JP2018502331A - 完全な全固体エレクトロクロミックスタックのための高速熱処理方法 - Google Patents
完全な全固体エレクトロクロミックスタックのための高速熱処理方法 Download PDFInfo
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- G02F1/15—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour based on an electrochromic effect
- G02F1/1514—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour based on an electrochromic effect characterised by the electrochromic material, e.g. by the electrodeposited material
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- C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
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- C03B25/025—Glass sheets
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- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
- C03C17/3411—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions with at least two coatings of inorganic materials
- C03C17/3417—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions with at least two coatings of inorganic materials all coatings being oxide coatings
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- G—PHYSICS
- G02—OPTICS
- G02F—OPTICAL DEVICES OR ARRANGEMENTS FOR THE CONTROL OF LIGHT BY MODIFICATION OF THE OPTICAL PROPERTIES OF THE MEDIA OF THE ELEMENTS INVOLVED THEREIN; NON-LINEAR OPTICS; FREQUENCY-CHANGING OF LIGHT; OPTICAL LOGIC ELEMENTS; OPTICAL ANALOGUE/DIGITAL CONVERTERS
- G02F1/00—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics
- G02F1/01—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour
- G02F1/15—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour based on an electrochromic effect
- G02F1/1514—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour based on an electrochromic effect characterised by the electrochromic material, e.g. by the electrodeposited material
- G02F1/1523—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour based on an electrochromic effect characterised by the electrochromic material, e.g. by the electrodeposited material comprising inorganic material
- G02F1/1524—Transition metal compounds
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- G—PHYSICS
- G02—OPTICS
- G02F—OPTICAL DEVICES OR ARRANGEMENTS FOR THE CONTROL OF LIGHT BY MODIFICATION OF THE OPTICAL PROPERTIES OF THE MEDIA OF THE ELEMENTS INVOLVED THEREIN; NON-LINEAR OPTICS; FREQUENCY-CHANGING OF LIGHT; OPTICAL LOGIC ELEMENTS; OPTICAL ANALOGUE/DIGITAL CONVERTERS
- G02F1/00—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics
- G02F1/01—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour
- G02F1/15—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour based on an electrochromic effect
- G02F1/153—Constructional details
- G02F1/155—Electrodes
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2217/00—Coatings on glass
- C03C2217/20—Materials for coating a single layer on glass
- C03C2217/21—Oxides
- C03C2217/219—CrOx, MoOx, WOx
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2217/00—Coatings on glass
- C03C2217/20—Materials for coating a single layer on glass
- C03C2217/21—Oxides
- C03C2217/228—Other specific oxides
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2217/00—Coatings on glass
- C03C2217/20—Materials for coating a single layer on glass
- C03C2217/21—Oxides
- C03C2217/23—Mixtures
- C03C2217/231—In2O3/SnO2
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2217/00—Coatings on glass
