラクトン、7-デセン-4-オリド、2-デセン-5-オリドなどの不飽和ラクトンが挙げられる。 Saturated lactones such as γ-decalactone, γ-undecalactone, γ-dodecalactone, δ-decalactone, δ-undecalactone, δ-dodecalactone, 7-decene-4-olid, 2-decene-5 as lactone compounds. -Saturated lactones such as oride can be mentioned.
酸化合物として酢酸、酪酸、2-メチル酪酸、ヘキサン酸、オクタン酸、デカン酸、ステアリン酸、オレイン酸、リノール酸、リノレン酸などの飽和・不飽和脂肪酸が挙げられる。 Examples of the acid compound include saturated and unsaturated fatty acids such as acetic acid, butyric acid, 2-methylbutyric acid, hexanoic acid, octanoic acid, decanoic acid, stearic acid, oleic acid, linoleic acid and linolenic acid.
含窒素化合物としてインドール、スカトール、ピリジン、アルキル置換ピラジン、アントラニル酸メチルなどが挙げられる。 Examples of the nitrogen-containing compound include indole, skatole, pyridine, alkyl-substituted pyrazine, and methyl anthranilate.
含硫化合物としてメタンチオール、ジメチルスルフィド、ジメチルジスルフィド、メチオノール、メチオナール、アリルイソチオシアネートなどが挙げられる。 Examples of the sulfur-containing compound include methanethiol, dimethyl sulfide, dimethyl disulfide, methionol, methional, allyl isothiocyanate and the like.
天然精油としてはスイートオレンジ、ビターオレンジ、プチグレン、レモン、ベルガモット、マンダリン、ネロリ、ペパーミント、スペアミント、ラベンダー、カモミール、ローズマリー、ユーカリ、セージ、バジル、ローズ、ゼラニウム、ジャスミン、イランイラン、アニス、クローブ、ジンジャー、ナツメグ、カルダモン、スギ、ヒノキ、ベチバー、パチョリ、ラブダナムなどが挙げられる。 Natural essential oils include sweet orange, bitter orange, petitgrain, lemon, bergamot, mandarin, neroli, peppermint, spearmint, lavender, chamomile, rosemary, eucalyptus, sage, basil, rose, geranium, jasmine, Iran Iran, anis, cloves, Ginger, nutmeg, cardamon, cedar, hinoki, vechibar, patchouli, lovedanum, etc. can be mentioned.
天然香料としてはヒヤシンスアブソリュート、ローズアブソリュート、チュベローズアブソリュート、バニラアブソリュート、ガルバナムレジノイドなどが挙げられる。 Examples of natural fragrances include hyacinth absolute, rose absolute, tuberose absolute, vanilla absolute, galbanum resinoid and the like.
また、各種のエキスとしてハーブ・スパイス抽出物、コーヒー・緑茶・紅茶・ウーロン茶抽出物など、乳または乳加工品およびこれらのリパーゼ・プロテアーゼなどの酵素分解物などが挙げられる。 In addition, various extracts include herbs / spice extracts, coffee / green tea / black tea / oolong tea extracts, milk or processed dairy products, and enzymatic decomposition products such as lipases / proteases thereof.
加えて、他の香料成分として、「特許庁、周知慣用技術集(香料)第II部食品香料、平成12年1月14日発行」または「合成香料、化学と商品知識、増補新版、化学工業日報発行」に記載されている合成香料、天然精油、天然香料、動植物エキス等を挙げることができる。 In addition, as other perfume ingredients, "Patent Office, Well-known Conventional Technology Collection (Fragrance) Part II Food Fragrance, Issued January 14, 2000" or "Synthetic Fragrance, Chemistry and Product Knowledge, Augmented New Edition, Chemical Industry" Examples thereof include synthetic fragrances, natural essential oils, natural fragrances, animal and plant extracts described in "Daily Report Issue".
なお、上記他の香料成分は、1種単独で用いられてもよいし、2種以上の組み合わせで用いられてもよい。 The other fragrance components may be used alone or in combination of two or more.
また、他の添加剤としては、特に制限されず、公知のものが使用できるが、例えば、水、エタノール、エチレングリコール、1,2-プロピレングリコール、ジプロピレングリコール、グリセリン、ヘキシルグリコール、ベンジルベンゾエート、トリアセチン、トリエチルシトレート、ジエチルフタレート、ハーコリン、中鎖脂肪酸トリグリセライド、中鎖脂肪酸ジグリセライド等の溶剤または香料保留剤を挙げることができる。なお、上記他の添加剤は、1種単独で用いられてもよいし、2種以上の組み合わせで用いられてもよい。 The other additives are not particularly limited, and known ones can be used, and examples thereof include water, ethanol, ethylene glycol, 1,2-propylene glycol, dipropylene glycol, glycerin, hexyl glycol, and benzyl benzoate. Examples thereof include solvents such as triacetin, triethylcitrate, diethylphthalate, harcholine, medium-chain fatty acid triglyceride, and medium-chain fatty acid diglyceride, or fragrance-retaining agents. The other additives may be used alone or in combination of two or more.
