JP2021091684A - Plant extract composition and method for preparing the same - Google Patents

Abstract

To provide a method for preparing a plant extract composition.SOLUTION: Extract from Cirsium japonicum, Glycine tomentella, Murraya paniculata, Ventilago elegans, Hibiscus mutabilis, Coptis quinquefolia Miq., Ficus formosana Maxim, Catunaregam spinosa, Ficus pumil and Ampelopsis brevipedunculata is provided, a plant composition is immersed in water, the plant composition is immersed in a first solution, and the plant composition is heated with water, resulting in a plant extract composition.SELECTED DRAWING: Figure 1

Description

An object of the present invention is to provide an extraction composition and a method for preparing the same, and specifically, the present invention relates to a plant extract composition and a method for preparing the same.

In recent years, as calls for a return to nature have increased, attention has been focused on plant extracts. The definition of plant extracts is not exactly the same in countries around the world, but in general, plants are used as raw materials and physically and chemically extracted according to the usage and usage of the final product extracted. And through the separation process, one or more active ingredients in the plant are obtained and concentrated.

Aromatherapy is a natural remedy that uses essential oils extracted from aroma plants as a medium and is absorbed into the body through the respiratory tract and skin by massage, bathing, incense, etc. to relieve mental stress and improve health. Aromatherapy is an alternative medicine that began in ancient Egypt and has become popular in modern Europe, but is not recognized in mainstream medicine.

A plant steam bath uses the smoke produced by burning the plant extract or the steam produced by the boiling of the plant extract to put the active ingredients of the plant extract into the pores and warps of the skin and penetrate the internal organs. It is a method in which the active ingredient is transferred to the whole body by direct absorption to produce an effect. The steam bath has a warming effect on the skin, promotes the active ingredient of the plant extract, makes uniform contact with the skin, and enhances the permeability of cells, so that the heat factor and the atomized active ingredient are absorbed by the skin surface. It penetrates into keratin, is transported in the dermis layer, and finally enters the blood circulation, raises the skin temperature and dilates the capillaries, promotes blood and lymph circulation, reduces the burden on the heart, and metabolizes. The penetration effect of the essence of the plant extract is greatly improved. The plant steam bath not only beneficially regulates unbalanced organ function, relaxes one's mood, relaxes muscles, thereby improving sleep and achieving a balance of physiology and psychology. It purifies blood and reduces blood viscosity, increases the elasticity of blood vessels, prevents illness, improves complexion, relieves fatigue and dizziness due to impaired blood circulation, and regulates meridian diseases.

An object of the present invention is to combine the prepared plant extract composition with a plant vapor bath to achieve the best effect.

To achieve the above object, the present application provides a plant extract composition and a method for preparing the same. The plant extract composition can achieve the effects of promoting metabolism, regulating physical strength, reducing inflammatory symptoms and promoting wound healing by removing and detoxifying the user's moisture.

An object of the present invention is to provide a method for preparing a plant extract composition. The method: (. Coptis quinquefolia Miq) Noazami (Cirsium japonicum), Hirohayabumame (Glycine tomentella), Murraya paniculata (Murraya paniculata), Kazanabiki (Ventilago elegans), mutabilis (Hibiscus mutabilis), Baikaouren, Taiwan Ficus (Ficus formosana Maxim), A step of providing a plant composition containing Coptis quinque (Catunaregam spinosa), a citis quinque (Ficus plumil) and a citris quinque (Ampelopsis brevipedunculata), a step of immersing the plant composition in water, and a step of immersing the plant composition in a first solution. The step includes a step of heating the plant composition and water together to obtain a plant extract composition.

More preferably, the method for preparing the plant extract composition further comprises the step of cooling the plant extract composition to room temperature under a humidity of 40 to 50 degrees Celsius to remove residues.

More preferably, the step of heating with the water comprises heating on low heat for 5 hours.

More preferably, the first solution contains water and vinegar and has a pH value between 7.2 and 7.8.

More preferably, the ratio of Cirsium japonicum in the plant composition is 8.0 to 12.0 wt. %, The proportion of Hirohaya bean is 10.0 to 14.0 wt. %, The ratio of jessamine is 10.0 to 14.0 wt. %, The ratio of Kazanaviki is 10.0 to 14.0 wt. %, The ratio of Fuyo is 8.0 to 12.0 wt. %, The ratio of coptis quinque is 8.0 to 12.0 wt. %, The ratio of Taiwan Inubiwa is 6.0 to 10.0 wt. %, The ratio of Harizakuro is 7.0 to 11.0 wt. %, The ratio of Climbing fig is 6.0 to 10.0 wt. %, And the proportion of Kirehano grapes is 7.0-11.0 wt. %.

