JP2011195454A - Substrate for fragrance - Google Patents
Substrate for fragrance Download PDFInfo
- Publication number
- JP2011195454A JP2011195454A JP2010060281A JP2010060281A JP2011195454A JP 2011195454 A JP2011195454 A JP 2011195454A JP 2010060281 A JP2010060281 A JP 2010060281A JP 2010060281 A JP2010060281 A JP 2010060281A JP 2011195454 A JP2011195454 A JP 2011195454A
- Authority
- JP
- Japan
- Prior art keywords
- fragrance
- talc
- substrate
- perfume
- base
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 239000003205 fragrance Substances 0.000 title claims abstract description 47
- 239000000758 substrate Substances 0.000 title abstract description 6
- 239000000454 talc Substances 0.000 claims abstract description 9
- 229910052623 talc Inorganic materials 0.000 claims abstract description 9
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 5
- 239000000344 soap Substances 0.000 claims abstract 3
- 239000002184 metal Substances 0.000 claims 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract description 10
- 239000002304 perfume Substances 0.000 abstract description 6
- 238000013329 compounding Methods 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 238000011156 evaluation Methods 0.000 description 10
- 239000000843 powder Substances 0.000 description 6
- HQKMJHAJHXVSDF-UHFFFAOYSA-L magnesium stearate Chemical compound [Mg+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O HQKMJHAJHXVSDF-UHFFFAOYSA-L 0.000 description 4
- PRAKJMSDJKAYCZ-UHFFFAOYSA-N squalane Chemical compound CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 description 4
- 239000002537 cosmetic Substances 0.000 description 3
- GRWFGVWFFZKLTI-IUCAKERBSA-N (-)-α-pinene Chemical compound CC1=CC[C@@H]2C(C)(C)[C@H]1C2 GRWFGVWFFZKLTI-IUCAKERBSA-N 0.000 description 2
- 241000207199 Citrus Species 0.000 description 2
- WEEGYLXZBRQIMU-UHFFFAOYSA-N Eucalyptol Chemical compound C1CC2CCC1(C)OC2(C)C WEEGYLXZBRQIMU-UHFFFAOYSA-N 0.000 description 2
- QUKGYYKBILRGFE-UHFFFAOYSA-N benzyl acetate Chemical compound CC(=O)OCC1=CC=CC=C1 QUKGYYKBILRGFE-UHFFFAOYSA-N 0.000 description 2
- 239000011230 binding agent Substances 0.000 description 2
- 235000020971 citrus fruits Nutrition 0.000 description 2
- 210000001072 colon Anatomy 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- -1 dipentaerythritol fatty acid ester Chemical class 0.000 description 2
- SHZIWNPUGXLXDT-UHFFFAOYSA-N ethyl hexanoate Chemical compound CCCCCC(=O)OCC SHZIWNPUGXLXDT-UHFFFAOYSA-N 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- XMGQYMWWDOXHJM-UHFFFAOYSA-N limonene Chemical compound CC(=C)C1CCC(C)=CC1 XMGQYMWWDOXHJM-UHFFFAOYSA-N 0.000 description 2
- 235000019359 magnesium stearate Nutrition 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000010445 mica Substances 0.000 description 2
- 229910052618 mica group Inorganic materials 0.000 description 2
- JXTPJDDICSTXJX-UHFFFAOYSA-N n-Triacontane Natural products CCCCCCCCCCCCCCCCCCCCCCCCCCCCCC JXTPJDDICSTXJX-UHFFFAOYSA-N 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 235000019629 palatability Nutrition 0.000 description 2
- 238000005507 spraying Methods 0.000 description 2
- 229940032094 squalane Drugs 0.000 description 2
- XOOUIPVCVHRTMJ-UHFFFAOYSA-L zinc stearate Chemical compound [Zn+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O XOOUIPVCVHRTMJ-UHFFFAOYSA-L 0.000 description 2
- UFLHIIWVXFIJGU-ARJAWSKDSA-N (Z)-hex-3-en-1-ol Chemical compound CC\C=C/CCO UFLHIIWVXFIJGU-ARJAWSKDSA-N 0.000 description 1
