JP2021143127A - Gommage cosmetic composition - Google Patents
Gommage cosmetic composition Download PDFInfo
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- JP2021143127A JP2021143127A JP2020040483A JP2020040483A JP2021143127A JP 2021143127 A JP2021143127 A JP 2021143127A JP 2020040483 A JP2020040483 A JP 2020040483A JP 2020040483 A JP2020040483 A JP 2020040483A JP 2021143127 A JP2021143127 A JP 2021143127A
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- JP
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- Prior art keywords
- cosmetic composition
- gommage
- gommage cosmetic
- mass
- skin
- Prior art date
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- 239000008117 stearic acid Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000012438 synthetic essential oil Substances 0.000 description 1
- 229920003002 synthetic resin Polymers 0.000 description 1
- TUNFSRHWOTWDNC-HKGQFRNVSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCC[14C](O)=O TUNFSRHWOTWDNC-HKGQFRNVSA-N 0.000 description 1
- BORJONZPSTVSFP-UHFFFAOYSA-N tetradecyl 2-hydroxypropanoate Chemical compound CCCCCCCCCCCCCCOC(=O)C(C)O BORJONZPSTVSFP-UHFFFAOYSA-N 0.000 description 1
- 229940042585 tocopherol acetate Drugs 0.000 description 1
- 229960002703 undecylenic acid Drugs 0.000 description 1
- 229930195735 unsaturated hydrocarbon Natural products 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 229920002554 vinyl polymer Polymers 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
- 239000010497 wheat germ oil Substances 0.000 description 1
- 235000010493 xanthan gum Nutrition 0.000 description 1
- 239000000230 xanthan gum Substances 0.000 description 1
- 229920001285 xanthan gum Polymers 0.000 description 1
- 229940082509 xanthan gum Drugs 0.000 description 1
- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8105—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- A61K8/8111—Homopolymers or copolymers of aliphatic olefines, e.g. polyethylene, polyisobutene; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/28—Rubbing or scrubbing compositions; Peeling or abrasive compositions; Containing exfoliants
Abstract
Description
本発明はゴマージュ化粧料組成物に関する。 The present invention relates to a gommage cosmetic composition.
従来のゴマージュ化粧料は、水に溶解させた高分子樹脂が肌の上で乾燥するときにゴマージュが形成されることにより角質を除去する。もしくは、酸を含有する低いｐＨのゲルを肌の上に塗布することでｐＨが上がり、剤形が変化してゴマージュが形成されることにより角質を除去する。 Conventional gommage cosmetics remove keratin by forming gommage when the polymer resin dissolved in water dries on the skin. Alternatively, a low pH gel containing an acid is applied onto the skin to raise the pH and change the dosage form to form a gommage, thereby removing dead skin cells.
肌の上で乾燥するときにゴマージュが形成されるタイプのゴマージュ化粧料では、浴室等の湿度の高い場所又は水の存在下ではゴマージュが形成されにくかったり、またはゴマージュが形成されるのに時間がかかったりするという問題があった。また、低いｐＨのゲルであるタイプのゴマージュ化粧料では、ｐＨが低いため肌への刺激が強いという問題があった。 In the type of gommage cosmetics that form gommage when it dries on the skin, it is difficult to form gommage in a humid place such as a bathroom or in the presence of water, or it takes time for gommage to form. There was a problem that it took. In addition, the gommage cosmetics, which are gels having a low pH, have a problem that they are strongly irritating to the skin because the pH is low.
これに対応し、特許文献１は肌への刺激性が少ないゴマージュ化粧料を開示している。
特許文献１のゴマージュ化粧料組成物は、不要な皮膚成分を除去するためのゴマージュ化粧料組成物であって、粘着性固形物とこの粘着性固形物を分散する揮発性の分散媒とからなり、前記分散媒が揮散したときに粘着性固形物が析出する析出性粘着剤と、揮発性油剤とを含有することを特徴とする。皮膚の不要物を吸着、除去する粘着性固形物は、ビニル構造を有する化合物を単量体として含む重合体、共重合体およびこれらの塩から選ばれる１種または２種以上である。
Correspondingly, Patent Document 1 discloses a gommage cosmetic that is less irritating to the skin.
The gommage cosmetic composition of Patent Document 1 is a gommage cosmetic composition for removing unnecessary skin components, and comprises a sticky solid substance and a volatile dispersion medium for dispersing the sticky solid substance. It is characterized by containing a precipitating pressure-sensitive adhesive in which a sticky solid matter is precipitated when the dispersion medium is volatilized, and a volatile oil agent. The sticky solid that adsorbs and removes unnecessary substances on the skin is one or more selected from polymers, copolymers, and salts thereof containing a compound having a vinyl structure as a monomer.
特許文献２は、ポリビニルアルコール１〜１０質量％ 、ポリオキシプロピレンポリグリセリルエーテル１０〜３０質量％、及びアクリル酸系水溶性高分子０．１〜５質量％を含有するピーリング剤について開示している。このピーリング剤はｐＨが中性付近であり、ポリビニルアルコール、ポリオキシプロピレンポリグリセリルエーテル、及びアクリル酸系水溶性高分子を特定の割合で配合することにより洗浄性、しっとり感、及び塗擦時間の短縮を達成している。 Patent Document 2 discloses a peeling agent containing 1 to 10% by mass of polyvinyl alcohol, 10 to 30% by mass of polyoxypropylene polyglyceryl ether, and 0.1 to 5% by mass of an acrylic acid-based water-soluble polymer. This peeling agent has a pH near neutral, and by blending polyvinyl alcohol, polyoxypropylene polyglyceryl ether, and acrylic acid-based water-soluble polymer in a specific ratio, detergency, moist feeling, and shortening of rubbing time can be shortened. Achieved.
本発明が解決すべき課題は、肌への刺激が少なく、皮膚不要物の除去作用に優れたゴマージュ化粧料組成物を提供することにある。 An object to be solved by the present invention is to provide a gommage cosmetic composition which is less irritating to the skin and has an excellent action of removing unnecessary skin substances.
本発明者らは、上記の課題解決のため鋭意検討した結果、驚くべきことに、ポリイソプレンをゴマージュ化粧料組成物に配合すると、角質を効果的に除去できることを見出し、本発明を完成するに至った。 As a result of diligent studies to solve the above problems, the present inventors have surprisingly found that when polyisoprene is added to a gommage cosmetic composition, keratin can be effectively removed, and the present invention is completed. I arrived.
本発明は、以下に記載の実施形態を包含する。 The present invention includes the embodiments described below.
項１．ポリイソプレンを含有するゴマージュ化粧料組成物。 Item 1. Gommage cosmetic composition containing polyisoprene.
項２．ｐＨが４〜９である項１に記載のゴマージュ化粧料組成物。 Item 2. Item 2. The gommage cosmetic composition according to Item 1, which has a pH of 4 to 9.
項３．ポリイソプレンの含有量が０．０１〜５０質量％である項１又は２に記載のゴマージュ化粧料組成物。 Item 3. Item 2. The gommage cosmetic composition according to Item 1 or 2, wherein the content of polyisoprene is 0.01 to 50% by mass.
項４．水を５０質量％以上含有する項１〜３のいずれか一項に記載のゴマージュ化粧料組成物。 Item 4. Item 6. The gommage cosmetic composition according to any one of Items 1 to 3, which contains 50% by mass or more of water.
