JP2013201908A - Method for producing flavor oil and flavor oil - Google Patents

Method for producing flavor oil and flavor oil Download PDF

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JP2013201908A
JP2013201908A JP2012071256A JP2012071256A JP2013201908A JP 2013201908 A JP2013201908 A JP 2013201908A JP 2012071256 A JP2012071256 A JP 2012071256A JP 2012071256 A JP2012071256 A JP 2012071256A JP 2013201908 A JP2013201908 A JP 2013201908A
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oil
flavor
solid component
hydrophilic solvent
flavor oil
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JP5926997B2 (en
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Takashi Aizawa
貴志 相澤
Kenichi Shimizu
健一 清水
Masako Miyata
真子 宮田
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Tablemark Co Ltd
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Abstract

PROBLEM TO BE SOLVED: To provide a method for producing flavor oil reduced in color staining to water system, and flavor oil obtained by the method.SOLUTION: This method for producing flavor oil is characterized by mixing oil obtained after edible oil and one or more kinds selected from vegetable and spice are heated, and a solid component obtained after a solid component obtained after edible oil and one or more kinds selected from vegetable and spice are heated is washed by a hydrophilic solvent. This flavor oil is obtained by mixing oil obtained after edible oil and one or more kinds selected from vegetable and spice are heated, and a solid component obtained after a solid component obtained after edible oil and one or more kinds selected from vegetable and spice are heated is washed by a hydrophilic solvent.

Description

本発明は、水系への色移りが低減された香味油の製造方法、並びに該方法により得られた香味油に関する。   The present invention relates to a method for producing a flavor oil with reduced color transfer to an aqueous system, and a flavor oil obtained by the method.

香味油とは、野菜、畜肉、魚介類等の香味を有する素材や、香辛料等が有する風味を食用油脂に付加したものである。香味油を、調味料や加熱調理時の油脂(炒め油、油ちょう油等)として用いた場合、食品に対して良好な風味を簡便に付与することが可能となる。香味油としては、ネギ、タマネギ、ニンニク、ショウガ等の香味野菜の香味を有するものが広く用いられている。
香味油は通常、油脂と、香味を有する素材や香辛料とを共に加熱処理することにより製造される。具体的には、植物性食用油脂に、細断または摩砕した野菜を加えて加熱昇温し、必要により加熱状態で保持した後、油相(油性成分)を採取する方法が知られている(例えば特許文献1参照)。
近年では、食用油脂中で野菜や香辛料を焦がすことなく、香味のみを食用油脂に付加する香味油の製造方法も検討されている。例えば特許文献2には、香味物質中の香気成分を、液体状態又は超臨界状態の二酸化炭素中に溶解、移行させ、二酸化炭素を気化させた後、食用油に接触させて、二酸化炭素中の香気成分を食用油に吸収させる香味油の製造方法が開示されている。特許文献3には、摩砕した生ニンニクと食用油脂とを0℃以上且つ常温以下で接触させた後、残渣を分離し、食用油脂加工品を得る方法が記載されている。
また、近年では、風味の付加に用いた素材や香辛料を製造後に分離することなく、該素材や香辛料を含有する状態で供される具材入りの香味油も広く用いられている。
Flavored oil is obtained by adding flavors such as vegetables, livestock meat, and seafood, and flavors of spices to edible fats and oils. When the flavor oil is used as a seasoning or a fat or oil during cooking (such as stir-fried oil or oiled oil), it is possible to easily give a good flavor to food. As flavor oil, what has the flavor of flavor vegetables, such as a leek, an onion, a garlic, ginger, is widely used.
A flavor oil is normally manufactured by heat-processing oil and fat, the raw material and spice which have a flavor together. Specifically, there is known a method of collecting oil phase (oil-based component) after adding shredded or ground vegetables to vegetable edible oil and heating to raise the temperature and holding it in a heated state if necessary. (For example, refer to Patent Document 1).
In recent years, a method for producing a flavor oil in which only a flavor is added to an edible oil and fat without scorching vegetables and spices in the edible oil and fat has been studied. For example, in Patent Document 2, the aroma component in the flavor substance is dissolved and transferred into carbon dioxide in a liquid state or a supercritical state, and after vaporizing carbon dioxide, it is brought into contact with edible oil, A method for producing a flavor oil in which an aroma component is absorbed by an edible oil is disclosed. Patent Document 3 describes a method in which ground raw garlic and edible fat / oil are brought into contact at 0 ° C. or more and normal temperature or less, and then the residue is separated to obtain a processed edible fat / oil product.
In recent years, flavor oils containing ingredients provided in a state containing the raw materials and spices without widely separating the raw materials and spices used for the addition of flavor after production have been widely used.

特開昭56−58450号公報JP-A-56-58450 特開平6−125707号公報JP-A-6-125707 特開平9−121767号公報JP-A-9-121767

上記特許文献1のような従来の製造方法により得られる香味油は、食用油脂中で野菜や香辛料を焦がすことによって食用油脂に野菜由来の風味及びローストによる風味を付与するものであり、得られた香味油は茶褐色又は黒褐色となる。香味油を水系の食品、例えばスープ等に添加した場合、該水系の食品に色移りを引き起こし、食品の外観の美麗さが損なわれるという問題がある。水系への色移りを引き起こす成分は主に野菜や香辛料に由来する水溶性成分であるため、上述したような具材を含有する香味油では該問題が特に顕著となる。そのため、水系への色移りを低減できる香味油やその製造方法が求められている。   The flavor oil obtained by the conventional manufacturing method like the said patent document 1 imparts the vegetable-derived flavor and the roasted flavor to the edible fat by scorching vegetables and spices in the edible fat. The flavor oil becomes brownish brown or blackish brown. When flavor oil is added to water-based foods such as soups, there is a problem in that the water-based foods cause color transfer and the beauty of the appearance of the food is impaired. Since the component causing the color transfer to the aqueous system is a water-soluble component mainly derived from vegetables and spices, this problem is particularly noticeable in flavor oils containing ingredients as described above. Therefore, there is a need for a flavor oil and a method for producing the same that can reduce color transfer to an aqueous system.

特許文献2〜3に記載されたような焦がしを伴わない香味油の製造方法は、色移りの低減を目的としたものではないが、野菜や香辛料を焦がすことがないため、色移りは多少なりとも低減されると考えられる。
しかしながら、特許文献2の方法は、従来の方法に比して格段に工程が煩雑となるため、工業上実施が困難であり、現実的でない。また、特許文献2〜3の方法では、野菜の甘みを食用油脂に付加することはできるが、焦げに由来するローストの風味を付与できず、風味の点で改善の余地がある。
Although the method for producing flavor oil without scoring as described in Patent Documents 2 to 3 is not intended to reduce the color transfer, it does not burn vegetables and spices, so the color transfer is somewhat. Both are considered to be reduced.
However, since the method of Patent Document 2 is much more complicated than the conventional method, it is difficult to implement industrially and is not practical. Moreover, in the method of patent documents 2-3, although the sweetness of vegetables can be added to edible fats and oils, the roasted flavor derived from a burn cannot be provided, but there exists room for improvement in the point of flavor.

本発明は、上記事情に鑑みてなされたものであって、水系への色移りが低減された香味油の製造方法、並びに該方法により得られた香味油を提供することを目的とする。   This invention is made | formed in view of the said situation, Comprising: It aims at providing the manufacturing method of the flavor oil by which the color transfer to an aqueous system was reduced, and the flavor oil obtained by this method.

本発明者らは、上記課題を解決すべく鋭意研究した結果、水系への色移りが主に、固形成分に付着した又は固形成分中に存在する水溶性成分に起因すること、並びに、固形成分を親水性溶媒で洗浄して該水溶性成分を除去することにより、水系への色移りを低減可能であることを見出し、本発明を完成させた。   As a result of diligent research to solve the above-mentioned problems, the present inventors have found that the color transfer to an aqueous system is mainly caused by a water-soluble component attached to or present in the solid component, and the solid component. The present invention was completed by finding that the color transfer to the aqueous system can be reduced by removing the water-soluble component by washing with a hydrophilic solvent.

