JP2014074655A - Tensile strength testing method of filament-reinforced metal matrix composite material and tensile test piece - Google Patents

Tensile strength testing method of filament-reinforced metal matrix composite material and tensile test piece Download PDF

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JP2014074655A
JP2014074655A JP2012222249A JP2012222249A JP2014074655A JP 2014074655 A JP2014074655 A JP 2014074655A JP 2012222249 A JP2012222249 A JP 2012222249A JP 2012222249 A JP2012222249 A JP 2012222249A JP 2014074655 A JP2014074655 A JP 2014074655A
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long fiber
strength
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tensile strength
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JP5893542B2 (en
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Hirotaka Kamijiyou
弘貴 上條
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Railway Technical Research Institute
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Abstract

PROBLEM TO BE SOLVED: To provide a tensile strength testing method of a filament-reinforced metal matrix composite material capable of stably and precisely performing a tensile strength test.SOLUTION: The tensile strength testing method is a method to test on a filament-reinforced metal matrix composite material in the longitudinal direction, in which plural high strength continuous filaments (12) are disposed adjacent to the central axis thereof along a longitudinal direction of a rod-like matrix metal (11). The rod-like matrix metal (11) has a parallel portion (13) where a part in the longitudinal direction is reduced in thickness and a pair of grip portions (14) formed at both outer end portions interposed by the parallel portion (13) therebetween. After gripping the grip portions (14) with chucks of the test machine, the parallel portion (13) is pulled by separating the chucks away from each other. The high strength continuous filaments (12) are extended from both outer ends of the grip portions (14) being fixed thereto.

Description

本発明は、長繊維強化複合材料の引張強度試験方法及び引張試験片に関し、特に、棒状体のマトリクス金属の長手方向に沿ってその中心軸近傍に複数本の高強度連続長繊維を配置させた長繊維強化金属基複合材料の該長手方向への引張強度試験方法及び引張試験片に関する。   The present invention relates to a tensile strength test method and a tensile test piece of a long fiber reinforced composite material, and in particular, a plurality of high-strength continuous long fibers are arranged in the vicinity of the central axis along the longitudinal direction of a rod-like matrix metal. The present invention relates to a tensile strength test method in the longitudinal direction of a long fiber reinforced metal matrix composite material and a tensile test piece.

引張強度の測定対象たる被測定部材(若しくは、被測定材料)から作製された引張試験片の両端にある掴み部を引張試験機の一対の対向するチャックにそれぞれ把持させ、このチャックを相対的に離間せしめて測定対象の引張強度を測定する引張強度試験が行われている。かかる測定対象が長繊維を含む複合材料(長繊維強化複合材料)であって、その長繊維の伸びる方向への引張強度を測定する場合、該方向に沿って引張試験片を作製し引張強度試験が行われる。   The gripping portions at both ends of the tensile test piece made from the member to be measured (or the material to be measured) whose tensile strength is to be measured are respectively held by a pair of opposing chucks of the tensile tester, and the chuck is relatively A tensile strength test is performed in which the tensile strength of the object to be measured is measured after being separated. When the object to be measured is a composite material containing long fibers (long fiber reinforced composite material) and the tensile strength in the direction in which the long fibers extend is measured, a tensile test piece is prepared along the direction and a tensile strength test is performed. Is done.

例えば、特許文献1では、建築資材としての鉄筋の代替としてコンクリートに埋設される長繊維強化複合材料であって、複数本の連続するアラミド繊維を束ねてその周面を樹脂で固めた棒状体の長繊維強化複合材料の引張強度試験方法が開示されている。高い引張強度を有するアラミド連続長繊維の耐力に抗し得るように棒状体を圧縮して引張試験機のチャックに把持させようとすると、棒状体が圧縮座屈してチャック滑りを生じたり、長繊維を損傷しチェック切れを起こしたりして、引張強度を測定出来なかった。そこで、棒状体におけるチャックの把持部を樹脂でモールドして耐座屈圧縮強度を上げ、長繊維を損傷させることなく引張試験機のチャックで強力に圧縮把持できるようにしている。   For example, in Patent Document 1, a long-fiber reinforced composite material embedded in concrete as an alternative to a reinforcing bar as a building material, which is a rod-shaped body in which a plurality of continuous aramid fibers are bundled and the peripheral surface thereof is hardened with a resin. A method for testing the tensile strength of long fiber reinforced composite materials is disclosed. When trying to compress the rod-shaped body so that it can resist the proof strength of aramid continuous long fiber with high tensile strength and hold it by the chuck of the tensile tester, the rod-shaped body will be compressed and buckled, causing chuck slip, The tensile strength could not be measured. In view of this, the gripping portion of the chuck in the rod-shaped body is molded with resin to increase the buckling resistance, so that it can be strongly compressed and gripped by the chuck of the tensile tester without damaging the long fibers.

また、特許文献2でも、ガラス繊維の如き高い引張強度を有する連続長繊維の束にエポキシ樹脂の如き熱硬化性樹脂を含浸させた棒状体の長繊維強化複合材料の引張強度試験方法を開示している。ここでは、連続長繊維の束に熱硬化性樹脂を含浸させ、その両端を円筒治具に巻き付けた上で熱硬化性樹脂を硬化させて円筒治具に固定し、該円筒治具同士を相対的に離間せしめて引張強度を測定している。   Patent Document 2 also discloses a tensile strength test method for a long fiber reinforced composite material of a rod-like body in which a bundle of continuous long fibers having high tensile strength such as glass fibers is impregnated with a thermosetting resin such as an epoxy resin. ing. Here, a bundle of continuous long fibers is impregnated with a thermosetting resin, and both ends thereof are wound around a cylindrical jig, and then the thermosetting resin is cured and fixed to the cylindrical jig. The tensile strength is measured by separating them.

