JP2012025965A - Oil-forming apparatus - Google Patents

Oil-forming apparatus Download PDF

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JP2012025965A
JP2012025965A JP2011208766A JP2011208766A JP2012025965A JP 2012025965 A JP2012025965 A JP 2012025965A JP 2011208766 A JP2011208766 A JP 2011208766A JP 2011208766 A JP2011208766 A JP 2011208766A JP 2012025965 A JP2012025965 A JP 2012025965A
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oil
capacitor
gas
condenser
melting
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JP5586099B2 (en
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Akinori Ito
昭典 伊東
Hitoshi Itagaki
仁 板垣
Yasuo Ishikawa
泰男 石川
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MATSUDA KENSETSU KK
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MATSUDA KENSETSU KK
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Abstract

PROBLEM TO BE SOLVED: To provide an oil-forming apparatus which can efficiently isolate light oil from heavy oil at the time of liquefaction of plastics to oil, and brings wide application.SOLUTION: A second melting cylinder 3 is connected to a first melting cylinder 2, and moreover, an inclined vaporizing part 4 is connected to the second melting cylinder 3. A catalyst cylinder 13 is erected in the vicinity of the upper end of the vaporizing part 4. Vaporized gas from the catalyst cylinder 13 is led to a first condenser 17 cooled by air to collect heavy oil. Gas which is not liquefied in this place is led to a second condenser 18 which is cooled by cooling water to collect light oil. Offgas which is not condensed in both condensers is discharged through a water cylinder.

Description

本発明は、プラスチックを油に戻すための油化装置に関する。   The present invention relates to an oil making apparatus for returning plastic to oil.

一般に、プラスチックを溶融してプラスチックのガスを気化させ、この気化ガスを冷却して液化せしめるための油化装置が知られている。   2. Description of the Related Art Generally, an oiling apparatus is known for melting plastic to vaporize plastic gas and cooling the vaporized gas to liquefy it.

特開2000−1677JP2000-1677

ところが、上述の先行技術においては、重質油と軽質油が混合した混合油が採集されるので、採集した混合油の用途が狭く、単に燃焼させて使用するしかなかった。   However, in the above-described prior art, since a mixed oil in which heavy oil and light oil are mixed is collected, the use of the collected mixed oil is narrow and can only be used after burning.

そこで、本発明の油化装置においては、プラスチックを溶融させる溶融部と溶融プラスチックを気化させる気化部とを有し、この気化部から気化したプラスチックの気化ガスをコンデンサによって冷却して液化する油化装置において、前記コンデンサを複数設け、コンデンサの冷却に温度差を設けて異なる種類の油を採集するようにした。   Therefore, in the oiling apparatus of the present invention, the oiling unit has a melting part for melting the plastic and a vaporizing part for vaporizing the molten plastic, and the plastic vaporized from the vaporizing part is cooled by a condenser and liquefied. In the apparatus, a plurality of the capacitors are provided, and different types of oil are collected by providing a temperature difference in cooling the capacitors.

また、前記コンデンサを第1コンデンサと第2コンデンサで構成し、第1コンデンサを空気で冷却して重質油を液化し、前記第2コンデンサを冷却水で冷却して第1コンデンサで液化しなかった液化ガスを液化せしめて軽質油を採集するようにすることが好ましい。   Further, the capacitor is composed of a first capacitor and a second capacitor, the first capacitor is cooled with air to liquefy heavy oil, and the second capacitor is cooled with cooling water and not liquefied with the first capacitor. It is preferable to collect light oil by liquefying the liquefied gas.

更に、また 前記第2コンデンサによって液化されないオフガスを各コンデンサに接続されたそれぞれのタンクに供給し、その後水筒内に送り、この水筒内の水の高さを調節することにより前記気化ガスを液化する系内の圧力を調節するようにすることが好ましい。   Further, off gas that is not liquefied by the second condenser is supplied to each tank connected to each condenser, and then sent into a water bottle, and the vaporized gas is liquefied by adjusting the height of water in the water bottle. It is preferable to adjust the pressure in the system.

