JP2020063224A - Solid cosmetic composition, and method for producing solid cosmetic composition - Google Patents
Solid cosmetic composition, and method for producing solid cosmetic composition Download PDFInfo
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- JP2020063224A JP2020063224A JP2018197476A JP2018197476A JP2020063224A JP 2020063224 A JP2020063224 A JP 2020063224A JP 2018197476 A JP2018197476 A JP 2018197476A JP 2018197476 A JP2018197476 A JP 2018197476A JP 2020063224 A JP2020063224 A JP 2020063224A
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- cosmetic composition
- mass
- solid cosmetic
- solid
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Landscapes
- Cosmetics (AREA)
Abstract
Description
本発明は、固形化粧料組成物およびその製造方法に関する。 The present invention relates to a solid cosmetic composition and a method for producing the same.
近年、人気が高まっている化粧料として、固形化粧料がある。この固形化粧料は、主成分として半固形〜固形油を含んでいるため、常温での剤型は半固形〜固形であるが、手や肌などに触れると体温で半固形〜固形油が融解して液状になり、伸ばし広げやすい物性になることが特徴である。 BACKGROUND ART In recent years, solid cosmetics have become popular as cosmetics. This solid cosmetic contains semi-solid to solid oil as the main component, so the formulation at room temperature is semi-solid to solid, but when it comes into contact with hands or skin, the semi-solid to solid oil melts at body temperature. The characteristic is that it becomes liquid and has physical properties that make it easy to stretch and spread.
固形化粧料は、肌（特に顔、手、足）、爪など、全身に用いることができる。一般に、固形化粧料を肌に塗布することによって、肌が保湿され、潤うことが知られている。
市販されている固形化粧料の形態としては、成形後に包装されたもの、缶やビンに充填されたもの、スティックタイプのもの等が挙げられる。
The solid cosmetics can be used for the whole body such as skin (particularly face, hands, feet) and nails. It is generally known that skin is moisturized and moisturized by applying solid cosmetics to the skin.
Examples of commercially available solid cosmetics include those packaged after molding, those packed in cans and bottles, those of stick type, and the like.
固形化粧料についての先行技術としては、例えば、特許文献１において、（ｉ）（ａ）外部層に対して１０〜４５重量％の量の硬質植物性バター、及び（ｂ）外部層に対して５５〜８０重量％の量の軟質植物性バターを含む外部層と、（ii）（ａ）軟質植物性バター組成物、（ｂ）フォンダン、又は（ｃ）液体化粧品である内部コアとを含む固形化粧品組成物が開示されている。特許文献２では、植物性バターを含む固体化粧品組成物であって、前記固体組成物が、その中に気泡を分散させており、前記気泡が、前記固体化粧品組成物の体積の少なくとも２０％を形成する、固体組成物が開示されている。 As a prior art for solid cosmetics, for example, in Patent Document 1, (i) (a) hard vegetable butter in an amount of 10 to 45% by weight with respect to the outer layer, and (b) with respect to the outer layer. A solid comprising an outer layer comprising soft vegetable butter in an amount of 55-80% by weight, and (ii) (a) a soft vegetable butter composition, (b) fondant, or (c) an inner core which is a liquid cosmetic. Cosmetic compositions are disclosed. In Patent Document 2, a solid cosmetic composition comprising vegetable butter, wherein the solid composition has air bubbles dispersed therein, the air bubbles making up at least 20% of the volume of the solid cosmetic composition. Forming, solid compositions are disclosed.
特許文献１に開示された発明は、肌に塗布するとべたつきがあり、使い心地がよくなかった。特許文献２に開示された発明は、肌に塗布するとべたつきがあることや、油脂の酸化安定性が懸念された。
このようなことから、本発明は、主成分として半固形〜固形油を含んでいながら、肌に塗布してもべたつかず、酸化安定性の高い固形化粧料を提供することを課題とする。
The invention disclosed in Patent Document 1 is not sticky when applied to the skin and is not comfortable to use. The invention disclosed in Patent Document 2 was concerned about stickiness when applied to the skin and oxidative stability of fats and oils.
In view of the above, the present invention has an object to provide a solid cosmetic containing semisolid to solid oil as a main component, which is not sticky even when applied to the skin and has high oxidation stability.
本発明者らは上記課題を解決すべく鋭意検討した。その結果、以下の構成を有する固形化粧料およびその製造方法は上記課題を解決できることを見出し、本発明を完成するに至った。 The present inventors have diligently studied to solve the above problems. As a result, they have found that a solid cosmetic having the following constitution and a method for producing the same can solve the above problems, and completed the present invention.