ところで、JIS K7162やJIS Z2241の引張強度試験では、棒状体の中央部の断面積を減じて耐力を低下させた応力集中部を与えた引張試験片を用いて、この両端部をチャックで把持し相対的に離間せしめることで、該中央部のみを変形させて引張強度を測定している。かかる試験方法を用いても、長繊維を分散させた棒状体の長繊維強化複合材料の引張強度を測定し得る。また、特許文献1及び2のような、マトリクスとしての樹脂と比較して非常に高い引張強度を有する連続長繊維を分散させた棒状体の長繊維強化複合材料についても、応力集中部である中央部の断面積をより大きく減じて耐力を大きく低下させることで引張強度を測定し得る。   By the way, in the tensile strength test of JIS K7162 and JIS Z2241, the both ends are gripped with a chuck using a tensile test piece provided with a stress concentration part in which the cross-sectional area of the central part of the rod-like body is reduced to reduce the proof stress. By separating them relatively, only the central part is deformed and the tensile strength is measured. Even when such a test method is used, the tensile strength of a long fiber reinforced composite material of a rod-like body in which long fibers are dispersed can be measured. Further, the long fiber reinforced composite material of the rod-like body in which continuous long fibers having a very high tensile strength compared with the resin as a matrix as in Patent Documents 1 and 2 are also used as the stress concentration part. The tensile strength can be measured by greatly reducing the cross-sectional area of the portion and greatly reducing the yield strength.

更に、特許文献3では、複数本を束ねた高分子連続長繊維を円筒形状の金属管体内に挿入してスエージング加工し、丸棒体のマトリクス金属の長手方向に沿ってその中心軸近傍に複数本の連続長繊維を配置させた長繊維強化金属基複合材料の製造方法を開示している。かかる複合材料であっても、棒状体の中央部の断面積を減じることができて、上記したような引張試験片を作製し得る。   Furthermore, in Patent Document 3, polymer continuous long fibers bundled with a plurality of strands are inserted into a cylindrical metal tube and swaged, and in the vicinity of the central axis along the longitudinal direction of the matrix metal of the round bar. A method for producing a long fiber reinforced metal matrix composite in which a plurality of continuous long fibers are arranged is disclosed. Even with such a composite material, the cross-sectional area of the central portion of the rod-shaped body can be reduced, and the tensile test piece as described above can be produced.

特開平04−274730号公報Japanese Patent Laid-Open No. 04-274730 特開平11−183340号公報JP-A-11-183340 特開2008−235259号公報JP 2008-235259 A

特許文献3の長繊維強化金属基複合材料では、棒状体の中心軸近傍に高い引張強度を有する連続長繊維が集中して配置されているため、棒状体の外周から断面積を減じても当該部分の耐力の低下は小さく、この両側にある把持部をチャックで把持し相対的に離間せしめても、当該部分のみを変形させることができない。また、棒状体を外周から把持する場合、チャックとマトリクス金属を固定出来たとしても、マトリクス金属と連続長繊維とが連続長繊維の破断前に滑りを生じて、いわゆる「繊維抜け」を生じてしまうこともある。すなわち、安定して精度よく引張強度を測定できないのである。   In the long fiber reinforced metal matrix composite material of Patent Document 3, continuous long fibers having high tensile strength are concentrated and arranged in the vicinity of the central axis of the rod-shaped body, so that even if the cross-sectional area is reduced from the outer periphery of the rod-shaped body, The decrease in the yield strength of the part is small, and even if the gripping parts on both sides are gripped by the chuck and are relatively separated from each other, only the part cannot be deformed. In addition, when gripping the rod-shaped body from the outer periphery, even if the chuck and the matrix metal can be fixed, the matrix metal and the continuous long fiber slip before the continuous long fiber breaks, so-called “fiber loss” occurs. Sometimes it ends up. That is, the tensile strength cannot be measured stably and accurately.

本発明は、かかる事情に鑑みてなされたものであって、その目的とするところは、安定して精度よく引張強度を測定することのできる長繊維強化金属基複合材料の引張強度試験方法及び引張試験片を提供することにある。   The present invention has been made in view of such circumstances, and an object of the present invention is to provide a tensile strength test method and tensile strength of a long fiber reinforced metal matrix composite that can stably and accurately measure tensile strength. It is to provide a test piece.

本発明による長繊維強化金属基複合材料の引張強度試験方法は、棒状体のマトリクス金属の長手方向に沿ってその中心軸近傍に複数本の高強度連続長繊維を配置させた長繊維強化金属基複合材料の該長手方向への引張強度試験方法であって、前記長手方向の一部に太さを減じた平行部を与えるとともに前記平行部を挟んだ両外側部に掴み部を設け、試験機のチャックに前記掴み部を把持させるとともに前記チャックを離間させて前記平行部を引っ張る試験方法において、前記高強度連続長繊維を前記掴み部のさらに両外側部に延長させてこれを前記掴み部に固着させることを特徴とする。   The tensile strength test method for long fiber reinforced metal matrix composites according to the present invention is a long fiber reinforced metal matrix in which a plurality of high strength continuous long fibers are arranged in the vicinity of the central axis along the longitudinal direction of the matrix metal of the rod-shaped body. A method for testing the tensile strength of a composite material in the longitudinal direction, in which a parallel portion with a reduced thickness is provided in a part of the longitudinal direction, and gripping portions are provided on both outer side portions sandwiching the parallel portion. In the test method in which the grip portion is gripped by the chuck and the parallel portion is pulled by separating the chuck, the high-strength continuous long fiber is further extended to both outer portions of the grip portion, and this is applied to the grip portion. It is made to adhere.

かかる発明によれば、高強度連続長繊維の端部をチャックに把持される掴み部に固着させて、チャックの移動によって高強度連続長繊維とマトリクス金属とが相対的に滑ることを抑制し、長繊維強化金属基複合材料について安定して精度よく引張強度試験を行うことができるのである。   According to such an invention, the end portion of the high-strength continuous long fiber is fixed to the grip portion gripped by the chuck, and the high-strength continuous long fiber and the matrix metal are prevented from relatively sliding due to the movement of the chuck, It is possible to perform a tensile strength test stably and accurately for a long fiber reinforced metal matrix composite.