気化部から気化したプラスチックガスを冷却して凝縮させるコンデンサを複数設け、各コンデンサの冷却温度に差を設ければ、重質油と軽質油に効率よく別けることができ、重質油はバーナの燃料に軽質油は作動機械のエンジンに供給するガソリン、灯油の代替になり得る。また、特に、冷却温度の高い第1コンデンサには、室温空気を使用し、冷却温度の低い第2コンデンサには、常温冷却水を使用すれば、特に格別な冷却手段を設ける必要がなくなる。更にまた、オフガスを水筒内に送り、水筒内の水の高さを調整することにより気化ガスの液化系内の圧力が調節でき、これにより第1、第2コンデンサ17、18内を流れるガス流量が調整され得る。   By providing multiple condensers that cool and condense the plastic gas vaporized from the vaporization section and providing a difference in the cooling temperature of each condenser, it is possible to efficiently separate heavy oil from light oil. Light oil as fuel can replace gasoline and kerosene supplied to the engine of the working machine. In particular, if room temperature air is used for the first condenser having a high cooling temperature and room temperature cooling water is used for the second condenser having a low cooling temperature, it is not necessary to provide a special cooling means. Furthermore, the pressure in the liquefaction system of the vaporized gas can be adjusted by sending off-gas into the water bottle and adjusting the height of the water in the water bottle, whereby the gas flow rate flowing in the first and second capacitors 17 and 18 is adjusted. Can be adjusted.

図1は、本発明の概略構成図である。FIG. 1 is a schematic configuration diagram of the present invention. 図2は、溶解部、気化部の端部構成図である。FIG. 2 is an end configuration diagram of the dissolving part and the vaporizing part. 図3は、気化ガスの配管図である。FIG. 3 is a piping diagram of the vaporized gas. 図4は、溶融プラスチックの液面計の構成図である。FIG. 4 is a configuration diagram of a liquid plastic level gauge. 図5は、温度計の配置図である。FIG. 5 is a layout diagram of thermometers. 図6は、コンデンサの機能図である。FIG. 6 is a functional diagram of the capacitor. 図7は、気化部の上部構成図である。FIG. 7 is an upper configuration diagram of the vaporization unit.

以下、図面を参照して本発明の実施形態について説明する。   Hereinafter, embodiments of the present invention will be described with reference to the drawings.

図1において、本発明の油化装置Mは破砕したプラスチックを投入するポッパー1を有し、このポッパー1は、プラスチックを溶融する第1溶融部2の一端部に取付けられ、この第1溶融部2の他端には、第1溶融部2と直交して伸びる第2溶融部3の一端が接続され、この第2溶融部3の他端には、傾斜して伸び、溶融プラスチックを気化させる気化部4の下端が接続されている、なお、前記各第1、第2溶融部2、3及び気化部4は円筒管でその中にはリードスクリューが収納され、このリードスクリューの回転によりプラスチックが順次送られていく。各管の周囲には、面状ヒータh、h…hが巻回され、この面状ヒータh、h…hにより各管内のプラスチック及びその溶融液及び気化ガスが加熱される。前記面状ヒータh及び各管2、3、4は断熱材iで被覆されている。前記各管の端部には、モータm、m、mが設けられこれらモータmは前記リードスクリューに連なり、各リードスクリューを所定速度で回転させる。   In FIG. 1, an oil making apparatus M according to the present invention has a popper 1 for charging crushed plastic, and this popper 1 is attached to one end of a first melting part 2 for melting plastic, and this first melting part. The other end of 2 is connected to one end of a second melting part 3 extending perpendicularly to the first melting part 2, and the other end of the second melting part 3 extends at an angle to vaporize the molten plastic. The lower end of the vaporizing section 4 is connected. Each of the first, second melting sections 2 and 3 and the vaporizing section 4 is a cylindrical tube in which a lead screw is housed. Are sent sequentially. A sheet heater h, h... H is wound around each pipe, and the plastic, its melt and vaporized gas in each pipe are heated by the sheet heater h, h. The planar heater h and the tubes 2, 3, 4 are covered with a heat insulating material i. Motors m, m, and m are provided at the ends of the pipes. The motors m are connected to the lead screws and rotate the lead screws at a predetermined speed.