すなわち、本発明は、下記の特徴を有する香味油の製造方法、及び香味油を提供するものである。
[1]食用油脂と、野菜及び香辛料から選ばれる1種以上とを加熱した後に得られる油分と、
食用油脂と、野菜及び香辛料から選ばれる1種以上とを加熱した後の固形成分を、親水性溶媒によって洗浄した後に得られた固形成分と、
を混合することを特徴とする香味油の製造方法。
[2](1−1)食用油脂と、野菜及び香辛料から選ばれる1種以上とを加熱して香味油を得る工程と、
(1−2)前記香味油を、油分と固形成分とに分離する工程と、
(1−3)前記固形成分を親水性溶媒によって洗浄する工程と、
(1−4)前記工程(1−2)で得られた油分と、前記工程(1−3)で得られた洗浄後の固形成分とを混合する工程と、
を有する[1]の香味油の製造方法。
[3](2−1)食用油脂と、野菜及び香辛料から選ばれる1種以上とを加熱して香味油を得る工程と、
(2−2)前記香味油を親水性溶媒と混合させる工程と、
(2−3)混合させた後の香味油を、油分と固形成分と水層とに分離する工程と、
(2−4)前記油分と、前記固形成分とを混合する工程と、
を有する[1]の製造方法。
[4](3−1)食用油脂と、野菜及び香辛料から選ばれる1種以上とを加熱して香味油を得る工程と、
(3−2)前記香味油を、親水性溶媒と混合させる工程と、
(3−3)混合させた後の香味油を、油分と固形成分と水層とに分離する工程と、
(3−4)前記固形成分を、親水性溶媒によって洗浄する工程と、
(3−5)前記工程(3−3)で得られた油分と、前記工程(3−4)で得られた洗浄後の固形成分とを混合する工程と、
を有する[1]の香味油の製造方法。
[5](4−1)食用油脂と、野菜及び香辛料から選ばれる1種以上とを加熱して香味油を得る工程と、
(4−2)前記香味油を、油分と固形成分とに分離する工程と、
(4−3)前記油分を親水性溶媒と混合させる工程と、
(4−4)前記工程(4−3)で得られた混合液中の油分と、水層とを分離する工程と、
(4−5)前記固形成分を親水性溶媒によって洗浄する工程と、
(4−6)前記工程(4−4)で得られた油分と、前記工程(4−5)で得られた洗浄後の固形成分とを混合する工程と、
を有する[1]の香味油の製造方法。
[6]さらに、乳化剤を添加する工程を有する[1]〜[5]のいずれかの香味油の製造方法。
[7][1]〜[6]のいずれかの香味油の製造方法を用いて得られた香味油。
[8]含有量が5質量%となるように90℃以上のお湯に添加した場合のOD420nmの吸光度が0.4以下である[7]の香味油。
[9]食用油脂と、野菜及び香辛料から選ばれる1種以上とを加熱した後に得られる油分と、
食用油脂と、野菜及び香辛料から選ばれる1種以上とを加熱した後に得られる固形成分を、親水性溶媒で洗浄した後の固形成分と、を混合して得られる香味油。
That is, this invention provides the manufacturing method of flavor oil which has the following characteristics, and flavor oil.
[1] An oil obtained after heating an edible fat and one or more selected from vegetables and spices;
A solid component obtained after washing the edible oil and fat and one or more selected from vegetables and spices with a hydrophilic solvent;
A method for producing a flavor oil, comprising mixing
[2] (1-1) A step of heating a cooking oil and fat and at least one selected from vegetables and spices to obtain a flavor oil;
(1-2) separating the flavor oil into an oil and a solid component;
(1-3) washing the solid component with a hydrophilic solvent;
(1-4) A step of mixing the oil obtained in the step (1-2) with the washed solid component obtained in the step (1-3);
[1] The method for producing a flavor oil according to claim 1.
[3] (2-1) A step of obtaining a flavor oil by heating edible oil and fat and one or more selected from vegetables and spices;
(2-2) mixing the flavor oil with a hydrophilic solvent;
(2-3) separating the flavor oil after mixing into an oil, a solid component, and an aqueous layer;
(2-4) mixing the oil and the solid component;
The manufacturing method of [1] which has these.
[4] (3-1) A step of heating the edible oil and fat and one or more selected from vegetables and spices to obtain a flavor oil;
(3-2) mixing the flavor oil with a hydrophilic solvent;
(3-3) separating the flavor oil after mixing into an oil, a solid component, and an aqueous layer;
(3-4) washing the solid component with a hydrophilic solvent;
(3-5) a step of mixing the oil obtained in the step (3-3) and the solid component after washing obtained in the step (3-4);
[1] The method for producing a flavor oil according to claim 1.
[5] (4-1) A step of heating the edible oil and fat and one or more selected from vegetables and spices to obtain a flavor oil;
(4-2) separating the flavor oil into an oil and a solid component;
(4-3) mixing the oil with a hydrophilic solvent;
(4-4) a step of separating the oil in the mixed liquid obtained in the step (4-3) and the aqueous layer;
(4-5) washing the solid component with a hydrophilic solvent;
(4-6) a step of mixing the oil obtained in the step (4-4) with the washed solid component obtained in the step (4-5);
[1] The method for producing a flavor oil according to claim 1.
[6] The method for producing a flavor oil according to any one of [1] to [5], further comprising a step of adding an emulsifier.
[7] A flavor oil obtained using the method for producing a flavor oil according to any one of [1] to [6].
[8] The flavor oil according to [7], wherein the absorbance at OD 420 nm when added to hot water of 90 ° C. or higher so that the content is 5% by mass is 0.4 or lower.
[9] An oil obtained after heating an edible oil and fat and one or more selected from vegetables and spices;
A flavor oil obtained by mixing a solid component obtained by washing a solid component obtained after heating an edible oil and fat and one or more selected from vegetables and spices with a hydrophilic solvent.

本発明の香味油の製造方法によれば、水系への色移りが低減された香味油を得ることができる。
該香味油の製造方法により得られた香味油は、水系への色移りが低減されたものであるため、スープ等の水系の液部を有する食品に用いた場合にも該液部へ色移りすることがなく、用いる食品の外観を損なうことがない。
According to the method for producing a flavor oil of the present invention, a flavor oil with reduced color transfer to an aqueous system can be obtained.
Since the flavor oil obtained by the method for producing the flavor oil has a reduced color transfer to the aqueous system, the color transfer to the liquid part is also possible when used in foods having an aqueous liquid part such as soup. And the appearance of the food used is not impaired.

本発明において、「香味油」とは、野菜や香辛料が有する風味を食用油脂に付加したものをいう。
本発明の香味油の製造方法(以下、単に「製造方法」ということがある。)は、食用油脂と野菜及び香辛料から選ばれる1種以上とを加熱した後に得られる油分と、食用油脂と野菜及び香辛料から選ばれる1種以上とを加熱した後の固形成分を、親水性溶媒によって洗浄した後に得られた固形成分と、を混合するものである。
すなわち、本発明の製造方法では、食用油脂と野菜及び香辛料から選ばれる1種以上とを加熱して得られた香味油のうち、固形成分を親水性溶媒によって洗浄した後に、前記香味油の油分と再度混合することを特徴とする。香味油の固形成分を親水性溶媒で洗浄することにより、水系への色移りの原因となる水溶性の成分を除去することができる。また、本発明の製造方法で得られた香味油は、食用油脂と野菜及び香辛料から選ばれる1種以上とを加熱することにより、野菜や香辛料に由来する甘い香りと、ローストによる香ばしい香りとをバランスよく兼ね備えた良好な風味となる。
In the present invention, “flavor oil” refers to a product obtained by adding the flavor of vegetables and spices to edible fats and oils.
The method for producing a flavor oil of the present invention (hereinafter sometimes simply referred to as “manufacturing method”) includes an oil obtained after heating an edible oil and fat and one or more selected from vegetables and spices, and an edible oil and vegetable. And a solid component obtained after washing the solid component after heating one or more selected from spices with a hydrophilic solvent.
That is, in the production method of the present invention, among flavor oils obtained by heating edible oils and fats and one or more selected from vegetables and spices, the solid components are washed with a hydrophilic solvent, and then the oil content of the flavor oils is obtained. And mixing again. By washing the solid component of the flavor oil with a hydrophilic solvent, the water-soluble component that causes color transfer to the aqueous system can be removed. In addition, the flavor oil obtained by the production method of the present invention heats edible fats and oils and at least one selected from vegetables and spices, thereby producing a sweet scent derived from vegetables and spices and a fragrant scent by roasting. Good flavor with a good balance.