上記した発明において、前記掴み部のさらに外側部には前記棒状体の太さを減じるよう前記マトリクス金属を切削した延長部を与えられていることを特徴としてもよい。かかる発明によれば、平行部に対して掴み部及び外側部において高強度連続長繊維とマトリクス金属との接触面積を相対的に増加させて、高強度連続長繊維の端部をチャックに把持される掴み部に固着させて、チャックの移動によって高強度連続長繊維とマトリクス金属とが相対的に滑ることを抑制し、長繊維強化金属基複合材料について安定して精度よく引張強度試験を行うことができる。   In the above-described invention, an extension portion obtained by cutting the matrix metal may be provided on the outer side portion of the grip portion so as to reduce the thickness of the rod-shaped body. According to this invention, the contact area between the high-strength continuous long fibers and the matrix metal is relatively increased in the grip portion and the outer portion with respect to the parallel portion, and the end portion of the high-strength continuous long fibers is gripped by the chuck. The high strength continuous long fiber and the matrix metal are prevented from slipping relatively by the movement of the chuck, and the tensile strength test is performed stably and accurately on the long fiber reinforced metal matrix composite. Can do.

上記した発明において、前記延長部からさらに外側部に前記高強度連続長繊維を貫通させこれを前記延長部の端部に固定する係止片を与えることを特徴としてもよい。かかる発明によれば、係止片により高強度連続長繊維をさらに延長部の端部に固定し、高強度連続長繊維の端部をチャックに把持される掴み部にさらに確実に固着させて、チャックの移動によって高強度連続長繊維とマトリクス金属とが相対的に滑ることを抑制し、長繊維強化金属基複合材料について安定して精度よく引張強度試験を行うことができる。   In the above-described invention, the high-strength continuous long fiber may be penetrated from the extension portion to the outer side portion, and a locking piece for fixing the high-strength continuous long fiber to the end portion of the extension portion may be provided. According to such an invention, the high-strength continuous long fiber is further fixed to the end of the extension portion by the locking piece, and the end of the high-strength continuous long fiber is more securely fixed to the grip portion gripped by the chuck, It is possible to suppress the relative slip of the high-strength continuous long fibers and the matrix metal due to the movement of the chuck, and to perform the tensile strength test stably and accurately for the long fiber reinforced metal matrix composite material.

上記した発明において、前記掴み部からさらに外側部に前記高強度連続長繊維を貫通させこれを前記掴み部の端部に固定する係止片を与えることを特徴としてもよい。かかる発明によれば、係止片により高強度連続長繊維を掴み部の端部に固定し、高強度連続長繊維の端部をチャックに把持される掴み部にさらに確実に固着させて、チャックの移動によって高強度連続長繊維とマトリクス金属とが相対的に滑ることを抑制し、長繊維強化金属基複合材料について安定して精度よく引張強度試験を行うことができる。   In the above-mentioned invention, the high-strength continuous long fiber may be further penetrated from the grip portion to the outer side portion, and a locking piece for fixing the high-strength continuous long fiber to the end portion of the grip portion may be provided. According to this invention, the high-strength continuous long fiber is fixed to the end of the grip portion by the locking piece, and the end of the high-strength continuous long fiber is more securely fixed to the grip portion gripped by the chuck. It is possible to suppress the relative slip of the high-strength continuous long fibers and the matrix metal by the movement of the long-strength, and to perform the tensile strength test stably and accurately with respect to the long-fiber reinforced metal matrix composite material.

上記した発明において、前記掴み部から貫通した前記高強度連続長繊維を折り返した上で前記係止片を与えることを特徴としてもよい。かかる発明によれば、高強度連続長繊維の掴み部の端部への固定をより確実にし、高強度連続長繊維の端部をチャックに把持される掴み部にさらに確実に固着させて、チャックの移動によって高強度連続長繊維とマトリクス金属とが相対的に滑ることを抑制し、長繊維強化金属基複合材料について安定して精度よく引張強度試験を行うことができる。   In the above-described invention, the high-strength continuous long fiber penetrating from the grip portion may be folded back to give the locking piece. According to this invention, the high-strength continuous long fiber is more securely fixed to the end of the grip portion, and the end of the high-strength continuous long fiber is more securely fixed to the grip portion gripped by the chuck. It is possible to suppress the relative slip of the high-strength continuous long fibers and the matrix metal by the movement of the long-strength, and to perform the tensile strength test stably and accurately for the long-fiber reinforced metal matrix composite.

上記した発明において、前記係止片は前記高強度連続長繊維をかしめるように与えることを特徴としてもよい。かかる発明によれば、高強度連続長繊維を係止片によって強固に固定でき、高強度連続長繊維の端部をチャックに把持される掴み部にさらに確実に固着させて、チャックの移動によって高強度連続長繊維とマトリクス金属とが相対的に滑ることを抑制し、長繊維強化金属基複合材料について安定して精度よく引張強度試験を行うことができる。   In the above-described invention, the locking piece may be provided so as to caulk the high-strength continuous long fibers. According to this invention, the high-strength continuous long fiber can be firmly fixed by the locking piece, and the end of the high-strength continuous long fiber can be more firmly fixed to the grip portion gripped by the chuck, and the high-strength continuous long fiber can be increased by moving the chuck. It is possible to suppress the relative slip of the continuous long fiber and the matrix metal, and to perform the tensile strength test stably and accurately for the long fiber reinforced metal matrix composite.

また、本発明による長繊維強化金属基複合材料の引張試験片は、上記した引張強度試験方法に用いられるものであることを特徴とする。   Moreover, the tensile test piece of the long fiber reinforced metal matrix composite material according to the present invention is used for the above-described tensile strength test method.

かかる発明によれば、高強度連続長繊維の端部を掴み部に固着させて、引張強度試験において高強度連続長繊維とマトリクス金属とが相対的に滑ることを抑制し、長繊維強化金属基複合材料について安定して精度よく引張強度試験を行うことができる。   According to this invention, the end of the high-strength continuous long fiber is fixed to the grip portion, and the high-strength continuous long fiber and the matrix metal are prevented from relatively sliding in the tensile strength test, and the long-fiber reinforced metal base The tensile strength test can be performed stably and accurately on the composite material.

長繊維強化複合棒材の外観を示す斜視図である。It is a perspective view which shows the external appearance of a long fiber reinforced composite bar. 本発明による方法で用いられる引張試験片の断面図である。It is sectional drawing of the tensile test piece used with the method by this invention. 本発明による引張強度試験の方法を示す図である。It is a figure which shows the method of the tensile strength test by this invention. 本発明による方法で用いられる他の引張試験片の断面図である。It is sectional drawing of the other tensile test piece used with the method by this invention. 本発明による方法で用いられる他の引張試験片の断面図である。It is sectional drawing of the other tensile test piece used with the method by this invention. 本発明による方法で用いられる他の引張試験片の断面図である。It is sectional drawing of the other tensile test piece used with the method by this invention.

