JP2021046369A - Skin cosmetic composition - Google Patents
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- JP2021046369A JP2021046369A JP2019169697A JP2019169697A JP2021046369A JP 2021046369 A JP2021046369 A JP 2021046369A JP 2019169697 A JP2019169697 A JP 2019169697A JP 2019169697 A JP2019169697 A JP 2019169697A JP 2021046369 A JP2021046369 A JP 2021046369A
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- cosmetic composition
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- 239000002537 cosmetic Substances 0.000 title claims abstract description 35
- 239000000203 mixture Substances 0.000 title claims abstract description 13
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 59
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims abstract description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229920005862 polyol Polymers 0.000 claims abstract description 6
- 150000003077 polyols Chemical class 0.000 claims abstract description 6
- 235000011187 glycerol Nutrition 0.000 claims description 28
- 230000003020 moisturizing effect Effects 0.000 abstract description 10
- 229920000223 polyglycerol Polymers 0.000 abstract 1
- 125000003976 glyceryl group Chemical group [H]C([*])([H])C(O[H])([H])C(O[H])([H])[H] 0.000 description 10
- 230000000694 effects Effects 0.000 description 5
- 230000000052 comparative effect Effects 0.000 description 4
- 229940105990 diglycerin Drugs 0.000 description 4
- GPLRAVKSCUXZTP-UHFFFAOYSA-N diglycerol Chemical compound OCC(O)COCC(O)CO GPLRAVKSCUXZTP-UHFFFAOYSA-N 0.000 description 4
- -1 alkyl glucoside Chemical class 0.000 description 3
- 238000011156 evaluation Methods 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 239000002649 leather substitute Substances 0.000 description 3
- 150000001298 alcohols Chemical class 0.000 description 2
- 230000001771 impaired effect Effects 0.000 description 2
- 239000000049 pigment Substances 0.000 description 2
- 229920001296 polysiloxane Polymers 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 230000001953 sensory effect Effects 0.000 description 2
- 239000004925 Acrylic resin Substances 0.000 description 1
- 229920000178 Acrylic resin Polymers 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 1
- 229920002683 Glycosaminoglycan Polymers 0.000 description 1
- 239000004166 Lanolin Chemical class 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 239000004677 Nylon Substances 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 description 1
- 239000006096 absorbing agent Substances 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 229920006318 anionic polymer Polymers 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 239000003899 bactericide agent Substances 0.000 description 1
- 229920006317 cationic polymer Polymers 0.000 description 1
- 239000002734 clay mineral Substances 0.000 description 1
- 239000000539 dimer Substances 0.000 description 1
- SZXQTJUDPRGNJN-UHFFFAOYSA-N dipropylene glycol Chemical compound OCCCOCCCO SZXQTJUDPRGNJN-UHFFFAOYSA-N 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 229930182478 glucoside Natural products 0.000 description 1
- 229940039717 lanolin Drugs 0.000 description 1
- 235000019388 lanolin Nutrition 0.000 description 1
- 239000006210 lotion Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229920001778 nylon Polymers 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 239000000419 plant extract Substances 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000003352 sequestering agent Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 229920003176 water-insoluble polymer Polymers 0.000 description 1
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Abstract
Description
本発明は、皮膚化粧料組成物に関するものである。 The present invention relates to a skin cosmetic composition.
化粧水のような大部分を水で構成された水性化粧料は、肌の環境を整えるために用いられる基礎化粧品であり、保湿や肌のｐＨを調整することを目的として使用される。 Aqueous cosmetics, which are mostly composed of water such as lotion, are basic cosmetics used for adjusting the environment of the skin, and are used for the purpose of moisturizing and adjusting the pH of the skin.
水性化粧料は大部分が水であるため、油性成分が配合された化粧料に比べさっぱりとした感触が得られるものの、肌は親油性であるため、比較的肌になじみにくいといった問題があった。 Since most of the water-based cosmetics are water, a refreshing feel can be obtained compared to cosmetics containing oily ingredients, but since the skin is lipophilic, there is a problem that it is relatively difficult to fit into the skin. ..