また、第1、第2溶融部2、3の接続部及び第2溶融部2と気化部4の接続部には、垂直の接続管5、6がそれぞれ設けられ、この接続管5、6を介して安全(気化ガスの燃焼防止)のための窒素7、8が管内に導入される。前記ホッパー1の下方には、送り管10が設けられ、この送り管10にはホッパー1内のプラスチックを一定量第1溶融管2に送り込むためのロータリーバルブ9が設けられている。   In addition, vertical connection pipes 5 and 6 are provided at the connection parts of the first and second melting parts 2 and 3 and the connection part of the second melting part 2 and the vaporization part 4, respectively. Therefore, nitrogen 7 and 8 for safety (preventing combustion of vaporized gas) are introduced into the pipe. Below the hopper 1, a feed pipe 10 is provided. The feed pipe 10 is provided with a rotary valve 9 for feeding a certain amount of plastic in the hopper 1 into the first melting pipe 2.

前記送り管10の近傍の溶融筒2は冷却ジャケットCを有し、プラスチックがホッパー1近くで溶融しないようになっている。   The melting cylinder 2 in the vicinity of the feed tube 10 has a cooling jacket C so that the plastic does not melt near the hopper 1.

そして、前記送り管10にも窒素12が送り込まれる。前記気化部4の上端部には、垂直上方に伸びる触媒筒13が設けられ、この触媒筒13内には、ゼオライト触媒が収納されている。前記触媒は有効細孔径9〜10mmでSiO2/Al23比が2.5位が好ましい合成ゼオライトであり、2.4〜4.7mmの大きさの球状品である。この触媒はC3以上のn−パラフィンを分解できるのでPEの処理に適している。 Nitrogen 12 is also fed into the feed tube 10. A catalyst cylinder 13 extending vertically upward is provided at the upper end of the vaporizing section 4, and a zeolite catalyst is accommodated in the catalyst cylinder 13. The catalyst is a synthetic zeolite having an effective pore diameter of 9 to 10 mm and an SiO 2 / Al 2 O 3 ratio of about 2.5, and is a spherical product having a size of 2.4 to 4.7 mm. This catalyst is suitable for treating PE because it can decompose n-paraffins of C 3 or higher.

前記気化部4の前記触媒筒13の取付位置より上端に近い位置には、下方に残渣管14が伸び、この残果敢14の中間には、バルブ5が設けられ、このバルブ15はロータリーバルブで残渣管14の上部を密閉状態で維持しつつ残渣をその下端に設けた残渣タンク16に排出する。   A residue pipe 14 extends downward at a position closer to the upper end than the attachment position of the catalyst cylinder 13 of the vaporization section 4, and a valve 5 is provided in the middle of the residue 14, and the valve 15 is a rotary valve. While maintaining the top of the residue pipe 14 in a sealed state, the residue is discharged to a residue tank 16 provided at the lower end thereof.

前記第1溶融部2と気化部4間には、2つの第1、第2コンデンサ17、18が設けられ、一方の第1コンデンサ17は重質油用で、触媒筒13を通った気化ガスを凝縮させて液化させ重質油を生成させるためのもので空気によって気化ガスを冷却する。前記第2コンデンサ18はコンデンサ17を通った気化ガスを凝縮させて液化し軽質油を生成させるためのもので、冷却水が供給される。重質油は凝縮温度が高いため、空気冷却でよく、断熱材iで被覆されている。   Two first and second condensers 17 and 18 are provided between the first melting part 2 and the vaporization part 4. One of the first condensers 17 is for heavy oil and vaporized gas that has passed through the catalyst cylinder 13. The gas is condensed and liquefied to produce heavy oil, and the vaporized gas is cooled by air. The second condenser 18 is for condensing the vaporized gas that has passed through the condenser 17 to liquefy it to produce light oil, and is supplied with cooling water. Since heavy oil has a high condensation temperature, it may be air-cooled and covered with a heat insulating material i.