本発明は、例えば以下の［１］〜［７］である。
［１］シアバター（Ａ）を１５〜８０質量％と、ココアバター（Ｂ）を１５〜８０質量％と、アビシニアンオイル、メドウフォームオイル、および抗酸化剤から選ばれる少なくとも１種の成分（Ｃ）を０．１〜１０質量％と、植物性液状油（Ｄ）（但し、アビシニアンオイルおよびメドウフォームオイルを除く）を０．１〜２０質量％とを含む、固形化粧料組成物。
［２］ミツロウ（Ｅ）を１〜５０質量％含む、［１］に記載の固形化粧料組成物。
［３］アビシニアンオイルを０．１〜５質量％含む、［１］または［２］に記載の固形化粧料組成物。
［４］メドウフォームオイルを０．１〜５質量％含む、［１］〜［３］のいずれかに記載の固形化粧料組成物。
［５］シアバター（Ａ）とココアバター（Ｂ）との質量の合計が６０〜９９質量％である、［１］〜［４］のいずれかに記載の固形化粧料組成物。
［６］［１］〜［５］のいずれかに記載の固形化粧料組成物を製造するための方法であって、
工程（１）：シアバター（Ａ）およびココアバター（Ｂ）を溶解し、溶解液aを得る工程、工程（２）：工程（１）で得られた溶解液aと、アビシニアンオイル、メドウフォームオイル、および抗酸化剤から選ばれる少なくとも１種の成分（Ｃ）と、植物性液状油（Ｄ）とを混合し、混合液bを得る工程、工程（３）：工程（２）で得られた混合液bを冷却する冷却工程とを含む、固形化粧料組成物の製造方法。
［７］前記工程（３）が、冷却開始から２時間以内に、混合液ｂの中心温度が１０℃以下に到達する冷却工程である［６］に記載の固形化粧料組成物の製造方法。
The present invention is, for example, the following [1] to [7].
[1] 15 to 80% by mass of shea butter (A), 15 to 80% by mass of cocoa butter (B), and at least one component (C) selected from abyssinian oil, meadow foam oil, and antioxidant. 0.1 to 10% by mass, and 0.1 to 20% by mass of the vegetable liquid oil (D) (excluding abyssinian oil and meadow foam oil), but a solid cosmetic composition.
[2] The solid cosmetic composition according to [1], which contains 1 to 50 mass% of beeswax (E).
[3] The solid cosmetic composition according to [1] or [2], which contains 0.1 to 5 mass% of abyssinian oil.
[4] The solid cosmetic composition according to any one of [1] to [3], which contains 0.1 to 5 mass% of meadow foam oil.
[5] The solid cosmetic composition according to any one of [1] to [4], wherein the total mass of shea butter (A) and cocoa butter (B) is 60 to 99 mass%.
[6] A method for producing the solid cosmetic composition according to any one of [1] to [5],
Step (1): a step of dissolving shea butter (A) and cocoa butter (B) to obtain a solution a, step (2): the solution a obtained in step (1), abyssinian oil, and meadow foam Step (3) of mixing at least one component (C) selected from oils and antioxidants with vegetable liquid oil (D) to obtain mixed liquid b, step (3): obtained in step (2) And a cooling step of cooling the mixed liquid b.
[7] The method for producing a solid cosmetic composition according to [6], wherein the step (3) is a cooling step in which the central temperature of the mixed liquid b reaches 10 ° C. or lower within 2 hours from the start of cooling.
本発明は、主成分として半固形〜固形油を含んでいながら、肌に塗布してもべたつかず、酸化安定性の高い固形化粧料を提供できる。 INDUSTRIAL APPLICABILITY The present invention can provide a solid cosmetic that contains semisolid to solid oil as a main component, is not sticky when applied to the skin, and has high oxidation stability.
次に本発明の固形化粧料組成物およびその製造方法について具体的に説明する。
＜固形化粧料組成物＞
本発明において固形化粧料組成物とは、剤形が室温（２５℃）で半固形〜固形の化粧料組成物であり、非常に粘度の高いクリームや軟膏を意味する。
本発明の固形化粧料組成物は、シアバター（Ａ）を１５〜８０質量％と、ココアバター（Ｂ）を１５〜８０質量％と、アビシニアンオイル、メドウフォームオイル、および抗酸化剤から選ばれる少なくとも１種の成分（Ｃ）を０．１〜１０質量％と、植物性液状油（Ｄ）（但し、アビシニアンオイルおよびメドウフォームオイルを除く）を０．１〜２０質量％とを含む。
Next, the solid cosmetic composition of the present invention and the method for producing the same will be specifically described.
<Solid cosmetic composition>
In the present invention, the solid cosmetic composition is a semi-solid to solid cosmetic composition having a dosage form at room temperature (25 ° C.) and means a cream or an ointment having a very high viscosity.
The solid cosmetic composition of the present invention comprises 15 to 80% by mass of shea butter (A), 15 to 80% by mass of cocoa butter (B), and is selected from abyssinian oil, meadow foam oil, and antioxidant. It contains 0.1 to 10 mass% of at least one component (C), and 0.1 to 20 mass% of vegetable liquid oil (D) (excluding abyssinian oil and meadow foam oil).
本発明の固形化粧料組成物は、任意で、ミツロウ（Ｅ）を１〜５０質量％含むことも好ましく、２０〜３０質量％含むことがより好ましい。また、必要に応じて、その他の成分を含んでいてもよい。
なお、上記の各成分の含有量は、固形化粧料組成物を１００質量％とした場合の含有量を示している。
The solid cosmetic composition of the present invention optionally contains 1 to 50% by mass of beeswax (E), and more preferably 20 to 30% by mass. Moreover, you may contain the other component as needed.
The content of each of the above components indicates the content when the solid cosmetic composition is 100% by mass.
