JP2013537877A5 - - Google Patents

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JP2013537877A5
JP2013537877A5 JP2013526572A JP2013526572A JP2013537877A5 JP 2013537877 A5 JP2013537877 A5 JP 2013537877A5 JP 2013526572 A JP2013526572 A JP 2013526572A JP 2013526572 A JP2013526572 A JP 2013526572A JP 2013537877 A5 JP2013537877 A5 JP 2013537877A5
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composite
sulfur
metal
organic compound
complex
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JP2013526572A
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JP2013537877A (en
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Priority claimed from PCT/IB2011/053646 external-priority patent/WO2012028989A1/en
Publication of JP2013537877A publication Critical patent/JP2013537877A/en
Publication of JP2013537877A5 publication Critical patent/JP2013537877A5/ja
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Claims (15)

（ａ）少なくとも１種の金属イオンに配位結合した少なくとも１種の少なくとも２座の有機化合物を含む多孔質の金属−有機骨格材料を、保護ガス雰囲気下で熱分解する工程であって、前記少なくとも１種の少なくとも２座の有機化合物は窒素を含まない工程、
を含む炭素含有複合体の製造方法。 (A) a step of thermally decomposing a porous metal-organic framework material containing at least one at least one bidentate organic compound coordinated to at least one metal ion under a protective gas atmosphere, At least one at least bidentate organic compound does not contain nitrogen,
The manufacturing method of the carbon containing composite_body | complex containing. 前記熱分解を少なくとも５００℃で行う、請求項１に記載の方法。   The method of claim 1, wherein the pyrolysis is performed at least at 500 ° C. 前記保護ガス雰囲気は窒素を含む、請求項１又は２に記載の方法。   The method according to claim 1, wherein the protective gas atmosphere contains nitrogen. 前記少なくとも１種の金属イオンは、Ｍｇ、Ａｌ、Ｚｒ、Ｔｉ、Ｖ、Ｃｒ、Ｍｏ、Ｆｅ、Ｃｏ、Ｃｕ、Ｎｉ及びＺｎからなる金属の群から選択されるイオンである、請求項１〜３の何れか１項に記載の方法。   The at least one metal ion is an ion selected from the group of metals consisting of Mg, Al, Zr, Ti, V, Cr, Mo, Fe, Co, Cu, Ni and Zn. The method according to any one of the above. 前記窒素を含まない少なくとも１種の少なくとも２座の有機化合物は、ジカルボン酸、トリカルボン酸又はテトラカルボン酸から誘導される、請求項１〜４の何れか１項に記載の方法。   The method according to any one of claims 1 to 4, wherein the at least one at least bidentate organic compound not containing nitrogen is derived from a dicarboxylic acid, a tricarboxylic acid or a tetracarboxylic acid. （ｂ）工程（ａ）で得られた複合体から１種以上の金属成分を少なくとも部分的に除去する工程、
を更に含む、請求項１〜５の何れか１項に記載の方法。 (B) a step of at least partially removing one or more metal components from the composite obtained in step (a);
The method according to any one of claims 1 to 5, further comprising: 前記１種以上の金属成分は少なくとも１種の金属酸化物を含む、請求項６に記載の方法。   The method of claim 6, wherein the one or more metal components comprise at least one metal oxide. 前記少なくとも部分的な除去は、アルカリ性または酸性の液体を用いて洗い流すことにより行う、請求項６又は７に記載の方法。   The method according to claim 6 or 7, wherein the at least partial removal is performed by rinsing with an alkaline or acidic liquid. （ｃ）工程（ａ）又は（ｂ）から得られた複合体に硫黄を含浸する工程、
を更に含む、請求項１〜８の何れか１項に記載の方法。 (C) impregnating the composite obtained from step (a) or (b) with sulfur;
The method according to any one of claims 1 to 8, further comprising: 前記含浸を混合及びこれに次ぐ加熱により行う、請求項９に記載の方法。   The method according to claim 9, wherein the impregnation is performed by mixing and subsequent heating. 前記硫黄を固体として又は溶液中で使用する、請求項９又は１０に記載の方法。   The process according to claim 9 or 10, wherein the sulfur is used as a solid or in solution. 請求項１〜１１の何れか１項に記載の方法により得られる複合体。   The composite_body | complex obtained by the method of any one of Claims 1-11. 請求項１〜１１の何れか１項に記載の方法により得られる複合体の、少なくとも１種の材料の貯蔵、除去、制御放出、化学反応を目的として前記少なくとも１種の材料を吸収するための、又は担体としての使用方法。 A complex obtained by the method according to any one of claims 1 to 11, for absorbing said at least one material for the purpose of storage, removal, controlled release, chemical reaction of at least one material. , or the use of a carrier. 請求項９〜１１の何れか１項に記載の方法により得られる複合体を含む硫黄電極。   The sulfur electrode containing the composite_body | complex obtained by the method of any one of Claims 9-11. 請求項１４に記載の硫黄電極のＬｉ−硫黄電池への使用方法。 The method for using the sulfur electrode according to claim 14 for a Li-sulfur battery.
JP2013526572A 2010-09-01 2011-08-18 Method for producing carbon-containing composite Withdrawn JP2013537877A (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP10174939.8 2010-09-01
EP10174939 2010-09-01
PCT/IB2011/053646 WO2012028989A1 (en) 2010-09-01 2011-08-18 Process for producing carbon-comprising composite

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JP2013537877A JP2013537877A (en) 2013-10-07
JP2013537877A5 true JP2013537877A5 (en) 2014-10-02

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EP (1) EP2611766A4 (en)
JP (1) JP2013537877A (en)
KR (1) KR20130101038A (en)
CN (1) CN103180282A (en)
AU (1) AU2011298030A1 (en)
BR (1) BR112013004984A2 (en)
CA (1) CA2809928A1 (en)
MX (1) MX2013002219A (en)
RU (1) RU2013114186A (en)
TW (1) TW201223962A (en)
WO (1) WO2012028989A1 (en)

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