項５．０．０１〜２０質量％のポリイソプレン、０．０１〜１０質量％の増粘剤、及び０．０１〜５０質量％の湿潤剤を含有する項１〜４のいずれか一項に記載のゴマージュ化粧料組成物。 Item 5. In any one of Items 1 to 4, which contains 0.01 to 20% by mass of polyisoprene, 0.01 to 10% by mass of a thickener, and 0.01 to 50% by mass of a wetting agent. The gommage cosmetic composition described.
項６．ポリイソプレンの、ゴマージュ化粧料組成物を製造するための使用。 Item 6. Use of polyisoprene to make gommage cosmetic compositions.
本発明のゴマージュ化粧料組成物は、肌への少ない刺激で、皮膚不要物を除去することができる。本発明のゴマージュ化粧料組成物は、水分の存在下でも皮膚不要物の除去作用を奏し、水で濡れた肌にも使用できる。 The gommage cosmetic composition of the present invention can remove unnecessary skin substances with less irritation to the skin. The gommage cosmetic composition of the present invention has an action of removing unnecessary skin substances even in the presence of water, and can be used on water-wet skin.
以下、本発明の実施の形態を説明する。 Hereinafter, embodiments of the present invention will be described.
本明細書において、「ゴマージュ化粧料組成物」とは、固形物質を含有する化粧料組成物であって、皮膚に塗布して該固形物質による擦過を利用して皮膚不要物を除去する化粧料のことを指す。 In the present specification, the "gommage cosmetic composition" is a cosmetic composition containing a solid substance, which is applied to the skin and scraped by the solid substance to remove unnecessary skin substances. Refers to.
本明細書において、「皮膚不要物」は、古くなった角質、過剰に分泌された脂質、角栓などを包含する。 As used herein, "skin-free material" includes aged keratin, excessively secreted lipids, keratin plugs, and the like.
本発明のゴマージュ化粧料組成物は、ポリイソプレンを含有する。 The gommage cosmetic composition of the present invention contains polyisoprene.
ポリイソプレンは、−ＣＨ2−Ｃ（ＣＨ3）＝ＣＨ−ＣＨ2−の構造を繰り返し単位として有するポリマーである。ポリイソプレンは、イソプレンのみが重合してなるホモポリマーであってもよいし、イソプレンと他の不飽和有機化合物との共重合体すなわちコポリマーであってもよい。他の不飽和有機化合物としては、ブテン、スチレン等の不飽和炭化水素が挙げられる。或いは、ポリイソプレンは、その一部の二重結合が水素添加により単結合化されていてもよい。入手の容易さの点で、ポリイソプレンはイソプレンのホモポリマーであることが好ましい。 Polyisoprene is a polymer having a structure of −CH 2 −C (CH 3 ) = CH −CH 2 − as a repeating unit. The polyisoprene may be a homopolymer obtained by polymerizing only isoprene, or may be a copolymer or copolymer of isoprene and another unsaturated organic compound. Other unsaturated organic compounds include unsaturated hydrocarbons such as butene and styrene. Alternatively, a part of the double bond of polyisoprene may be single-bonded by hydrogenation. In terms of availability, polyisoprene is preferably a homopolymer of isoprene.
ポリイソプレンの分子量は特に限定されないが、数平均分子量で３００〜１０００００の範囲内であることが好ましく、１０００〜１０００００の範囲内であることがより好ましく、５０００〜６００００の範囲内であることがさらに好ましい。ポリイソプレンの単量体の重合度は、５〜１５００の範囲内であることが好ましく、１５〜１５００の範囲内であることが好ましく、７０〜９００の範囲内であることが好ましい。 The molecular weight of polyisoprene is not particularly limited, but the number average molecular weight is preferably in the range of 300 to 100,000, more preferably in the range of 1,000 to 100,000, and further preferably in the range of 5,000 to 60,000. preferable. The degree of polymerization of the polyisoprene monomer is preferably in the range of 5 to 1500, preferably in the range of 15 to 1500, and preferably in the range of 70 to 900.
ポリイソプレンの含有量は特に限定されないが、皮膚不要物の除去効果の点で、ゴマージュ化粧料組成物全量に対して０．０１〜５０質量％であることが好ましく、０．１〜３０質量％であることがより好ましく、１〜２０質量％であることが更に好ましい。 The content of polyisoprene is not particularly limited, but is preferably 0.01 to 50% by mass, preferably 0.1 to 30% by mass, based on the total amount of the gommage cosmetic composition, in terms of the effect of removing unnecessary skin substances. Is more preferable, and 1 to 20% by mass is further preferable.
本発明のゴマージュ化粧料組成物は、水をさらに含有してもよい。水を含有する場合、水の含有量は、ポリイソプレン及び他の成分の含有量に応じて適宜設定することができる。水の含有量は特に限定されないが、ゴマージュ化粧料組成物全量に対して２０〜９９質量％であることが好ましく、５０〜９７質量％であることがより好ましく、７０〜９５質量％であることが更に好ましい。一つの特定の好ましい実施形態では、ゴマージュ化粧料組成物は水を５０質量％以上含有する。 The gommage cosmetic composition of the present invention may further contain water. When water is contained, the content of water can be appropriately set according to the content of polyisoprene and other components. The content of water is not particularly limited, but is preferably 20 to 99% by mass, more preferably 50 to 97% by mass, and 70 to 95% by mass with respect to the total amount of the Gommage cosmetic composition. Is more preferable. In one particular preferred embodiment, the gommage cosmetic composition contains 50% by weight or more of water.