また、グリセリン脂肪酸エステル、ソルビタン脂肪酸エステル、プロピレングリコール脂肪酸エステル、ショ糖脂肪酸エステル、レシチン、キラヤサポニン、カゼインナトリウムなどの乳化剤を添加してもよい。かような乳化剤を添加することにより、本発明の一形態に係る香料組成物は、乳化香料として使用することができる。 Further, emulsifiers such as glycerin fatty acid ester, sorbitan fatty acid ester, propylene glycol fatty acid ester, sucrose fatty acid ester, lecithin, kiraya saponin, and sodium caseinate may be added. By adding such an emulsifier, the fragrance composition according to one embodiment of the present invention can be used as an emulsified fragrance.
さらにまた、アラビアガムやデキストリンなどの乳化香料を添加してもよい。かような乳化香料を添加した後、さらに乾燥することで、本発明の一形態に係る香料組成物は、粉末香料として使用することができる。 Furthermore, emulsified flavors such as gum arabic and dextrin may be added. By further drying after adding such an emulsified fragrance, the fragrance composition according to one embodiment of the present invention can be used as a powdered fragrance.
本発明のデヒドロローズオキシドを有効成分として含んでなる香料組成物は、上記のようにそれ自体単独で、またはデヒドロローズオキシドを含んでなる香料組成物を調製して、各種の飲料に添加することにより、飲料の飲みごたえ感を増強することができる。 The perfume composition containing the dehydrorose oxide of the present invention as an active ingredient may be added to various beverages by itself as described above or by preparing a perfume composition containing the dehydrorose oxide. Therefore, it is possible to enhance the feeling of drinking of the beverage.
本実施形態に係る飲料としては、特に限定されないが、飲みごたえ感の増強を求められる飲料であることが好ましく、例えば、炭酸飲料、コーラ飲料、果汁入り炭酸飲料、乳類入り炭酸飲料などの炭酸飲料類;オレンジ果汁飲料、グレープフルーツ果汁飲料、レモン果汁飲料、りんご果汁飲料、ぶどう果汁飲料、ピーチ果汁飲料、パイナップル果汁飲料、マンゴー果汁飲料などの果汁飲料類;トマトジュース、ミックス野菜飲料、にんじんジュース、青汁などの野菜飲料類;スポーツドリンク、ニアウォーター飲料、ハチミツ飲料、豆乳、ビタミン補給飲料、ミネラル補給飲料、栄養ドリンク、滋養ドリンク、乳酸菌飲料、乳飲料、ビールテイスト飲料などのソフト飲料類;緑茶飲料、紅茶飲料、ウーロン茶飲料、ハーブティー、ミルクティー、コーヒー飲料などの嗜好飲料類;ビール、ワイン、チューハイ、カクテルドリンク、発泡酒、日本酒、果実酒、薬味酒などのアルコール飲料類を挙げることができる。 The beverage according to the present embodiment is not particularly limited, but is preferably a beverage that is required to enhance the feeling of drinking, and for example, carbonic acid such as a carbonated beverage, a cola beverage, a carbonated beverage containing fruit juice, and a carbonated beverage containing milk. Beverages: Orange fruit juice drinks, grapefruit juice drinks, lemon juice drinks, apple juice drinks, grape juice drinks, peach juice drinks, pineapple juice drinks, mango juice drinks and other fruit juice drinks; tomato juice, mixed vegetable drinks, carrot juice, Vegetable beverages such as green juice; sports drinks, near water beverages, honey beverages, soy milk, vitamin supplement beverages, mineral supplement beverages, nutritional drinks, nourishing drinks, lactic acid bacteria beverages, milk beverages, beer-taste beverages and other soft beverages; green tea Beverages, tea beverages, oolong tea beverages, herbal teas, milk teas, coffee beverages and other favorite beverages; can.