本発明の製造方法では、まず、食用油脂と野菜及び香辛料から選ばれる1種以上とを加熱して香味油を製造する。
本発明において用いられる食用油脂としては、通常食品に用いられる油脂であれば特に限定されるものではなく、植物性油脂、動物性油脂、及びそれらの加工油脂のいずれであってもよい。また、加熱する際に液状となる油脂であればよく、液状油脂であってもよく、常温で固体である固形油脂を加熱溶融したものであってもよい。
植物性油脂としては、キャノーラ油を代表とする菜種油、大豆油、ゴマ油、ココナッツ油、コーン油、オリーブ油、綿実油、ベニバナ油、米油、ヒマワリ油、落花生を代表とするナッツ油等が挙げられる。植物油は、1種の植物原料のみから得られた油であってもよく、2種以上の植物原料から得られた油を混合した油であってもよい。また、植物油は、予め分離精製処理、脱酸処理、脱色処理等がなされたものであってもよい。このような植物油としては、脱酸、脱色等の処理がなされた白絞油、白絞油にさらにロウ分の除去処理を施したサラダ油が挙げられる。
動物性油脂としては、牛脂、ラード等が挙げられる。
加工油脂としては、ショートニング、バター、マーガリン等が挙げられる。
食用油脂は1種を単独で用いてもよく、2種以上を組み合わせて用いてもよい。
なかでも、本発明における食用油脂としては、食用油脂に由来する独特の香りが弱く、香味を付与しやすいことから、白絞油又はサラダ油が好ましい。
食用油脂の使用量は、野菜及び香辛料から選ばれる1種以上の1質量部に対して、1〜200質量部であることが好ましく、2〜5質量部であることがより好ましい。
In the production method of the present invention, first, flavor oil is produced by heating edible fats and oils and at least one selected from vegetables and spices.
The edible oil / fat used in the present invention is not particularly limited as long as it is an oil / fat usually used in foods, and may be any of vegetable oil / animal oil / fat and processed oil / fat thereof. Moreover, what is necessary is just fats and oils which become liquid at the time of heating, liquid oils and fats may be sufficient, and solid fats and oils which are solid at normal temperature may be heat-melted.
Examples of vegetable oils include rapeseed oil typified by canola oil, soybean oil, sesame oil, coconut oil, corn oil, olive oil, cottonseed oil, safflower oil, rice oil, sunflower oil, and nut oil typified by peanut. The vegetable oil may be an oil obtained from only one kind of plant material, or may be an oil obtained by mixing oils obtained from two or more kinds of plant materials. The vegetable oil may have been subjected to separation and purification treatment, deoxidation treatment, decolorization treatment and the like in advance. Examples of such vegetable oils include white squeezed oil that has been subjected to treatments such as deoxidation and decolorization, and salad oil obtained by subjecting white squeezed oil to a wax removal treatment.
Animal fats and oils include beef tallow and lard.
Examples of the processed fats and oils include shortening, butter, margarine and the like.
Edible fats and oils may be used alone or in combination of two or more.
Among them, white squeezed oil or salad oil is preferable as the edible oil / fat in the present invention because the unique fragrance derived from the edible oil / fat is weak and easily imparts a flavor.
It is preferable that it is 1-200 mass parts with respect to 1 mass part or more of 1 type chosen from vegetables and a spice, and, as for the usage-amount of edible fats and oils, it is more preferable that it is 2-5 mass parts.

本発明において用いられる野菜としては特に限定されるものではなく、所望の香味を有する野菜を目的に応じて適宜選択することができる。例えば、タマネギ、ニンニク、ネギ、ニラ、キャベツ、レタス、ホウレンソウ等の葉菜類;ショウガ、ゴボウ、ニンジン、ダイコン等の根菜類;タケノコ、アスパラ等の茎菜類;トウモロコシ、カボチャ、トマト、ピーマン、ブロッコリー、ナス等の果菜類等が挙げられる。これらの野菜は予め前処理を施されていてもよい。前処理としては例えば、細断する、粉砕する等の処理が挙げられる。
野菜は、1種を単独で用いてもよく、2種以上を組み合わせて用いてもよい。
The vegetable used in the present invention is not particularly limited, and a vegetable having a desired flavor can be appropriately selected according to the purpose. For example, leaf vegetables such as onion, garlic, leek, leek, cabbage, lettuce, spinach; root vegetables such as ginger, burdock, carrot, radish; stem vegetables such as bamboo shoot, asparagus; corn, pumpkin, tomato, pepper, broccoli Examples include fruit vegetables such as eggplant. These vegetables may be pretreated in advance. Examples of the pretreatment include chopping and pulverization.
A vegetable may be used individually by 1 type and may be used in combination of 2 or more type.

本発明において「香辛料」とは、香り、色、辛み、コクみ等を素材又は食品に付与することを目的とする植物由来の調味料である。例えば、アニス、オレガノ、カレーリーフ、グリーンペッパー、コショウ、クローブ、コリアンダー、サフラン、サンショウ、シナモン、タイム、唐辛子、マスタード等の単一の素材からなるもの;五香粉、ガラムマサラ、カレー粉、七味唐辛子、チリパウダー等の複数の素材からなるものが挙げられる。
香辛料は、1種を単独で用いてもよく、2種以上を組み合わせて用いてもよい。
また、野菜及び香辛料から選ばれる1種以上としては、少なくとも野菜又は香辛料のいずれかであればよく、野菜と香辛料とを併用してもよい。
なかでも、本発明における野菜及び香辛料から選ばれる1種以上としては、香味の力価が強い野菜であることが好ましく、タマネギ、ニンニク、ショウガ及びネギから選択される1種以上であることが好ましい。
In the present invention, the “spicy” is a plant-derived seasoning for the purpose of imparting a fragrance, color, spiciness, richness and the like to a material or food. For example, anise, oregano, curry leaf, green pepper, pepper, clove, coriander, saffron, cinnamon, thyme, chili, mustard, etc. And those made of a plurality of materials such as chili powder.
A spice may be used individually by 1 type, and may be used in combination of 2 or more type.
Moreover, as 1 or more types chosen from a vegetable and a spice, it should just be either a vegetable or a spice, and you may use a vegetable and a spice together.
Especially, as 1 or more types chosen from the vegetables and spices in this invention, it is preferable that it is a vegetable with strong titer of flavor, and it is preferable that they are 1 or more types selected from an onion, a garlic, ginger, and a leek. .

本発明の製造方法では、加熱時に食用油脂、野菜及び香辛料以外の副原料を用いてもよい。副原料としては例えば、食塩、糖類、醤油、味噌、出汁等の調味料;澱粉類;植物性タンパク質;肉、肉分解物等の動物性たん白質、増粘剤、膨張剤、品質改良剤、酸化防止剤、乳化剤等の添加剤等が挙げられる。   In the production method of the present invention, auxiliary ingredients other than edible oils and fats, vegetables and spices may be used during heating. Examples of auxiliary ingredients include seasonings such as salt, sugar, soy sauce, miso, and soup; starches; vegetable proteins; animal proteins such as meat and meat degradation products, thickeners, swelling agents, quality improvers, Examples include antioxidants, additives such as emulsifiers, and the like.

本発明において、食用油脂と、野菜及び香辛料から選ばれる1種以上とを加熱する方法は特に限定されるものではないが、例えば、食用油脂と野菜や香辛料と、必要に応じて用いる副原料との混合物を加熱することにより、食用油脂中で野菜や香辛料を油ちょうする方法;食用油脂のみを加熱し、所望の温度に達した後、野菜や香辛料と、必要に応じて用いる副原料とを添加してさらに加熱することにより、食用油脂中で野菜や香辛料を油ちょうする方法;食用油脂と野菜や香辛料と、必要に応じて用いる副原料とを加熱した状態で炒める方法、等が挙げられる。   In the present invention, the method of heating the edible oil and fat and one or more selected from vegetables and spices is not particularly limited, but for example, the edible oil and fat, vegetables and spices, and auxiliary materials used as necessary A method of heating vegetables and spices in edible fats and oils by heating the mixture, and after heating only the edible fats and oils and reaching the desired temperature, the vegetables and spices and auxiliary ingredients used as needed A method of adding vegetables and spices in edible oil and fat by adding and further heating; a method of frying edible oil and fat, vegetables and spices, and auxiliary ingredients used as necessary, and the like, etc. .