- UIVPNOBLHXUKDX-UHFFFAOYSA-N 3,5,5-trimethylhexyl 3,5,5-trimethylhexanoate Chemical compound CC(C)(C)CC(C)CCOC(=O)CC(C)CC(C)(C)C UIVPNOBLHXUKDX-UHFFFAOYSA-N 0.000 description 1
- HIQIXEFWDLTDED-UHFFFAOYSA-N 4-hydroxy-1-piperidin-4-ylpyrrolidin-2-one Chemical compound O=C1CC(O)CN1C1CCNCC1 HIQIXEFWDLTDED-UHFFFAOYSA-N 0.000 description 1
- 239000005995 Aluminium silicate Substances 0.000 description 1
- 239000004375 Dextrin Substances 0.000 description 1
- 229920001353 Dextrin Polymers 0.000 description 1
- 239000004264 Petrolatum Substances 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- MVNCAPSFBDBCGF-UHFFFAOYSA-N alpha-pinene Natural products CC1=CCC23C1CC2C3(C)C MVNCAPSFBDBCGF-UHFFFAOYSA-N 0.000 description 1
- 235000012211 aluminium silicate Nutrition 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 229940007550 benzyl acetate Drugs 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 235000019425 dextrin Nutrition 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 230000008034 disappearance Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- XYIBRDXRRQCHLP-UHFFFAOYSA-N ethyl acetoacetate Chemical compound CCOC(=O)CC(C)=O XYIBRDXRRQCHLP-UHFFFAOYSA-N 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- UFLHIIWVXFIJGU-UHFFFAOYSA-N hex-3-en-1-ol Natural products CCC=CCCO UFLHIIWVXFIJGU-UHFFFAOYSA-N 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 229940100554 isononyl isononanoate Drugs 0.000 description 1
- 229940074928 isopropyl myristate Drugs 0.000 description 1
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 1
- 229940087305 limonene Drugs 0.000 description 1
- 235000001510 limonene Nutrition 0.000 description 1
- 229940057948 magnesium stearate Drugs 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000002688 persistence Effects 0.000 description 1
- 229940066842 petrolatum Drugs 0.000 description 1
- 235000019271 petrolatum Nutrition 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- GRWFGVWFFZKLTI-UHFFFAOYSA-N rac-alpha-Pinene Natural products CC1=CCC2C(C)(C)C1C2 GRWFGVWFFZKLTI-UHFFFAOYSA-N 0.000 description 1
- 229910052814 silicon oxide Inorganic materials 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- NRLLZRJXDKUVHM-UHFFFAOYSA-N tridecyl 7-methyloctanoate Chemical compound CCCCCCCCCCCCCOC(=O)CCCCCC(C)C NRLLZRJXDKUVHM-UHFFFAOYSA-N 0.000 description 1
- 229940105125 zinc myristate Drugs 0.000 description 1
- 229940057977 zinc stearate Drugs 0.000 description 1
- GBFLQPIIIRJQLU-UHFFFAOYSA-L zinc;tetradecanoate Chemical compound [Zn+2].CCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCC([O-])=O GBFLQPIIIRJQLU-UHFFFAOYSA-L 0.000 description 1
Landscapes
- Cosmetics (AREA)
Abstract
Description
本発明は、香水、オーデトワレ、オーデコロンなど、不特定なフレグランスの香りを持続させるという快適な使用性を提供するフレグランス用下地である。 The present invention is a fragrance base material that provides a comfortable usability of sustaining an unspecified fragrance scent such as perfume, eau de toilette, and eau de cologne.
香りを付与することを目的とした香水、オーデトワレ、オーデコロン等のフレグランスは、通常は香料とエタノールを主成分とする。 Fragrances such as perfume, eau de toilette, and eau de cologne for the purpose of imparting a scent usually contain a fragrance and ethanol as main components.
それらに配合される香料成分の中には、短時間で揮散してしまうものがある。特にフレッシュ感、清涼感、みずみずしさをもつシトラスノート、グリーンノート、フルーティーノートなど嗜好性の高いライトな香りは持続性が期待できない。 Some of the fragrance components blended therein are volatilized in a short time. In particular, a light fragrance with high palatability such as citrus note, green note, and fruity note with freshness, refreshment, and freshness cannot be expected to last.