本発明の香料組成物におけるデヒドロローズオキシドの含有量は、混合される他の香料成分により異なり一概には言えないが、香料組成物の全体質量に対して下限値としては、0.5ppb、1ppb、5ppb、10ppb、20ppb、50ppb、100ppb、200ppbが例示でき、上限値としては、10%、5%、2%、1%、0.5%、0.2%、0.1%、500ppbが例示でき、これら下限及び上限値の任意の組み合わせを挙げることができる。特に、0.5ppb~10%(本明細書においては「~」は上限値および下限値を含む範囲を意味する)、好ましくは、1ppb~5%、より好ましくは5ppb~1%、特に好ましくは10ppb~0.5%、より特に好ましくは50ppb~0.1%の範囲とすることができる。 The content of dehydrorose oxide in the fragrance composition of the present invention varies depending on the other fragrance components to be mixed and cannot be unequivocally determined, but the lower limit with respect to the total mass of the fragrance composition is 0.5 ppb, 1 ppb. , 5ppb, 10ppb, 20ppb, 50ppb, 100ppb, 200ppb can be exemplified, and the upper limit values are 10%, 5%, 2%, 1%, 0.5%, 0.2%, 0.1% and 500ppb. By way of example, any combination of these lower and upper limits can be mentioned. In particular, 0.5 ppb to 10% (in the present specification, "-" means a range including an upper limit value and a lower limit value), preferably 1 ppb to 5%, more preferably 5 ppb to 1%, and particularly preferably. It can be in the range of 10 ppb to 0.5%, more particularly preferably 50 ppb to 0.1%.
本発明の飲料におけるデヒドロローズオキシドの含有量は、飲料の種類や形態に応じて異なり一概には言えないが、通常、飲料の重量を基準として、飲料の全体質量に対して下限値としては、0.05ppt、0.1ppt、0.2ppt、0.5ppt、1ppt、5ppt、10ppt、20pptが例示でき、上限値としては、10ppm、5ppm、2ppm、1ppm、0.5ppm、0.2ppm、0.1ppm、50ppbが例示でき、これら下限及び上限値の任意の組み合わせを挙げることができる。特に、0.05ppt~10ppm、好ましくは0.1ppt~5ppm、より好ましくは0.5ppt~1ppm、特に好ましくは1ppt~0.5ppm、より特に好ましくは5ppt~0.1ppmの濃度範囲とすることができる。 The content of dehydrorose oxide in the beverage of the present invention varies depending on the type and form of the beverage and cannot be unequivocally determined. Examples thereof are 0.05 ppt, 0.1 ppt, 0.2 ppt, 0.5 ppt, 1 ppt, 5 ppt, 10 ppt, and 20 ppt, and the upper limit values are 10 ppm, 5 ppm, 2 ppm, 1 ppm, 0.5 ppm, 0.2 ppm, 0. Examples include 1 ppm and 50 ppb, and any combination of these lower and upper limits can be mentioned. In particular, the concentration range may be 0.05 ppt to 10 ppm, preferably 0.1 ppt to 5 ppm, more preferably 0.5 ppt to 1 ppm, particularly preferably 1 ppt to 0.5 ppm, and more particularly preferably 5 ppt to 0.1 ppm. can.
以下、本発明を実施例によりさらに具体的に説明する。なお、本発明はこれらに限定されるものではない。 Hereinafter, the present invention will be described in more detail with reference to Examples. The present invention is not limited to these.
以下の実施例に示すデヒドロローズオキシドは、既知の方法、例えば、特許文献7の方法に従って調製を行った。 The dehydrorose oxides shown in the following examples were prepared according to a known method, for example, the method of Patent Document 7.
参考例1:紅茶抽出物の製造
紅茶葉1000gをミキサーにて粉砕し、水(90℃)15kgおよびアスコルビン酸ナトリウム1.5gを添加し、40℃まで冷却した。これに、タンナーゼ1.5gを加えて40℃、8時間静置反応させ、90℃で10分間加熱して酵素失活した後、吸引濾過により茶葉とエキスを分離し、紅茶エキス13kgを得た。この抽出液をロータリーエバポレーターにて減圧濃縮し、紅茶抽出物620gを得た。この紅茶抽出物を実施例1に供した。
Reference Example 1: Production of black tea extract 1000 g of black tea leaves were crushed with a mixer, 15 kg of water (90 ° C) and 1.5 g of sodium ascorbate were added, and the mixture was cooled to 40 ° C. To this, 1.5 g of tannase was added, and the mixture was allowed to stand at 40 ° C. for 8 hours, heated at 90 ° C. for 10 minutes to inactivate the enzyme, and then the tea leaves and the extract were separated by suction filtration to obtain 13 kg of black tea extract. .. This extract was concentrated under reduced pressure using a rotary evaporator to obtain 620 g of black tea extract. This black tea extract was subjected to Example 1.