＜シアバター（Ａ）＞
本発明の固形化粧料組成物は、シアバター（Ａ）を１５〜８０質量％含み、２５〜７５質量％含むことが好ましく、３０〜７３質量％含むことがより好ましい。
本発明の固形化粧料組成物で用いるシアバター（Ａ）は、室温（２５℃）において、固形状のシアバターであれば特に限定されないが、脱臭、脱色しているものが好ましい。
シアバター（Ａ）として、具体的には、Ｓｈｅａ Ｂｕｔｔｅｒ ＲＦＯ（株式会社ＣＥＬＭＹＯＮ社製）等を用いることができる。
本発明ではシアバター（Ａ）を、後述するココアバター（Ｂ）と組み合わせて用いる。
<Shea butter (A)>
The solid cosmetic composition of the present invention contains 15 to 80% by mass of shea butter (A), preferably 25 to 75% by mass, and more preferably 30 to 73% by mass.
The shea butter (A) used in the solid cosmetic composition of the present invention is not particularly limited as long as it is solid shea butter at room temperature (25 ° C), but it is preferably deodorized and decolorized.
As the shea butter (A), specifically Shea Butter RFO (manufactured by CELMYON Co., Ltd.) or the like can be used.
In the present invention, shea butter (A) is used in combination with cocoa butter (B) described later.
＜ココアバター（Ｂ）＞
本発明の固形化粧料組成物は、ココアバター（Ｂ）を１５〜８０質量％含み、２５〜７０質量％含むことが好ましく、３０〜６５質量％含むことがより好ましい。
本発明の固形化粧料組成物は、ココアバター（Ｂ）は、室温（２５℃）において、固形状のココアバターであれば特に限定されないが、脱臭、脱色しているものが好ましい。
ココアバター（Ｂ）として、具体的には、ＣＯＣＯＡ ＢＵＴＴＥＲ ＲＦ（株式会社ＣＥＬＭＹＯＮ社製）等を用いることができる。
<Cocoa butter (B)>
The solid cosmetic composition of the present invention contains cocoa butter (B) in an amount of 15 to 80% by mass, preferably 25 to 70% by mass, and more preferably 30 to 65% by mass.
The solid cosmetic composition of the present invention is not particularly limited as long as the cocoa butter (B) is solid cocoa butter at room temperature (25 ° C.), but it is preferably deodorized and decolorized.
As the cocoa butter (B), specifically, COCOA BUTTER RF (manufactured by CELMYON Co., Ltd.) or the like can be used.
本発明の固形化粧料組成物は、上述したシアバター（Ａ）とココアバター（Ｂ）との質量の合計が６０〜９９質量％であることが好ましく、６５〜９５質量％であることがより好ましい。 In the solid cosmetic composition of the present invention, the total mass of the shea butter (A) and the cocoa butter (B) described above is preferably 60 to 99% by mass, and more preferably 65 to 95% by mass. preferable.
＜成分（Ｃ）＞
本発明の固形化粧料組成物は、アビシニアンオイル、メドウフォームオイル、および抗酸化剤から選ばれる少なくとも１種の成分（Ｃ）を０．１〜１０質量％含み、１〜５質量％含むことが好ましく、２〜４質量％含むことがより好ましい。
<Component (C)>
The solid cosmetic composition of the present invention contains 0.1 to 10% by mass, and preferably 1 to 5% by mass of at least one component (C) selected from abyssinian oil, meadow foam oil, and antioxidant. It is preferable that the content is 2 to 4% by mass.
本発明の固形化粧料組成物は、成分（Ｃ）を上記の量含むことによって、酸化による品質劣化を抑制することができる。
本発明で用いるアビシニアンオイルは、クランベアビシニカの種子から抽出される油のことを指す。本発明の固形化粧料組成物は、アビシニアンオイルを配合することで、肌に塗布した際の保湿効果が高く、さらさらとした使い心地になることや、酸化による品質劣化を抑制することから好ましい。本発明の固形化粧料組成物はアビシニアンオイルを、０．１〜５質量％含むことが好ましく、１〜３質量％含むことがより好ましい。
The solid cosmetic composition of the present invention can suppress the quality deterioration due to oxidation by containing the component (C) in the above amount.
The abyssinian oil used in the present invention refers to an oil extracted from seeds of clan bear vicinica. The solid cosmetic composition of the present invention is preferably blended with abyssinian oil, since it has a high moisturizing effect when applied to the skin, provides a smooth feeling to use, and suppresses quality deterioration due to oxidation. The solid cosmetic composition of the present invention preferably contains 0.1 to 5 mass% of abyssinian oil, and more preferably 1 to 3 mass%.
本発明で用いるメドウフォームオイルは、メドウフォームの種子から抽出される油のことを指し、トコフェロール類を多く含むものが好ましい。本発明の固形化粧料組成物は、メドウフォームオイルを配合することで、保湿効果が高く、剤の伸びがよくなることや、酸化による品質劣化を抑制することから好ましい。本発明の固形化粧料組成物はメドウフォームオイルを、０．１〜５質量％含むことが好ましく、１〜４質量％含むことがより好ましい。 The meadowfoam oil used in the present invention refers to an oil extracted from meadowfoam seeds, and preferably contains a large amount of tocopherols. The solid cosmetic composition of the present invention is preferable because it has a high moisturizing effect, improves the elongation of the agent, and suppresses the deterioration of quality due to oxidation, by incorporating a meadow foam oil. The solid cosmetic composition of the present invention preferably contains the meadow foam oil in an amount of 0.1 to 5% by mass, more preferably 1 to 4% by mass.