Another object of the present invention is to obtain Noazami extract, Hirohayabu bean extract, Gekitsu extract, Kazanabiki extract, Fuyo extract, Baikaouren extract, Taiwan Inubiwa extract, Harizakuro extract, Oitabi extract and Kirehano grape extract. To provide a plant extract composition comprising.

More preferably, the total ion chromatography (TIC) profile of the plant extract composition is 2.167 ± 0.5 minutes, 2.662 ± 0.5 minutes, 4.203 ± 0.5 minutes, 78. There are peaks at 23 ± 0.5 minutes, 79.033 ± 0.5 minutes, 79.792 ± 0.5 minutes, and 82.327 ± 0.5 minutes.

More preferably, the plant extract composition has total ion chromatography as shown in FIG.

More preferably, the plant extract composition is a plant extract composition for a plant steam bath.

When the above plant extract composition is used in the form of a plant vapor bath bath salt, it helps to remove moisture and detoxify the user, thus promoting metabolism, regulating physical fitness, reducing inflammatory symptoms and healing wounds. The effect of promotion can be achieved.

The following detailed description with reference to the accompanying drawings will be more apparent to engineers in the art. Of which:
It is a schematic flowchart of the preparation method 10 of the plant extract composition according to the Example of this application. It is a photograph of the appearance of the plant extract composition according to the Example of this application. It is a total ion chromatography of the plant extract composition according to the Example of this application. FIG. 5 is an effect diagram in which a user uses a plant extract composition according to an embodiment of the present application via a plant steam bath. FIG. 5 is an effect diagram in which a user uses a plant extract composition according to an embodiment of the present application via a plant steam bath.

Hereinafter, examples of the method for preparing the plant extract composition will be described with reference to the drawings, but for ease of understanding, the same elements are designated by the same reference numerals in the following examples.

Any numerical range described herein is intended to cover all subranges within the same numerical accuracy range. For example, the range "1.0 to 10.0" is all subranges between the minimum value 1.0 and the maximum value 10.0, and the minimum value 1.0 and the maximum value 10.0 (that is, the minimum value value). Is 1.0 or more and the maximum value is 10.0 or less). For example, 1.1 to 8.6. The maximum number limits described herein are intended to include all lower numerical limits therein, and all minimum number limits described herein are said to be such. It is intended to include the limits of all the higher numbers in.

The specific value described herein as "about" is ± 10%, preferably ± 5%, more preferably ± 1%, even more preferably ± 0.1% of the specific value due to measurement error. It can be understood that it covers the difference between.

As used herein, the term "room temperature" refers to a temperature of about 20 to 35 ° C.

In the present specification, "small fire" is a kind of fire used for decoction of Chinese herbs, and is also called "slow fire", and usually refers to a heating method in which the temperature rises slowly and water evaporates slowly. .. Refers to heating at about 80-150 ° C.

As used herein, the term "vegetable vapor bath" refers to an administration method in which a solution is heated, vaporized into a gas, and then absorbed.

FIG. 1 is a schematic flowchart of a method 10 for preparing a plant extract composition according to an embodiment of the present application. As shown in FIG. 1, the method 10 for preparing the plant extract composition comprises step S101 for providing the plant composition, step S103 for immersing the plant composition in water, and first the plant composition. Includes step S015 of immersion in the solution and step S107 of heating the plant composition and water together to obtain a plant extract composition.

In step S101, Cirsium japonicum, Orange jessamine, Orange jessamine, Confederate rose, Coptis quinque, Ficus erecta, Climbing fig, and Climbing fig are collected and washed to provide the plant composition of the present invention. According to one embodiment, the material is washed with running water to remove soil and impurities on its surface, more preferably at a flow rate of 4 little per minute.

According to one example, the proportion of Cirsium japonicum in the plant composition is 8.0-12.0 wt. %, More preferably 9.0 to 11.0 wt. %, More preferably 10.0 wt. %, And the proportion of hirohayabume is 10.0 to 14.0 wt. %, More preferably 11.0 to 13.0 wt. %, More preferably 12.0 wt. %, And the proportion of jessamine is 10.0 to 14.0 wt. %, More preferably 11.0 to 13.0 wt. %, More preferably 12.0 wt. %, And the proportion of Kazanaviki is 10.0 to 14.0 wt. %, More preferably 11.0 to 13.0 wt. %, More preferably 12.0 wt. %, And the proportion of Fuyo is 8.0 to 12.0 wt. %, More preferably 9.0 to 11.0 wt. %, More preferably 10.0 wt. %, And the proportion of coptis quinque is 8.0 to 12.0 wt. %, More preferably 9.0 to 11.0 wt. %, More preferably 10.0 wt. %, And the ratio of Taiwan Ficus erecta is 6.0 to 10.0 wt. %, More preferably 7.0-9.0 wt. %, More preferably 8.0 wt. %, And the proportion of Hari pomegranate is 7.0 to 11.0 wt. %, More preferably 8.0 to 10.0 wt. %, More preferably 9.0 wt. %, And the proportion of figs is 6.0 to 10.0 wt. %, More preferably 7.0-9.0 wt. %, More preferably 8.0 wt. %, And the proportion of Kirehano grapes is 7.0-11.0 wt. %, More preferably 8.0 to 10.0 wt. %, More preferably 9.0 wt. %. However, the present invention is not limited to this.