実施例1:紅茶フレーバーへのデヒドロローズオキシドの添加
表1に示す紅茶フレーバー処方に基づき香料組成物を調製した。すなわち、デヒドロローズオキシド希釈液(デヒドロローズオキシドが1%となるようにエタノールで希釈:デヒドロローズオキシドが香料組成物中に10ppm)を含有するものを本発明品1、デヒドロローズオキシド希釈液を添加していないものを比較品1とした。
Example 1: Addition of Dehydrorose Oxide to Black Tea Flavor A flavor composition was prepared based on the black tea flavor formulation shown in Table 1. That is, the product containing the dehydrorose oxide diluted solution (diluted with ethanol so that the dehydrorose oxide is 1%: 10 ppm of the dehydrorose oxide in the fragrance composition) is added to the product 1 of the present invention and the dehydrorose oxide diluted solution. The one that was not used was designated as Comparative Product 1.
それぞれの紅茶フレーバーについて、水に0.1%賦香し、よく訓練された13名のパネリストにより、飲みごたえ感について官能評価を行った、その結果、パネリスト13名中12名が本発明品1を添加した水の方が飲みごたえ感があるものと評価した。 For each black tea flavor, 0.1% of the aroma was added to water, and 13 well-trained panelists performed a sensory evaluation of the feeling of drinking. As a result, 12 out of 13 panelists of the present invention 1 It was evaluated that the water to which was added was more responsive to drinking.
実施例2:デヒドロローズオキシドの添加濃度による比較
表1の紅茶フレーバーについて、表1のデヒドロローズオキシド希釈液に代えて希釈液に対するデヒドロローズオキシドの濃度が0.1ppm(香料組成物中に0.1ppb)、1ppm(香料組成物中に1ppb)、10ppm(香料組成物中に10ppb)、100ppm(香料組成物中に100ppb)、0.1%(香料組成物中に1ppm)、1%(香料組成物中に10ppm:本発明品1)、10%(香料組成物中に100ppm)、100%(無希釈:香料組成物中に0.1%)を調製した。
Example 2: Comparison by Addition Concentration of Dehydrorose Oxide Regarding the tea flavor in Table 1, the concentration of dehydrorose oxide with respect to the diluted solution was 0.1 ppm (0. In the flavor composition) instead of the dehydrorose oxide diluted solution in Table 1. 1 ppb), 1 ppm (1 ppb in fragrance composition), 10 ppm (10 ppb in fragrance composition), 100 ppm (100 ppb in fragrance composition), 0.1% (1 ppm in fragrance composition), 1% (fragrance) 10 ppm in the composition: product 1 of the present invention), 10% (100 ppm in the fragrance composition) and 100% (undiluted: 0.1% in the fragrance composition) were prepared.
比較品1を水に0.1%添加した飲料をコントロールとして、デヒドロローズオキシドを添加した紅茶フレーバーを水に0.1%添加し、コントロールを対照として飲みごたえ感について官能評価を実施した。官能評価は13名のよく訓練されたパネリストにより、以下の評価基準で評価を行った。パネリスト13名の平均的な評価点を含む官能評価結果を表2に示す。 A beverage containing 0.1% of Comparative Product 1 in water was used as a control, and a black tea flavor containing dehydrorose oxide was added in 0.1% of water, and a sensory evaluation was performed on the feeling of drinking with the control as a control. The sensory evaluation was performed by 13 well-trained panelists according to the following evaluation criteria. Table 2 shows the sensory evaluation results including the average evaluation points of 13 panelists.
(評価基準)
1:コントロールと比較して飲みごたえ感は非常に弱い;
2:コントロールと比較して飲みごたえ感は弱い;
3:コントロールと比較して飲みごたえ感は変化なし;
4:コントロールと比較して飲みごたえ感は強い;
5:コントロールと比較して飲みごたえ感は非常に強い。
(Evaluation criteria)
1: Very weak to drink compared to control;
2: The feeling of drinking is weak compared to the control;
3: There is no change in the feeling of drinking compared to the control;
4: The feeling of drinking is stronger than that of the control;
5: The feeling of drinking is very strong compared to the control.
デヒドロローズオキシドの紅茶フレーバー中の濃度が0.1ppbの場合は、コントロールと大差がないが、紅茶フレーバーに1ppb含有させると、飲みごたえ感が強くなる。さらに紅茶フレーバー中の濃度を高くすると、飲みごたえ感がさらに強くなった。 When the concentration of dehydrorose oxide in the black tea flavor is 0.1 ppb, it is not much different from the control, but when the black tea flavor contains 1 ppb, the feeling of drinking becomes stronger. Further, when the concentration in the black tea flavor was increased, the feeling of drinking became stronger.