加熱温度は、90〜200℃であることが好ましく、120〜180℃がより好ましく、140〜170℃がさらに好ましい。上記下限値以上とすることにより、風味を強いものとすることができ、且つ、野菜や香辛料に由来する甘い香り及びローストによる香ばしい香りを食用油脂に良好に付与することができる。また、上記上限値以下とすることにより、高温による風味の劣化や、過剰なロースト感を抑制することができる。
加熱は、上記加熱温度まで徐々に昇温した後、所望の温度に達した時点で加熱を終了してもよく、上記加熱温度で一定時間保持して加熱してもよい。なかでも、風味の力価を強めることができるため、上記加熱温度にて一定時間保持することが好ましい。保持時間(加熱時間)としては、1〜600分間であることが好ましく、10〜360分間であることがより好ましく、30〜180分間であることがさらに好ましく、60〜120分間であることが特に好ましい。
The heating temperature is preferably 90 to 200 ° C, more preferably 120 to 180 ° C, and further preferably 140 to 170 ° C. By setting it as the said lower limit or more, a flavor can be made strong and the sweet fragrance derived from vegetables and spices and the fragrant fragrance by roast can be favorably provided to edible fats and oils. Moreover, the deterioration of the flavor by high temperature and an excessive roast feeling can be suppressed by setting it as the said upper limit or less.
The heating may be gradually raised to the above heating temperature, and then terminated when the desired temperature is reached, or may be held for a certain period of time at the above heating temperature. Especially, since the titer of flavor can be strengthened, it is preferable to hold at the heating temperature for a certain period of time. The holding time (heating time) is preferably 1 to 600 minutes, more preferably 10 to 360 minutes, further preferably 30 to 180 minutes, and particularly preferably 60 to 120 minutes. preferable.

本発明の製造方法においては、加熱処理により製造された香味油の固形成分を、親水性溶媒で洗浄した後に、再度当該香味油の油分と混合する。香味油の固形成分は、主に加熱に用いた野菜や香辛料からなる。加熱処理により香味油を製造し、当該香味油中の固形成分を洗浄し、再び当該香味油の油分と混合する方法は特に限定されない。例えば、本発明の製造方法は、以下の第一〜第四の方法により実施することができる。但し、本発明の製造方法が、これらの方法に限定されないことは言うまでもない。   In the production method of the present invention, the solid component of the flavor oil produced by the heat treatment is washed with a hydrophilic solvent and then mixed with the oil content of the flavor oil again. The solid component of the flavor oil is mainly composed of vegetables and spices used for heating. There is no particular limitation on the method of producing the flavor oil by heat treatment, washing the solid components in the flavor oil, and mixing again with the oil content of the flavor oil. For example, the production method of the present invention can be carried out by the following first to fourth methods. However, it goes without saying that the production method of the present invention is not limited to these methods.

(第一の方法)
本発明の製造方法の第一の方法は、
(1−1)食用油脂と、野菜及び香辛料から選ばれる1種以上とを加熱して香味油を得る工程と、
(1−2)前記香味油を、油分と固形成分とに分離する工程と、
(1−3)前記固形成分を親水性溶媒によって洗浄する工程と、
(1−4)前記工程(1−2)で得られた油分と、前記工程(1−3)で得られた洗浄後の固形成分とを混合する工程と、
を有する。
以下、各工程を「工程(1−1)」等という。後述する他の方法においても同様である。
(First method)
The first method of the production method of the present invention is:
(1-1) A step of heating a cooking oil and fat and one or more selected from vegetables and spices to obtain a flavor oil;
(1-2) separating the flavor oil into an oil and a solid component;
(1-3) washing the solid component with a hydrophilic solvent;
(1-4) A step of mixing the oil obtained in the step (1-2) with the washed solid component obtained in the step (1-3);
Have
Hereinafter, each process is referred to as “process (1-1)” or the like. The same applies to other methods described later.

[(工程(1−1)]
本方法では、まず工程(1−1)として、食用油脂と、野菜及び香辛料から選ばれる1種以上とを加熱して香味油を得る。
工程(1−1)における食用油脂、野菜及び香辛料から選ばれる1種以上、加熱方法は前記同様である。
[(Step (1-1)]
In this method, first, as step (1-1), an edible oil and fat and one or more selected from vegetables and spices are heated to obtain a flavor oil.
One or more types selected from edible oils and fats, vegetables and spices in step (1-1), the heating method is the same as described above.

[(工程(1−2)]
次いで、工程(1−2)において、工程(1−1)で得られた香味油を、油分と固形成分とに分離する。
油分と固形成分とを分離する方法としては特に限定されるものではなく、ろ過、遠心分離等の常法により行うことができる。例えば、80〜200Mesh程度の篩用金網等を用いることにより、油分と固形成分とを分離することができる。
また、工程(1−1)で得られた香味油は、加熱中に野菜や香辛料から発生した微量の水分を含有する場合がある。該水分は、工程(1−2)において油分及び固形成分とは別に除去してもよく、油分が微量の水分を含有していてもよい。
[(Step (1-2)]
Next, in step (1-2), the flavor oil obtained in step (1-1) is separated into an oil component and a solid component.
It does not specifically limit as a method of isolate | separating an oil component and a solid component, It can carry out by conventional methods, such as filtration and centrifugation. For example, an oil component and a solid component can be separated by using a sieve wire mesh of about 80 to 200 mesh.
Moreover, the flavor oil obtained at the process (1-1) may contain the trace amount water | moisture content which generate | occur | produced from the vegetable and the spice during heating. The moisture may be removed separately from the oil and solid components in the step (1-2), and the oil may contain a trace amount of moisture.

[(工程(1−3)]
次に、工程(1−2)で得られた固形成分を、親水性溶媒によって洗浄する。本発明において「洗浄」とは、固形成分と親水性溶媒とを一過的に接触させ、固形成分に付着した成分を親水性溶媒で洗い流す方法のみならず、固形成分を親水性溶媒に浸漬した後、親水性溶媒に由来する水層を除去する方法も含む概念である。後者の場合、親水性溶媒に接触させ、必要に応じて攪拌や静置を行うことにより、固形成分に付着した、又は固形成分中に存在する水溶性成分が親水性溶媒中へ移行する。
接触させる方法は特に限定されるものではなく、例えば固形成分を入れた容器中に親水性溶媒を注ぐ、親水性溶媒中に固形成分を投入する、等の方法が挙げられる。
[(Step (1-3)]
Next, the solid component obtained in the step (1-2) is washed with a hydrophilic solvent. In the present invention, “washing” means not only a method in which a solid component and a hydrophilic solvent are brought into contact with each other temporarily, and the component adhering to the solid component is washed away with the hydrophilic solvent, but the solid component is immersed in the hydrophilic solvent. The concept also includes a method for removing the aqueous layer derived from the hydrophilic solvent. In the latter case, the water-soluble component adhering to the solid component or existing in the solid component is transferred into the hydrophilic solvent by bringing into contact with the hydrophilic solvent and stirring or standing as necessary.
The method of contacting is not particularly limited, and examples thereof include a method in which a hydrophilic solvent is poured into a container containing a solid component, and a solid component is poured into a hydrophilic solvent.

工程(1−3)における親水性溶媒は、親水性を有し、且つ食品に使用できる溶媒であれば特に限定されるものではない。親水性溶媒としては例えば、水、エタノール、水とエタノールとの混合液等が挙げられる。水とエタノールとを混合して用いる場合、親水性溶媒全量に対するエタノールの含有割合は、10〜90質量%が好ましく、50〜60質量%が特に好ましい。
これらの親水性溶媒は常温で用いてもよく、加温して用いてもよい。具体的には、親水性溶媒として水を用いる場合、常温の水であってもよく、50〜90℃のお湯であってもよい。
親水性溶媒の使用量は、固形成分に十分に接触しうる量であれば特に限定されるものではないが、固形成分1質量部に対して、1〜20質量部の親水性溶媒を用いることが好ましく、1〜5質量部がより好ましい。
The hydrophilic solvent in the step (1-3) is not particularly limited as long as it is hydrophilic and can be used for food. Examples of the hydrophilic solvent include water, ethanol, a mixed solution of water and ethanol, and the like. When mixing and using water and ethanol, 10 to 90 mass% is preferable and, as for the content rate of ethanol with respect to the hydrophilic solvent whole quantity, 50 to 60 mass% is especially preferable.
These hydrophilic solvents may be used at normal temperature or may be used after heating. Specifically, when water is used as the hydrophilic solvent, it may be water at room temperature or hot water of 50 to 90 ° C.
The amount of the hydrophilic solvent used is not particularly limited as long as the amount can sufficiently contact the solid component, but 1 to 20 parts by mass of the hydrophilic solvent is used with respect to 1 part by mass of the solid component. Is preferable, and 1 to 5 parts by mass is more preferable.

