JP2013544280A - Cosmetic composition comprising sodium polyacrylate and a water-soluble polymer - Google Patents

Cosmetic composition comprising sodium polyacrylate and a water-soluble polymer Download PDF

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JP2013544280A
JP2013544280A JP2013541881A JP2013541881A JP2013544280A JP 2013544280 A JP2013544280 A JP 2013544280A JP 2013541881 A JP2013541881 A JP 2013541881A JP 2013541881 A JP2013541881 A JP 2013541881A JP 2013544280 A JP2013544280 A JP 2013544280A
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cosmetic composition
water
sodium polyacrylate
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キュム ソン キム
ジョン ウン パク
ヨウン ジョン キム
ヒョン チュン キム
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Amorepacific Corp
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A61K8/731—Cellulose; Quaternized cellulose derivatives
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin

Abstract

【課題】本発明はポリアクリル酸ナトリウム(ｓｏｄｉｕｍ ｐｏｌｙａｃｒｙｌａｔｅ)と水溶性ポリマーの組合せを含む化粧料組成物に提供する。
【解決手段】高分子原料であるポリアクリル酸ナトリウム及び水溶性天然増粘剤である水溶性ポリマーを含有してシャーベットと類似の見掛け及び物性を有し、皮膚に保湿及び柔軟感又は角質除去効果を提供するゲルタイプの化粧料組成物を提供する。
【選択図】図１The present invention provides a cosmetic composition comprising a combination of sodium polyacrylate and a water-soluble polymer.
SOLUTION: It contains sodium polyacrylate, which is a polymer raw material, and a water-soluble polymer, which is a water-soluble natural thickener, and has the appearance and physical properties similar to those of sherbet. A gel-type cosmetic composition is provided.
[Selection] Figure 1

Description

本発明は、ポリアクリル酸ナトリウムと水溶性ポリマーの組合せを含む化粧料組成物に関する。   The present invention relates to a cosmetic composition comprising a combination of sodium polyacrylate and a water-soluble polymer.

近年、‘自然主義’のトレンドと共に天然素材化粧品に対する関心が絶えず増加しつつこのような素材を用いて皮膚保湿問題を解決しようとする動きが増えている。これによって一般家庭でも即刻で集中的な皮膚管理のために、蜂蜜、黄土、きゅうりなどを利用した天然素材のパックを利用して皮膚管理をしている。パック剤形の化粧品は一時的に皮膚の上に薄い被膜を着せて外部への水分蒸発を遮断させて皮膚をしっとりとし、有効成分を効果的に浸透させる特性を有する剤形として最近このようなパック剤形の化粧品に対する関心がだんだん増えている。   In recent years, along with the trend of 'naturalism', interest in natural cosmetics is constantly increasing, and there is an increasing movement to solve the skin moisturizing problem using such materials. In this way, even in ordinary households, skin management is performed using natural material packs using honey, ocher, cucumber, etc. for instant and intensive skin management. Packed cosmetic products have recently been used as a dosage form that has a characteristic of applying a thin film on the skin to block moisture evaporation to the outside and moisturizing the skin and effectively infiltrating the active ingredients. There is a growing interest in cosmetics in pack dosage forms.

一方、化粧品は粘性と弾性が入り組まれている複雑なレオロジー的性質を有する製品である。混合される原料の特性を利用して多様な見掛け及び物性を有する剤形を製造することができる。このようなレオロジー的性質と剤形の物性に重要な原料としては高分子物質を挙げることができ、使用される高分子物質の特性によって化粧品の見掛け、質感、物性、及び使用感が大きく変わる。したがって、多様な性質の高分子原料をスクリーニングし、各剤形に適した高分子原料を利用して多様な特性の製品を製造しようとする努力が続いている。   On the other hand, a cosmetic product is a product having complicated rheological properties in which viscosity and elasticity are complicated. Using the characteristics of the raw materials to be mixed, dosage forms having various appearances and physical properties can be produced. Examples of raw materials important for such rheological properties and physical properties of the dosage form include polymer substances, and the appearance, texture, physical properties, and feeling of use of cosmetics vary greatly depending on the characteristics of the polymer substance used. Accordingly, there are ongoing efforts to screen high molecular raw materials having various properties and to manufacture products having various characteristics using high molecular raw materials suitable for each dosage form.

本発明者らはシャーベットと類似の化粧品剤形を製造するために研究した結果、高分子物質であるポリアクリル酸ナトリウムと水溶性天然増粘剤を含有する場合、シャーベットと類似の化粧品剤形を製造することができ、このような剤形は柔らかい物性を有すると共に消費者がより容易に皮膚管理に利用することができることを発見し、本発明を完成するようになった。   The present inventors have studied to produce a cosmetic dosage form similar to sherbet, and as a result, when the polymer substance contains sodium polyacrylate and a water-soluble natural thickener, a cosmetic dosage form similar to sherbet is used. It has been discovered that such dosage forms have soft physical properties and can be more easily utilized by consumers for skin management, thus completing the present invention.