実施例3:ビールフレーバーへのデヒドロローズオキシドの添加
表3に示す成分を使用しビールフレーバーを調製した。すなわち、表3のデヒドロローズオキシド希釈液に対するデヒドロローズオキシドの濃度が0.1ppm(香料組成物中に0.1ppb)、1ppm(香料組成物中に1ppb)、10ppm(香料組成物中に10ppb)、100ppm(香料組成物中に100ppb)、0.1%(香料組成物中に1ppm)、1%(香料組成物中に10ppm)、10%(香料組成物中に100ppm)、100%(無希釈:香料組成物中に0.1%)を調製した。また、デヒドロローズオキシド希釈液を添加していないものを比較品2とした。
Example 3: Addition of Dehydrorose Oxide to Beer Flavor A beer flavor was prepared using the components shown in Table 3. That is, the concentration of dehydrorose oxide with respect to the dehydrorose oxide diluent in Table 3 was 0.1 ppm (0.1 ppb in the fragrance composition), 1 ppm (1 ppb in the fragrance composition), and 10 ppm (10 ppb in the fragrance composition). , 100 ppm (100 ppb in perfume composition), 0.1% (1 ppm in perfume composition), 1% (10 ppm in perfume composition), 10% (100 ppm in perfume composition), 100% (none) Dilution: 0.1%) was prepared in the perfume composition. Further, the product to which the dehydrorose oxide diluted solution was not added was designated as Comparative Product 2.
それぞれのビールフレーバーを水に0.1%添加し、比較品2を水に0.1%となるように添加した飲料をコントロールとし、コントロールを対照として飲みごたえ感について官能評価を実施した。官能評価は13名のよく訓練されたパネリストにより、実施例2と同様の評価基準で評価を行った。パネリスト13名の平均的な評価点を含む官能評価結果を表4に示す。 A beverage in which 0.1% of each beer flavor was added to water and Comparative Product 2 was added to water at 0.1% was used as a control, and a sensory evaluation was performed on the feeling of drinking with the control as a control. The sensory evaluation was performed by 13 well-trained panelists according to the same evaluation criteria as in Example 2. Table 4 shows the sensory evaluation results including the average evaluation points of 13 panelists.
デヒドロローズオキシドのビールフレーバー中の濃度が0.1ppbの場合は、コントロールと大差がないが、ビールフレーバーに1ppb含有させると、飲みごたえ感が強くなる。さらにビールフレーバー中の濃度を高くすると、飲みごたえ感がさらに強くなった。 When the concentration of dehydrorose oxide in the beer flavor is 0.1 ppb, it is not much different from the control, but when the beer flavor contains 1 ppb, the feeling of drinking becomes stronger. Further, when the concentration in the beer flavor was increased, the feeling of drinking became stronger.
実施例4:アップルフレーバーへのデヒドロローズオキシドの添加
表5に示すアップルフレーバー処方に基づき香料組成物を調製した。すなわち、デヒドロローズオキシド希釈液(デヒドロローズオキシドが1%となるようにエタノールで希釈:デヒドロローズオキシドが香料組成物中に10ppm)を含有するものを本発明品17、デヒドロローズオキシド希釈液を添加していないものを比較品3とした。
Example 4: Addition of Dehydrorose Oxide to Apple Flavor A perfume composition was prepared based on the apple flavor formulation shown in Table 5. That is, the product containing the dehydrorose oxide diluted solution (diluted with ethanol so that the dehydrorose oxide is 1%: 10 ppm of the dehydrorose oxide in the fragrance composition) is added to the product 17 of the present invention and the dehydrorose oxide diluted solution. The one that was not used was designated as Comparative Product 3.
それぞれのアップルフレーバーについて、水に0.1%賦香し、よく訓練された13名のパネリストにより、飲みごたえ感について官能評価を行った、その結果、パネリスト13名全員が本発明品17を添加した水の方が飲みごたえ感があるものと評価した。 For each apple flavor, 0.1% was aromatized in water, and 13 well-trained panelists performed a sensory evaluation of the feeling of drinking. As a result, all 13 panelists added the product 17 of the present invention. It was evaluated that the water that had been drained was more satisfying to drink.
実施例5:炭酸飲料へのデヒドロローズオキシドの添加
水1000mLに対して、果糖ぶどう糖液糖(Bx=75°)90g、クエン酸3.3gを溶解させ、クエン酸三ナトリウムを用いてpH3.5に調整後、レモンフレーバー(長谷川香料株式会社製)を1gおよびデヒドロローズオキシドを炭酸飲料中に表6に示す0.01ppt~10ppmの濃度になるように添加し、カーボネーション後65℃×10分間殺菌することにより本発明の炭酸飲料を調製した。
Example 5: Addition of dehydrorose oxide to a carbonated drink 90 g of fructose-glucose liquid sugar (Bx = 75 °) and 3.3 g of citric acid are dissolved in 1000 mL of water, and pH 3.5 is used with trisodium citrate. Add 1 g of lemon flavor (manufactured by Hasegawa Fragrance Co., Ltd.) and dehydrorose oxide to carbonated drinks to a concentration of 0.01 ppt to 10 ppm shown in Table 6 and 65 ° C x 10 minutes after carbonation. The carbonated drink of the present invention was prepared by sterilization.