親水性溶媒に接触させた後の固形成分と、水層とを分離する方法は特に限定されるものではない。水層は通常、親水性溶媒と、固形成分に由来する水溶性成分とからなるものであって、該水層を固形成分から分離することによって該水溶性成分が固形成分から除去される。すなわち、工程(1−3)を経ることにより、固形成分が洗浄される結果、水系への色移りの低減された香味油を製造することができる。
固形成分と水層とを分離する方法は特に限定されるものではなく、ろ過、遠心分離等の常法により行うことができる。遠心分離を用いる場合であれば、公知の遠心分離機を用いて、500〜10000rpmで1〜120秒間の遠心分離を行うことにより、固形成分と水層とを分離することができる。
The method for separating the solid component after contact with the hydrophilic solvent and the aqueous layer is not particularly limited. The aqueous layer is usually composed of a hydrophilic solvent and a water-soluble component derived from the solid component, and the water-soluble component is removed from the solid component by separating the aqueous layer from the solid component. That is, by passing through a process (1-3), the solid component is wash | cleaned, As a result, the flavor oil by which the color transfer to an aqueous system was reduced can be manufactured.
The method for separating the solid component and the aqueous layer is not particularly limited, and can be performed by a conventional method such as filtration or centrifugation. If centrifugation is used, the solid component and the aqueous layer can be separated by performing centrifugation at 500 to 10,000 rpm for 1 to 120 seconds using a known centrifuge.

本方法では、工程(1−3)の固形成分の洗浄を複数回、例えば1〜5回行ってもよい。すなわち、洗浄を2回行う場合であれば、工程(1−3)を行った後に、工程(1−3)で得られた洗浄後の固形成分をさらに親水性溶媒に接触させ、その後、接触させた後の固形成分と、水層とを分離してもよい。固形成分の洗浄を複数回行うことにより、固形分由来の水溶性成分をより確実に除去することが可能となり、水系への色移りをさらに低減することができる。   In this method, the washing of the solid component in the step (1-3) may be performed a plurality of times, for example, 1 to 5 times. That is, if cleaning is performed twice, after performing step (1-3), the washed solid component obtained in step (1-3) is further contacted with a hydrophilic solvent, and then contacted. You may isolate | separate the solid component after making it make and an aqueous layer. By washing the solid component a plurality of times, the water-soluble component derived from the solid content can be more reliably removed, and the color transfer to the aqueous system can be further reduced.

工程(1−3)を複数回行う場合、該複数回の工程(1−3)で用いる親水性溶媒の種類は同じであってもよく、異なっていてもよい。また、2回目以降の工程(1−3)で用いる親水性溶媒としては、未使用の水、エタノール、水とエタノールとの混合液等を用いてもよく、前段の工程(1−3)(例えば1回目の工程(1−3))において洗浄に用いられ、分離された水層を用いてもよい。親水性溶媒を繰り返し用いることにより、親水性溶媒の使用量及び工程のコストを低減できる。   When performing a process (1-3) in multiple times, the kind of hydrophilic solvent used by this multiple times of process (1-3) may be the same, and may differ. In addition, as the hydrophilic solvent used in the second and subsequent steps (1-3), unused water, ethanol, a mixed solution of water and ethanol, or the like may be used, and the previous step (1-3) ( For example, a separated aqueous layer used for washing in the first step (1-3)) may be used. By repeatedly using the hydrophilic solvent, the amount of the hydrophilic solvent used and the cost of the process can be reduced.

[工程(1−4)]
最後に、工程(1−2)において分離された油分と、工程(1−3)を単回又は複数回行うことにより分離された洗浄後の固形成分とを混合することにより、色移りの低減された香味油を製造することができる。
[Step (1-4)]
Finally, the color transfer is reduced by mixing the oil component separated in step (1-2) and the washed solid component separated by performing step (1-3) once or multiple times. Flavored oil can be produced.

(第二の方法)
本発明の製造方法の第二の方法は、
(2−1)食用油脂と、野菜及び香辛料から選ばれる1種以上とを加熱して香味油を得る工程と、
(2−2)前記香味油を親水性溶媒と混合させる工程と、
(2−3)混合させた後の香味油を、油分と固形成分と水層とに分離する工程と、
(2−4)前記油分と、前記固形成分とを混合する工程と、
を有する。
(Second method)
The second method of the production method of the present invention is:
(2-1) A step of heating the edible oil and fat and one or more selected from vegetables and spices to obtain a flavor oil;
(2-2) mixing the flavor oil with a hydrophilic solvent;
(2-3) separating the flavor oil after mixing into an oil, a solid component, and an aqueous layer;
(2-4) mixing the oil and the solid component;
Have

[工程(2−1)]
本方法における工程(2−1)は、前記工程(1−1)と同様である。
[Step (2-1)]
The step (2-1) in this method is the same as the step (1-1).

[工程(2−2)]
本方法では、工程(2−1)で得られた香味油を、親水性溶媒と混合させる。親水性溶媒と混合させ、必要に応じて攪拌や静置を行うことにより、香味油中に存在する(特に、固形成分に付着して存在する、又は固形成分中に存在する)水溶性成分が親水性溶媒中へ移行する。
工程(2−1)における親水性溶媒としては、工程(1−3)の説明において上述したものと同様である。
親水性溶媒の使用量は、香味油と十分に混合しうる量であれば特に限定されるものではないが、香味油1質量部に対して、0.5〜10質量部の親水性溶媒を用いることが好ましく、1〜3質量部がより好ましい。また、親水性溶媒の使用量は、香味油中の固形成分1質量部に対して、1〜20質量部の親水性溶媒を用いることが好ましく、1〜5質量部がより好ましい。
[Step (2-2)]
In this method, the flavor oil obtained in the step (2-1) is mixed with a hydrophilic solvent. By mixing with a hydrophilic solvent and stirring or standing as necessary, water-soluble components present in the flavor oil (particularly, attached to the solid component or present in the solid component) Move into a hydrophilic solvent.
The hydrophilic solvent in the step (2-1) is the same as that described above in the description of the step (1-3).
Although the usage-amount of a hydrophilic solvent will not be specifically limited if it is the quantity which can be fully mixed with flavor oil, 0.5-10 mass parts hydrophilic solvent is added with respect to 1 mass part of flavor oil. It is preferable to use 1 to 3 parts by mass. Moreover, it is preferable to use 1-20 mass parts hydrophilic solvent with respect to 1 mass part of solid components in flavor oil, and, as for the usage-amount of a hydrophilic solvent, 1-5 mass parts is more preferable.

[工程(2−3)]
次いで、工程(2−2)において親水性溶媒と混合させた香味油、すなわち親水性溶媒及び香味油を有する液を、油分と固形成分と水層とに分離する。香味油中の水溶性成分が油分及び固形成分から除去されることにより、水系への色移りの低減された香味油を製造することができる。
油分と固形成分と水層とを分離する方法は特に限定されるものではない。例えば、ろ過、遠心分離等の常法により、固形成分と、油分及び水層からなる液体成分とを分離した後、さらに遠心分離等を行うことによって、油分と水層とを分離してもよく;遠心分離等を用い、条件を適切なものとすることにより、油分と固形成分と水層とを一段階で分離してもよい。前者の方法であれば、固形成分と液体成分との分離は上述した工程(1−2)と同様に行うことができ、油分と水層との分離は公知の遠心分離機を用いて、1000〜10000rpmで1〜120秒間の遠心分離を行うことにより行うことができる。
[Step (2-3)]
Next, the flavor oil mixed with the hydrophilic solvent in the step (2-2), that is, the liquid having the hydrophilic solvent and the flavor oil is separated into an oil component, a solid component, and an aqueous layer. By removing the water-soluble component in the flavor oil from the oil and solid components, a flavor oil with reduced color transfer to the aqueous system can be produced.
The method for separating the oil, the solid component and the aqueous layer is not particularly limited. For example, the oil component and the aqueous layer may be separated by separating the solid component and the liquid component composed of the oil component and the aqueous layer by a conventional method such as filtration and centrifugation, and further performing centrifugation or the like. An oil, a solid component, and an aqueous layer may be separated in one step by using centrifugal separation or the like to make the conditions appropriate. In the former method, the solid component and the liquid component can be separated in the same manner as in the above-described step (1-2), and the oil component and the aqueous layer can be separated by using a known centrifuge. It can be performed by centrifuging at 10000 rpm for 1 to 120 seconds.