それらを解決するために、香水コロン組成物中にあらかじめ香料を高度分岐環状デキストリンに含浸したさせたものを配合する技術（特許文献１参照）や酸化珪素を主成分としたメソポーラス粉体に予め香料を保持させ、それを化粧料に配合する技術（特許文献２参照）が提案されている。 In order to solve these problems, a technique for blending a perfume colon composition previously impregnated with a highly branched cyclic dextrin (see Patent Document 1) and a mesoporous powder mainly composed of silicon oxide are used in advance. Has been proposed (see Patent Document 2).
しかしながら、これらの技術を応用した製品で上市されているものは、通常のフレグランスと比べ非常に少なく、消費者の香りに関する嗜好性による商品の選択性が低い。 However, products that have been marketed using these technologies are very few compared to ordinary fragrances, and the selectivity of products due to consumer preference for fragrance is low.
本発明者はこのような事情を鑑み、消費者にとって香りの選択性が高い、通常のフレグランスを使用し、嗜好性の高いライトな香りの持続性を高めることを目的としたフレグランス用下地を発明した。 In view of such circumstances, the present inventors invented a base for fragrances that uses ordinary fragrances with high scent selectivity for consumers and aims to enhance the sustainability of light scents with high palatability. did.
フレグランス用下地とは、香料とエタノールを主成分とした通常の香水、オーデトワレ、オーデコロン等のフレグランスを塗布もしくはアトマイザーを用いて噴霧する前に、その塗布・噴霧部位に塗布して使用するものであり、本発明者が、一般消費者が購入できる市場にて販売されているものを見つけだすことはできなかった。 Fragrance groundwork is used by applying to the application / spraying site before applying or spraying fragrances such as normal perfume, eau de toilette, eau de cologne, etc. with fragrance and ethanol as main components. The present inventor has not been able to find what is sold in a market that can be purchased by general consumers.
本発明は、タルクを高含有し、ライトな香りの持続性を高めることを特徴とするフレグランス用下地である。 The present invention is a fragrance substrate characterized by containing a high amount of talc and enhancing the durability of a light scent.
本フレグランス用下地を構成するタルクとしては、通常化粧料に用いられるものであれば特に限定されない。その効果を損なわない範囲で必要に応じて他の成分、例えば肌への付着性向上のため、ステアリン酸亜鉛、ミリスチン酸亜鉛、ステアリン酸マグネシウムなどの金属石鹸、ワセリン、ジペンタエリトリット脂肪酸エステル、スクワラン、ミリスチン酸イソプロピル、イソノナン酸イソノニル、イソノナン酸トリデシルなどの油剤を適宜１種もしくは２種以上組み合わせて配合することができる。 The talc constituting the fragrance base is not particularly limited as long as it is usually used in cosmetics. As necessary, other components such as zinc stearate, zinc myristate, magnesium stearate, petrolatum, dipentaerythritol fatty acid ester, as long as the effect is not impaired Oil agents such as squalane, isopropyl myristate, isononyl isononanoate, and tridecyl isononanoate can be blended in appropriate combination of one or more.
また、その形態はルースタイプの粉末状でも良いし、またバインダー等と混合してプレス状としてもよい、さらには練り状にしても構わない。バインダーとして上記のような油剤を適宜１種もしくは２種以上組み合わせて配合することができる。 Further, the form may be a loose type powder, or may be mixed with a binder or the like to form a press, or may be a kneaded form. As the binder, the above-mentioned oil agents can be blended appropriately or in combination of two or more.
上記の成分のほかに、通常化粧料に用いられる成分として例えば、他の粉体、界面活性剤、酸化防止剤、防腐剤、紫外線防止剤、色材、美容剤などを配合することができる。 In addition to the above-mentioned components, other powders, surfactants, antioxidants, preservatives, UV inhibitors, colorants, cosmetics, and the like can be blended as components that are usually used in cosmetics.
＜実験＞
下記の表１にあげる粉体に関して、表２に示す清涼感、みずみずしさをもつライトな香りに寄与する香料成分の持続性に関して下記のように評価した。
<Experiment>
Regarding the powders listed in Table 1 below, the sustainability of the fragrance components that contribute to the light scent with a refreshing feeling and freshness shown in Table 2 was evaluated as follows.