そして、第1コンデンサ17により生成された重質油は、重質油タンク19に貯蔵され、第2コンデンサ18により生成された軽質油は軽質油タンク20に貯蔵される。   The heavy oil produced by the first condenser 17 is stored in the heavy oil tank 19, and the light oil produced by the second condenser 18 is stored in the light oil tank 20.

つぎに、前記第1、第2溶融部2、3及び気化部(図示なし)のリードスクリューの軸受部分には、気化ガスの外部への漏れを防止するためのカバー30、31が設けられ、これらカバー30、31にはパイプ32、33が接続され、これらパイプ32、33は集合管34に接続され、この集合管の端部にはファン35が設けられ、これにより漏れガスは外部に排出される。   Next, covers 30, 31 for preventing leakage of vaporized gas to the outside are provided on the bearing portions of the lead screw of the first and second melting portions 2, 3 and the vaporization portion (not shown), Pipes 32 and 33 are connected to these covers 30 and 31, and these pipes 32 and 33 are connected to a collecting pipe 34, and a fan 35 is provided at the end of the collecting pipe, whereby exhaust gas is discharged to the outside. Is done.

図3において、前記触媒管13を通過した気化ガスは配管40を通って第1コンデンサ17に入って液化されて重質油となり、更に配管41を通って重質油タンク19に貯蔵される。   In FIG. 3, the vaporized gas that has passed through the catalyst pipe 13 enters the first condenser 17 through the pipe 40 and is liquefied to become heavy oil, and is further stored in the heavy oil tank 19 through the pipe 41.

そして、第1コンデンサ17により液化されない気化ガスは配管42を通って第2コンデンサ18に入り液化された軽質油は配管43を通って軽質油タンク20に貯蔵される。前記第2コンデンサ18によって液化されなかったオフガスは配管100を通って両タンク19、20に入り、このオフガスは配管49を通って水筒48内の水中に入り、水から出たオフガスはアキュムレータ50、吸引ポンプ51を通ってバーナー52で燃焼され、このバーナー52は水タンク53を加熱してお湯を作る。前記水筒48内の水の高さhを調節する事により図3に示す気化ガス、液化系内の圧力が調節され、各コンデンサ17、18内を流れるガス流量が調整される。   The vaporized gas that is not liquefied by the first capacitor 17 enters the second capacitor 18 through the pipe 42 and the light oil liquefied is stored in the light oil tank 20 through the pipe 43. The off gas that has not been liquefied by the second condenser 18 enters the tanks 19 and 20 through the pipe 100, and the off gas enters the water in the water bottle 48 through the pipe 49, and the off gas discharged from the water is accumulated in the accumulator 50, It is burned by a burner 52 through a suction pump 51, and the burner 52 heats a water tank 53 to make hot water. By adjusting the height h of the water in the water bottle 48, the vaporized gas and the pressure in the liquefaction system shown in FIG. 3 are adjusted, and the flow rate of the gas flowing through the capacitors 17 and 18 is adjusted.

次いで、図4において前記気化部4には、液化したプラスチックの液面Sを検出するための液面計mが設けられ、この液面計mは間隔を配して設けた窒素吹出口60、61とコントローラ62からなり、窒素の吹出圧を検出することにより液面の位置が判る。図4においては、吹出口60の圧が吹出口61より高いので、液面Sは吹出口60、61の中間にあることが判る。   Next, in FIG. 4, the vaporization unit 4 is provided with a liquid level meter m for detecting the liquid level S of the liquefied plastic, and the liquid level meter m is provided with a nitrogen outlet 60 provided at intervals. 61 and a controller 62, and the position of the liquid level can be determined by detecting the nitrogen blowing pressure. In FIG. 4, since the pressure of the air outlet 60 is higher than that of the air outlet 61, it can be seen that the liquid level S is in the middle of the air outlets 60 and 61.