本発明のゴマージュ化粧料組成物は、使用後のしっとり感を向上させるため、油剤をさらに含有してもよい。油剤としては、例えば天然動植物油脂類、半合成油脂、炭化水素油、高級脂肪酸、エステル油、グリセライド油、シリコーン油等が挙げられる。上記天然動植物油脂類及び半合成油脂としては、例えばアボガド油、アマニ油、アーモンド油、オリーブ油、カルナウバロウ、キャンデリラロウ、牛脂、牛脚脂、牛骨脂、硬化牛脂、小麦胚芽油、ゴマ油、米胚芽油、米糠油、サフラワー油、大豆油、ツバキ油、月見草油、トウモロコシ油、菜種油、馬脂、パーム油、パーム核油、ヒマシ油、硬化ヒマシ油、ヒマワリ油、ホホバ油、マカデミアナッツ油、ミツロウ、ミンク油、綿実油、ヤシ油、硬化ヤシ油、落花生油、ラノリン、液状ラノリン、還元ラノリン、ラノリンアルコール、ラノリン脂肪酸イソプロピル、ＰＯＥラノリンアルコールエーテル、ラノリン脂肪酸ポリエチレングリコール、ＰＯＥ水素添加ラノリンアルコールエステル等が挙げられる。上記炭化水素油としては、例えばスクワラン、スクワレン、セレシン、パラフィン、パラフィンワックス、流動パラフィン、マイクロクリスタリンワックス、ワセリン等が挙げられる。上記高級脂肪酸としては、例えばラウリン酸、ミリスチン酸、パルミチン酸、ステアリン酸、ベヘン酸、ウンデシレン酸、オレイン酸、リノール酸、リノレン酸、イソステアリン酸、１２−ヒドロキシステアリン酸等が挙げられる。上記エステル油としては、例えばイソノナン酸イソノニル、アジピン酸ジイソブチル、アジピン酸２−ヘキシルデシル、アジピン酸ジ−２−ヘプチルウンデシル、イソステアリン酸イソステアリル、トリイソステアリン酸トリメチロールプロパン、２−エチルヘキサン酸セチル、ジ−２−エチルヘキサン酸ネオペンチルグリコール、トリ−２−エチルヘキサン酸トリメチロールプロパン、テトラ−２−エチルヘキサン酸ペンタエリスリトール、オクタン酸セチル、オレイン酸オレイル、オレイン酸オクチルドデシル、オレイン酸デシル、ジカプリン酸ネオペンチルグリコール、コハク酸２−エチルヘキシル、ステアリン酸イソセチル、ステアリン酸ブチル、セバシン酸ジイソプロピル、乳酸セチル、乳酸ミリスチル、パルミチン酸２−エチルヘキシル、パルミチン酸２−ヘキシルデシル、パルミチン酸２−ヘプチルウンデシル、１２−ヒドロキシステアリン酸コレステリル、リンゴ酸ジイソステアリル等が挙げられる。上記グリセライド油としては、例えばトリイソオクタン酸グリセライド、トリイソステアリン酸グリセライド、トリイソパルミチン酸グリセライド、トリ２−エチルヘキサン酸グリセライド、トリミリスチン酸グリセライド等が挙げられる。上記シリコーン油としては、例えばジメチルポリシロキサン、メチルフェニルポリシロキサン、メチルハイドロジェンポリシロキサン、デカメチルシクロペンタシロキサン、オクタメチルシクロペンタシロキサン、ドデカメチルシクロヘキサシロキサン、ステアロキシシリコーン等の高級アルコキシ変成シリコーン、アルキル変成シリコーン、高級脂肪酸エステル変性シリコーン、高級脂肪酸エーテル変性シリコーン、動植物の精油類、合成精油等が挙げられる。上記油剤は単独で用いてもよく、２種以上を混合して用いてもよい。 The gommage cosmetic composition of the present invention may further contain an oil agent in order to improve the moist feeling after use. Examples of the oil agent include natural animal and vegetable oils and fats, semi-synthetic oils and fats, hydrocarbon oils, higher fatty acids, ester oils, glyceride oils, silicone oils and the like. Examples of the natural animal and vegetable fats and oils and semi-synthetic fats and oils include avocado oil, flaxseed oil, almond oil, olive oil, carnauba wax, candelilla wax, beef fat, beef leg fat, beef bone fat, hardened beef fat, wheat germ oil, sesame oil, and rice. Germ oil, rice bran oil, safflower oil, soybean oil, camellia oil, evening primrose oil, corn oil, rapeseed oil, horse fat, palm oil, palm kernel oil, sunflower oil, hardened sunflower oil, sunflower oil, jojoba oil, macadamia nut oil, Mitsuro, mink oil, cottonseed oil, palm oil, hardened palm oil, peanut oil, lanolin, liquid lanolin, reduced lanolin, lanolin alcohol, lanolin fatty acid isopropyl, POE lanolin alcohol ether, lanolin fatty acid polyethylene glycol, POE hydrogenated lanolin alcohol ester, etc. Can be mentioned. Examples of the hydrocarbon oil include squalane, squalene, selecin, paraffin, paraffin wax, liquid paraffin, microcrystalline wax, petrolatum and the like. Examples of the higher fatty acid include lauric acid, myristic acid, palmitic acid, stearic acid, behenic acid, undecylenic acid, oleic acid, linoleic acid, linolenic acid, isostearic acid, and 12-hydroxystearic acid. Examples of the ester oil include isononyl isononanoate, diisobutyl adipate, 2-hexyldecyl adipate, di-2-heptylundesyl adipate, isostearyl isostearate, trimethylpropane triisostearate, and cetyl 2-ethylhexanoate. , Neopentyl glycol di-2-ethylhexanoate, Trimethylolpropane tri-2-ethylhexanoate, pentaerythritol tetra-2-ethylhexanoate, cetyl octanoate, oleyl oleate, octyldodecyl oleate, decyl oleate, Neopentyl glycol dicaprate, 2-ethylhexyl succinate, isocetyl stearate, butyl stearate, diisopropyl sebacate, cetyl lactate, myristyl lactate, 2-ethylhexyl palmitate, 2-hexyldecyl palmitate, 2-heptyl undecyl palmitate , 12-Cholesteryl 12-hydroxystearate, diisostearyl malate and the like. Examples of the glyceride oil include triisooctanoic acid glyceride, triisostearate glyceride, triisopalmitate glyceride, tri2-ethylcaproic acid glyceride, and trimyristic glyceride. Examples of the silicone oil include higher alkoxy modified silicones such as dimethylpolysiloxane, methylphenylpolysiloxane, methylhydrogenpolysiloxane, decamethylcyclopentasiloxane, octamethylcyclopentasiloxane, dodecamethylcyclohexasiloxane, and stearoxysilicone. Examples thereof include alkyl-modified silicones, higher fatty acid ester-modified silicones, higher fatty acid ether-modified silicones, animal and plant essential oils, and synthetic essential oils. The oil agent may be used alone or in combination of two or more.
油剤の配合濃度は特に限定されないが、ゴマージュ組成物全量に対して０．０１〜４０質量％、好ましくは０．１〜３０質量％、更に好ましくは１〜２０質量％配合することが好ましい。 The blending concentration of the oil agent is not particularly limited, but it is preferably 0.01 to 40% by mass, preferably 0.1 to 30% by mass, and more preferably 1 to 20% by mass with respect to the total amount of the gommage composition.