In step S103, the plant composition provided in step S101 is immersed in water to further remove the water-soluble toxic substance, and the plant composition from which the water-soluble toxic substance has been removed is immersed in step S105.

In step S105, by immersing the plant composition from which the water-soluble toxic substance has been removed in the first solution to soften it, the active ingredient in the plant composition can be easily extracted in a later step. The first solution used has a pH value of about 7.2-7.8 and contains vinegar and pure water. The immersion time in step S105 can be about 20 to 30 hours, preferably 22 to 28 hours, more preferably 24 hours.

Finally, in step S107, the soaked and softened plant composition and water are heated on a small fire for about 2-6 hours, preferably 3-5 hours, more preferably 5 hours to extract the plants of the present invention. Obtain the composition.

In one example, the plant extract composition of the present invention is cooled to room temperature under a humidity of 40-50 ° C., after which the residue can be removed and stored and stored in a container of ceramic or glass material. Is good. The plant extract composition of the present invention obtained according to the above method is a yellowish brown liquid as shown in FIG. FIG. 2 is a photograph of the appearance of the plant extract composition according to the embodiment of the present invention.

The plant extract composition of the present invention obtained according to the above method is subjected to GC / MS analysis by an Agilent 7890B gas chromatograph and an Agilent 5977A mass spectrometer with the following parameters: injection volume: 1 μl; injection temperature: 280. ° C; Carrier gas: He; Column: DB-5MS 30m * 0.25mm * 0.25μm; Column flow rate: 1.0mL / min; Ion source temperature (MS source temperature): 230 ° C.; Quad temperature (MA quad temperature) : 150 ° C .; MS scan range: 40 m / z to 550 m / z; and the GC oven heating program is shown in Table 1 below.

Methanol is quantified to 10 mL (concentration 1000 μg / mL) using 0.01 g menthol as a high concentration standard solution. Quantify to 1 mL with methanol (concentration 10 μg / mL) as a low concentration standard solution using 10 μL high concentration standard solution. Then, for analysis, 1.0232 g of the plant extract composition of the example of the present invention is quantified to 10 mL. The results obtained can be subjected to relative quantification with respect to the peak value at the area value of 100 ppm menthol to obtain the percentage of relative quantification. The results are shown in FIG.

FIG. 3 is a total ion chromatography (TIC) spectrum of the plant extract composition of the examples of the present invention obtained after SGS HPLC mass spectrometry. As can be seen from FIG. 3, the plant extract composition of the examples of the present invention includes 2.167 ± 0.5 minutes, 2.662 ± 0.5 minutes, 4.203 ± 0.5 minutes, 78.23. There are peak values at ± 0.5 minutes, 79.033 ± 0.5 minutes, 79.792 ± 0.5 minutes, and 82.327 ± 0.5 minutes.

As can be seen from FIG. 3, the newly synthesized molecular compound is contained in the plant extract composition of the examples of the present invention obtained by using more than 10 kinds of catalytic ionization in plants in nature. Tables 2-4 below show some of the components of the plant extract composition of the examples of the present invention obtained after SGS HPLC mass spectrometry.

From Tables 2-4 above, the plant extract compositions of the examples of the present invention are 3-hydroxybutanone, crown ether-5, pyruvic acid, methoxyethylamine, triethylphosphine, valine acid, cyclopentadione, 2-hydroxy. Includes -2-cyclopentene-1-one, stearic acid, and alcohol. Among them, Crown-5 has the characteristics that it easily absorbs water and is easily mixed with water, has a strong selective complexing power for potassium / sodium ions, and is efficient in entering and exiting the cell membrane. It has an effect as a phase transfer catalyst. Therefore, other active ingredients in the plant extract composition of the present embodiment can be effectively incorporated into the circulation of the human body, and absorption can be promoted to improve the desired effect. Pyruvic acid has the effect of suppressing the oxidation of oxygen free radicals in the body, preventing damage to free radicals, and protecting the body from functional damage during cardiac reperfusion injury and acute renal failure. Valine is an essential amino acid that can promote muscle metabolism, improve muscle coordination, promote brain strength, stabilize mood and accelerate wound healing treatment. Stearic acid can prevent oxidation.