前記第1、第2溶融管2、3、気化部4内の温度を測定するための温度計70は各管の管壁wにセラミックの保護体71内に挿入された熱電対72を有しており、保護体71により管壁の温度を検出せずに管内の温度を検出するようになっている。   A thermometer 70 for measuring the temperature in the first and second melting tubes 2 and 3 and the vaporizing section 4 has a thermocouple 72 inserted in a ceramic protective body 71 on the wall w of each tube. Therefore, the temperature inside the pipe is detected by the protector 71 without detecting the temperature of the pipe wall.

図6において、第1コンデンサ17には、ファン81によって空気が送り込まれるが、この空気の排出口85には温度計83と流量計84が設けられ、排出空気の温度と流量に応じてファン81をコントロールすれば、第1コンデンサ17の冷却温度が調節でき、これにより重質油の質が調節される。   In FIG. 6, air is sent to the first condenser 17 by a fan 81, and a thermometer 83 and a flow meter 84 are provided at the air outlet 85, and the fan 81 is provided according to the temperature and flow rate of the discharged air. Can control the cooling temperature of the first condenser 17, thereby adjusting the quality of the heavy oil.

また、前記溶融部2内には溶融時のプラスチックから水蒸気が発生するが、この水蒸気は配管80を介して第1コンデンサ17に送り込まれて第1コンデンサ17内の温度を調整する。第1コンデンサ17は200〜300℃が好ましく、この温度で重質油が液化する。   Further, water vapor is generated from the plastic at the time of melting in the melting part 2, and this water vapor is sent to the first capacitor 17 through the pipe 80 to adjust the temperature in the first capacitor 17. The first capacitor 17 is preferably 200 to 300 ° C., and heavy oil liquefies at this temperature.

次に残渣管の他の実施例について説明する。   Next, another embodiment of the residue pipe will be described.

図7において、気化部4の触媒筒13より斜め上方位置から下方に残渣釜91が設けられ、この残渣釜91の可能には開閉蓋93が設けられるとともにその周囲にはヒータhが設けられ、この残渣釜に入った気化ガスは加熱されて触媒筒13に入る。この残渣釜により残渣に完全に気化していないプラスチックが混じってもここで気化するので、残渣釜には完全に残渣のみが残るここととなり、所定量の残渣が溜まった後に開閉蓋93を開放して残渣タンク92に残渣を収納する。また、残渣管内に降りてきた気化ガスがその中で液化して油が残渣タンクに入るということもない。なお、残渣釜91の入口8には出張り90が設けられ、この出張り90によって残渣が釜の周壁に付着するのが防止される。   In FIG. 7, a residue pot 91 is provided from a position obliquely above and below the catalyst cylinder 13 of the vaporization unit 4. The residue pot 91 is provided with an open / close lid 93 and a heater h around it. The vaporized gas contained in the residue kettle is heated and enters the catalyst cylinder 13. Even if plastic that is not completely vaporized is mixed with the residue in this residue kettle, it is vaporized here, so that only the residue remains in the residue kettle, and the opening / closing lid 93 is opened after a predetermined amount of residue has accumulated. Then, the residue is stored in the residue tank 92. In addition, the vaporized gas that has fallen into the residue pipe does not liquefy and oil does not enter the residue tank. In addition, a protrusion 90 is provided at the inlet 8 of the residue pot 91, and the protrusion 90 prevents the residue from adhering to the peripheral wall of the pot.

本油化装置は、特に廃プラスチックの油化に用いられ、小型油化装置に適している。   The present oil making apparatus is particularly used for oiling waste plastics, and is suitable for a small oil making apparatus.