本発明のゴマージュ化粧料組成物は、製剤の安定化のため、増粘剤をさらに含有してもよい。増粘剤としては有機増粘剤と無機増粘剤が挙げられ、有機増粘剤としては天然の有機増粘剤と、半合成の有機増粘剤と、合成の有機増粘剤とが挙げられる。次のようなものが挙げられる。天然の有機増粘剤としては、例えば、キサンタンガム、アラアビアガム、トラガカントガム、ガラクタン、グアガム、キャロブガム、カラヤガム、カラギーナン、ペクチン、カンテン、クインスシード（マルメロ）、アルゲコロイド（カッソウエキス）、デンプン（コメ、トウモロコシ、バレイショ、コムギ）、グリチルリチン酸等の植物性高分子、コラーゲン、カゼイン、アルブミン、ゼラチン等の動物系高分子が挙げられる。半合成の有機増粘剤としては、例えば、カルボキシメチルデンプン、メチルヒドロキシプロピルデンプン等のデンプン系高分子、メチルセルロース、ニトロセルロース、エチルセルロース、メチルヒドロキシプロピルセルロース、ヒドロキシエチルセルロース、セルロース硫酸ナトリウム、ヒドロキシプロピルメチルセルロース、ヒドロキシプロピルセルロース、カルボキシメチルセルロースナトリウム（ＣＭＣ）、結晶セルロース、セルロース末等のセルロース系高分子、アルギン酸ナトリウム、アルギン酸プロピレングリコールエステル等のアルギン酸系高分子が挙げられる。合成の有機増粘剤としては、例えば、ポリビニルアルコール、ポリビニルメチルエーテル、ポリビニルピロリドン、カルボキシビニルポリマー(カルボマー)、アルキル変性カルボキシビニルポリマー等のビニル系高分子、ポリエチレングリコール１５００、４０００、６０００等のポリオキシエチレン系高分子、ポリオキシエチレンポリオキシプロピレン共重合体共重合系高分子、ポリアクリル酸ナトリウム、ポリエチルアクリレート、ポリアクリルアミド等のアクリル系高分子、ポリエチレンイミン、カチオンポリマー、架橋型Ｎ，Ｎ−ジメチルアクリルアミド−２−アクリルアミドー２−メチルプロパンスルホン酸ナトリウム共重合体等が挙げられる。無機増粘剤としては例えば、ベントナイト、ケイ酸ＡｌＭｇ(ビーガム)、ラポナイト、ヘクトライト、無水ケイ酸等が挙げられる。 増粘剤としては、これらの中から１種又は２種以上を適宜選択して用いることが可能である。 The gommage cosmetic composition of the present invention may further contain a thickener for stabilizing the formulation. Examples of the thickener include an organic thickener and an inorganic thickener, and examples of the organic thickener include a natural organic thickener, a semi-synthetic organic thickener, and a synthetic organic thickener. Be done. The following can be mentioned. Natural organic thickeners include, for example, xanthan gum, alaavia gum, tragacanto gum, galactan, guar gum, carob gum, karaya gum, carrageenan, pectin, canten, quince seed (malmero), algae colloid (casso extract), starch (rice, corn, potato). , Wheat), vegetable polymers such as glycyrrhizic acid, and animal polymers such as collagen, casein, albumin, and gelatin. Examples of the semi-synthetic organic thickener include starch-based polymers such as carboxymethyl starch and methyl hydroxypropyl starch, methyl cellulose, nitrocellulose, ethyl cellulose, methyl hydroxypropyl cellulose, hydroxyethyl cellulose, cellulosic sodium sulfate, and hydroxypropyl methyl cellulose. Examples thereof include cellulosic polymers such as hydroxypropyl cellulose, sodium carboxymethyl cellulose (CMC), crystalline cellulose and cellulosic powder, and alginate polymers such as sodium alginate and propylene glycol alginate. Examples of the synthetic organic thickener include vinyl-based polymers such as polyvinyl alcohol, polyvinyl methyl ether, polyvinyl pyrrolidone, carboxyvinyl polymer (carbomer) and alkyl-modified carboxyvinyl polymer, and poly such as polyethylene glycol 1500, 4000 and 6000. Oxyethylene polymer, polyoxyethylene polyoxypropylene copolymer copolymer polymer, acrylic polymer such as sodium polyacrylate, polyethyl acrylate, polyacrylamide, polyethylene imine, cationic polymer, crosslinked N, N -Dimethylacrylamide-2-acrylamide-2-methylpropanate Sodium copolymer and the like can be mentioned. Examples of the inorganic thickener include bentonite, AlMg silicate (beagum), laponite, hectorite, silicic anhydride and the like. As the thickener, one kind or two or more kinds can be appropriately selected and used from these.
増粘剤の配合濃度は特に限定されないが、ゴマージュ組成物全量に対して０．０１〜１０質量％であることが好ましく、０．０１〜７質量％であることがより好ましく、０．０１〜５質量％であることが更に好ましい。 The blending concentration of the thickener is not particularly limited, but is preferably 0.01 to 10% by mass, more preferably 0.01 to 7% by mass, and 0.01 to 7% by mass, based on the total amount of the gommage composition. It is more preferably 5% by mass.
本発明のゴマージュ化粧料組成物は、皮膚に対する水分保持のため、湿潤剤をさらに含有してもよい。湿潤剤としては、多価アルコール、例えば、グリセリン、プロピレングリコール、ジプロピレングリコール、ポリプロピレングリコール、ポリエチレングリコール、ソルビトール、ヒドロキシプロピルソルビトール、ヘキシレングリコール、１，３−ブチレングリコール、セラミド類、スフィンゴ糖脂質類、エイジツ抽出物、１，２，６−ヘキサントリオール、エトキシル化グリセリン、プロポキシル化グリセリンまたはその混合物が挙げられる。 また、タンパク質、ムコ多糖、コラーゲン、エラスチン、ケラチン等の湿潤剤が挙げられる。 The gommage cosmetic composition of the present invention may further contain a wetting agent for retaining moisture on the skin. Wetting agents include polyhydric alcohols such as glycerin, propylene glycol, dipropylene glycol, polypropylene glycol, polyethylene glycol, sorbitol, hydroxypropyl sorbitol, hexylene glycol, 1,3-butylene glycol, ceramides, sphingoliglycolides. , Agetsu extract, 1,2,6-hexanetriol, ethoxylated glycerin, propoxylated glycerin or a mixture thereof. In addition, wetting agents such as protein, mucopolysaccharide, collagen, elastin, and keratin can be mentioned.
湿潤剤の配合濃度は特に限定されないが、ゴマージュ組成物全量に対して０．０１〜８０質量％であることが好ましく、０．１〜５０質量％であることがより好ましく、１〜２０質量％であることが更に好ましい。 The blending concentration of the wetting agent is not particularly limited, but is preferably 0.01 to 80% by mass, more preferably 0.1 to 50% by mass, and 1 to 20% by mass with respect to the total amount of the gommage composition. Is more preferable.
本発明のゴマージュ化粧料組成物は、界面活性剤をさらに含有してもよい。界面活性剤としては、例えば非イオン界面活性剤、アニオン界面活性剤、カチオン界面活性剤、両性界面活性剤などが挙げられる。界面活性剤として、例えば、アルキルグルコシド、プロピレングリコール脂肪酸エステル、グリセリン脂肪酸エステル、POEグリセリン脂肪酸エステル、ポリグリセリン脂肪酸エステル、ソルビタン脂肪酸エステル、POEソルビタン脂肪酸エステル、POEソルビット脂肪酸エステル、POEヒマシ油、POE硬化ヒマシ油、POEステロール、POE水素添加ステロール、ポリエチレングリコール脂肪酸エステル、POEアルキルエーテル、POEポリオキシプロピレンアルキルエーテル、POEラノリン、POEラノリンアルコール、POEミツロウ誘導体、POEアルキルアミン、POE脂肪酸アミド、POEアルキルエーテルリン酸、POEアルキルエーテルリン酸塩、Ｃ１２〜Ｃ２０のアルキルエーテルカルボン酸塩、Ｃ１２〜Ｃ２０高級脂肪酸エステルのスルホン酸塩(例えばスルホコハク酸ジオクチルナトリウム、ラウリルスルホ酢酸ナトリウムなど)、Ｃ１２〜Ｃ２０のアルキルリン酸塩、Ｃ１２〜Ｃ２０のアルキル硫酸塩、アシルアミノ酸塩などが挙げられる。 The gommage cosmetic composition of the present invention may further contain a surfactant. Examples of the surfactant include nonionic surfactants, anionic surfactants, cationic surfactants, amphoteric surfactants and the like. As surfactants, for example, alkyl glucoside, propylene glycol fatty acid ester, glycerin fatty acid ester, POE glycerin fatty acid ester, polyglycerin fatty acid ester, sorbitan fatty acid ester, POE sorbitan fatty acid ester, POE sorbit fatty acid ester, POE castor oil, POE cured castor Oil, POE sterol, POE hydrogenated sterol, polyethylene glycol fatty acid ester, POE alkyl ether, POE polyoxypropylene alkyl ether, POE lanolin, POE lanolin alcohol, POE beeswax derivative, POE alkylamine, POE fatty acid amide, POE alkyl ether phosphoric acid , POE alkyl ether phosphates, C12-C20 alkyl ether carboxylates, C12-C20 higher fatty acid ester sulfonates (eg sodium dioctyl sulfosuccinate, sodium lauryl sulfoacetate, etc.), alkyl phosphates C12-C20 , C12-C20 alkyl sulfates, acyl fatty acid salts and the like.