本発明で用いる抗酸化剤として、具体的には、テトラヘキシルデカン酸アスコルビル、ステアリン酸アスコルビル、パルミチン酸アスコルビル、トコフェロール類、ローズマリー抽出物、茶抽出物、ジブチルヒドロキシトルエン、ブチルヒドロキシアニソール、フェノール系酸化防止剤が挙げられる。これらの中でも、酸化安定性が高く、製剤にした際の香りや色への影響が少ないことからなことから、テトラヘキシルデカン酸アスコルビル、ステアリン酸アスコルビル、パルミチン酸アスコルビル、トコフェロール類が好ましい。本発明の固形化粧料組成物が、抗酸化剤を含む場合には、０．０１〜１０質量％含むことが好ましく、０．０５〜１質量％含むことがより好ましい。なお、本発明の固形化粧料組成物において、抗酸化剤が成分（Ｃ）の下限である０．１質量％より少ない場合には、アビシニアンオイルおよびメドウフォームオイルから選択される少なくとも一方と併用すればよい。 As the antioxidant used in the present invention, specifically, ascorbyl tetrahexyldecanoate, ascorbyl stearate, ascorbyl palmitate, tocopherols, rosemary extract, tea extract, dibutylhydroxytoluene, butylhydroxyanisole, phenolic oxidation Examples include inhibitors. Of these, ascorbyl tetrahexyldecanoate, ascorbyl stearate, ascorbyl stearate, ascorbyl palmitate, and tocopherols are preferable because they have high oxidative stability and have little influence on the scent and color when formulated. When the solid cosmetic composition of the present invention contains an antioxidant, it is preferably contained in an amount of 0.01 to 10% by mass, more preferably 0.05 to 1% by mass. In the solid cosmetic composition of the present invention, when the amount of the antioxidant is less than the lower limit of 0.1% by mass of component (C), it may be used in combination with at least one selected from abyssinian oil and meadow foam oil. Good.
成分（Ｃ）は、１種単独で用いても、２種以上組み合わせて用いてもよい。成分（Ｃ）としては、アビシニアンオイル、メドウフォームオイル、および抗酸化剤から選ばれる少なくとも２種の成分であることが好ましく、アビシニアンオイルおよびメドウフォームオイルであるか、アビシニアンオイル、メドウフォームオイル、および抗酸化剤であることがより好ましい。 As the component (C), one type may be used alone, or two or more types may be used in combination. The component (C) is preferably at least two kinds of components selected from abyssinian oil, meadowfoam oil, and antioxidant, and is abyssinian oil and meadowfoam oil, or abyssinian oil, meadowfoam oil, and More preferably, it is an antioxidant.
成分（Ｃ）としてアビシニアンオイルおよびメドウフォームオイルを用いる場合には、アビシニアンオイル：メドウフォームオイル（質量比）が、１：０．１〜１：１０であることが好ましい。 When using Abyssinian oil and Meadow foam oil as a component (C), it is preferable that Abyssinian oil: Meadow foam oil (mass ratio) is 1: 0.1 to 1:10.
また、成分（Ｃ）として、アビシニアンオイル、メドウフォームオイル、および抗酸化剤を用いる場合には、アビシニアンオイル：抗酸化剤（質量比）が、１：０．０１〜１：１０であることが好ましい。 Moreover, when using abyssinian oil, meadowfoam oil, and an antioxidant as a component (C), abyssinian oil: antioxidant (mass ratio) may be 1: 0.01 to 1:10. preferable.
＜植物性液状油（Ｄ）＞
本発明の固形化粧料組成物は、植物性液状油（Ｄ）を０．１〜２０質量％含み、１〜１０質量％含むことが好ましい。
本発明の固形化粧料組成物で用いる植物性液状油（Ｄ）には、アビシニアンオイルおよびメドウフォームオイルは含まれず、これらは前述の成分（Ｃ）に該当する。
<Vegetable liquid oil (D)>
The solid cosmetic composition of the present invention contains the vegetable liquid oil (D) in an amount of 0.1 to 20% by mass, and preferably 1 to 10% by mass.
The vegetable liquid oil (D) used in the solid cosmetic composition of the present invention does not include abyssinian oil and meadow foam oil, and these correspond to the above-mentioned component (C).
植物性液状油（Ｄ）として、具体的には、マルラオイル、バオバブオイル、アルガンオイル、モリンガオイル、ホホバオイル、アプリコットオイル、ココナツオイル、アーモンドオイル、スウィートアーモンドオイル、オリーブオイル、ヒマワリオイル、グレープシードオイル、パッションフラワーオイル、ワイルドアフリカンカラバシュオイル、ザクロオイル、ローズヒップオイル、シーバックソーンオイル、ハイビスカスオイル、クランベリーオイル、ラズベリーオイル、アボカドオイル、マカダミアオイル、ニームオイル、ウチワサボテンオイル、米油、セサミオイル、バラニテスオイル、ヘンプシードオイル、アムラオイルが挙げられる。これらの中でも、肌に塗布した際の保湿効果が高く、肌のオイルバランスを整え、さらさらとした使い心地に優れるという観点から、バオバブオイル、マルラオイルが好ましい。 Specific examples of the vegetable liquid oil (D) include marula oil, baobab oil, argan oil, moringa oil, jojoba oil, apricot oil, coconut oil, almond oil, sweet almond oil, olive oil, sunflower oil, grape seed oil. , Passion flower oil, wild african calabash oil, pomegranate oil, rosehip oil, sea buckthorn oil, hibiscus oil, cranberry oil, raspberry oil, avocado oil, macadamia oil, neem oil, prickly pear cactus oil, rice oil, sesame oil , Balanites oil, hemp seed oil, Amla oil. Among these, baobab oil and marula oil are preferable from the viewpoints of having a high moisturizing effect when applied to the skin, adjusting the oil balance of the skin, and excellent in a smooth and comfortable use.