前記の課題に対応する先行技術文献として、ポリエーテル変性シリコーンと酸性ムコ多糖類を含有した水性皮膚化粧料が提案されている（特許文献１参照）。しかし、この提案は、安全性の面で忌避されることのあるポリエーテル変性シリコーンを用いている。 As a prior art document corresponding to the above problem, an aqueous skin cosmetic containing a polyether-modified silicone and an acidic mucopolysaccharide has been proposed (see Patent Document 1). However, this proposal uses polyether-modified silicone, which can be repelled in terms of safety.
また、ジプロピレングリコール、ポリオキシアルキレンアルキルグルコシドなどを含有する皮膚外用剤が提案されている（特許文献２参照）。この提案では、次に使用する化粧水等の機能性化粧料の肌馴染み改善効果を謳うものの、化粧水自体への配合ではないため、２度にわたる化粧料の塗布が必要となる。 Further, a skin external preparation containing dipropylene glycol, polyoxyalkylene alkyl glucoside and the like has been proposed (see Patent Document 2). In this proposal, although the effect of improving the skin familiarity of the functional cosmetics such as the toner to be used next is touted, the cosmetics need to be applied twice because it is not added to the toner itself.
したがって、安全性の高い原料を用い、皮膚化粧料自体の肌馴染みが良い組成物の開発が求められている。 Therefore, it is required to develop a composition which uses highly safe raw materials and has a good skin compatibility with the skin cosmetic itself.
本発明が解決しようとする課題は、肌馴染みが良く保湿効果の高い皮膚化粧料組成物を提供することである。 An object to be solved by the present invention is to provide a skin cosmetic composition having a good skin compatibility and a high moisturizing effect.
本発明者らは、上記課題を解決するため鋭意検討した結果、成分（Ａ）、（Ｂ）、（Ｃ）を含有する皮膚化粧料が上記課題を解決し得る事を見出し、本発明を完成するに至った。
（Ａ）ポリオキシアルキレンポリオールエーテル
（Ｂ）多価アルコール
（Ｃ）水
As a result of diligent studies to solve the above problems, the present inventors have found that a skin cosmetic containing the components (A), (B) and (C) can solve the above problems, and completed the present invention. I came to do it.
(A) Polyoxyalkylene polyol ether (B) Multihydric alcohol (C) Water
本発明は、肌馴染みが良く保湿効果の高い皮膚化粧料の開発を可能とするものである。 The present invention enables the development of skin cosmetics that are well-adapted to the skin and have a high moisturizing effect.
本発明に用いられる（Ａ）ポリオキシアルキレンポリオールエーテルとしては、グリセリン又はポリグリセリンにエチレンオキサイド（以下、「ＥＯ」と略記する）又はプロピレンオキサイド（以下、「ＰＯ」と略記する）が付加したものが好ましい。前記ポリオキシアルキレンポリオールエーテルとしては、グリセリンにＥＯの平均付加モル数が３であるグリセレス−３、グリセリンにＥＯの平均付加モル数が７であるグリセレス−７、グリセリンにＥＯの平均付加モル数が１２であるグリセレス−１２、グリセリンにＥＯの平均付加モル数が１８であるグリセレス−１８、グリセリンにＥＯの平均付加モル数が２０であるグリセレス−２０、グリセリンにＥＯの平均付加モル数が２６であるグリセレス−２６、グリセリンにＥＯの平均付加モル数が３１であるグリセレス−３１、グリセリンにＰＯの平均付加モル数が３であるＰＰＧ−３グリセリル、グリセリンにＰＯの平均付加モル数が６であるＰＰＧ−６グリセリル、グリセリンにＰＯの平均付加モル数が８であるＰＰＧ−８グリセリル、グリセリンにＰＯの平均付加モル数が９であるＰＰＧ−９グリセリル、グリセリンにＰＯの平均付加モル数が１０であるＰＰＧ−１０グリセリル、グリセリンにＰＯの平均付加モル数が１６であるＰＰＧ−１６グリセリル、グリセリンにＰＯの平均付加モル数が２４であるＰＰＧ−２４グリセリル、グリセリンにＰＯの平均付加モル数が２７であるＰＰＧ−２７グリセリル、グリセリンにＰＯの平均付加モル数が５０であるＰＰＧ−５０グリセリル、グリセリンにＰＯの平均付加モル数が７０であるＰＰＧ−７０グリセリル、ジグリセリンにＰＯの平均付加モル数が９であるＰＰＧ−９ジグリセリル、ジグリセリンにＰＯの平均付加モル数が１４であるＰＰＧ−１４ジグリセリルなどが挙げられる。これらの中でも、肌馴染みを向上させる点からＰＰＧ−９ジグリセリル、ＰＰＧ−１４ジグリセリルが好ましい。 The (A) polyoxyalkylene polyol ether used in the present invention is glycerin or polyglycerin to which ethylene oxide (hereinafter abbreviated as “EO”) or propylene oxide (hereinafter abbreviated as “PO”) is added. Is preferable. The polyoxyalkylene polyol ether has glyceres-3 having an average EO addition molar number of 3 to glycerin, glyceres-7 having an average EO addition molar number of 7 to glycerin, and an EO addition molar number to glycerin. 