本発明のゴマージュ化粧料組成物は、ｐＨ調整のために、中和剤をさらに含有してもよい。中和剤としては、例えばトリエタノールアミン、モノエタノールアミンなどのアルカノールアミン、アンモニア、水酸化ナトリウム、水酸化カリウムなどの無機塩基、アルギニンなどの塩基性アミノ酸などが挙げられる。 The gommage cosmetic composition of the present invention may further contain a neutralizing agent for pH adjustment. Examples of the neutralizing agent include alkanolamines such as triethanolamine and monoethanolamine, inorganic bases such as ammonia, sodium hydroxide and potassium hydroxide, and basic amino acids such as arginine.
本発明のゴマージュ化粧料組成物は、防腐剤をさらに含有してもよい。防腐剤としては、例えば安息香酸塩、感光素、パラベン類、フェノキシエタノール、サリチル酸、ソルビン酸、イソプロピルメチルフェノールなどが挙げられる。 The gommage cosmetic composition of the present invention may further contain a preservative. Examples of preservatives include benzoate, photosensitizers, parabens, phenoxyethanol, salicylic acid, sorbic acid, isopropylmethylphenol and the like.
本発明のゴマージュ化粧料組成物は、上記成分以外に、化粧料の技術分野で通常使用される製剤化のための添加物を、目的の物性に応じて、本発明の特性を損なわない範囲において含有してもよい。そのような添加物としては、例えばスクラブ剤、イオウ、フルーツ酸、酸化防止剤、金属封鎖剤、香料、紫外線吸収剤、血行促進剤、各種抽出液、無機および有機顔料、無機および粘土鉱物、色素、清涼剤、制汗剤、皮膚賦活化剤などが挙げられる。 In addition to the above-mentioned ingredients, the gommage cosmetic composition of the present invention contains additives for formulation usually used in the technical field of cosmetics, depending on the desired physical properties, as long as the characteristics of the present invention are not impaired. It may be contained. Such additives include, for example, scrubbing agents, sulfur, fruit acids, antioxidants, metal sequestering agents, fragrances, UV absorbers, blood circulation promoters, various extracts, inorganic and organic pigments, inorganic and clay minerals, pigments. , Cooling agents, antiperspirants, skin activators and the like.
このような添加物の配合濃度は特に限定されないが、０．００１〜１０質量％が好ましく、０．０１〜５質量％が好ましい。 The blending concentration of such an additive is not particularly limited, but is preferably 0.001 to 10% by mass, preferably 0.01 to 5% by mass.
本発明のゴマージュ化粧料組成物は好ましくはｐＨが４〜９であり、より好ましくはｐＨが５〜９であり、さらに好ましくはｐＨが６〜８である。本発明のゴマージュ化粧料組成物は、ポリイソプレンという化学的に安定なポリマーがそれ自体、皮膚不要物の除去作用を奏する。このため、中性付近のｐＨでも角質を効果的に除去できる。また、ｐＨが４〜９であると、皮膚不要物の除去のために酸を使用する化粧料と比較して肌への刺激が少ない。 The gommage cosmetic composition of the present invention preferably has a pH of 4 to 9, more preferably a pH of 5 to 9, and even more preferably a pH of 6 to 8. In the gommage cosmetic composition of the present invention, a chemically stable polymer called polyisoprene itself acts to remove unnecessary skin substances. Therefore, keratin can be effectively removed even at a pH near neutral. In addition, when the pH is 4 to 9, there is less irritation to the skin as compared with cosmetics that use an acid for removing unnecessary skin substances.
本発明のゴマージュ化粧料組成物は、ポリイソプレンが皮膚不要物の除去作用を奏する。このため、ゴマージュ化粧料組成物を塗布し、皮膚を擦ると、皮膚不要物が速やかに析出し、短時間に皮膚不要物を除去することができる。このため、ゴマージュ化粧料組成物を水に濡れた肌でも使用することができる。また、本発明のゴマージュ化粧料組成物は皮膚不要物の除去作用に優れているため、メーキャップ化粧品の汚れ落ちにも優れている。さらに、本発明のゴマージュ化粧料組成物はｐＨが中性付近であるため、肌への刺激性が少ない。 In the gommage cosmetic composition of the present invention, polyisoprene acts to remove unnecessary skin substances. Therefore, when the gommage cosmetic composition is applied and the skin is rubbed, the skin unnecessary substances are rapidly precipitated, and the skin unnecessary substances can be removed in a short time. Therefore, the Gommage cosmetic composition can be used even on wet skin. Further, since the gommage cosmetic composition of the present invention is excellent in removing unnecessary skin substances, it is also excellent in removing stains from makeup cosmetics. Furthermore, since the Gommage cosmetic composition of the present invention has a pH near neutral, it is less irritating to the skin.
本発明のゴマージュ化粧料組成物は、顔用にも全身用にも使用することができる。 The gommage cosmetic composition of the present invention can be used for both the face and the whole body.
本発明の好ましい特定の実施形態のゴマージュ化粧料組成物は、０．０１〜２０質量％のポリイソプレン、０．０１〜１０質量％の増粘剤、及び０．０１〜５０質量％の湿潤剤を含有する。このため、水に濡れた肌に使用することができ、肌への刺激性が少なく、かつ皮膚不要物の除去作用が優れている。 The Gommage cosmetic compositions of the preferred specific embodiments of the present invention are 0.01-20% by weight polyisoprene, 0.01-10% by weight thickener, and 0.01-50% by weight wetting agent. Contains. Therefore, it can be used on water-wet skin, is less irritating to the skin, and has an excellent effect of removing unnecessary skin substances.
本発明のより好ましい特定の実施形態のゴマージュ化粧料組成物は、０．０１〜２０質量％のポリイソプレン、０．０１〜１０質量％の増粘剤、及び０．０１〜５０質量％の湿潤剤を含有し、ｐＨが４〜９である。このため、水に濡れた肌に使用することができ、肌への刺激性が少なく、かつ皮膚不要物の除去作用が優れている。 The Gommage cosmetic composition of a more preferred particular embodiment of the present invention comprises 0.01-20% by weight polyisoprene, 0.01-10% by weight thickener, and 0.01-50% by weight wetting. It contains an agent and has a pH of 4-9. Therefore, it can be used on water-wet skin, is less irritating to the skin, and has an excellent effect of removing unnecessary skin substances.
本発明の別の好ましい特定の実施形態のゴマージュ化粧料組成物は、０．０１〜２０質量％のポリイソプレン、０．０１〜１０質量％の増粘剤、及び０．０１〜５０質量％の湿潤剤を含有し、水の含有量が５０〜９７質量％である。このため、水に濡れた肌に使用することができ、肌への刺激性が少なく、かつ皮膚不要物の除去作用が優れている。 Another preferred particular embodiment of the Gommage cosmetic composition of the present invention is 0.01-20% by weight polyisoprene, 0.01-10% by weight thickener, and 0.01-50% by weight. It contains a wetting agent and has a water content of 50-97% by mass. Therefore, it can be used on water-wet skin, is less irritating to the skin, and has an excellent effect of removing unnecessary skin substances.