本発明による引張強度の測定対象となる長繊維強化金属基複合材料について、図1を用いて説明する。   A long fiber reinforced metal matrix composite material to be measured for tensile strength according to the present invention will be described with reference to FIG.

図1に示すように、長繊維強化金属基複合材料である長繊維強化複合棒材(複合線材)100は、長尺の線状体であり、例えば、鉄道において軌道に沿って空中に吊架支持されて電力を導く電力線などに使用される。長繊維強化複合棒材100は、丸棒形状の線状体であるマトリクス金属11と、かかる線状体の引張強度を高めるために強化材として与えられる高強度連続長繊維12とからなる。特に、電力線として使用される長繊維強化複合棒材100は、マトリクス金属11として、導電性の銅、銅系合金、アルミニウム又はアルミニウム系合金などを用いられるが、他の用途にあっては適宜、異なる金属材料を用い得る。更に、高強度連続長繊維12は、強化材として少なくともマトリクス金属11よりも高い引張強度を有し、例えば、炭素繊維やアラミド繊維などの連続した長尺の高強度繊維である。高強度連続長繊維12の引張強度が高いほど、同じ引張強度を長繊維強化複合棒材100に与えるために挿入される高強度連続長繊維12の量を減じることができ、コストを削減できるとともに、例えば、電力線などに使用される場合にあっては、電力の輸送を担うマトリクス金属11の構成比を高くし得て、より大電流を流し得るようになるのである。   As shown in FIG. 1, a long fiber reinforced composite rod (composite wire) 100, which is a long fiber reinforced metal matrix composite material, is a long linear body, for example, suspended in the air along a track in a railway. Used for power lines that are supported to conduct power. The long fiber reinforced composite rod 100 is composed of a matrix metal 11 which is a round rod-shaped linear body, and high-strength continuous long fibers 12 which are given as a reinforcing material in order to increase the tensile strength of the linear body. In particular, the long fiber reinforced composite rod 100 used as a power line is made of conductive copper, a copper-based alloy, aluminum, an aluminum-based alloy, or the like as the matrix metal 11, but as appropriate for other applications, Different metal materials can be used. Furthermore, the high-strength continuous long fibers 12 have a tensile strength higher than that of the matrix metal 11 as a reinforcing material, and are continuous long high-strength fibers such as carbon fibers and aramid fibers. As the tensile strength of the high-strength continuous long fibers 12 is higher, the amount of the high-strength continuous long fibers 12 inserted to give the same tensile strength to the long-fiber reinforced composite rod 100 can be reduced, and the cost can be reduced. For example, in the case of being used for a power line or the like, the composition ratio of the matrix metal 11 responsible for the transportation of electric power can be increased, and a larger current can flow.

長繊維強化複合棒材100において、高強度連続長繊維12はマトリクス金属11の長手方向に沿って中心軸近傍に集合配置されている。このような長繊維強化複合棒材100は、例えば、高強度連続長繊維12の束を一度、ばらして開繊し、繊維のそれぞれにマトリクス金属11と実質的に同材料からなるメッキを施した上で再度、束ね、これをマトリクス金属11となる金属管の中に挿入した上でスエージング加工をして得られる。かかる方法により、高強度連続長繊維12の集合配置された領域である長繊維集合領域16において、マトリクス金属11と実質的に同材料からなるメッキ金属が高強度連続長繊維12の単繊維同士の間に侵入配置され、マトリクス金属11の長手方向に沿って中心軸近傍に高強度連続長繊維12の一本一本が独立しつつ集合配置されるようになる。   In the long fiber reinforced composite rod 100, the high-strength continuous long fibers 12 are arranged in the vicinity of the central axis along the longitudinal direction of the matrix metal 11. In such a long fiber reinforced composite rod 100, for example, a bundle of high-strength continuous long fibers 12 is separated once and opened, and each of the fibers is plated with substantially the same material as the matrix metal 11. It is obtained by bundling again and inserting it into a metal tube to be the matrix metal 11 and swaging. By this method, in the long fiber assembly region 16, which is a region where the high-strength continuous long fibers 12 are aggregated and arranged, the plating metal made of substantially the same material as the matrix metal 11 is formed between the single fibers of the high-strength continuous long fibers 12. The high-strength continuous long fibers 12 are gathered and arranged independently in the vicinity of the central axis along the longitudinal direction of the matrix metal 11.

[実施例1]
次に、本発明による1つの実施例による引張強度試験方法で使用される引張試験片について図2を用いて説明するとともに、その試験方法を図3を用いて説明する。
[Example 1]
Next, a tensile test piece used in a tensile strength test method according to one embodiment of the present invention will be described with reference to FIG. 2, and the test method will be described with reference to FIG.

図2に示すように、引張試験片10は、長繊維強化複合棒材100(図1参照)を所定の長さに切断し、その長手方向の中央部近傍において、外周からマトリクス金属11の径を減じるように切削加工して与えられる。すなわち、長手方向の中央部において断面円形の平行部13と、平行部13から長手方向両外側へ向けて径を徐々に大きくしたR部13aと、これに連続する掴み部14とからなる。なお、平行部13の切削加工において、マトリクス金属11のみを切削加工し、長繊維集合領域16を切削加工していないため、高強度連続長繊維12が切断されることはない。更に、掴み部14は、その周面に雄ネジ部14aを加工されている。掴み部14の外側には、マトリクス金属11を切削加工し掴み部14から径を減じられた延長部15が加工されている。つまり、引張試験片10は、JIS Z2241に規定される断面を円形とする棒状試験片の掴み部の外側に略円柱形状の延長部15を設けた形状を有する。なお、掴み部14は、使用する引張試験機の試験片取付部に取付け可能な形状であればよく、例えばフランジ形状やくさび形状などの他の形状とし得る。   As shown in FIG. 2, the tensile test piece 10 is obtained by cutting a long fiber reinforced composite rod 100 (see FIG. 1) into a predetermined length, and the diameter of the matrix metal 11 from the outer periphery in the vicinity of the center in the longitudinal direction. It is given by cutting to reduce. That is, it comprises a parallel portion 13 having a circular cross section at the central portion in the longitudinal direction, an R portion 13a having a diameter gradually increased from the parallel portion 13 toward both outer sides in the longitudinal direction, and a gripping portion 14 continuous therewith. In the cutting of the parallel portion 13, only the matrix metal 11 is cut and the long fiber assembly region 16 is not cut, so that the high-strength continuous long fibers 12 are not cut. Further, the gripping part 14 has a male threaded part 14a formed on its peripheral surface. On the outer side of the gripping part 14, an extension part 15 in which the matrix metal 11 is cut and the diameter is reduced from the gripping part 14 is processed. That is, the tensile test piece 10 has a shape in which a substantially cylindrical extension portion 15 is provided outside a grip portion of a rod-like test piece having a circular cross section defined by JIS Z2241. In addition, the grip part 14 should just be a shape which can be attached to the test piece attachment part of the tensile testing machine to be used, for example, can be made into other shapes, such as a flange shape and a wedge shape.