- C03C2217/90—Other aspects of coatings
- C03C2217/94—Transparent conductive oxide layers [TCO] being part of a multilayer coating
- C03C2217/948—Layers comprising indium tin oxide [ITO]
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- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2218/00—Methods for coating glass
- C03C2218/10—Deposition methods
- C03C2218/15—Deposition methods from the vapour phase
- C03C2218/154—Deposition methods from the vapour phase by sputtering
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- C03C2218/30—Aspects of methods for coating glass not covered above
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- G02F—OPTICAL DEVICES OR ARRANGEMENTS FOR THE CONTROL OF LIGHT BY MODIFICATION OF THE OPTICAL PROPERTIES OF THE MEDIA OF THE ELEMENTS INVOLVED THEREIN; NON-LINEAR OPTICS; FREQUENCY-CHANGING OF LIGHT; OPTICAL LOGIC ELEMENTS; OPTICAL ANALOGUE/DIGITAL CONVERTERS
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- G02F1/15—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour based on an electrochromic effect
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Abstract
Description
‐第一の透明導電層;
‐酸化状態に応じて光学的特性(吸光度/反射率)が変化する材料から形成されるエレクトロクロミック層;
‐イオン伝導性でありそして電気絶縁性である固体電解質の層;
‐対向電極;及び
‐第二の透明導電層;
透明導電層のうちのどちらかは、場合によって透明基材と接触している。
(a)ガラスシートの一つの面上に、以下を逐次的に含む完全な全固体エレクトロクロミックスタックを形成すること:
‐ 透明導電性酸化物の第一の層(TCO1);
‐ カソード着色無機エレクトロクロミック材料の層であって、エレクトロクロミック電極と呼ばれる層(EC);
‐ イオン伝導性無機固体電解質の層(CI);
‐ カチオンインターカレーション材料の層であり、対向電極と呼ばれる層(CE);
及び
‐ 透明導電性酸化物の第二の層(TCO2);並びに
(b)少なくとも五つの無機層からなる、この完全なエレクトロクロミックスタックを、500と2000nmの間を含む波長を有する放射線を用いて照射することによって熱処理することであって、前述の放射線は、エレクトロクロミックスタックに面して設置された放射装置から生じ、前述の放射装置と前述の基材との間で相対的な運動が作り出され、それによって、短い期間にわたって、有利には100ミリ秒よりも短い期間にわたって少なくとも300℃に等しい温度にまでエレクトロクロミックスタックを上昇させる。
プロトン全固体エレクトロクロミックスタックのレーザーアニール
基材:Planilux(100mmx100mmx2.1mm)
TCO1:ITO(500nm)
エレクトロクロミック層:IrOx(85nm)
固体電解質:WO3(100nm)/Ta2O5(200nm)
対向電極:HxWO3(400nm)
TCO2:ITO(100nm)
リチウム全固体エレクトロクロミックスタックのレーザーアニール
‐ 基材:Planilux(100mmx100mmx2.2mm)
‐ 反射防止コーティング
‐ TCO1:ITO(350nm)
‐ エレクトロクロミック層:WO3(350nm)
‐ 固体電解質:SiOx(30nm)
‐ 対向電極:NiWOx(250nm)
‐ TCO2:ITO(400nm)
‐ 反射防止コーティング。
レーザー源:レーザーダイオード980nm、CWモード
レーザー出力:約1400W
走行スピード:10m/分
レーザービームは、作用面において、100mmの長さ及び0.1mmの幅のレーザーラインを形成した。
Claims (10)
- 以下の工程を含む、エレクトロクロミックグレージングユニットを製造するための方法:
(a)逐次的に以下を含む完全な全固体エレクトロクロミックスタックを、ガラスシートの一つの面上に形成すること:
‐ 透明導電性酸化物の第一の層(TCO1);
‐ カソード着色無機エレクトロクロミック材料の層であって、エレクトロクロミック電極(EC)と呼ばれる層;
‐ イオン伝導性無機固体電解質の層(CI);
‐ カチオンインターカレーション材料の層であって、対向電極(CE)と呼ばれる層;及び
‐ 透明導電性酸化物の第二の層(TCO2);並びに
(b)500と2000nmの間を含む波長を有する放射線を用いた照射によって前記完全なエレクトロクロミックスタックを熱処理することであって、前記放射線は、前記エレクトロクロミックスタックに対面して設置された放射装置から発生し、前記放射装置と前記基材との間に相対運動が作り出され、それにより前記エレクトロクロミックスタックは、短い持続時間の間、好ましくは100ミリ秒よりも短い持続時間の間、少なくとも300℃と等しい温度に上昇する。 - 完全な全固体エレクトロクロミックスタックを形成する前記工程は、好ましくは、350℃と450℃の間及び特には370℃と410℃の間を含む温度でのアニーリングレア内における最終アニーリング工程を含むことを特徴とする、請求項1に記載の方法。
- 前記透明導電性酸化物層TCO1及びTCO2を形成する前記透明導電性酸化物は、インジウムスズ混合酸化物(ITO)並びにアルミニウムドープ及び/又はガリウムドープされた酸化亜鉛によって形成される群から選ばれる、請求項1又は2に記載の方法。
- 前記エレクトロクロミック電極ECの前記カソード着色無機エレクトロクロミック材料は、酸化タングステン(WOx)である、請求項1〜3のいずれか一項に記載の方法。
- 前記対向電極(CE)の前記カチオンインターカレーション材料は、タングステンニッケル混合酸化物(NiWO)及び酸化イリジウムによって形成される群から選ばれる、請求項1〜4のいずれか一項に記載の方法。
- 前記イオン伝導性無機固体電解質(IC)は、シリカ(SiO2)、酸化タンタル(Ta2O5)及び酸化ニオブ(Nb2O5)によって形成される群から選ばれる、請求項1〜5のいずれか一項に記載の方法。
- 前記第一の面の反対側にある前記基材のその面の温度は、前記熱処理の間に100℃、又はさらには50℃、及び特には30℃を超えない、請求項1〜6のいずれか一項に記載の方法。