[工程(2−4)]
最後に、工程(2−3)において分離された油分と、固形成分とを混合することにより、色移りの低減された香味油を製造することができる。
[Step (2-4)]
Finally, by mixing the oil component separated in the step (2-3) and the solid component, a flavor oil with reduced color transfer can be produced.

(第三の方法)
本発明の製造方法の第三の方法は、
(3−1)食用油脂と、野菜及び香辛料から選ばれる1種以上とを加熱して香味油を得る工程と、
(3−2)前記香味油を、親水性溶媒と混合させる工程と、
(3−3)混合させた後の香味油を、油分と固形成分と水層とに分離する工程と、
(3−4)前記固形成分を、親水性溶媒によって洗浄する工程と、
(3−5)前記工程(3−3)で得られた油分と、前記工程(3−4)で得られた洗浄後の固形成分とを混合する工程と、
を有する。
(Third method)
The third method of the production method of the present invention is:
(3-1) A step of heating a cooking oil and fat and one or more selected from vegetables and spices to obtain a flavor oil;
(3-2) mixing the flavor oil with a hydrophilic solvent;
(3-3) separating the flavor oil after mixing into an oil, a solid component, and an aqueous layer;
(3-4) washing the solid component with a hydrophilic solvent;
(3-5) a step of mixing the oil obtained in the step (3-3) and the solid component after washing obtained in the step (3-4);
Have

[工程(3−1)〜(3−3)]
本方法における工程(3−1)〜(3−3)は、第二の方法の工程(2−1)〜(2−3)と同様である。
[Steps (3-1) to (3-3)]
Steps (3-1) to (3-3) in this method are the same as steps (2-1) to (2-3) in the second method.

[工程(3−4)]
工程(3−4)では、工程(3−3)で得られた固形成分を、親水性溶媒によって洗浄する。親水性溶媒に接触させ、必要に応じて攪拌や静置を行うことにより、工程(3−3)後に残存した水溶性成分をさらに親水性溶媒中へ移行させることができる。
工程(3−4)における洗浄方法及び親水性溶媒としては、工程(1−3)と同様である。
工程(3−4)において用いる親水性溶媒と、前記工程(3−2)において用いる親水性溶媒とは同じであっても異なっていてもよい。また、工程(3−4)では、工程(3−3)において分離された水層を親水性溶媒として用いてもよい。親水性溶媒を繰り返し用いることにより、親水性溶媒の使用量及び工程のコストを低減できる。
本工程により再度固形成分が洗浄されるため、水系への色移りがさらに低減された香味油を製造することができる。
本方法では、第一の方法と同様に、工程(3−4)の固形成分の洗浄を複数回、例えば1〜5回行ってもよい。
[Step (3-4)]
In step (3-4), the solid component obtained in step (3-3) is washed with a hydrophilic solvent. The water-soluble component remaining after the step (3-3) can be further transferred into the hydrophilic solvent by bringing it into contact with the hydrophilic solvent and stirring or standing as necessary.
The washing method and the hydrophilic solvent in the step (3-4) are the same as those in the step (1-3).
The hydrophilic solvent used in the step (3-4) and the hydrophilic solvent used in the step (3-2) may be the same or different. In step (3-4), the aqueous layer separated in step (3-3) may be used as a hydrophilic solvent. By repeatedly using the hydrophilic solvent, the amount of the hydrophilic solvent used and the cost of the process can be reduced.
Since the solid component is washed again by this step, a flavor oil with further reduced color transfer to the aqueous system can be produced.
In this method, similarly to the first method, washing of the solid component in the step (3-4) may be performed a plurality of times, for example, 1 to 5 times.

[工程(3−5)]
最後に、工程(3−3)において分離された油分と、工程(3−4)を単回又は複数回行って得られた洗浄後の固形成分とを混合することにより、色移りの低減された香味油を製造することができる。
[Step (3-5)]
Finally, the color transfer is reduced by mixing the oil separated in the step (3-3) and the washed solid component obtained by performing the step (3-4) once or plural times. Flavor oil can be produced.

(第四の方法)
本発明の製造方法の第四の方法は、
(4−1)食用油脂と、野菜及び香辛料から選ばれる1種以上とを加熱して香味油を得る工程と、
(4−2)前記香味油を、油分と固形成分とに分離する工程と、
(4−3)前記油分を親水性溶媒と混合させる工程と、
(4−4)前記工程(4−3)で得られた混合液中の油分と、水層とを分離する工程と、
(4−5)前記固形成分を親水性溶媒によって洗浄する工程と、
(4−6)前記工程(4−4)で得られた油分と、前記工程(4−5)で得られた洗浄後の固形成分とを混合する工程と、
を有する。
(Fourth method)
The fourth method of the production method of the present invention is:
(4-1) A step of heating the edible oil and fat and at least one selected from vegetables and spices to obtain a flavor oil;
(4-2) separating the flavor oil into an oil and a solid component;
(4-3) mixing the oil with a hydrophilic solvent;
(4-4) a step of separating the oil in the mixed liquid obtained in the step (4-3) and the aqueous layer;
(4-5) washing the solid component with a hydrophilic solvent;
(4-6) a step of mixing the oil obtained in the step (4-4) with the washed solid component obtained in the step (4-5);
Have

[工程(4−1)〜(4−2)]
本方法における工程(4−1)〜(4−2)は、第一の方法の工程(1−1)〜(1−2)と同様である。
[Steps (4-1) to (4-2)]
Steps (4-1) to (4-2) in this method are the same as steps (1-1) to (1-2) in the first method.

[工程(4−3)]
本方法では、工程(4−2)で得られた油分を、親水性溶媒と混合させる。親水性溶媒に混合させ、必要に応じて攪拌や静置を行うことにより、油分中に分散した水溶性成分を親水性溶媒中へ移行させることができる。
工程(4−3)における混合させる方法及び親水性溶媒としては、工程(2−2)と同様である。
[Step (4-3)]
In this method, the oil obtained in step (4-2) is mixed with a hydrophilic solvent. The water-soluble component dispersed in the oil can be transferred into the hydrophilic solvent by mixing with a hydrophilic solvent and stirring or standing as necessary.
The method of mixing in step (4-3) and the hydrophilic solvent are the same as in step (2-2).

[工程(4−4)]
工程(4−4)では、前記工程(4−3)で得られた混合液中の油分と、水層とを分離する。工程(4−3)及び工程(4−4)を経ることにより、油分が洗浄され、水系への色移りの低減された香味油を製造することができる。
本方法では、工程(4−3)及び(4−4)の油分の洗浄を複数回、例えば1〜5回行ってもよい。複数回の洗浄は、洗浄対象が油分である以外は第一の方法と同様である。
[Step (4-4)]
In the step (4-4), the oil component in the mixed solution obtained in the step (4-3) and the aqueous layer are separated. By passing through a process (4-3) and a process (4-4), an oil component is wash | cleaned and the flavor oil by which the color transfer to an aqueous system was reduced can be manufactured.
In this method, the washing of the oil in the steps (4-3) and (4-4) may be performed a plurality of times, for example, 1 to 5 times. The multiple cleaning is the same as the first method except that the object to be cleaned is oil.