したがって、本発明は高分子原料であるポリアクリル酸ナトリウム及び水溶性天然増粘剤を含有してシャーベットと類似の見掛け及び物性を有する化粧料組成物を提供することを目的とする。   Accordingly, an object of the present invention is to provide a cosmetic composition containing sodium polyacrylate, which is a polymer raw material, and a water-soluble natural thickener and having appearance and physical properties similar to those of sherbet.

また、本発明は皮膚に保湿効果、柔軟効果又は角質除去効果を提供する化粧料組成物を提供することを目的とする。   Another object of the present invention is to provide a cosmetic composition that provides the skin with a moisturizing effect, a softening effect, or an exfoliating effect.

上記目的を達成するために、本発明はポリアクリル酸ナトリウム及び水溶性増粘剤を含む化粧料組成物を提供する。   In order to achieve the above object, the present invention provides a cosmetic composition comprising sodium polyacrylate and a water-soluble thickener.

本発明の化粧料組成物はシャーベットと類似の剤形を有しており、柔らかい物性を有すると共に消費者がより容易に皮膚管理に利用することができ、皮膚に保湿効果、柔軟効果又は角質除去効果を提供する。   The cosmetic composition of the present invention has a dosage form similar to that of sherbet, has soft physical properties and can be more easily used by consumers for skin management, moisturizing effect, softening effect or exfoliation on the skin Providing an effect.

実施例1〜６及び比較例１〜２の化粧料組成物の塗布の後、皮膚水分量を測定した結果を示す図面である。It is drawing which shows the result of having measured the skin moisture content after application | coating of the cosmetic composition of Examples 1-6 and Comparative Examples 1-2.

本発明の化粧料組成物はポリアクリル酸ナトリウムと水溶性増粘剤を含む。
本発明において使用する高分子原料であるポリアクリル酸ナトリウムは組成物の全重量に対して１.５〜３．０重量%の量で含有される。また、ポリアクリル酸ナトリウム単独使用の時の粘弾性は１０〜１５Ｎであれば良い。 The cosmetic composition of the present invention contains sodium polyacrylate and a water-soluble thickener.
Sodium polyacrylate, which is a polymer raw material used in the present invention, is contained in an amount of 1.5 to 3.0% by weight based on the total weight of the composition. The viscoelasticity when using sodium polyacrylate alone may be 10 to 15N.

本発明において水溶性増粘剤としてはセルロースガム、キサンタンガム、ジェランガム、寒天（agar）などの水溶性ポリマーを使用することができ、その他にタマリンドガム、グアーガム、アラビアガムなどを使用することができる。セルロースガム類としてはＣ．Ｍ．Ｃ−Ｎａ陽イオンセルロースパウダーなどがあり、キサンタンガム類はＫｅｌｔｒｏｌ−Ｆなどがあり、ジェランガム類としてはＫＥＬＣＯＧＥＬなどがある。上記水溶性増粘剤は組成物の全重量に対して０．２５〜０．５重量%の量で含有される。   In the present invention, water-soluble polymers such as cellulose gum, xanthan gum, gellan gum and agar can be used as the water-soluble thickener, and tamarind gum, guar gum, gum arabic and the like can also be used. Cellulose gums include C.I. M.M. There are C-Na cation cellulose powders, xanthan gums include Keltrol-F, and gellan gums include KELCOGEL. The water-soluble thickener is contained in an amount of 0.25 to 0.5% by weight based on the total weight of the composition.

本発明の化粧料組成物は粘弾性が１０〜１８Ｎの範囲であれば良い。   The cosmetic composition of the present invention may have a viscoelasticity in the range of 10 to 18N.

本発明の化粧料組成物はその剤形において特別に限定されるものではなく、 例えば柔軟化粧水、栄養化粧水、乳液、マッサージクリーム、栄養クリーム、パックなどの剤形を有する化粧料組成物であることができ、特に、本発明の化粧料組成物は好ましくは可溶化剤形のマスクパック類、乳化剤形のマスクパック類又はクリームなどの形態に剤形化されることができる。   The cosmetic composition of the present invention is not particularly limited in its dosage form. For example, it is a cosmetic composition having a dosage form such as soft lotion, nutritional lotion, emulsion, massage cream, nutritional cream, and pack. In particular, the cosmetic composition of the present invention can be preferably formulated in the form of solubilizing mask packs, emulsifying mask packs or creams.