延長部15を有する引張試験片10では、後述する引張試験における応力集中部である平行部13の長繊維集合領域16の長さに対して、掴み部14の前後の長繊維集合領域16の長さを延長部15の分だけ延長している。これにより、掴み部14を長手方向外側に引っ張ったときのマトリクス金属11と高強度連続長繊維12の摩擦力を掴み部14の前後で相対的に増加させ、掴み部14に高強度連続長繊維12を固着させるのである。つまり、延長部15の長さは高強度連続長繊維12の束の強度に応じて決定してもよい。   In the tensile test piece 10 having the extension portion 15, the length of the long fiber assembly region 16 before and after the grip portion 14 with respect to the length of the long fiber assembly region 16 of the parallel portion 13 which is a stress concentration portion in a tensile test described later. The length is extended by the extension 15. As a result, the frictional force between the matrix metal 11 and the high-strength continuous long fibers 12 when the grip portion 14 is pulled outward in the longitudinal direction is relatively increased before and after the grip portion 14, and the high-strength continuous long fibers are applied to the grip portion 14. 12 is fixed. That is, the length of the extension 15 may be determined according to the strength of the bundle of high-strength continuous long fibers 12.

図3に示すように、引張試験機の試験片取付部90は、引張試験片10の掴み部14と螺合する雌ネジ部93aを有するグリップ93と、グリップ93を吊下軸支するチャックフレーム92と、チャックフレーム92に接続されるロッド91との1組をそれぞれ上下に対向させるように配置している。下方のロッド91は固定され、図示しないサーボモータに接続された上方のロッド91が上方に移動することで1組のグリップ93同士が一軸線上で離間移動する。上方のロッド91には適宜、図示しないロードセルが組み込まれる。なお、グリップ93の雌ネジ部93aを袋穴とすると、引張試験片10を螺合させて取り付けたときに空気が抜けづらく、これを防止する目的などで雌ネジ部93aと一軸に貫通穴93bが設けられている。   As shown in FIG. 3, the test piece mounting portion 90 of the tensile tester includes a grip 93 having an internal thread portion 93 a that is screwed with the grip portion 14 of the tensile test piece 10, and a chuck frame that supports the grip 93 in a suspended manner. 92 and a rod 91 connected to the chuck frame 92 are arranged so as to face each other vertically. The lower rod 91 is fixed, and the upper rod 91 connected to a servo motor (not shown) moves upward, so that the pair of grips 93 moves apart on one axis. A load cell (not shown) is appropriately incorporated in the upper rod 91. Note that if the female threaded portion 93a of the grip 93 is a bag hole, it is difficult for air to escape when the tensile test piece 10 is screwed and attached, and for the purpose of preventing this, the through-hole 93b uniaxially with the female threaded portion 93a. Is provided.

引張強度試験は、試験片取付部90に引張試験片10の掴み部14を外周から把持させてこれを取り付けて行われる。引張試験片10は、延長部15をグリップ93に設けられた貫通穴93bに挿入させつつ、雄ネジ部14aを雌ネジ部93aに螺合させる。これにより、引張試験片10の両側の掴み部14をそれぞれ上下のグリップ93に固定させて試験片取付部90に取り付けられる。引張強度試験では、サーボモータにより上方のロッド91を介して上方のグリップ93を上昇させ、引張試験片10に長手方向の引張荷重を負荷させる。なお、上方のロッド91に接続された図示しないロードセルにより、引張試験片10に与えられる引張荷重が計測できる。   The tensile strength test is carried out by attaching the gripping portion 14 of the tensile test piece 10 to the test piece mounting portion 90 from the outer periphery. The tensile test piece 10 screws the male screw portion 14a into the female screw portion 93a while inserting the extension portion 15 into the through hole 93b provided in the grip 93. Accordingly, the grip portions 14 on both sides of the tensile test piece 10 are fixed to the upper and lower grips 93 and attached to the test piece attachment portion 90. In the tensile strength test, the upper grip 93 is raised via the upper rod 91 by a servo motor, and a tensile load in the longitudinal direction is applied to the tensile test piece 10. The tensile load applied to the tensile test piece 10 can be measured by a load cell (not shown) connected to the upper rod 91.

ところで、引張試験片10において、掴み部14に対して径の小さい平行部13の耐力は、掴み部14に対して相対的に低い。しかしながら、マトリクス金属11と高強度連続長繊維12との引張強度差が大きいと、マトリクス金属11の径だけを減じても、平行部13の相対的な耐力の低下は小さいのである。   By the way, in the tensile test piece 10, the proof stress of the parallel portion 13 having a small diameter with respect to the grip portion 14 is relatively low with respect to the grip portion 14. However, if the difference in tensile strength between the matrix metal 11 and the high-strength continuous long fibers 12 is large, even if only the diameter of the matrix metal 11 is reduced, the decrease in the relative proof strength of the parallel portion 13 is small.