[工程(4−5)]
工程(4−5)は、第一の方法の工程(1−3)と同様である。工程(4−5)を経ることにより、固形成分が洗浄され、水系への色移りの低減された香味油を製造することができる。
工程(4−5)における親水性溶媒としては、第一の方法と同様のものを用いることができる。工程(4−5)において用いる親水性溶媒と、前記工程(4−3)において用いる親水性溶媒とは同じであっても異なっていてもよい。また、工程(4−5)では、工程(4−4)において油分と分離された水層を親水性溶媒として用いてもよい。親水性溶媒を繰り返し用いることにより、親水性溶媒の使用量及び工程のコストを低減できる。
本方法では、第一の方法と同様に、工程(4−5)の固形成分の洗浄を複数回、例えば1〜5回行ってもよい。
[Step (4-5)]
Step (4-5) is the same as step (1-3) of the first method. By passing through a process (4-5), a solid component is wash | cleaned and the flavor oil by which the color transfer to an aqueous system was reduced can be manufactured.
As the hydrophilic solvent in the step (4-5), the same solvent as in the first method can be used. The hydrophilic solvent used in the step (4-5) and the hydrophilic solvent used in the step (4-3) may be the same or different. In step (4-5), the water layer separated from the oil component in step (4-4) may be used as the hydrophilic solvent. By repeatedly using the hydrophilic solvent, the amount of the hydrophilic solvent used and the cost of the process can be reduced.
In this method, similarly to the first method, washing of the solid component in the step (4-5) may be performed a plurality of times, for example, 1 to 5 times.

[工程(4−6)]
最後に、工程(4−4)を単回又は複数回行って得られた油分と、工程(4−5)を単回又は複数回行って得られた洗浄後の固形成分とを混合することにより、色移りの低減された香味油を製造することができる。
[Step (4-6)]
Finally, mixing the oil obtained by performing step (4-4) once or a plurality of times and the solid component after washing obtained by performing step (4-5) once or a plurality of times. Thus, a flavor oil with reduced color transfer can be produced.

第一〜第四の方法により得られた香味油は、そのまま食品に用いられてもよく、他の工程を経た後に用いられてもよい。具体的には、添加剤を添加する工程、ろ過する工程、加熱殺菌する工程等が挙げられる。
添加剤としては、乳化剤、酸化防止剤、品質改良剤、保存料、着色料、香料等が挙げられる。なかでも乳化剤を添加することにより、水系に香味油を添加した場合に香味油の油滴が小さくなり、水系が格納された容器の内壁に香味油が多量に付着することを防止できるため好ましい。
ろ過はフィルターや篩を用いて常法により行うことができる。
加熱殺菌は、公知の装置を用いて、80〜150℃で0.5〜60分間加熱することにより行うことができる。
The flavor oil obtained by the 1st-4th method may be used for food as it is, and may be used after passing through other processes. Specifically, the process of adding an additive, the process of filtering, the process of heat-sterilizing, etc. are mentioned.
Examples of additives include emulsifiers, antioxidants, quality improvers, preservatives, colorants, and fragrances. In particular, it is preferable to add an emulsifier because when the flavor oil is added to the aqueous system, the oil droplets of the flavor oil become small and a large amount of flavor oil can be prevented from adhering to the inner wall of the container in which the aqueous system is stored.
Filtration can be performed by a conventional method using a filter or a sieve.
The heat sterilization can be performed by heating at 80 to 150 ° C. for 0.5 to 60 minutes using a known apparatus.

上記本発明の製造方法により得られる香味油は、水系への色移りが低減されるものであるため、水系の液体部への色移りが敬遠される食品において好適に用いることができる。具体的には、本発明の製造方法によって製造される香味油は、含有量が5質量%となるように90℃以上のお湯に添加した場合のOD420nmの吸光度が0.4以下、好ましくは0.35以下、より好ましくは0.3以下、さらに好ましくは0.25以下となる。吸光度は常法により測定することができる。   The flavor oil obtained by the production method of the present invention has a reduced color transfer to the aqueous system, and therefore can be suitably used in foods where the color transfer to the aqueous liquid part is avoided. Specifically, the flavor oil produced by the production method of the present invention has an absorbance at OD 420 nm of 0.4 or less, preferably 0 when added to hot water of 90 ° C. or higher so that the content is 5% by mass. .35 or less, more preferably 0.3 or less, and still more preferably 0.25 or less. Absorbance can be measured by conventional methods.

次に実施例を示して本発明をさらに詳細に説明するが、本発明は以下の実施例に限定されるものではない。表1〜3中、「EtOH」はエタノールを意味する。   EXAMPLES Next, although an Example is shown and this invention is demonstrated further in detail, this invention is not limited to a following example. In Tables 1 to 3, “EtOH” means ethanol.

[比較製造例1]
サラダ油132g及びゴマ油132g、並びに予め細断したニンニク30g、ショウガ5g、及びネギ2gを、表1記載の温度において、表1記載の時間加熱した後冷却し、香味油を製造した。
得られた香味油を、含有量が5質量%となるように90℃のお湯に添加し、OD420nmの吸光度を測定して色移りの評価を行った。結果を表1に示す。
[Comparative Production Example 1]
132 g of salad oil, 132 g of sesame oil, and 30 g of chopped garlic, 5 g of ginger, and 2 g of leeks were heated at the temperatures shown in Table 1 for the time shown in Table 1 and then cooled to produce flavor oil.
The obtained flavor oil was added to hot water of 90 ° C. so that the content was 5% by mass, and the absorbance at OD 420 nm was measured to evaluate the color transfer. The results are shown in Table 1.

[製造例1〜5;第一の方法]
表1に示す加熱条件とした以外は、上記比較製造例1と同様にして香味油を製造した後、得られた加熱後の香味油を、油分と固形成分とに固液分離した。
次いで、回収された固形成分を表1中に示す溶媒に接触させた後、接触させた固形成分と水層とに分離して、固形成分の洗浄を行った。製造例2及び4は、固形成分の洗浄を2回行った。
その後、加熱後に分離した油分と、洗浄後の固形成分とを混合し、香味油を製造した。得られた各例の香味油について、比較製造例1と同様に吸光度を測定した結果、及び比較製造例1の吸光度との差を表1に示す。
[Production Examples 1 to 5; First method]
Except having set it as the heating conditions shown in Table 1, after manufacturing flavor oil like the said comparative manufacture example 1, the flavor oil after the obtained heating was solid-liquid-separated into the oil component and the solid component.
Next, the recovered solid component was brought into contact with the solvent shown in Table 1, and then separated into a contacted solid component and an aqueous layer, and the solid component was washed. In Production Examples 2 and 4, the solid component was washed twice.
Then, the oil component isolate | separated after a heating and the solid component after washing | cleaning were mixed, and flavor oil was manufactured. Table 1 shows the results of measuring the absorbance of each of the obtained flavor oils in the same manner as in Comparative Production Example 1 and the difference from the absorbance in Comparative Production Example 1.

[製造例6〜8;第二の方法]
表2に示す加熱条件とした以外は、上記比較製造例1と同様にして香味油を製造した後、該香味油を表2中に示す溶媒と混合させ、その後油分と固形成分と水層とに分離して、香味油全体の洗浄を行った。
その後、分離された油分と固形成分とを混合し、香味油を製造した。得られた各例の香味油について、比較製造例1と同様に吸光度を測定した結果、及び比較製造例1の吸光度との差を表2に示す。
[Production Examples 6 to 8; Second method]
Except having set it as the heating conditions shown in Table 2, after manufacturing flavor oil like the said comparative manufacture example 1, this flavor oil is mixed with the solvent shown in Table 2, and an oil component, a solid component, and an aqueous layer after that The whole flavor oil was washed.
Thereafter, the separated oil and the solid component were mixed to produce a flavor oil. Table 2 shows the results of measuring the absorbance of each of the obtained flavor oils in the same manner as in Comparative Production Example 1 and the difference from the absorbance in Comparative Production Example 1.

[製造例9〜13;第三の方法]
表2に示す加熱条件とした以外は、上記比較製造例1と同様にして香味油を製造した後、該香味油を表2中に示す(1)の溶媒と混合し、その後油分と固形成分と水層とに分離して、香味油全体の洗浄を行った。
次いで、回収された固形成分を表2中に示す(2)の溶媒に接触させた後、接触させた固形成分と水層とに分離して、固形成分の洗浄を行った。
その後、分離した油分と、固形成分とを混合し、香味油を製造した。得られた各例の香味油について、比較製造例1と同様に吸光度を測定した結果、及び比較製造例1の吸光度との差を表2に示す。
[Production Examples 9 to 13; Third Method]
Except having set it as the heating conditions shown in Table 2, after manufacturing a flavor oil like the said comparative manufacture example 1, this flavor oil is mixed with the solvent of (1) shown in Table 2, and an oil component and a solid component after that And the water layer were separated, and the entire flavor oil was washed.
Next, the recovered solid component was brought into contact with the solvent (2) shown in Table 2, and then separated into a contacted solid component and an aqueous layer, and the solid component was washed.
Thereafter, the separated oil and the solid component were mixed to produce a flavor oil. Table 2 shows the results of measuring the absorbance of each of the obtained flavor oils in the same manner as in Comparative Production Example 1 and the difference from the absorbance in Comparative Production Example 1.