以下、本発明の内容を実施例及び試験例によって具体的に説明する。これら実施例は本発明の内容を理解するために提示されるものであるだけであり、本発明の権利範囲がこれら実施例に限定されるものではない。   Hereinafter, the contents of the present invention will be specifically described with reference to Examples and Test Examples. These examples are presented only for the purpose of understanding the contents of the present invention, and the scope of rights of the present invention is not limited to these examples.

[試験例１]ポリアクリル酸ナトリウムの含量による粘弾性とピーリング効果の評価
以下の表１の組成でポリアクリル酸ナトリウムを多様な含量で含ませて化粧料組成物を製造し、これら組成物の粘弾性及びピーリング効果を測定した。ピーリング効果程度はパネル１０名の点数を平均としたものである。 [Test Example 1] Evaluation of Viscoelasticity and Peeling Effect Depending on the Content of Sodium Polyacrylate A cosmetic composition was produced by containing various amounts of sodium polyacrylate in the composition shown in Table 1 below. Viscoelasticity and peeling effect were measured. The degree of peeling effect is the average of the scores of 10 panelists.

粘弾性の測定はレオメーター(Ｓｕｎ ｓｃｉｅｎｔｉｆｉｃ ｃｏ.，ＬＴＤ)を利用して測定し、ピーリング効果はパネル１０名を選定して５分間ローリング後のピーリング程度を１０点満点を基準で測定した。   The viscoelasticity was measured by using a rheometer (Sun scientific co., LTD), and the peeling effect was measured on the basis of 10 points on the peeling degree after rolling for 5 minutes by selecting 10 panelists.

Figure 2013544280
Figure 2013544280

上記の表１によれば、ポリアクリル酸ナトリウムの含量が増加するほど粘弾性も比例的に増加するが、粘弾性があまり高くなればピーリング効果はむしろ減少することが分かる。   According to Table 1 above, it can be seen that the viscoelasticity increases proportionally as the content of sodium polyacrylate increases, but if the viscoelasticity is too high, the peeling effect decreases rather.

[試験例２]ポリアクリル酸ナトリウム及び水溶性増粘剤との組合せ
上記試験例１の結果に基づいて、ポリアクリル酸ナトリウムの含量はピーリング効果が大きいことで出た２重量％又は２．５重量％とし、様々な水溶性増粘剤を使用して以下表２の組成で化粧料組成物を製造した。 [Test Example 2] Combination of sodium polyacrylate and water-soluble thickener Based on the results of Test Example 1 above, the content of sodium polyacrylate was 2% by weight or 2.5% due to the large peeling effect. A cosmetic composition was prepared with the composition shown in Table 2 below using various water-soluble thickeners in weight%.

製造した組成物の粘弾性及びピーリング効果を測定し、この結果は以下の表２に記載した。ピーリング効果程度はパネル１０名の点数を平均としたものである。   The viscoelasticity and peeling effect of the produced composition was measured and the results are listed in Table 2 below. The degree of peeling effect is the average of the scores of 10 panelists.

Figure 2013544280
Figure 2013544280

上記の表２によれば、ポリアクリル酸ナトリウムを単独使用した上記試験例１の表１に示した粘弾性及びピーリング効果程度と比べて、水溶性増粘剤を組み合わせて使用した場合、粘弾性がより高く、かつ安定し、ピーリング効果も格段に良いことを確認することができる。特にセルロースガム、キサンタンガム、ジェランガムをポリアクリル酸ナトリウムと共に使用する場合、効果が優れたことが分かる。
また、水溶性２種以上の増粘剤を組み合わせて使用する場合にも粘弾性及びピーリング効果が良い。 According to Table 2 above, viscoelasticity is obtained when a water-soluble thickener is used in combination as compared to the viscoelasticity and peeling effect degree shown in Table 1 of Test Example 1 using sodium polyacrylate alone. Can be confirmed to be higher and more stable and have a significantly better peeling effect. In particular, when cellulose gum, xanthan gum and gellan gum are used together with sodium polyacrylate, it can be seen that the effect is excellent.
In addition, viscoelasticity and peeling effect are good when two or more water-soluble thickeners are used in combination.

[試験例３]水溶性増粘剤の多様な含量による組合せ
以下の表３の組成で水溶性増粘剤を多様な含量で含ませて化粧料組成物を製造し、これら組成物の粘弾性及びピーリング効果を測定した。
ピーリング効果程度はパネル１０名の点数を平均としたものである。測定結果は以下の表４に示す。 [Test Example 3] Combinations with various contents of water-soluble thickeners Cosmetic compositions were prepared with various contents of water-soluble thickeners having the compositions shown in Table 3 below. And the peeling effect was measured.
The degree of peeling effect is the average of the scores of 10 panelists. The measurement results are shown in Table 4 below.