本発明のさらに別の好ましい特定の実施形態のゴマージュ化粧料組成物は、０．０１〜２０質量％のポリイソプレン、０．０１〜１０質量％の増粘剤、及び０．０１〜５０質量％の湿潤剤を含有し、水の含有量が５０〜９７質量％であり、ｐＨが４〜９である。このため、水に濡れた肌に使用することができ、肌への刺激性が少なく、かつ皮膚不要物の除去作用が優れている。 Yet another preferred particular embodiment of the Gommage cosmetic composition of the present invention is 0.01-20% by weight polyisoprene, 0.01-10% by weight thickener, and 0.01-50% by weight. The wetting agent is contained, the content of water is 50 to 97% by mass, and the pH is 4 to 9. Therefore, it can be used on water-wet skin, is less irritating to the skin, and has an excellent effect of removing unnecessary skin substances.
本発明のゴマージュ化粧料組成物の形態は、皮膚に塗布できればいずれの剤型でも良く、好ましくは化粧水、ジェル、乳液、クリームなどが挙げられる。或いは、本発明のゴマージュ化粧料を、プロパン、ブタンなどの天然ガス、窒素ガス、炭酸ガス、ジメチルエーテルなどの噴出剤と共に混合し、エアゾールとして密封容器に充填してもよい。 The form of the gommage cosmetic composition of the present invention may be any dosage form as long as it can be applied to the skin, and preferred examples thereof include lotion, gel, milky lotion, and cream. Alternatively, the gommage cosmetic of the present invention may be mixed with a natural gas such as propane or butane, a propellant such as nitrogen gas, carbon dioxide gas, or dimethyl ether, and filled in a sealed container as an aerosol.
本発明のゴマージュ化粧料組成物の製造方法は特に限定されず、所定の組成となるよう各成分を混合すればよい。混合時には必要に応じて加熱してもよい。本発明の好ましい製造方法は、油剤を溶解後、そこに予め分散・溶解させた水溶性の成分を投入し、目的の剤型に応じて適宜撹拌・乳化後、ポリイソプレンを投入し、適宜撹拌・乳化することを含む。ポリイソプレンを投入する段階は問わず、油剤溶解後に投入し、分散・溶解させた水溶性剤を投入してから撹拌・乳化しても良い。どの段階でｐＨを調整してもよく、目的に応じてその他の成分をいつ投入しても良い。 The method for producing the gommage cosmetic composition of the present invention is not particularly limited, and each component may be mixed so as to have a predetermined composition. When mixing, it may be heated if necessary. In the preferred production method of the present invention, after dissolving the oil agent, a water-soluble component dispersed and dissolved in advance is added thereto, and the mixture is appropriately stirred and emulsified according to the desired dosage form, and then polyisoprene is added and appropriately stirred.・ Including emulsification. Regardless of the stage at which polyisoprene is added, it may be added after the oil agent has been dissolved, and the dispersed / dissolved water-soluble agent may be added before stirring / emulsification. The pH may be adjusted at any stage, and other components may be added at any time depending on the purpose.
以下に実施例を挙げて本発明をより具体的に説明するが、本発明はこれらに限定されない。 Hereinafter, the present invention will be described in more detail with reference to examples, but the present invention is not limited thereto.
試験例１ ポリイソプレンを含有するゴマージュ化粧料組成物の製造及び評価
１．ゴマージュ化粧料組成物の製造
実施例１
７０〜８０℃で分散したグリセリン、カルボマー、精製水に水酸化カリウムを入れて中和し、基剤の水性ゲルを作製した。そこへビニゾール３７００（ポリイソプレンの樹脂エマルション、大同化成工業株式会社、ポリイソプレン含有量６３〜７２重量％）を、最終組成物の１０質量％となるよう投入し、撹拌し、実施例１のゴマージュ化粧料組成物を得た。
実施例２
実施例１のビニゾール３７００をビニゾール３７０１Ｃ（ポリイソプレンの樹脂エマルション、大同化成工業株式会社、ポリイソプレン含有量５２〜６０重量％）とした以外は、実施例１と同様の方法で、実施例２のゴマージュ化粧料組成物を得た。
実施例３
実施例１のビニゾール３７００をセポレックス ＩＲ１００−Ｈ（ポリイソプレンの樹脂エマルション、住友精化株式会社、ポリイソプレン含有量６６重量％）とした以外は、実施例１と同様の方法で、実施例３のゴマージュ化粧料組成物を得た。
比較例１
実施例１のビニゾール３７００をＤＡＩＴＯＳＯＬ５０００ＡＤ（アクリル酸コポリマーのエマルション、大東化成工業株式会社、ポリマー含有量５０重量％）とした以外は、実施例１と同様の方法で、比較例１のゴマージュ化粧料組成物を得た。
比較例２
実施例１のビニゾール３７００をビニゾール２１４０Ｌ（酢酸ビニル−アクリル酸コポリマー、大同化成工業株式会社、ポリマー含有量４５〜５０重量％）とした以外は、実施例１と同様の方法で、比較例２のゴマージュ化粧料組成物を得た。
比較例３
実施例１のビニゾール３７００をビニゾール２１４０ＬＨ（酢酸ビニル−アクリル酸コポリマー、大同化成工業株式会社、ポリマー含有量４５〜５０重量％）とした以外は、実施例１と同様の方法で、比較例３のゴマージュ化粧料組成物を得た。
比較例４
実施例１のビニゾール３７００をＤＯＷＳＩＬ ＨＭＷ ２２２０ ＮＯＮ−ＩＯＮＩＣ ＥＭＵＬＳＩＯＮ（ダウコーポレート社、ジビニルジメチコン−ジメチコンコポリマー）とした以外は、実施例１と同様の方法で、比較例４のゴマージュ化粧料組成物を得た。
実施例１〜３及び比較例１〜４のゴマージュ化粧料組成物の組成を表１に示す。
Test Example 1 Production and evaluation of gommage cosmetic composition containing polyisoprene
1. 1. Production of Gommage Cosmetic Composition Example 1
Potassium hydroxide was added to glycerin, carbomer, and purified water dispersed at 70 to 80 ° C. to neutralize the mixture, and an aqueous gel as a base was prepared. Vinizol 3700 (polyisoprene resin emulsion, Daido Kasei Kogyo Co., Ltd., polyisoprene content 63 to 72% by mass) was added thereto so as to be 10% by mass of the final composition, stirred, and the gommage of Example 1 was added. A cosmetic composition was obtained.
Example 2
The method of Example 2 was the same as that of Example 1 except that Vinizol 3700 of Example 1 was changed to Vinizol 3701C (resin emulsion of polyisoprene, Daido Kasei Kogyo Co., Ltd., polyisoprene content 52 to 60% by weight). A gommage cosmetic composition was obtained.
Example 3
Example 3 in the same manner as in Example 1 except that Vinizol 3700 of Example 1 was used as Sepolex IR100-H (resin emulsion of polyisoprene, Sumitomo Seika Chemical Co., Ltd., polyisoprene content 66% by weight). A gommage cosmetic composition was obtained.
Comparative Example 1
Gommage cosmetic composition of Comparative Example 1 in the same manner as in Example 1 except that Vinizol 3700 of Example 1 was DAITOSOL5000AD (emulsion of acrylic acid copolymer, Daito Kasei Kogyo Co., Ltd., polymer content 50% by weight). I got something.
Comparative Example 2
Comparative Example 2 in the same manner as in Example 1 except that Vinizol 3700 of Example 1 was used as Vinizol 2140 L (vinyl acetate-acrylic acid copolymer, Daido Kasei Kogyo Co., Ltd., polymer content 45 to 50% by weight). A gommage cosmetic composition was obtained.