[製造例14〜17;第四の方法]
表3に示す加熱条件とした以外は、上記比較製造例1と同様にして香味油を製造した後、得られた加熱後の香味油を、油分と固形成分とに固液分離した。
次いで、回収された油分を表3中に示す(1)の溶媒と混合させ、その後油分と水層とに分離して、油分の洗浄を行った。
その後、回収された固形成分を表3中に示す(2)の溶媒に接触させた後、接触させた固形成分と水層とに分離して、固形成分の洗浄を行った。製造例17は、油分洗浄後の水層の液を固形成分洗浄液とした。
最後に、洗浄後の油分と固形成分とを混合し、香味油を製造した。得られた各例の香味油について、比較製造例1と同様に吸光度を測定した結果、及び比較製造例1の吸光度との差を表3に示す。
[Production Examples 14 to 17; Fourth Method]
Except having set it as the heating conditions shown in Table 3, after manufacturing flavor oil like the said comparative manufacture example 1, the obtained flavor oil after the heating was solid-liquid-separated into the oil component and the solid component.
Next, the recovered oil was mixed with the solvent (1) shown in Table 3, and then separated into an oil and an aqueous layer, and the oil was washed.
Then, after making the collect | recovered solid component contact the solvent of (2) shown in Table 3, it isolate | separated into the contacted solid component and water layer, and wash | cleaned the solid component. In Production Example 17, the aqueous layer liquid after oil cleaning was used as a solid component cleaning liquid.
Finally, the washed oil and solid components were mixed to produce a flavor oil. About the obtained flavor oil of each case, the result of having measured the light absorbency similarly to the comparative manufacture example 1 and the difference with the light absorbency of the comparative manufacture example 1 are shown in Table 3.

Figure 2013201908
Figure 2013201908

Figure 2013201908
Figure 2013201908

Figure 2013201908
Figure 2013201908

上記の結果から、本発明の製造方法により製造された製造例1〜17の香味油は、比較製造例1の香味油に比して、水系への色移りが低減されていることが確認できた。   From the above results, it can be confirmed that the flavor oils of Production Examples 1 to 17 produced by the production method of the present invention have reduced color transfer to the aqueous system as compared with the flavor oil of Comparative Production Example 1. It was.

本発明の香味油の製造方法は、食品製造分野で好適に利用可能である。   The method for producing a flavor oil of the present invention can be suitably used in the field of food production.

Claims (9)

食用油脂と、野菜及び香辛料から選ばれる1種以上とを加熱した後に得られる油分と、
食用油脂と、野菜及び香辛料から選ばれる1種以上とを加熱した後の固形成分を、親水性溶媒によって洗浄した後に得られた固形成分と、
を混合することを特徴とする香味油の製造方法。
An oil obtained after heating an edible oil and fat and one or more selected from vegetables and spices;
A solid component obtained after washing the edible oil and fat and one or more selected from vegetables and spices with a hydrophilic solvent;
A method for producing a flavor oil, comprising mixing
(1−1)食用油脂と、野菜及び香辛料から選ばれる1種以上とを加熱して香味油を得る工程と、
(1−2)前記香味油を、油分と固形成分とに分離する工程と、
(1−3)前記固形成分を親水性溶媒によって洗浄する工程と、
(1−4)前記工程(1−2)で得られた油分と、前記工程(1−3)で得られた洗浄後の固形成分とを混合する工程と、
を有する請求項1に記載の香味油の製造方法。
(1-1) A step of heating a cooking oil and fat and one or more selected from vegetables and spices to obtain a flavor oil;
(1-2) separating the flavor oil into an oil and a solid component;
(1-3) washing the solid component with a hydrophilic solvent;
(1-4) A step of mixing the oil obtained in the step (1-2) with the washed solid component obtained in the step (1-3);
The manufacturing method of the flavor oil of Claim 1 which has this.
(2−1)食用油脂と、野菜及び香辛料から選ばれる1種以上とを加熱して香味油を得る工程と、
(2−2)前記香味油を親水性溶媒と混合させる工程と、
(2−3)混合させた後の香味油を、油分と固形成分と水層とに分離する工程と、
(2−4)前記油分と、前記固形成分とを混合する工程と、
を有する請求項1に記載の香味油の製造方法。
(2-1) A step of heating the edible oil and fat and one or more selected from vegetables and spices to obtain a flavor oil;
(2-2) mixing the flavor oil with a hydrophilic solvent;
(2-3) separating the flavor oil after mixing into an oil, a solid component, and an aqueous layer;
(2-4) mixing the oil and the solid component;
The manufacturing method of the flavor oil of Claim 1 which has this.
(3−1)食用油脂と、野菜及び香辛料から選ばれる1種以上とを加熱して香味油を得る工程と、
(3−2)前記香味油を、親水性溶媒と混合させる工程と、
(3−3)混合させた後の香味油を、油分と固形成分と水層とに分離する工程と、
(3−4)前記固形成分を、親水性溶媒によって洗浄する工程と、
(3−5)前記工程(3−3)で得られた油分と、前記工程(3−4)で得られた洗浄後の固形成分とを混合する工程と、
を有する請求項1に記載の香味油の製造方法。
(3-1) A step of heating a cooking oil and fat and one or more selected from vegetables and spices to obtain a flavor oil;
(3-2) mixing the flavor oil with a hydrophilic solvent;
(3-3) separating the flavor oil after mixing into an oil, a solid component, and an aqueous layer;
(3-4) washing the solid component with a hydrophilic solvent;
(3-5) a step of mixing the oil obtained in the step (3-3) and the solid component after washing obtained in the step (3-4);
The manufacturing method of the flavor oil of Claim 1 which has this.
(4−1)食用油脂と、野菜及び香辛料から選ばれる1種以上とを加熱して香味油を得る工程と、
(4−2)前記香味油を、油分と固形成分とに分離する工程と、
(4−3)前記油分を親水性溶媒と混合させる工程と、
(4−4)前記工程(4−3)で得られた混合液中の油分と、水層とを分離する工程と、
(4−5)前記固形成分を親水性溶媒によって洗浄する工程と、
(4−6)前記工程(4−4)で得られた油分と、前記工程(4−5)で得られた洗浄後の固形成分とを混合する工程と、
を有する請求項1に記載の香味油の製造方法。
(4-1) A step of heating the edible oil and fat and at least one selected from vegetables and spices to obtain a flavor oil;
(4-2) separating the flavor oil into an oil and a solid component;
(4-3) mixing the oil with a hydrophilic solvent;
(4-4) a step of separating the oil in the mixed liquid obtained in the step (4-3) and the aqueous layer;
(4-5) washing the solid component with a hydrophilic solvent;
(4-6) a step of mixing the oil obtained in the step (4-4) with the washed solid component obtained in the step (4-5);
The manufacturing method of the flavor oil of Claim 1 which has this.
さらに、乳化剤を添加する工程を有する請求項1〜5のいずれか一項に記載の香味油の製造方法。   Furthermore, the manufacturing method of the flavor oil as described in any one of Claims 1-5 which has the process of adding an emulsifier. 請求項1〜6のいずれか一項に記載の香味油の製造方法を用いて得られた香味油。   The flavor oil obtained using the manufacturing method of the flavor oil as described in any one of Claims 1-6. 含有量が5質量%となるように90℃以上のお湯に添加した場合のOD420nmの吸光度が0.4以下である請求項7に記載の香味油。   The flavor oil according to claim 7, wherein the absorbance at OD 420 nm when added to hot water of 90 ° C or higher so that the content is 5% by mass is 0.4 or lower. 食用油脂と、野菜及び香辛料から選ばれる1種以上とを加熱した後に得られる油分と、
食用油脂と、野菜及び香辛料から選ばれる1種以上とを加熱した後に得られる固形成分を、親水性溶媒によって洗浄した後の固形成分と、を混合して得られる香味油。
An oil obtained after heating an edible oil and fat and one or more selected from vegetables and spices;
A flavor oil obtained by mixing a solid component obtained after heating an edible fat and oil and one or more selected from vegetables and spices with a hydrophilic solvent.
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