1…ホッパー
2…第1溶融部
3…第2溶融部
4…気化部
13…触媒筒
14…残渣管
17…第1コンデンサ
18…第2コンデンサ
91…残渣釜
DESCRIPTION OF SYMBOLS 1 ... Hopper 2 ... 1st fusion | melting part 3 ... 2nd fusion | melting part 4 ... Vaporization part 13 ... Catalyst cylinder 14 ... Residue pipe | tube 17 ... 1st capacitor | condenser 18 ... 2nd capacitor | condenser 91 ... Residue pot

Claims (3)

プラスチックを溶融させる溶融部と溶融プラスチックを気化させる気化部とを有し、この気化部から気化したプラスチックの気化ガスをコンデンサによって冷却して液化する油化装置において、
前記コンデンサを複数設け、コンデンサの冷却に温度差を設けて異なる種類の油を採集したことを特徴とする油化装置。
In the oiling apparatus that has a melting part for melting the plastic and a vaporizing part for vaporizing the molten plastic, and cools and liquefies the vaporized plastic vaporized from the vaporizing part with a capacitor,
An oiling apparatus comprising a plurality of the capacitors and collecting different types of oil by providing a temperature difference in cooling the capacitors.
前記コンデンサを第1コンデンサと第2コンデンサで構成し、第1コンデンサを空気で冷却して重質油を液化し、前記第2コンデンサを冷却水で冷却して第1コンデンサで液化しなかった液化ガスを液化せしめて軽質油を採集したことを特徴とする請求項1記載の油化装置。   The capacitor is composed of a first capacitor and a second capacitor, the first capacitor is cooled with air to liquefy heavy oil, and the second capacitor is cooled with cooling water and liquefied without being liquefied by the first capacitor. 2. The oil making apparatus according to claim 1, wherein light oil is collected by liquefying the gas. 前記第2コンデンサによって液化されないオフガスを各コンデンサに接続されたそれぞれのタンクに供給し、その後水筒内に送り、この水筒内の水の高さを調節することにより前記気化ガスを液化する系内の圧力を調節するようにしたことを特徴とする請求項2記載の油化装置。   The off-gas that is not liquefied by the second condenser is supplied to each tank connected to each condenser, and then sent into the water bottle, and the height of the water in the water bottle is adjusted to liquefy the vaporized gas in the system. 3. The oil making apparatus according to claim 2, wherein the pressure is adjusted.
JP2011208766A 2011-09-26 2011-09-26 Oiling equipment Expired - Fee Related JP5586099B2 (en)

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH06136368A (en) * 1992-10-26 1994-05-17 Houjiyou:Kk Method for converting waste into oil
JPH07216363A (en) * 1994-02-03 1995-08-15 Hitachi Zosen Corp System for liquefying waste plastic
JP2000001677A (en) * 1998-06-17 2000-01-07 Yoichi Wada Pyrolysis system for polymeric waste
JP2000180058A (en) * 1998-12-09 2000-06-30 Tokimec Inc Carbonizer
JP2000212574A (en) * 1999-01-21 2000-08-02 Hitachi Ltd Waste plastics liquefaction and combustion treatment system and its liquefaction and combustion method
JP2006152175A (en) * 2004-11-30 2006-06-15 Matsuda Kensetsu Kk Apparatus for conversion into oil

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH06136368A (en) * 1992-10-26 1994-05-17 Houjiyou:Kk Method for converting waste into oil
JPH07216363A (en) * 1994-02-03 1995-08-15 Hitachi Zosen Corp System for liquefying waste plastic
JP2000001677A (en) * 1998-06-17 2000-01-07 Yoichi Wada Pyrolysis system for polymeric waste
JP2000180058A (en) * 1998-12-09 2000-06-30 Tokimec Inc Carbonizer
JP2000212574A (en) * 1999-01-21 2000-08-02 Hitachi Ltd Waste plastics liquefaction and combustion treatment system and its liquefaction and combustion method
JP2006152175A (en) * 2004-11-30 2006-06-15 Matsuda Kensetsu Kk Apparatus for conversion into oil

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