植物性液状油（Ｄ）は、１種単独で用いても、２種以上組み合わせて用いてもよい。植物性液状油（Ｄ）がバオバブオイルおよびマルラオイルである場合には、バオバブオイル：マルラオイル（質量比）が、１：０．１〜１：１０であることが好ましい。 The liquid vegetable oil (D) may be used alone or in combination of two or more. When the vegetable liquid oil (D) is baobab oil and marula oil, the baobab oil: marula oil (mass ratio) is preferably 1: 0.1 to 1:10.
＜ミツロウ（Ｅ）＞
本発明の固形化粧料組成物は、任意で、ミツロウ（Ｅ）を１〜５０質量％含むことが好ましく、１５〜３５質量％含むことがより好ましい。
本発明の固形化粧料組成物は、任意で、ミツロウ（Ｅ）を上記の量含むことによって、剤の形状安定性が増すことから好ましい。
<Beeswax (E)>
The solid cosmetic composition of the present invention optionally contains 1 to 50% by mass of beeswax (E), and more preferably 15 to 35% by mass.
The solid cosmetic composition of the present invention is preferable because it optionally contains the above-mentioned amount of beeswax (E) because the shape stability of the agent is increased.
＜その他成分＞
本発明の固形化粧料組成物は、本発明の効果を損なわない範囲で、上記成分以外に、香料、色素（黄色、緑、茶色、青、オレンジ等）、エッセンシャルオイル、エキス、ラノリン、増粘剤、保湿剤、生薬類、ｐＨ調整剤、防腐剤、酸化防止剤、および等の添加剤を含有することができる。
<Other ingredients>
The solid cosmetic composition of the present invention, in the range that does not impair the effects of the present invention, in addition to the above components, fragrances, pigments (yellow, green, brown, blue, orange, etc.), essential oils, extracts, lanolin, thickeners. , Humectants, crude drugs, pH adjustors, preservatives, antioxidants, and the like can be added.
また、シアバター（Ａ）、ココアバター（Ｂ）と共に、マンゴバター、ムルムルバター、クパスバター、コクムバター、アボカドバターから選ばれる少なくとも１種を組み合わせて用いてもよい。 In addition, shea butter (A) and cocoa butter (B) may be used in combination with at least one selected from mango butter, murumuru butter, cupas butter, cok butter, and avocado butter.
香料として、具体的には、リナロール、リモネン、β-カリオフィレン、シス-3-ヘキセノール、ファルネソール、β-フェニルエチルアルコール、2,6-ノナジエナール、シトラール、α-ヘキシルシンナミックアルデヒド、β-イオノン、ι-カルボン、シクロペンタデカノン、リナリルアセテート、ベンジルベンゾエート、γ-ウンデカラクトン、オイゲノール、ローズオキサイド、インドール、フェニルアセトアルデヒドジメチルアセタール、オーランチオールが挙げられる。エッセンシャルオイルとして具体的には、ローズマリー、オレンジ、スウィートオレンジ、グレープフルーツ、ゆず、ベルガモット、ローズ、ラベンダー、シナモン、ユーカリ、サンダルウッド、ライム、レモン、レモングラス、フランキンセンス、ティーツリー、ムスク、セージ、コーヒー、イランイラン、カモミール、ゼラニウム、バニラ、ネロリが挙げられ、ローズ、ゆず、ラベンダー、オレンジ、ゼラニウム、ローズマリー、ベルガモットが好ましい。エキスとして、具体的には、アロエエキス、アロエベラ葉エキス、ハトムギ種子エキス、チャ葉エキス、コメヌカエキス、カモミール花エキス、ハマメリスエキス、ユキノシタエキス、ヒナギク花エキス、オリーブ葉エキス、カミツレエキス、アスナロエキス、シャクヤク根エキス、ユズ果実エキス、ダイズ種子エキス、ブドウ種子エキス、セージ葉エキス、ローズマリー葉エキス、ラベンダー花エキス、モモ種子エキス、ダイズ種子エキスが挙げられる。 As the fragrance, specifically, linalool, limonene, β-caryophyllene, cis-3-hexenol, farnesol, β-phenylethyl alcohol, 2,6-nonadienal, citral, α-hexylcinnamic aldehyde, β-ionone, ι -Carvone, cyclopentadecanone, linalyl acetate, benzyl benzoate, γ-undecalactone, eugenol, rose oxide, indole, phenylacetaldehyde dimethyl acetal and auranthiol. Specifically as essential oils, rosemary, orange, sweet orange, grapefruit, yuzu, bergamot, rose, lavender, cinnamon, eucalyptus, sandalwood, lime, lemon, lemongrass, frankincense, tea tree, musk, sage, coffee, Ylang-ylang, chamomile, geranium, vanilla, and neroli are mentioned, and rose, yuzu, lavender, orange, geranium, rosemary, and bergamot are preferable. As the extract, specifically, aloe extract, aloe vera leaf extract, coix seed extract, tea leaf extract, rice bran extract, chamomile flower extract, hamamelis extract, yukinoshita extract, daisy flower extract, olive leaf extract, chamomile extract, asunaro extract, peony extract. Examples include root extract, yuzu fruit extract, soybean seed extract, grape seed extract, sage leaf extract, rosemary leaf extract, lavender flower extract, peach seed extract, and soybean seed extract.