上記の方法と同様に調製した、デヒドロローズオキシドを添加していない炭酸飲料を比較品4とし、これをコントロールとして飲みごたえ感について官能評価を実施した。官能評価は13名のよく訓練されたパネリストにより、以下の評価基準で評価を行った。パネリスト13名の平均的な評価点を含む官能評価結果を表6に示す。 A carbonated drink to which dehydrorose oxide was not added, which was prepared in the same manner as in the above method, was designated as Comparative Product 4, and a sensory evaluation was performed on the feeling of drinking using this as a control. The sensory evaluation was performed by 13 well-trained panelists according to the following evaluation criteria. Table 6 shows the sensory evaluation results including the average evaluation points of 13 panelists.
(評価基準)
1:コントロールと比較して飲みごたえ感は非常に弱い;
2:コントロールと比較して飲みごたえ感は弱い;
3:コントロールと比較して飲みごたえ感は変化なし;
4:コントロールと比較して飲みごたえ感は強い;
5:コントロールと比較して飲みごたえ感は非常に強い。
(Evaluation criteria)
1: Very weak to drink compared to control;
2: The feeling of drinking is weak compared to the control;
3: There is no change in the feeling of drinking compared to the control;
4: The feeling of drinking is stronger than that of the control;
5: The feeling of drinking is very strong compared to the control.
デヒドロローズオキシドの炭酸飲料中の濃度が0.01pptの場合は、コントロールと大差がないが、炭酸飲料に0.1ppt含有させると、飲みごたえ感が強くなる。さらに炭酸飲料中の濃度を高くすると、飲みごたえ感がさらに強くなった。 When the concentration of dehydrorose oxide in the carbonated drink is 0.01 ppt, it is not much different from the control, but when 0.1 ppt is contained in the carbonated drink, the feeling of drinking becomes stronger. Further, when the concentration in the carbonated drink was increased, the feeling of drinking became stronger.
実施例6:ビールテイスト飲料へのデヒドロローズオキシドの添加
水1000mLに対して、難消化性デキストリン8g、マルトース2g、乳酸0.15g、リン酸0.085g、カラメル(池田糖化工業社製)0.3g、L-アスコルビン酸0.1g、キラヤニン製剤(丸善製薬社製)0.1g、イソアルファー酸0.0015gを溶解させ、クエン酸三ナトリウムを用いてpH3.85に調整後、比較品2のビールフレーバー1gならびにデヒドロローズオキシドをビールテイスト飲料中に表7に示す0.01ppt~10ppmの濃度になるように添加し、カーボネーション後65℃×10分間殺菌することにより本発明のビールテイスト飲料を調製した。
Example 6: Addition of dehydrorose oxide to beer-taste beverage For 1000 mL of water, 8 g of indigestible dextrin, 2 g of maltose, 0.15 g of lactic acid, 0.085 g of phosphoric acid, caramel (manufactured by Ikeda Saccharification Industry Co., Ltd.) 0. 3 g, L-ascorbic acid 0.1 g, Kirayanin preparation (manufactured by Maruzen Pharmaceutical Co., Ltd.) 0.1 g, and isoalphaic acid 0.0015 g were dissolved, adjusted to pH 3.85 with trisodium citrate, and then compared with Comparative Product 2. The beer-taste beverage of the present invention is prepared by adding 1 g of beer flavor and dehydrorose oxide to a beer-taste beverage at a concentration of 0.01 ppt to 10 ppm shown in Table 7 and sterilizing at 65 ° C. for 10 minutes after carbonation. Prepared.
上記の方法と同様に調製した、デヒドロローズオキシドを添加していないビールテイスト飲料を比較品5とし、これをコントロールとして飲みごたえ感について官能評価を実施した。官能評価は13名のよく訓練されたパネリストにより、実施例5と同様の評価基準で評価を行った。パネリスト13名の平均的な評価点を含む官能評価結果を表7に示す。 A beer-taste beverage to which dehydrorose oxide was not added, which was prepared in the same manner as in the above method, was designated as Comparative Product 5, and a sensory evaluation was performed on the feeling of drinking using this as a control. The sensory evaluation was performed by 13 well-trained panelists according to the same evaluation criteria as in Example 5. Table 7 shows the sensory evaluation results including the average evaluation points of 13 panelists.