Comparative Example 3
Comparative Example 3 in the same manner as in Example 1 except that Vinizol 3700 of Example 1 was changed to Vinizol 2140 LH (vinyl acetate-acrylic acid copolymer, Daido Kasei Kogyo Co., Ltd., polymer content 45 to 50% by weight). A gommage cosmetic composition was obtained.
Comparative Example 4
The gommage cosmetic composition of Comparative Example 4 was obtained in the same manner as in Example 1 except that Vinizol 3700 of Example 1 was used as DOWNIL HMW 2220 NON-IONIC EMULSION (Dow Corporate, divinyldimethicone-dimethicone copolymer). rice field.
The compositions of the Gommage cosmetic compositions of Examples 1 to 3 and Comparative Examples 1 to 4 are shown in Table 1.
２．評価
実施例１〜３及び比較例１〜４のゴマージュ化粧料組成物について以下の評価を行った。
＜析出性＞
所定条件下（２０℃、湿度５０％）下で、得られた各ゴマージュ化粧料組成物０．５ｇを、流水で２秒間濡らした手の甲にとり、人差し指・中指を用いて塗擦し、下記評価項目に従って、析出性の評価を行った。
◎：塗擦後、１０秒以内に析出物が出てくる。
○：塗擦後、２０秒以内に析出物が出てくる。
×：塗擦後、２０秒以上経過しても析出物がでてこない。
＜汚れ落ちの評価＞
所定条件（２０℃、湿度５０％）下で、人工皮膚（株式会社ビューラックス：バイオスキンプレート）に一般的なファンデーションを塗布し、得られた各ゴマージュ剤組成物約０．１５ｇを塗擦し、下記評価基準に従って汚れ落ちを評価した。
○：汚れが除去された。
×：汚れがほとんど除去されなかった。
＜結果＞
実施例１〜３のゴマージュ化粧料組成物では、素早く析出物が生じるとともに、刺激感を与えることなく、析出物を効率良く古い角質を巻き込みながら除去することができた。実施例１〜３のゴマージュ化粧料組成物はｐＨが中性付近である点でも刺激がなく優れていた。
比較例１のゴマージュ化粧料組成物は析出性及び汚れ落ちが良好であったが、比較例２及び３のゴマージュ化粧料組成物は析出性及び汚れ落ちともに劣っていた。
2. Evaluation The following evaluations were performed on the Gommage cosmetic compositions of Examples 1 to 3 and Comparative Examples 1 to 4.
<Precipitability>
Under predetermined conditions (20 ° C., humidity 50%), 0.5 g of each Gommage cosmetic composition obtained was placed on the back of a hand moistened with running water for 2 seconds, rubbed with the index finger and middle finger, and according to the following evaluation items. , Precipitability was evaluated.
⊚: Precipitates appear within 10 seconds after rubbing.
◯: Precipitates appear within 20 seconds after rubbing.
X: No precipitate appears even after 20 seconds or more have passed after rubbing.
<Evaluation of dirt removal>
Under predetermined conditions (20 ° C., humidity 50%), a general foundation was applied to artificial skin (Bulux Co., Ltd .: Bioskin Plate), and about 0.15 g of each obtained gommage agent composition was rubbed. The stain removal was evaluated according to the following evaluation criteria.
◯: Dirt was removed.
X: Almost no dirt was removed.
<Result>
In the Gommage cosmetic compositions of Examples 1 to 3, precipitates were quickly formed, and the precipitates could be efficiently removed while involving old keratin without giving a feeling of irritation. The Gommage cosmetic compositions of Examples 1 to 3 were also excellent in that the pH was near neutral without irritation.
The Gommage cosmetic composition of Comparative Example 1 had good precipitation and stain removal, but the Gommage cosmetic compositions of Comparative Examples 2 and 3 were inferior in both precipitation and stain removal.
試験例２ ポリイソプレン含有量の影響
１．ゴマージュ化粧料組成物の製造
実施例４
７０〜８０℃で分散したグリセリン、カルボマー、精製水に水酸化カリウムを入れて中和し、基剤の水性ゲルを作製した。そこへビニゾール３７０１Ｃを、最終組成物の０．５質量％となるよう投入し、撹拌し、実施例４のゴマージュ化粧料組成物を得た。
実施例５
実施例４のビニゾール３７０１Ｃの配合量を最終濃度０．５質量％から最終濃度３０質量％となるように変更した以外は、実施例４と同様の方法で、実施例５のゴマージュ化粧料組成物を得た。
実施例６
実施例４のビニゾール３７０１Ｃをセポレックス ＩＲ１００−Ｈとした以外は、実施例４と同様の方法で、実施例６のゴマージュ化粧料組成物を得た。
実施例７
実施例６のセポレックス ＩＲ１００−Ｈの配合量を最終濃度０．５質量％から最終濃度３０質量％となるように変更した以外は、実施例６と同様の方法で、実施例７のゴマージュ化粧料組成物を得た。
実施例４〜７のゴマージュ化粧料組成物の組成を表２に示す。
Test Example 2 Effect of polyisoprene content
1. 1. Production of Gommage Cosmetic Composition Example 4
Potassium hydroxide was added to glycerin, carbomer, and purified water dispersed at 70 to 80 ° C. to neutralize the mixture, and an aqueous gel as a base was prepared. Vinizol 3701C was added thereto so as to be 0.5% by mass of the final composition, and the mixture was stirred to obtain the Gommage cosmetic composition of Example 4.
Example 5
The gommage cosmetic composition of Example 5 was prepared in the same manner as in Example 4 except that the blending amount of Vinizol 3701C of Example 4 was changed from the final concentration of 0.5% by mass to the final concentration of 30% by mass. Got
Example 6
The Gommage cosmetic composition of Example 6 was obtained in the same manner as in Example 4 except that Vinizole 3701C of Example 4 was used as Sepolex IR100-H.
Example 7
The gommage cosmetics of Example 7 were prepared in the same manner as in Example 6 except that the blending amount of Sepolex IR100-H of Example 6 was changed from the final concentration of 0.5% by mass to the final concentration of 30% by mass. The composition was obtained.
The composition of the Gommage cosmetic composition of Examples 4 to 7 is shown in Table 2.
２．評価
実施例４〜７のゴマージュ化粧料組成物について以下の評価を行った。
＜析出性＞
所定条件下（２０℃、湿度５０％）下で、得られた各ゴマージュ化粧料組成物０．５ｇを、流水で２秒間濡らした手の甲にとり、人差し指・中指を用いて塗擦し、下記評価項目に従って、析出性の評価を行った。
◎：塗擦後、１０秒以内に析出物が出てくる。
○：塗擦後、２０秒以内に析出物が出てくる。
×：塗擦後、２０秒以上経過しても析出物がでてこない。
＜結果＞
実施例４〜７のゴマージュ化粧料組成物では、素早く析出物が生じるとともに、刺激感を与えることなく、析出物を効率良く古い角質を巻き込みながら除去することができた。実施例４〜７のゴマージュ化粧料組成物はｐＨが中性付近である点でも刺激がなく優れていた。
2. Evaluation The following evaluations were performed on the Gommage cosmetic compositions of Examples 4 to 7.
<Precipitability>
Under predetermined conditions (20 ° C., humidity 50%), 0.5 g of each Gommage cosmetic composition obtained was placed on the back of a hand moistened with running water for 2 seconds, rubbed with the index finger and middle finger, and according to the following evaluation items. , Precipitability was evaluated.
⊚: Precipitates appear within 10 seconds after rubbing.
◯: Precipitates appear within 20 seconds after rubbing.
X: No precipitate appears even after 20 seconds or more have passed after rubbing.