本発明の固形化粧料組成物は、水を実質的に含まないことが好ましい。水を実質的に含まないとは、各成分の不純物として存在する水や、本発明の固形化粧料組成物を製造する際に大気中から混入する水については、固形化粧料組成物に含まれていてもよいが、通常水を意図的に添加しないことを意味する。水を実質的に含まないとは、具体的には本発明の固形化粧料組成物中の水の含有量が、通常は０〜７質量％、好ましくは０〜５質量％であることを意味する。 The solid cosmetic composition of the present invention preferably contains substantially no water. Water that is substantially free of water includes water present as impurities of each component, and water mixed from the atmosphere when producing the solid cosmetic composition of the present invention, which is included in the solid cosmetic composition. However, it usually means that water is not intentionally added. To be substantially free of water means that the content of water in the solid cosmetic composition of the present invention is usually 0 to 7% by mass, preferably 0 to 5% by mass. To do.
＜固形化粧料組成物の製造方法＞
本発明の固形化粧料組成物は、例えば、以下の工程（１）〜（３）を含む製造方法により製造することができる。
工程（１）：シアバター（Ａ）およびココアバター（Ｂ）を溶解し、溶解液aを得る工程。
工程（２）：工程（１）で得られた溶解液aと、アビシニアンオイル、メドウフォームオイル、および抗酸化剤から選ばれる少なくとも１種の成分（Ｃ）と、植物性液状油（Ｄ）とを混合し、混合液bを得る工程。
工程（３）：工程（２）で得られた混合液bを冷却する冷却工程。
<Method for producing solid cosmetic composition>
The solid cosmetic composition of the present invention can be produced, for example, by a production method including the following steps (1) to (3).
Step (1): A step of dissolving shea butter (A) and cocoa butter (B) to obtain a solution a.
Step (2): The solution a obtained in Step (1), at least one component (C) selected from abyssinian oil, meadowfoam oil, and antioxidant, and a vegetable liquid oil (D) And a step of obtaining a mixed solution b.
Step (3): A cooling step of cooling the mixed liquid b obtained in the step (2).
前記工程（３）が、冷却開始から２時間以内に、混合液ｂの中心温度が１０℃以下に到達する冷却工程であることが、各成分が均一に分散した固形化粧料組成物を得る観点から好ましい。また、得られる固形化粧料組成物が、ボソボソとした感触になるのを防ぐ観点からも２時間以内に、混合液ｂの中心温度が１０℃以下に到達することが好ましい。 From the viewpoint of obtaining a solid cosmetic composition in which each component is uniformly dispersed, the step (3) is a cooling step in which the central temperature of the mixed liquid b reaches 10 ° C. or lower within 2 hours from the start of cooling. Is preferred. Further, it is preferable that the central temperature of the mixed solution b reaches 10 ° C. or lower within 2 hours from the viewpoint of preventing the obtained solid cosmetic composition from having a rough feel.
固形化粧料組成物の製造方法において、公知の方法で、各成分を溶解および混合することができる。シアバター（Ａ）およびココアバター（Ｂ）の溶解は、各成分を均一に混合するために、好ましくは加熱条件下、例えば６５〜８５℃の加熱条件下で行うことが好ましい。 In the method for producing a solid cosmetic composition, each component can be dissolved and mixed by a known method. The dissolution of shea butter (A) and cocoa butter (B) is preferably carried out under heating conditions, for example, under heating conditions of 65 to 85 ° C., in order to uniformly mix the respective components.
固形化粧料組成物の製造方法において、成形する工程は、（３）の工程の前または後に行うことができる。成形する工程を（３）の前に行う場合は、混合液ｂを缶やビン、そのほか任意の容器に充填し、容器のまま冷却工程を経て製品としてもよい。成形する工程を（３）の後に行う場合は、冷却工程を経たのち、得られたものを棒状に成形してスティックタイプの製品としてもよい。 In the method for producing a solid cosmetic composition, the molding step can be performed before or after the step (3). When the molding step is performed before (3), the mixed liquid b may be filled in a can, a bottle, or any other container, and the container may be cooled as it is to be a product. When the molding step is performed after (3), the obtained product may be molded into a stick shape after a cooling step to obtain a stick type product.
＜用途＞
本発明の固形化粧料組成物は、肌（特に顔、手、足）、爪など、全身に用いることができ、肌に塗布してもべたつかず、酸化安定性の高い固形化粧料である。
<Use>
INDUSTRIAL APPLICABILITY The solid cosmetic composition of the present invention is a solid cosmetic that can be used on the whole body such as the skin (particularly face, hands, feet) and nails, does not become sticky when applied to the skin, and has high oxidation stability.