デヒドロローズオキシドのビールテイスト飲料中の濃度が0.01pptの場合は、コントロールと大差がないが、ビールテイスト飲料に0.1ppt含有させると、飲みごたえ感が強くなる。さらにビールテイスト飲料中の濃度を高くすると、飲みごたえ感がさらに強くなった。 When the concentration of dehydrorose oxide in the beer-taste beverage is 0.01 ppt, it is not much different from the control, but when the beer-taste beverage contains 0.1 ppt, the feeling of drinking becomes stronger. Further, when the concentration in the beer-taste beverage was increased, the feeling of drinking became stronger.
実施例7:ニアウォーター飲料へのデヒドロローズオキシドの添加
水1000mLに対して、果糖25g、グラニュー糖20g、クエン酸1.4gを溶解させ、クエン酸三ナトリウムを用いてpH3.65に調整後、ピーチフレーバー(長谷川香料株式会社製)1gおよびデヒドロローズオキシドを飲料中10ppbの濃度となるように添加し、115℃×30秒間殺菌することにより本発明のニアウォーター飲料(本発明品37)を調製した。
Example 7: Addition of Dehydrorose Oxide to Near Water Beverage After dissolving 25 g of fructose, 20 g of granulated sugar and 1.4 g of citric acid in 1000 mL of water and adjusting the pH to 3.65 with trisodium citrate. The near water beverage of the present invention (product 37 of the present invention) was prepared by adding 1 g of peach flavor (manufactured by Hasegawa Fragrance Co., Ltd.) and dehydrorose oxide to a concentration of 10 ppb in the beverage and sterilizing at 115 ° C. for 30 seconds. did.
上記の方法と同様に調製した、デヒドロローズオキシドを添加していないニアウォーター飲料を比較品6とし、比較品6をコントロールとして本発明品37の飲みごたえ感について官能評価を実施した。官能評価は13名のよく訓練されたパネリストにより、実施例5と同様の評価基準で評価を行った。パネリスト13名の平均的な評価点を含む官能評価結果を表8に示す。 A near water beverage to which dehydrorose oxide was not added, which was prepared in the same manner as described above, was designated as Comparative Product 6, and a sensory evaluation was performed on the feeling of drinking of Product 37 of the present invention using Comparative Product 6 as a control. The sensory evaluation was performed by 13 well-trained panelists according to the same evaluation criteria as in Example 5. Table 8 shows the sensory evaluation results including the average evaluation points of 13 panelists.
上記の結果から、デヒドロローズオキシドを添加したニアウォーター飲料は、飲みごたえ感を向上させる効果を示した。 From the above results, the near water beverage to which dehydrorose oxide was added showed the effect of improving the feeling of drinking.
実施例8:りんご果汁飲料へのデヒドロローズオキシドの添加
水1000mLに対して、果糖ぶどう糖液糖125g、クエン酸2.3gを溶解させ、りんご濃縮透明果汁(果香社製)を果汁20%になるように添加し、クエン酸三ナトリウムを用いてpH3.45に調整後、デヒドロローズオキシドを飲料中10ppbの濃度となるように添加し、115℃×30秒間殺菌することにより本発明のりんご果汁飲料(本発明品38)を調製した。
Example 8: Addition of dehydrorose oxide to apple juice beverage 125 g of fructose-glucose liquid sugar and 2.3 g of citric acid are dissolved in 1000 mL of water to make apple concentrated transparent fruit juice (manufactured by Kaoru Co., Ltd.) 20% of fruit juice. After adjusting the pH to 3.45 with trisodium citrate, add dehydrorose oxide to a concentration of 10 ppb in the beverage and sterilize at 115 ° C for 30 seconds to make the apple juice of the present invention. A beverage (product 38 of the present invention) was prepared.
上記の方法と同様に調製した、デヒドロローズオキシドを添加していないりんご果汁飲料を比較品7とし、比較品7をコントロールとして本発明品38の飲みごたえ感について官能評価を実施した。官能評価は13名のよく訓練されたパネリストにより、実施例5と同様の評価基準で評価を行った。パネリスト13名の平均的な評価点を含む官能評価結果を表9に示す。 An apple juice beverage to which dehydrorose oxide was not added, which was prepared in the same manner as in the above method, was designated as Comparative Product 7, and a sensory evaluation was performed on the feeling of drinking of Product 38 of the present invention using Comparative Product 7 as a control. The sensory evaluation was performed by 13 well-trained panelists according to the same evaluation criteria as in Example 5. Table 9 shows the sensory evaluation results including the average evaluation points of 13 panelists.
上記の結果から、デヒドロローズオキシドを添加したりんご果汁飲料は、飲みごたえ感を向上させる効果を示した。 From the above results, the apple juice beverage to which dehydrorose oxide was added showed an effect of improving the feeling of drinking.