- 前記放射装置は、レーザーであり、好ましくは、前記エレクトロクロミックスタックにおいて前記エレクトロクロミックスタックの全幅をカバーするラインを形成するレーザービームを射出するレーザーである、請求項1〜7のいずれか一項に記載の方法。
- 前記放射装置は、フラッシュランプである、請求項1〜7のいずれか一項に記載の方法。
- 前記エレクトロクロミックスタックのすべての前記薄い層は、マグネトロンスパッタリングによって堆積される、請求項1〜9のいずれか一項に記載の方法。
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Application Number | Priority Date | Filing Date | Title |
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FR1463473A FR3031197B1 (fr) | 2014-12-31 | 2014-12-31 | Procede de traitement thermique rapide d'un empilement electrochrome tout solide complet |
FR1463473 | 2014-12-31 | ||
PCT/FR2015/053382 WO2016108000A1 (fr) | 2014-12-31 | 2015-12-08 | Procédé de traitement thermique rapide d'un empilement électrochrome tout solide complet |
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EP (1) | EP3241068B1 (ja) |
JP (1) | JP6741669B2 (ja) |
CN (2) | CN107111198A (ja) |
DK (1) | DK3241068T3 (ja) |
ES (1) | ES2702994T3 (ja) |
FR (1) | FR3031197B1 (ja) |
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US20190041550A1 (en) * | 2017-08-04 | 2019-02-07 | Vitro Flat Glass Llc | Flash Annealing of Transparent Conductive Oxide and Semiconductor Coatings |
FR3088850B1 (fr) * | 2018-11-28 | 2020-12-11 | Saint Gobain | Procede de fabrication d’un vitrage electrochrome |
FR3105212A1 (fr) * | 2019-12-20 | 2021-06-25 | Saint-Gobain Glass France | Procédé de traitement thermique rapide de couches minces sur substrats en verre trempé |
FR3105459B1 (fr) * | 2019-12-20 | 2023-06-23 | Saint Gobain | Trempe thermique d’une electrode travail |
CN111338149B (zh) * | 2020-03-24 | 2023-07-28 | 江苏繁华应材科技股份有限公司 | 一种含氮电致变色器件及其制备方法 |
CN113376917A (zh) * | 2021-06-04 | 2021-09-10 | 中国航发北京航空材料研究院 | 一种电致变色器件及其工作电极的制备方法 |
CN115291451A (zh) * | 2022-08-26 | 2022-11-04 | 浙江景昇薄膜科技有限公司 | 一种实现对比度调节功能的透明显示器组件及其制备方法 |
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JP2006235632A (ja) * | 2005-02-23 | 2006-09-07 | Sage Electrochromics Inc | エレクトロクロミックデバイスおよびその製造方法 |
JP2007108750A (ja) * | 2005-10-11 | 2007-04-26 | Sage Electrochromics Inc | 改善されたイオン伝導体層を有するエレクトロクロミック素子 |
US20070128905A1 (en) * | 2003-06-12 | 2007-06-07 | Stuart Speakman | Transparent conducting structures and methods of production thereof |
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JP2011187336A (ja) * | 2010-03-09 | 2011-09-22 | Sumitomo Chemical Co Ltd | 透明導電膜の改質方法及び透明導電膜付基板の製造方法 |
FR2989388A1 (fr) * | 2012-04-17 | 2013-10-18 | Saint-Gobain Glass France | Procede d'obtention d'un substrat muni d'un revetement |
WO2014132000A1 (fr) * | 2013-03-01 | 2014-09-04 | Saint-Gobain Glass France | Procede de traitement thermique d'un revêtement |
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CN203838454U (zh) * | 2014-04-10 | 2014-09-17 | 吉林大学 | WO3-Ta2O5-NiO固态复合电致变色玻璃器件 |
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Publication number | Publication date |
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JP6741669B2 (ja) | 2020-08-19 |
EP3241068B1 (fr) | 2018-09-26 |
CN115903321A (zh) | 2023-04-04 |
US20180004058A1 (en) | 2018-01-04 |
ES2702994T3 (es) | 2019-03-06 |
DK3241068T3 (en) | 2019-01-21 |
WO2016108000A1 (fr) | 2016-07-07 |
PL3241068T3 (pl) | 2019-02-28 |
FR3031197B1 (fr) | 2017-06-16 |
FR3031197A1 (fr) | 2016-07-01 |
EP3241068A1 (fr) | 2017-11-08 |
US10739656B2 (en) | 2020-08-11 |
CN107111198A (zh) | 2017-08-29 |
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