上記したように、本実施例では、平行部13の長繊維集合領域16の長さに対して、掴み部14の前後の長繊維集合領域16の長さを延長部15の分だけ延長し、マトリクス金属11と高強度連続長繊維12の摩擦力を相対的に増加させて、掴み部14に高強度連続長繊維12を固着させている。つまり、グリップ93を介して引張荷重を負荷したときに、マトリクス金属11と高強度連続長繊維12とが相対的に滑ることを抑制されているから、引張荷重を増加させてもマトリクス金属11からなる金属線状体と高強度連続長繊維12とが分離することなく一体となってこの荷重を担うのである。これにより、平行部13の掴み部14に対する相対的な耐力の低下が小さくても、平行部13に応力を集中させ得て、引張試験片10を平行部13において引っ張って安定して破断させ得て、安定して精度よく引張強度試験を行うことができる。   As described above, in this embodiment, the length of the long fiber assembly region 16 before and after the grip portion 14 is extended by the extension portion 15 with respect to the length of the long fiber assembly region 16 of the parallel portion 13, The frictional force between the matrix metal 11 and the high-strength continuous long fibers 12 is relatively increased, and the high-strength continuous long fibers 12 are fixed to the grip portion 14. That is, when a tensile load is applied via the grip 93, the matrix metal 11 and the high-strength continuous long fibers 12 are prevented from slipping relatively, so even if the tensile load is increased, the matrix metal 11 Thus, the metal linear body and the high-strength continuous long fibers 12 are integrated and carry this load without separation. As a result, even if the relative yield strength of the parallel portion 13 relative to the grip portion 14 is small, stress can be concentrated on the parallel portion 13, and the tensile test piece 10 can be pulled at the parallel portion 13 to be stably broken. Thus, the tensile strength test can be performed stably and accurately.

なお、延長部15が貫通穴93bと干渉せずに試験片取付部90に引張試験片10を取り付け得る限り、掴み部14から径を減じることなく、若しくは、わずかに径を減じるだけでもよい。   In addition, as long as the extension part 15 can attach the tensile test piece 10 to the test piece attachment part 90 without interfering with the through-hole 93b, it is sufficient to reduce the diameter from the grip part 14 or slightly.

[実施例2]
次に、本発明による他の実施例の引張強度試験方法で用いられる引張試験片について図4を用いて説明するとともに、その試験方法を図3を適宜参照しつつ説明する。
[Example 2]
Next, a tensile test piece used in a tensile strength test method according to another embodiment of the present invention will be described with reference to FIG. 4, and the test method will be described with reference to FIG. 3 as appropriate.

図4に示すように、引張試験片20は、実施例1における引張試験片10に対し、両側の延長部15のさらに両側端に高強度連続長繊維12(若しくは、マトリクス金属11を含む長繊維集合領域16)を延長し、当該延長部分を延長部15の側端部に固定するよう、円筒形状の係止片21を与えられている。詳細には、係止片21は、その内側に高強度連続長繊維12を挿通させて、延長部15の側端面に接触させるようにして、圧着工具等によって径方向に圧縮加工されている。すなわち、係止片21は、高強度連続長繊維12にかしめて固定されている。かかる係止片21は、引張強度試験時に、高強度連続長繊維12が掴み部14及び延長部15に対して相対的に平行部13に向かう方向へと滑り移動することを規制している。つまり、高強度連続長繊維12の端部の掴み部14への固着をより確実にしている。また、実施例1の引張試験片10よりも延長部15の長さを短くすることもできる。   As shown in FIG. 4, the tensile test piece 20 is a high-strength continuous long fiber 12 (or a long fiber containing the matrix metal 11 at both ends of the extension 15 on both sides, compared to the tensile test piece 10 in Example 1. A cylindrical locking piece 21 is provided so as to extend the gathering region 16) and to fix the extension to the side end of the extension 15. Specifically, the locking piece 21 is compressed in the radial direction by a crimping tool or the like so that the high-strength continuous long fiber 12 is inserted into the locking piece 21 and is brought into contact with the side end surface of the extension portion 15. That is, the locking piece 21 is fixed to the high-strength continuous long fiber 12 by caulking. The locking piece 21 restricts the high-strength continuous long fiber 12 from sliding in the direction toward the parallel portion 13 relative to the grip portion 14 and the extension portion 15 during the tensile strength test. That is, the end portion of the high-strength continuous long fiber 12 is more securely fixed to the grip portion 14. Further, the length of the extension 15 can be made shorter than that of the tensile test piece 10 of Example 1.

かかる引張試験片20においても、グリップ93(図3を参照)を介して引張荷重を負荷したときに、マトリクス金属11と高強度連続長繊維12とが相対的に滑ることを抑制されているから、引張荷重を増加させてもマトリクス金属11からなる金属線状体と高強度連続長繊維12とが分離することなく一体となってこの荷重を担うのである。これにより、平行部13の掴み部14に対する相対的な耐力の低下が小さくても、平行部13に応力を集中させ得て、引張試験片10を平行部13において引っ張って安定して破断させ得て、安定して精度よく引張強度試験を行うことができる。   Also in the tensile test piece 20, when a tensile load is applied via the grip 93 (see FIG. 3), the matrix metal 11 and the high-strength continuous long fibers 12 are prevented from slipping relatively. Even if the tensile load is increased, the metal linear body made of the matrix metal 11 and the high-strength continuous long fibers 12 are integrated and carry this load without being separated. As a result, even if the relative yield strength of the parallel portion 13 relative to the grip portion 14 is small, stress can be concentrated on the parallel portion 13, and the tensile test piece 10 can be pulled at the parallel portion 13 to be stably broken. Thus, the tensile strength test can be performed stably and accurately.

なお、係止片21はかしめによらずとも、例えば接着剤によって高強度連続長繊維12に締結させたり、また他の方法によって固定されていてもよい。   Note that the locking piece 21 may be fastened to the high-strength continuous continuous fiber 12 by an adhesive, for example, or may be fixed by other methods without using caulking.

[実施例3]
更に、本発明による他の実施例の引張強度試験方法で用いられる引張試験片について図5を用いて説明するとともに、その試験方法を図3を適宜参照しつつ説明する。
[Example 3]
Further, a tensile test piece used in a tensile strength test method according to another embodiment of the present invention will be described with reference to FIG. 5, and the test method will be described with reference to FIG. 3 as appropriate.