Figure 2013544280
Figure 2013544280

Figure 2013544280
Figure 2013544280

上記の表４によれば、ポリアクリル酸ナトリウムを単独で使用した比較例1、２より、水溶性増粘剤と共に使用した実施例１〜６の場合が粘弾性程度がより高くピーリング効果も格段に高いことを確認することができる。   According to Table 4 above, the comparative examples 1 and 2 in which sodium polyacrylate was used alone had higher viscoelasticity in the cases of Examples 1 to 6 used in combination with the water-soluble thickener, and the peeling effect was also remarkable. Can be confirmed to be high.

[試験例４]皮膚保湿力の改善効果測定
乾燥を訴える成人男女もしくは乾燥肌の成人男女１０名(２９±３歳)を選抜し、恒温、恒湿条件(２４〜２６℃、相対湿度４０〜５０％)で1５分間待機させた後、実施例1〜６及び比較例1〜２の化粧料組成物を下腕に塗布して皮膚保湿力を比べた。塗布開始前と、塗布の後０、２、４、６、1２、２4時間が経過した時点でそれぞれコルネオメーター(Ｃｏｒｎｅｏｍｅｔｅｒ、Ｃ＋Ｋ社、ドイツ)で皮膚水分量を測定した。この結果を図1に示した。 [Test Example 4] Measurement of improvement effect of skin moisturizing power 10 adult men and women (29 ± 3 years old) complaining of dryness or dry skin were selected and kept at constant temperature and humidity (24-26 ° C, relative humidity 40- 50%), the cosmetic compositions of Examples 1 to 6 and Comparative Examples 1 and 2 were applied to the lower arm, and the skin moisturizing power was compared. Skin water content was measured with a corneometer (Corneometer, C + K, Germany) before the start of application and when 0, 2, 4, 6, 12, 24 hours had elapsed after application. The results are shown in FIG.

その結果、図１に表示されたように、実施例1〜６の組成物を塗布した場合の皮膚水分量が比較例1〜２の組成物を塗布した場合に比べ、より高い値を示すことが分かる。この皮膚水分量の増加は１日が経った２４時間後にも継続観察された。   As a result, as shown in FIG. 1, the amount of skin moisture when the compositions of Examples 1 to 6 are applied is higher than when the compositions of Comparative Examples 1 and 2 are applied. I understand. This increase in skin moisture was continuously observed 24 hours after 1 day.

Claims (8)

ポリアクリル酸ナトリウム及び水溶性増粘剤を含む化粧料組成物。   A cosmetic composition comprising sodium polyacrylate and a water-soluble thickener. 前記ポリアクリル酸ナトリウムは、組成物全重量に対して１．５〜２．５重量%の量で含有される請求項１に記載の化粧料組成物。   The cosmetic composition according to claim 1, wherein the sodium polyacrylate is contained in an amount of 1.5 to 2.5% by weight based on the total weight of the composition. 前記水溶性増粘剤は、セルロースガム、キサンタンガム、ジェランガム及び寒天からなる群より選択された１種以上である請求項１に記載の化粧料組成物。   The cosmetic composition according to claim 1, wherein the water-soluble thickener is at least one selected from the group consisting of cellulose gum, xanthan gum, gellan gum, and agar. 前記水溶性増粘剤は、組成物の全重量に対して０．２５〜０．５重量%の量で含有される請求項１に記載の化粧料組成物。   The cosmetic composition according to claim 1, wherein the water-soluble thickener is contained in an amount of 0.25 to 0.5% by weight based on the total weight of the composition. 前記組成物は、粘弾性が１０〜１８Ｎの範囲である請求項１に記載の化粧料組成物。   The cosmetic composition according to claim 1, wherein the composition has a viscoelasticity in the range of 10 to 18N. 前記組成物は、可溶化剤形のマスクパック類、乳化剤形のマスクパック類又はクリーム形態である請求項１〜５いずれか記載の化粧料組成物。   The cosmetic composition according to any one of claims 1 to 5, wherein the composition is in the form of a solubilizer-type mask pack, an emulsifier-type mask pack, or a cream. 請求項1〜６いずれか記載の化粧料組成物の角質除去用としての用途。   Use of the cosmetic composition according to any one of claims 1 to 6 for removing keratin. 請求項1〜６いずれか記載の化粧料組成物の皮膚保湿用としての用途。   Use of the cosmetic composition according to any one of claims 1 to 6 for moisturizing the skin.
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