12 glyceres-12, glycerin with an average EO molar addition of 18 glyceres-18, glycerin with an average EO molar addition of 20 glyceres-20, glycerin with an average EO molar addition of 26 A certain glyceres-26, glyceres-31 having an average EO addition molar number of 31 to glycerin, PPG-3 glyceryl having an average PO addition molar number of 3 to glycerin, and 6 PO addition moles to glycerin. PPG-6 glyceryl, PPG-8 glyceryl having an average PO addition molar number of 8 to glycerin, PPG-9 glyceryl having an average PO addition molar number of 9 to glycerin, and 10 PO addition moles to glycerin A certain PPG-10 glyceryl, PPG-16 glyceryl having an average PO addition molar number of 16 to glycerin, PPG-24 glyceryl having an average PO addition molar number of 24 to glycerin, and 27 PO addition moles to glycerin. PPG-27 glyceryl, PPG-50 glyceryl having an average PO addition molar number of 50 to glycerin, PPG-70 glyceryl having an average PO addition molar number of 70 to glycerin, and an average PO addition molar number to diglycerin. Examples thereof include PPG-9 diglyceryl having a value of 9 and PPG-14 diglyceryl having an average number of moles of PO added to diglycerin of 14. Among these, PPG-9 diglyceryl and PPG-14 diglyceryl are preferable from the viewpoint of improving skin compatibility.
成分（Ａ）の含有量は、皮膚化粧料の肌馴染み向上効果の点から皮膚化粧料全量に対し２〜３５質量％であることが好ましい。 The content of the component (A) is preferably 2 to 35% by mass with respect to the total amount of the skin cosmetics from the viewpoint of improving the skin familiarity of the skin cosmetics.
本発明に用いられる（Ｂ）グリセリン又はポリグリセリンとしては、グリセリン、グリセリンの２量体であるジグリセリン、グリセリンの３量体であるトリグリセリン、グリセリンの４量体であるテトラグリセリン、グリセリンの６量体であるヘキサグリセリン、グリセリンの１０量体であるデカグリセリン、グリセリンの２０量体であるエイコサグリセリンなどが挙げられ、グリセリン、ジグリセリン、トリグリセリンを用いることが好ましい。 The (B) glycerin or polyglycerin used in the present invention includes glycerin, diglycerin which is a dimer of glycerin, triglycerin which is a trimeric of glycerin, and tetraglycerin and glycerin which are tetramers of glycerin. Examples thereof include hexaglycerin which is a metric, decaglycerin which is a decaglycerin of glycerin, and eikosaglycerin which is a 20-mer of glycerin, and it is preferable to use glycerin, diglycerin, and triglycerin.
成分（Ａ）と成分（Ｂ）の質量の総和に対する成分（Ａ）の含有量は、２０〜８０質量％であることが好ましい。２０〜８０質量％の範囲とすることで本発明の皮膚化粧料は、肌馴染み向上効果と保湿効果に優れる。 The content of the component (A) with respect to the total mass of the component (A) and the component (B) is preferably 20 to 80% by mass. When the range is 20 to 80% by mass, the skin cosmetic of the present invention is excellent in skin compatibility improving effect and moisturizing effect.
成分（Ａ）と成分（Ｂ）の質量の総和は、皮膚化粧料の肌馴染み向上効果の点から皮膚化粧料全量に対し５〜４０質量％が好ましい。 The total mass of the component (A) and the component (B) is preferably 5 to 40% by mass with respect to the total amount of the skin cosmetic from the viewpoint of improving the skin familiarity of the skin cosmetic.