実施例9:紅茶飲料へのデヒドロローズオキシドの添加
80℃の湯285mLに対して、紅茶葉(三井農林社製)5.7gを添加し、5分間抽出を行った。抽出後固液分離を行い、これに、果糖ぶどう糖液糖20g、グラニュー糖20g、L-アスコルビン酸ナトリウム0.3gを添加し、水を加えて1000mLとし、炭酸水素ナトリウムを用いてpH6.0になるように調整後、デヒドロローズオキシドを飲料中10ppbの濃度となるように添加し、135℃×30秒間殺菌することにより本発明の紅茶飲料(本発明品39)を調製した。
Example 9: Addition of dehydrorose oxide to black tea beverage 5.7 g of black tea leaves (manufactured by Mitsui Norin Co., Ltd.) was added to 285 mL of hot water at 80 ° C., and extraction was performed for 5 minutes. After extraction, solid-liquid separation is performed, to which 20 g of fructose-glucose liquid sugar, 20 g of granulated sugar, and 0.3 g of sodium L-ascorbate are added, water is added to make 1000 mL, and sodium hydrogen carbonate is used to adjust the pH to 6.0. The black tea beverage of the present invention (product 39 of the present invention) was prepared by adding dehydrorose oxide to a concentration of 10 ppb in the beverage and sterilizing at 135 ° C. for 30 seconds.
上記の方法と同様に調製した、デヒドロローズオキシドを添加していない紅茶飲料を比較品8とし、比較品8をコントロールとして本発明品39の飲みごたえ感について官能評価を実施した。官能評価は13名のよく訓練されたパネリストにより、実施例5と同様の評価基準で評価を行った。パネリスト13名の平均的な評価点を含む官能評価結果を表10に示す。 A black tea beverage to which dehydrorose oxide was not added, which was prepared in the same manner as described above, was designated as Comparative Product 8, and a sensory evaluation was performed on the feeling of drinking of Product 39 of the present invention using Comparative Product 8 as a control. The sensory evaluation was performed by 13 well-trained panelists according to the same evaluation criteria as in Example 5. Table 10 shows the sensory evaluation results including the average evaluation points of 13 panelists.
上記の結果から、デヒドロローズオキシドを添加した紅茶飲料は、飲みごたえ感を向上させる効果を示した。 From the above results, the black tea beverage to which dehydrorose oxide was added showed the effect of improving the feeling of drinking.
実施例10:コーヒー飲料へのデヒドロローズオキシドの添加
コーヒー豆(ブラジル産・No.4/5・L値20,コロンビア産・EX・L値20を7:3で使用)を粉砕し、得られたコーヒー豆45gに、沸騰した湯でペーパードリップし、コーヒー抽出液360gを得た後、水を加えて1000mLとした(Brix1.2%)。炭酸水素ナトリウムを用いてpH6.5になるように調整後、デヒドロローズオキシドを飲料中10ppbの濃度となるように添加し、121℃×10分間殺菌することにより本発明のコーヒー飲料(本発明品40)を調製した。
Example 10: Addition of Dehydrorose Oxide to Coffee Beverage Coffee beans (Brazilian No. 4/5 L value 20 and Colombian EX L value 20 used at 7: 3) were crushed and obtained. Paper drip was performed on 45 g of the coffee beans with boiling water to obtain 360 g of coffee extract, and then water was added to make 1000 mL (Brix 1.2%). After adjusting the pH to 6.5 with sodium hydrogen carbonate, dehydrorose oxide is added to a concentration of 10 ppb in the beverage, and the beverage is sterilized at 121 ° C. for 10 minutes to obtain the coffee beverage of the present invention (the product of the present invention). 40) was prepared.
上記の方法と同様に調製した、デヒドロローズオキシドを添加していないコーヒー飲料を比較品9とし、比較品9をコントロールとして本発明品40の飲みごたえ感について官能評価を実施した。官能評価は13名のよく訓練されたパネリストにより、実施例5と同様の評価基準で評価を行った。パネリスト13名の平均的な評価点を含む官能評価結果を表11に示す。 A coffee beverage to which dehydrorose oxide was not added, which was prepared in the same manner as described above, was designated as Comparative Product 9, and a sensory evaluation was performed on the feeling of drinking of Product 40 of the present invention using Comparative Product 9 as a control. The sensory evaluation was performed by 13 well-trained panelists according to the same evaluation criteria as in Example 5. Table 11 shows the sensory evaluation results including the average evaluation points of the 13 panelists.
上記の結果から、デヒドロローズオキシドを添加したコーヒー飲料は、飲みごたえ感を向上させる効果を示した。 From the above results, the coffee beverage to which dehydrorose oxide was added showed the effect of improving the feeling of drinking.
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