図5に示すように、引張試験片30は、実施例1における引張試験片10に対し、両側端の延長部15の代わりに、掴み部14の両側端に高強度連続長繊維12(若しくは、マトリクス金属11を含む長繊維集合領域16)を延長し、当該延長部分を掴み部14の側端部に固定するよう、円筒形状の係止片21を与えられている。ここにおいても、係止片21は、その内側に高強度連続長繊維12を挿通させて、掴み部14の側端面に接触させるようにして、圧着工具等によって径方向に圧縮加工される。係止片21は、引張強度試験時に、高強度連続長繊維12が掴み部14に対して相対的に平行部13に向かう方向へと滑り移動することを規制し、高強度連続長繊維12の端部の掴み部14への固着をより確実にしている。   As shown in FIG. 5, the tensile test piece 30 is different from the tensile test piece 10 in Example 1 in that the high-strength continuous long fibers 12 (or A cylindrical locking piece 21 is provided so as to extend the long fiber assembly region 16) including the matrix metal 11 and to fix the extended portion to the side end of the grip portion 14. Also in this case, the locking piece 21 is compressed in the radial direction by a crimping tool or the like so that the high-strength continuous long fiber 12 is inserted into the locking piece 21 and is brought into contact with the side end surface of the grip portion 14. The locking piece 21 restricts the high-strength continuous long fiber 12 from sliding in the direction toward the parallel portion 13 relative to the grip portion 14 during the tensile strength test. The end is firmly fixed to the grip 14.

かかる引張試験片30においても、グリップ93(図3を参照)を介して引張荷重を負荷したときに、マトリクス金属11と高強度連続長繊維12とが相対的に滑ることを抑制されているから、引張荷重を増加させてもマトリクス金属11からなる金属線状体と高強度連続長繊維12とが分離することなく一体となってこの荷重を担うのである。これにより、平行部13の掴み部14に対する相対的な耐力の低下が小さくても、平行部13に応力を集中させ得て、引張試験片10を平行部13において引っ張って安定して破断させ得て、安定して精度よく引張強度試験を行うことができる。   Also in the tensile test piece 30, when a tensile load is applied via the grip 93 (see FIG. 3), the matrix metal 11 and the high-strength continuous long fiber 12 are prevented from slipping relatively. Even if the tensile load is increased, the metal linear body made of the matrix metal 11 and the high-strength continuous long fibers 12 are integrated and carry this load without being separated. As a result, even if the relative yield strength of the parallel portion 13 relative to the grip portion 14 is small, stress can be concentrated on the parallel portion 13, and the tensile test piece 10 can be pulled at the parallel portion 13 to be stably broken. Thus, the tensile strength test can be performed stably and accurately.

[実施例4]
更に、本発明による他の実施例の引張強度試験方法で用いられる引張試験片について図6を用いて説明するとともに、その試験方法を図3を適宜参照しつつ説明する。
[Example 4]
Further, a tensile test piece used in a tensile strength test method according to another embodiment of the present invention will be described with reference to FIG. 6, and the test method will be described with reference to FIG. 3 as appropriate.

図6に示すように、引張試験片40は、実施例3における引張試験片30に対し、係止片21の代わりに、折り返し型係止片41を与えられている。折り返し型係止片41は、円筒形状の円筒体42とこの外側を覆うように嵌め込まれる一端を閉口された円筒形状の嵌め込み体43とを含む。円筒体42は、掴み部14の両側端に高強度連続長繊維12(若しくは、マトリクス金属11を含む長繊維集合領域16)を延長し、当該延長部分を貫挿されて、掴み部14の側端面に接触させるようにして与えられる。更に、円筒体42の側端から延長された高強度連続長繊維12は円筒体42の端面で外周側に折り返される。ここで、高強度連続長繊維12は複数本の束毎に分割して折り返してもよい。折り返された高強度連続長繊維12は円筒体42の外周面に圧着されるようにして、嵌め込み体43が円筒体42に嵌め込まれる。   As shown in FIG. 6, the tensile test piece 40 is provided with a folded-type locking piece 41 instead of the locking piece 21 with respect to the tensile test piece 30 in the third embodiment. The folding type locking piece 41 includes a cylindrical cylindrical body 42 and a cylindrical fitting body 43 whose one end is fitted so as to cover the outside thereof. The cylindrical body 42 extends the high-strength continuous long fibers 12 (or the long fiber assembly region 16 containing the matrix metal 11) to both ends of the grip portion 14, and the extension portion is inserted into the cylindrical body 42 so that the grip portion 14 side is extended. It is given so as to contact the end face. Furthermore, the high-strength continuous long fibers 12 extended from the side end of the cylindrical body 42 are folded back to the outer peripheral side at the end face of the cylindrical body 42. Here, the high-strength continuous long fibers 12 may be divided into a plurality of bundles and folded back. The fitting body 43 is fitted into the cylindrical body 42 so that the folded high-strength continuous long fiber 12 is crimped to the outer peripheral surface of the cylindrical body 42.

円筒体42及び嵌め込み体43によって、高強度連続長繊維12は折り返し型係止片41に圧着されて固定される。折り返し型係止片41では、高強度連続長繊維12が掴み部14に対して相対的に平行部13に向かう方向へ滑り移動することを規制されており、掴み部14に高強度連続長繊維12を固着させ得るのである。つまり、高強度連続長繊維12の端部の掴み部14への固着をより確実にしている。   By the cylindrical body 42 and the fitting body 43, the high-strength continuous long fibers 12 are pressure-bonded and fixed to the folding-type locking pieces 41. In the folding type locking piece 41, the high-strength continuous long fiber 12 is restricted from sliding and moving in the direction toward the parallel portion 13 relative to the grip portion 14. 12 can be fixed. That is, the end portion of the high-strength continuous long fiber 12 is more securely fixed to the grip portion 14.

かかる引張試験片40においても、グリップ93(図3を参照)を介して引張り荷重を負荷したときに、マトリクス金属11と高強度連続長繊維12とが相対的に滑ることを抑制されるから、引張荷重を増加させてもマトリクス金属11からなる金属線状体と高強度連続長繊維12とが分離することなく一体となってこの荷重を担うのである。これにより、平行部13の掴み部14に対する相対的な耐力の低下が小さくても、平行部13に応力を集中させ得て、引張試験片10を平行部13において引っ張って安定して破断させ得て、安定して精度よく引張強度試験を行うことができる。   Also in the tensile test piece 40, when a tensile load is applied via the grip 93 (see FIG. 3), the matrix metal 11 and the high-strength continuous long fiber 12 are restrained from sliding relatively. Even if the tensile load is increased, the metal linear body made of the matrix metal 11 and the high-strength continuous long fibers 12 are integrated and carry this load without being separated. As a result, even if the relative yield strength of the parallel portion 13 relative to the grip portion 14 is small, stress can be concentrated on the parallel portion 13, and the tensile test piece 10 can be pulled at the parallel portion 13 to be stably broken. Thus, the tensile strength test can be performed stably and accurately.