成分（Ｃ）の含有量は、皮膚化粧料全量に対し６０〜９０質量％が好ましい。６０〜９０質量％の範囲とすることで、塗布後のさっぱり感と肌馴染みの向上効果を両立させることができる。 The content of the component (C) is preferably 60 to 90% by mass with respect to the total amount of the skin cosmetics. By setting the content in the range of 60 to 90% by mass, it is possible to achieve both a refreshing feeling after application and an effect of improving skin familiarity.
本発明の皮膚化粧料組成物は、前記成分（Ａ）、（Ｂ）、（Ｃ）以外にも、本発明の効果を損なわない範囲で、その他の成分を含有することができる。前記その他の成分としては、特に制限は無く、皮膚化粧料に通常用いられるものの中から適宜選択することができ、例えば、油分、低級又は高級アルコール等のアルコール類、ラノリン誘導体、蛋白誘導体、アクリル樹脂分散液、カチオン性ポリマー、アニオン性ポリマー、ノニオン性ポリマー、ビタミン等の薬剤、殺菌剤、防腐剤、ｐＨ調整剤、酸化防止剤、金属封鎖剤、紫外線吸収剤、動植物抽出物又はその誘導体、色素、香料、顔料、無機粉体、粘土鉱物、ナイロン、ポリエチレン等の水不溶性ポリマー粉体などが挙げられる。その他の成分の含有量としては、本発明の効果を損なわない範囲で、目的に応じて適宜選択することができる。 The skin cosmetic composition of the present invention may contain other components in addition to the above components (A), (B) and (C) as long as the effects of the present invention are not impaired. The other components are not particularly limited and may be appropriately selected from those usually used in skin cosmetics. For example, oils, alcohols such as lower or higher alcohols, lanolin derivatives, protein derivatives, acrylic resins. Dispersions, cationic polymers, anionic polymers, nonionic polymers, chemicals such as vitamins, bactericides, preservatives, pH adjusters, antioxidants, metal sequestering agents, UV absorbers, animal and plant extracts or derivatives thereof, pigments , Perfume, pigment, inorganic powder, clay mineral, water-insoluble polymer powder such as nylon and polyethylene. The content of the other components can be appropriately selected depending on the intended purpose as long as the effects of the present invention are not impaired.
本発明の皮膚化粧料組成物の製造方法としては、特に制限は無く、目的に応じて適宜選択することができ、例えば、成分（Ａ）、（Ｂ）、（Ｃ）、その他の成分を混合して、得ることができる。 The method for producing the skin cosmetic composition of the present invention is not particularly limited and may be appropriately selected depending on the intended purpose. For example, ingredients (A), (B), (C) and other ingredients are mixed. And you can get it.
皮膚化粧料の人工皮革上での接触角は、共和界面科学（株）製ＤｒｏｐＭａｓｔｅｒ ＤＭ ３００を用いて測定した値であり、肌馴染み向上の点から９０°以下であることが好ましく、８５°以下であることがさらに好ましく、８０°以下であることが最も好ましい。 The contact angle of the skin cosmetic on artificial leather is a value measured using DropMaster DM 300 manufactured by Kyowa Interface Science Co., Ltd., and is preferably 90 ° or less, preferably 85 ° or less, from the viewpoint of improving skin familiarity. Is more preferable, and 80 ° or less is most preferable.
以下、実施例及び比較例により本発明をより具体的に説明するが、本発明の範囲はこれらの実施例により限定されるものではない。 Hereinafter, the present invention will be described in more detail with reference to Examples and Comparative Examples, but the scope of the present invention is not limited to these Examples.
ポリオキシアルキレンポリオールエーテル、多価アルコール、水を表１に示す組成で混合し、実施例１〜１０および比較例１〜３の皮膚化粧料を製造した。得られた皮膚化粧料について、人工皮革上での接触角を共和界面科学（株）製ＤｒｏｐＭａｓｔｅｒ ＤＭ ３００を用いて測定した。 Polyoxyalkylene polyol ether, polyhydric alcohol, and water were mixed in the compositions shown in Table 1 to produce skin cosmetics of Examples 1 to 10 and Comparative Examples 1 to 3. With respect to the obtained skin cosmetics, the contact angle on artificial leather was measured using DropMaster DM 300 manufactured by Kyowa Interface Science Co., Ltd.