次に本発明について実施例を示してさらに詳細に説明するが、本発明はこれらによって限定されるものではない。
〔実施例１〜５〕
表１に示す処方で各成分を混合することにより固形化粧料を製造し、以下の方法で評価した。なお、表中の処方の数値は、固形化粧料を１００質量％とした場合の、各成分の質量％を表している。結果を表１に示す。
なお、表１に記載の各成分は以下の市販品を用いた。
＜シアバター（Ａ）＞
シアバター：Ｓｈｅａ Ｂｕｔｔｅｒ ＲＦＯ（株式会社ＣＥＬＭＹＯＮ社製）
＜ココアバター（Ｂ）＞
ココアバター：ＣＯＣＯＡ ＢＵＴＴＥＲ ＲＦ（株式会社ＣＥＬＭＹＯＮ社製）
＜（Ｃ）＞
アビシニアンオイル：ＡＢＹＳＳＩＮＩＡＮ ＴＥＲＡＬ（株式会社ＣＥＬＭＹＯＮ社製）
メドウフォームオイル：ＭＥＡＤＯＷＦＯＡＭ ＴＥＲＡＬ（株式会社ＣＥＬＭＹＯＮ社製）
トコフェロール：ＶＩＴＡＭＩＮ Ｅ（ＸＩＡＮ ＬＹＰＨＡＲ ＢＩＯＴＥＣＨ社製）
＜植物性液状油（Ｄ）＞
バオバブオイル：ＢＡＯＢＡＢ ＴＥＲＡＬ（株式会社ＣＥＬＭＹＯＮ社製）
マルラオイル：ＭＡＲＵＬＡ ＴＥＲＡＬ（株式会社ＣＥＬＭＹＯＮ社製）
＜ミツロウ（Ｅ）＞
ミツロウ：ＢＺＷＡＸ ３６（株式会社ＣＥＬＭＹＯＮ社製）
＜その他＞
エッセンシャルオイル：Ｅｓｓｅｎｔｉａｌ Ｏｉｌ ＣＭ（株式会社ＣＥＬＭＹＯＮ社製）
アロエエキス：アロエベラエキス（Ｎａｔｕｒａｌ Ｃｏｓｍｅｔｉｃ Ｌａｂ社製）
ラノリン：ＬＡＮＯＬＩＮ ＵＳＰ（ＸＩＡＮ ＬＹＰＨＡＲ ＢＩＯＴＥＣＨ社製）
Next, the present invention will be described in more detail with reference to examples, but the present invention is not limited thereto.
[Examples 1 to 5]
Solid cosmetics were produced by mixing the components in the formulations shown in Table 1 and evaluated by the following methods. In addition, the numerical value of the prescription in the table represents the mass% of each component when the solid cosmetic is 100 mass%. The results are shown in Table 1.
The following commercially available products were used as the components shown in Table 1.
<Shea butter (A)>
Shea Butter: Shea Butter RFO (CELMYON Co., Ltd.)
<Cocoa butter (B)>
Cocoa butter: COCOA BUTTER RF (manufactured by CELMYON Co., Ltd.)
<(C)>
Abyssinian oil: ABYSSINIAN TERRAL (manufactured by CELMYON Co., Ltd.)
Meadow foam oil: MEADOWFOAM TERRAL (manufactured by CELMYON Co., Ltd.)
Tocopherol: VITAMIN E (manufactured by XIAN LYPHER BIOTECH)
<Vegetable liquid oil (D)>
Baobab oil: BAOBAB TERRAL (manufactured by CELMYON Co., Ltd.)
Marula Oil: MARULA TERRAL (CELMYON Co., Ltd.)
<Beeswax (E)>
Beeswax: BZWAX 36 (manufactured by CELMYON Co., Ltd.)
<Other>
Essential oil: Essential Oil CM (manufactured by CELMYON Co., Ltd.)
Aloe extract: Aloe vera extract (Natural Cosmetic Lab)
Lanolin: LANOLIN USP (manufactured by XIAN LYPHAR BIOTECH)
〔実施例１の製造〕
耐熱容器にシアバターおよびココアバターを全量入れ、約７０℃に加温し、シアバターおよびココアバターを融解させた。そこに、バオバブオイル、マルラオイル、アビシニアンオイル、メドウフォームオイル、エッセンシャルオイルを加え、混合した。混合したものを、成形容器に充填し、中心温度が２時間以内に１０℃以下になるよう冷蔵庫で冷却した。冷却後、適当な大きさに切断し、製品とした。
製品を肌に塗布し、使い心地を評価した。また、製品を市販の食品保存用容器に入れ、室温で８か月保管し、品質の変化を観察した。
[Production of Example 1]
All the shea butter and cocoa butter were put in a heat-resistant container and heated to about 70 ° C. to melt the shea butter and cocoa butter. Baobab oil, marula oil, abyssinian oil, meadowfoam oil, and essential oil were added thereto and mixed. The mixture was filled in a molding container and cooled in a refrigerator so that the central temperature was 10 ° C or lower within 2 hours. After cooling, the product was cut into an appropriate size.
The product was applied to the skin and the usability was evaluated. Further, the product was put in a commercially available food storage container and stored at room temperature for 8 months, and changes in quality were observed.