なお、折り返し型係止片41は、高強度連続長繊維12を円筒体42の外周面に圧着するものでなく、例えば、接着剤により、高強度連続長繊維12を円筒体42の外周面に接着してもよい。   The folding-type locking piece 41 does not press the high-strength continuous long fibers 12 to the outer peripheral surface of the cylindrical body 42. For example, the high-strength continuous long fibers 12 are bonded to the outer peripheral surface of the cylindrical body 42 by an adhesive. It may be glued.

上記した各実施例において、引張強度の測定対象となる長繊維強化金属基複合材料は、高強度連続長繊維の単繊維同士の間にマトリクス金属の配置されていない線状体、すなわち、金属材料からなる管体に長繊維束をそのままを挿通してスエージング加工して得た線状体や、長繊維束に接着剤等を含浸させたプリプレグを同様に挿通して得た線状体であってもよい。また、長繊維強化金属基複合材料は、例えば、角形断面形状など丸棒形状以外の線状体であってもよい。   In each of the embodiments described above, the long fiber reinforced metal matrix composite material to be measured for tensile strength is a linear body in which no matrix metal is arranged between single fibers of high-strength continuous long fibers, that is, a metal material. A linear body obtained by inserting a long fiber bundle as it is into a tubular body made by swaging and a linear body obtained by similarly inserting a prepreg impregnated with an adhesive into the long fiber bundle. There may be. The long fiber reinforced metal matrix composite material may be a linear body other than a round bar shape such as a square cross-sectional shape.

ここまで本発明による代表的実施例及びこれに基づく変形例を説明したが、本発明は必ずしもこれらに限定されるものではなく、当業者であれば、本発明の主旨又は添付した特許請求の範囲を逸脱することなく種々の代替実施例及び改変例を見出すことができるであろう。   Up to this point, representative embodiments and modifications based thereon have been described. However, the present invention is not necessarily limited thereto, and those skilled in the art will understand the gist of the present invention or the appended claims. Various alternative embodiments and modifications may be found without departing from the invention.

10 引張試験片
11 マトリクス金属
12 高強度連続長繊維
13 平行部
14 掴み部
100 長繊維強化複合棒材
DESCRIPTION OF SYMBOLS 10 Tensile test piece 11 Matrix metal 12 High-strength continuous long fiber 13 Parallel part 14 Grasp part 100 Long fiber reinforced composite rod

Claims (7)

棒状体のマトリクス金属の長手方向に沿ってその中心軸近傍に複数本の高強度連続長繊維を配置させた長繊維強化金属基複合材料の該長手方向への引張強度試験方法であって、
前記長手方向の一部に太さを減じた平行部を与えるとともに前記平行部を挟んだ両外側部に掴み部を設け、試験機のチャックに前記掴み部を把持させるとともに前記チャックを離間させて前記平行部を引っ張る試験方法において、前記高強度連続長繊維を前記掴み部のさらに両外側部に延長させてこれを前記掴み部に固着させることを特徴とする長繊維強化金属基複合材料の引張強度試験方法。
A method for testing the tensile strength in the longitudinal direction of a long fiber reinforced metal matrix composite in which a plurality of high-strength continuous fibers are arranged in the vicinity of the central axis along the longitudinal direction of a matrix metal of a rod-shaped body,
Provide a parallel part with reduced thickness in a part of the longitudinal direction and provide gripping parts on both outer sides sandwiching the parallel part, and make the chuck of the testing machine grip the gripping part and separate the chuck. In the test method for pulling the parallel part, the high-strength continuous long fiber is extended to both outer parts of the grip part and fixed to the grip part. Strength test method.
前記掴み部のさらに外側部には前記棒状体の太さを減じるよう前記マトリクス金属を切削した延長部を与えられていることを特徴とする請求項1記載の長繊維強化金属基複合材料の引張強度試験方法。   2. The tension of the long fiber reinforced metal matrix composite material according to claim 1, wherein an extension portion obtained by cutting the matrix metal is provided on the outer side portion of the grip portion so as to reduce the thickness of the rod-shaped body. Strength test method. 前記延長部からさらに外側部に前記高強度連続長繊維を貫通させこれを前記延長部の端部に固定する係止片を与えることを特徴とする請求項2記載の長繊維強化金属基複合材料の引張強度試験方法。   3. The long fiber reinforced metal matrix composite material according to claim 2, wherein the high strength continuous long fiber penetrates from the extension part to the outer side part, and a locking piece for fixing the high strength continuous long fiber to the end part of the extension part is provided. Tensile strength test method. 前記掴み部からさらに外側部に前記高強度連続長繊維を貫通させこれを前記掴み部の端部に固定する係止片を与えることを特徴とする請求項1記載の長繊維強化金属基複合材料の引張強度試験方法。   2. The long fiber reinforced metal matrix composite material according to claim 1, wherein the high strength continuous long fibers are further penetrated from the grip portion to the outer side portion, and a locking piece is provided to fix the high strength continuous long fiber to the end portion of the grip portion. Tensile strength test method. 前記掴み部から貫通した前記高強度連続長繊維を折り返した上で前記係止片を与えることを特徴とする請求項4記載の長繊維強化金属基複合材料の引張強度試験方法。   5. The tensile strength test method for a long fiber reinforced metal matrix composite material according to claim 4, wherein the high-strength continuous long fiber penetrating from the gripping portion is folded and then the locking piece is provided. 前記係止片は前記高強度連続長繊維をかしめるように与えることを特徴とする請求項3乃至5のうちの1つに記載の長繊維強化金属基複合材料の引張強度試験方法。   6. The method for testing the tensile strength of a long fiber reinforced metal matrix composite according to claim 3, wherein the locking piece is applied so as to caulk the high-strength continuous long fibers. 請求項1乃至6のうちの1の引張強度試験方法に用いられる長繊維強化金属基複合材料からなる引張試験片。
A tensile test piece comprising a long fiber reinforced metal matrix composite used in the tensile strength test method according to claim 1.
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