According to the components contained in the botanical extract composition of the examples of the present invention, when the botanical extract composition of the examples of the present invention is used by a plant steam bath, it removes moisture and detoxifies the user. It can achieve the effects of promoting metabolism, regulating physical strength, reducing inflammatory symptoms and promoting wound healing.

4 and 5 are effect diagrams after the user uses the plant extract composition of the embodiment in this case in the form of a plant vapor bath. Part (a) of FIG. 4 shows a situation in which the user has not yet used the plant extract composition of the embodiment of the present invention. Parts (b) to (f) of FIG. 4 show in order the length of time that the plant extract composition of the example was used in the plant steam bath. Part (b) of FIG. 4 shows that the user used the plant extract composition of the embodiment of the present invention in the shortest time. Part (f) of FIG. 4 shows that the user has been using the plant extract composition of the examples of the present invention for the longest time. From FIG. 4, it is clearly seen that the detoxifying and dehumidifying effects of the plant extract composition of this example accelerate the wound healing of the user. Part (a) of FIG. 5 shows a situation in which the user has not yet used the plant extract composition of the embodiment of the present invention. Part (b) of FIG. 5 shows the results after the user has used the plant extract composition of the examples of the present invention in the form of a plant vapor bath. From FIG. 5, it is clear that the use of the plant extract composition of this example in the form of a plant steam bath has the effect of removing edema and dehumidification.

The above description is merely an example and is not limiting. Any changes or amendments within the equivalent scope without departing from the scope and gist of the present invention shall be dealt with within the scope of the appended claims.

10 ... Method for preparing plant extract composition S101-S107 ... Step

Claims (9)

Noazami (Cirsium japonicum), Hirohayabumame (Glycine tomentella), Murraya paniculata (Murraya paniculata), Kazanabiki (Ventilago elegans), cotton rose (Hibiscus mutabilis), Baikaouren (Coptis quinquefolia Miq.), Taiwan Ficus (Ficus formosana Maxim), Harizakuro (Catunaregam spinosa ), A step of providing a plant composition containing Ficus plum and a step of immersing the plant composition in water, a step of immersing the plant composition in a first solution, and the above. A method for preparing a plant extract composition, which comprises a step of heating the plant composition and water together to obtain a plant extract composition. The method for preparing a plant extract composition according to claim 1, further comprising a step of cooling the plant extract composition to room temperature under a humidity of 40 to 50 ° C. to remove residues. The method for preparing a plant extract composition according to claim 1, wherein the step of heating with water includes heating on low heat for 5 hours. The method for preparing a plant extract composition according to claim 1, wherein the first solution contains water and vinegar, and the pH value is between 7.2 and 7.8. The ratio of Cirsium japonicum in the plant composition is 8.0 to 12.0 wt. %, The proportion of Hirohaya bean is 10.0 to 14.0 wt. %, The ratio of jessamine is 10.0 to 14.0 wt. %, The ratio of Kazanaviki is 10.0 to 14.0 wt. %, The ratio of Fuyo is 8.0 to 12.0 wt. %, The ratio of coptis quinque is 8.0 to 12.0 wt. %, The ratio of Taiwan Inubiwa is 6.0 to 10.0 wt. %, The ratio of Harizakuro is 7.0 to 11.0 wt. %, The ratio of Climbing fig is 6.0 to 10.0 wt. %, And the proportion of Kirehano grapes is 7.0-11.0 wt. The method for preparing a plant extract composition according to claim 1, wherein the composition is%. A plant extract characterized by containing Cirsium japonicum extract, Hirohaya bean extract, Gekkitsu extract, Kazanabiki extract, Fuyo extract, Coptis quinque extract, Taiwan Inubiwa extract, Harizakuro extract, Oitabi extract and Kirehano grape extract. Product composition. The total ion chromatography (TIC) profile of the plant extract composition was 2.167 ± 0.5 minutes, 2.662 ± 0.5 minutes, 4.203 ± 0.5 minutes, 78.23 ± 0. The plant extract composition according to claim 6, characterized by peaks at 5 minutes, 79.033 ± 0.5 minutes, 79.792 ± 0.5 minutes, and 82.327 ± 0.5 minutes. Stuff. The plant extract composition according to claim 6, wherein the plant extract composition has total ion chromatography shown in FIG. The plant extract composition according to claim 6, wherein the plant extract composition is a plant extract composition for a plant steam bath.

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