〔実施例２の製造〕
各成分の配合量を表１に記載の量に変更し、耐熱容器にシアバター、ココアバターおよびミツロウを全量入れ、約７０℃に加温した以外は、実施例１と同様に製造し、評価した。
[Production of Example 2]
Production was carried out in the same manner as in Example 1 except that the amounts of the respective components were changed to the amounts shown in Table 1, and all the shea butter, cocoa butter and beeswax were placed in a heat resistant container and heated to about 70 ° C., and evaluated. did.
〔実施例３〜５の製造〕
各成分の配合量を表１に記載の量に変更した以外は、実施例１と同様に製造し、評価した。なお、実施例１で配合されていない成分については、バオバブオイル、マルラオイル、アビシニアンオイル、メドウフォームオイル、エッセンシャルオイルと同時に添加した。
[Production of Examples 3 to 5]
Except that the blending amount of each component was changed to the amounts shown in Table 1, the same production and evaluation as in Example 1 were carried out. In addition, about the component which is not mix | blended in Example 1, it added at the same time as baobab oil, marula oil, abyssinian oil, meadow foam oil, and essential oil.
〔考察〕
実施例１〜５で製造した固形化粧料組成物は、肌に塗布してもべたつかず、保湿効果が高かった。また、実施例１〜５で製造した固形化粧料組成物は、室温で８か月以上保存した後において、脂質酸化による劣化臭の発生や変色が無く、物性も半固形〜固形を維持しており、酸化安定性の高い固形化粧料であった。
[Discussion]
The solid cosmetic compositions produced in Examples 1 to 5 were not sticky when applied to the skin and had a high moisturizing effect. In addition, the solid cosmetic compositions produced in Examples 1 to 5 have no deterioration odor or discoloration due to lipid oxidation after being stored at room temperature for 8 months or more, and maintain physical properties of semi-solid to solid. And was a solid cosmetic having high oxidation stability.
Claims (7)
ココアバター（Ｂ）を１５〜８０質量％と、
アビシニアンオイル、メドウフォームオイル、および抗酸化剤から選ばれる少なくとも１種の成分（Ｃ）を０．１〜１０質量％と、
植物性液状油（Ｄ）（但し、アビシニアンオイルおよびメドウフォームオイルを除く）を０．１〜２０質量％
とを含む、固形化粧料組成物。 15 to 80% by mass of shea butter (A),
Cocoa butter (B) is 15 to 80% by mass,
0.1 to 10% by mass of at least one component (C) selected from abyssinian oil, meadowfoam oil, and antioxidant,
0.1-20% by mass of vegetable liquid oil (D) (excluding abyssinian oil and meadow foam oil)
A solid cosmetic composition comprising:
工程（１）：シアバター（Ａ）およびココアバター（Ｂ）を溶解し、溶解液aを得る工程、
工程（２）：工程（１）で得られた溶解液aと、
アビシニアンオイル、メドウフォームオイル、および抗酸化剤から選ばれる少なくとも１種の成分（Ｃ）と、
植物性液状油（Ｄ）とを混合し、混合液bを得る工程
工程（３）：工程（２）で得られた混合液bを冷却する冷却工程
とを含む、固形化粧料組成物の製造方法。 A method for producing the solid cosmetic composition according to any one of claims 1 to 5,
Step (1): Dissolving shea butter (A) and cocoa butter (B) to obtain a solution a,
Step (2): the solution a obtained in step (1),
At least one component (C) selected from abyssinian oil, meadowfoam oil, and antioxidant,
Process for mixing liquid vegetable oil (D) to obtain mixed liquid b Process (3): Production of solid cosmetic composition, comprising cooling process for cooling mixed liquid b obtained in process (2) Method.
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20040131565A1 (en) * | 2002-10-29 | 2004-07-08 | Lee Letica | Lipstick composition containing essential oils |
| JP2008247882A (en) * | 2007-03-29 | 2008-10-16 | Velveteen Bunni Llc | Cosmetic and dermatological formulation with natural pigment and method of use |
| US20080279902A1 (en) * | 2007-05-09 | 2008-11-13 | Henry Steven Luria | Delivery System And Method To Deliver Homeopathic Complexes Comprising Homeopathic Colored Pigment Products For Cosmetic Use |
-
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20040131565A1 (en) * | 2002-10-29 | 2004-07-08 | Lee Letica | Lipstick composition containing essential oils |
| JP2008247882A (en) * | 2007-03-29 | 2008-10-16 | Velveteen Bunni Llc | Cosmetic and dermatological formulation with natural pigment and method of use |
| US20080279902A1 (en) * | 2007-05-09 | 2008-11-13 | Henry Steven Luria | Delivery System And Method To Deliver Homeopathic Complexes Comprising Homeopathic Colored Pigment Products For Cosmetic Use |
Non-Patent Citations (3)
| Title |
|---|
| BEAUTY KITCHEN, UK: "Night Halo Potent Sleep Mask", MINTEL GNPD [ONLINE], JPN6022049931, March 2017 (2017-03-01), ISSN: 0005050983 * |
| BORLIND, GERMANY: "Ultimate Matte Long Lasting Lipstick", MINTEL GNPD [ONLINE], JPN6022049930, July 2018 (2018-07-01), ISSN: 0005050982 * |
| SARAH CHAPMAN, UK: "Lip Enhancer Power Base & Tint Balm", MINTEL GNPD [ONLINE], JPN6023018017, June 2016 (2016-06-01), ISSN: 0005050981 * |
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