実施例１〜１０および比較例１〜３の皮膚化粧料について、肌馴染みの評価を実施した。評価項目としては、「人肌上での肌馴染み」、「保湿効果」の２点であり、４段階で評価した。 The skin cosmetics of Examples 1 to 10 and Comparative Examples 1 to 3 were evaluated for their familiarity with the skin. There were two evaluation items, "skin familiarity on human skin" and "moisturizing effect", which were evaluated on a four-point scale.
［人肌上での肌馴染み］
２０名のパネラーにより官能評価した。皮膚化粧料を１滴肌上に滴下し、伸ばした際の肌馴染みの良さについて５点満点として平均点を算出し、以下の基準より評価した。点数が高いほど肌馴染みが良好である。これらの結果を表１に示す。
（基準）
◎：４．０点以上
○：３．０点以上、４．０点未満
△：２．０点以上、３．０点未満
×：２．０点以下
[Familiarity with human skin]
Sensory evaluation was performed by 20 panelists. One drop of skin cosmetic was dropped on the skin, and the average score was calculated with a maximum of 5 points for the goodness of skin familiarity when stretched, and evaluated from the following criteria. The higher the score, the better the skin compatibility. These results are shown in Table 1.
(Standard)
⊚: 4.0 points or more ○: 3.0 points or more and less than 4.0 points Δ: 2.0 points or more and less than 3.0 points ×: 2.0 points or less
［保湿効果］
２０名のパネラーにより官能評価した。皮膚化粧料を肌上に塗布し、３０分後の保湿感ついて５点満点として平均点を算出し、以下の基準により評価した。点数が高いほど保湿効果が良好である。これらの結果を表１に示す。
（基準）
◎：４．０点以上
○：３．０点以上、４．０点未満
△：２．０点以上、３．０点未満
×：２．０点以下
[Moisturizing effect]
Sensory evaluation was performed by 20 panelists. A skin cosmetic was applied onto the skin, and the average score was calculated on a scale of 5 for the moisturizing feeling after 30 minutes, and evaluated according to the following criteria. The higher the score, the better the moisturizing effect. These results are shown in Table 1.
(Standard)
⊚: 4.0 points or more ○: 3.0 points or more and less than 4.0 points Δ: 2.0 points or more and less than 3.0 points ×: 2.0 points or less
ＰＰＧ−９ジグリセリルおよびＰＰＧ−１４ジグリセリルを配合した実施例１〜１０は、ＰＰＧ−９ジグリセリルおよびＰＰＧ−１４ジグリセリルを配合しない比較例１〜３に比べて人肌上での肌馴染みに優れ、保湿効果に優れていた。
中でも、人工皮革上での接触角が８０°以下である実施例３〜１０の皮膚化粧料は、特に肌馴染みに優れていた。
Examples 1 to 10 containing PPG-9 diglyceryl and PPG-14 diglyceryl are more familiar to human skin than Comparative Examples 1 to 3 not containing PPG-9 diglyceryl and PPG-14 diglyceryl. It was excellent in moisturizing effect.
Among them, the skin cosmetics of Examples 3 to 10 having a contact angle of 80 ° or less on artificial leather were particularly excellent in skin compatibility.
Claims (3)
（Ｂ）グリセリン又はポリグリセリンから選択される一種又は二種以上
（Ｃ）水
を含有する皮膚化粧料組成物。 (A) Polyoxyalkylene polyol ether (B) One or more selected from glycerin or polyglycerin (C) A skin cosmetic composition containing water.
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| JP2019169697A JP2021046369A (en) | 2019-09-18 | 2019-09-18 | Skin cosmetic composition |
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| JP (1) | JP2021046369A (en) |
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| JP2004339212A (en) * | 2003-04-22 | 2004-12-02 | Kao Corp | Cleansing composition |
| JP2006131520A (en) * | 2004-11-04 | 2006-05-25 | Sakamoto Yakuhin Kogyo Co Ltd | Moisturizing cosmetic |
| JP2007230950A (en) * | 2006-03-02 | 2007-09-13 | Sakamoto Yakuhin Kogyo Co Ltd | Highly moisturizing cosmetic |
| JP2016132623A (en) * | 2015-01-16 | 2016-07-25 | 株式会社マンダム | Skin lotion |
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