<Result>
In the Gommage cosmetic compositions of Examples 4 to 7, precipitates were quickly formed, and the precipitates could be efficiently removed while involving old keratin without giving a feeling of irritation. The Gommage cosmetic compositions of Examples 4 to 7 were also excellent in that the pH was near neutral without irritation.
試験例３ 剤形別のゴマージュ化粧料組成物の製造と評価
１．ゴマージュ化粧料組成物の製造
実施例８ 化粧水の製造
７０〜８０℃でＰＥＧ−６０水添ヒマシ油、酢酸トコフェロール、ジメチコンを溶解し（溶解物Ａ）、７０〜８０℃でグリセリン、１，３−ブチレングリコール、及び防腐剤を溶解し（溶解物Ｂ）、カルボマー及び精製水を分散し（分散物Ｃ）、水酸化カリウム及び水を溶解し（溶解物Ｄ）、溶解物Ａに溶解物Ａ及び分散物Ｃを投入し、これに溶解物Ｄを入れて中和し、基剤の水性ゲルを作製した。冷却後、そこへビニゾール３７０１Ｃ（Ｅ）を、最終組成物の１０質量％となるよう投入し、撹拌し、実施例８のゴマージュ化粧料組成物を得た。
実施例９ ジェルの製造
実施例８のカルボマーの量を最終濃度で０．５質量％となるよう変更した以外は、実施例８と同様の方法で、実施例９のゴマージュ化粧料組成物を得た。
実施例１０ 乳液の製造
溶解物Ａ，Ｂ，Ｃ，Ｄ，Ｅの各成分と配合量を表３のように変更した以外は、実施例８と同様の方法で、実施例１０のゴマージュ化粧料組成物を得た。
実施例１１ クリームの製造
溶解物Ａ，Ｂ，Ｃ，Ｄ，Ｅの各成分と配合量を表３のように変更した以外は、実施例８と同様の方法で、実施例１１のゴマージュ化粧料組成物を得た。
実施例８〜１１のゴマージュ化粧料組成物の組成を表３に示す。
Test Example 3 Production and evaluation of gommage cosmetic composition by dosage form
1. 1. Production of Gommage Cosmetic Composition Example 8 Production of Cosmetic Water Dissolve PEG-60 hydrogenated castor oil, tocopherol acetate, and dimethicone at 70-80 ° C (dissolution A), and glycerin at 70-80 ° C. , 1,3-butylene glycol, and preservatives (dissolved B), carbomer and purified water (disperse C), potassium hydroxide and water (dissolved D), lysate A The solution A and the dispersion C were added to the mixture, and the solution D was added thereto to neutralize the mixture to prepare an aqueous gel as a base. After cooling, Vinizol 3701C (E) was added thereto so as to be 10% by mass of the final composition, and the mixture was stirred to obtain the Gommage cosmetic composition of Example 8.
Example 9 Preparation of gel A gommage cosmetic composition of Example 9 was obtained in the same manner as in Example 8 except that the amount of carbomer in Example 8 was changed to 0.5% by mass in the final concentration. rice field.
Example 10 Production of Emulsion The gommage lotion of Example 10 was prepared in the same manner as in Example 8 except that the components and blending amounts of the lysates A, B, C, D and E were changed as shown in Table 3. The composition was obtained.
Example 11 Production of cream The gommage cosmetic of Example 11 was prepared in the same manner as in Example 8 except that the components and blending amounts of the lysates A, B, C, D, and E were changed as shown in Table 3. The composition was obtained.
The composition of the Gommage cosmetic composition of Examples 8 to 11 is shown in Table 3.
２．評価
実施例８〜１１のゴマージュ化粧料組成物について以下の評価を行った。
＜析出性＞
所定条件下（２０℃、湿度５０％）下で、得られた各ゴマージュ化粧料組成物０．５ｇを、流水で２秒間濡らした手の甲にとり、人差し指・中指を用いて塗擦し、下記評価項目に従って、析出性の評価を行った。
◎：塗擦後、１０秒以内に析出物が出てくる。
○：塗擦後、２０秒以内に析出物が出てくる。
×：塗擦後、２０秒以上経過しても析出物がでてこない。
＜汚れ落ちの評価＞
所定条件（２０℃、湿度５０％）下で、人工皮膚（株式会社ビューラックス：バイオスキンプレート）に一般的なファンデーションを塗布し、得られた各ゴマージュ剤組成物約０．１５ｇを塗擦し、下記評価基準に従って汚れ落ちを評価した。
○：汚れが除去された。
×：汚れがほとんど除去されなかった。
＜結果＞
実施例８の化粧水、実施例９のジェル、実施例１０の乳液、及び実施例１１のクリームのいずれの剤形でも、本発明のゴマージュ化粧料組成物は、素早く析出物が生じるとともに、刺激感を与えることなく、析出物が効率良く古い角質を巻き込みながら除去することができた。また、実施例８〜１１のゴマージュ化粧料組成物は汚れ落ちも良好であった。
2. Evaluation The following evaluations were performed on the Gommage cosmetic compositions of Examples 8 to 11.
<Precipitability>
Under predetermined conditions (20 ° C., humidity 50%), 0.5 g of each Gommage cosmetic composition obtained was placed on the back of a hand moistened with running water for 2 seconds, rubbed with the index finger and middle finger, and according to the following evaluation items. , Precipitability was evaluated.
⊚: Precipitates appear within 10 seconds after rubbing.
◯: Precipitates appear within 20 seconds after rubbing.
X: No precipitate appears even after 20 seconds or more have passed after rubbing.
<Evaluation of dirt removal>
Under predetermined conditions (20 ° C., humidity 50%), a general foundation was applied to artificial skin (Bulux Co., Ltd .: Bioskin Plate), and about 0.15 g of each obtained gommage agent composition was rubbed. The stain removal was evaluated according to the following evaluation criteria.
◯: Dirt was removed.
X: Almost no dirt was removed.
<Result>
In any of the dosage forms of the lotion of Example 8, the gel of Example 9, the emulsion of Example 10, and the cream of Example 11, the gommage cosmetic composition of the present invention rapidly produces precipitates and is irritating. The precipitate was able to efficiently remove the old keratin while entraining it without giving a feeling. In addition, the Gommage cosmetic compositions of Examples 8 to 11 were also good at removing stains.
Claims (6)
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| JP2020040483A JP2021143127A (en) | 2020-03-10 | 2020-03-10 | Gommage cosmetic composition |
| CN202110261852.6A CN113368008A (en) | 2020-03-10 | 2021-03-10 | Exfoliating cosmetic composition |
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| JP2505856B2 (en) * | 1988-04-12 | 1996-06-12 | 岩瀬コスファ株式会社 | Pack cosmetics |
| JP3212340B2 (en) * | 1992-01-27 | 2001-09-25 | アルケア株式会社 | Paste composition for skin protection |
| ITMI20030385A1 (en) * | 2003-03-04 | 2004-09-05 | Intercos Italia S P A Ora Intercos S P A | COSMETIC COMPOSITION INCLUDING POLYISOPRENE. |
| JP4979061B2 (en) * | 2006-04-18 | 2012-07-18 | 株式会社 資生堂 | Skin cosmetics |
| JP4450427B2 (en) * | 2007-11-13 | 2010-04-14 | 株式会社資生堂 | Skin cosmetics |
| JP2012020989A (en) * | 2010-06-17 | 2012-02-02 | Shiseido Co Ltd | Skin improving dermo-cosmetic |
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