ろ紙（東洋濾紙株式会社 定性濾紙Ｎｏ．１）上に、１０ｃｍ×１０ｃｍの正方形を描き、その正方形内に表１にあげた粉体を各１００ｍｇ量りとり、均一に塗布する。粉体塗布部に表２に示す香料成分を、１重量％エタノール溶液にしたものを定量アトマイザーを用いて噴霧（１噴霧当たり２５ｍｇ）し、一定時間後、ろ紙より１０ｃｍ離れた距離における香りに関して、専門パネル５名により評価した。 A 10 cm × 10 cm square is drawn on a filter paper (Toyo Filter Paper Co., Ltd. Qualitative Filter Paper No. 1), and 100 mg of each of the powders listed in Table 1 is weighed and applied uniformly. In the powder coating part, the fragrance components shown in Table 2 in a 1 wt% ethanol solution were sprayed using a quantitative atomizer (25 mg per spray), and after a certain time, the scent at a distance of 10 cm away from the filter paper, Evaluation was performed by 5 specialist panels.
＜評価＞
噴霧した香料成分の香りを
評価点 ３：強く感じる
２：明らかに感じる
１：かすかに感じる
０：感じない
とし、専門パネル５名の平均値を評価値とした。
<Evaluation>
Evaluation of the fragrance of the sprayed fragrance component 3: Feeling strongly 2: Feeling clearly 1: Feeling faint 0: Not feeling, the average value of five professional panels was used as the evaluation value.
＜評価＞
ブランク（ろ紙になにも塗布しないで、香料成分１重量％エタノール溶液を噴霧したもの）試験の香り消失時（評価値０：全員が香りを感じない）の評価値により、以下のように評価した。
◎：２．０以上
○：１．５以上、２．０未満
△：１．０以上、１．５未満
×：１．０未満
<Evaluation>
Evaluation as follows according to the evaluation value at the time of fragrance disappearance (evaluation value 0: nobody feels fragrance) in a blank (nothing applied to filter paper and sprayed with 1% by weight ethanol solution of fragrance component) did.
◎: 2.0 or more ○: 1.5 or more, less than 2.0 △: 1.0 or more, less than 1.5 ×: less than 1.0
リモネンに関する持続性の評価
α−ピネンに関する持続性の評価
ｃｉｓ−３−ヘキセノールに関する持続性の評価
１，８−シネオールに関する持続性の評価
カプロン酸エチルに関する持続性の評価
酢酸ベンジルに関する持続性の評価
アセト酢酸エチルに関する持続性の評価
表３〜表９の結果より明らかなように、本発明に関わるタルクは清涼感、みずみずしさをもつライトな香りに寄与する香料成分の香りの持続性を高めた。 As is clear from the results of Tables 3 to 9, talc according to the present invention enhanced the fragrance sustainability of the fragrance component contributing to a light fragrance having a refreshing feeling and freshness.
以下に実施例を挙げるが、本発明はこれらによって限定されるものではない。 Examples are given below, but the present invention is not limited thereto.
表１０に実施例１〜５及び比較例１〜３を示す。実施例１〜５及び比較例１〜３に関して、先述と同様の評価法を用いて評価した結果を表１１に示す。表１０中の数値は重量％である。
さらに実施例６、７を示す Further, Examples 6 and 7 are shown.
＜実施例６＞
フレグランス用下地（ルーセントタイプ）
成分 処方量（重量％）
（１）タルク ９０
（２）マイカ ７
（３）ステアリン酸マグネシウム ３
合計 １００
製法：成分（１）〜（３）をブレンダーにて混合し、これを粉砕機で粉砕後ふるいを通した。
<Example 6>
Fragrance base (Lucent type)
Ingredient Prescription amount (% by weight)
(1) Talc 90
(2) Mica 7
(3) Magnesium stearate 3
Total 100
Production method: Components (1) to (3) were mixed in a blender, and pulverized with a pulverizer and passed through a sieve.
＜実施例７＞
フレグランス用下地（プレストタイプ）
成分 処方量（重量％）
（１）タルク ７０
（２）マイカ １０
（３）カオリン ７
（４）ステアリン酸亜鉛 ６
（５）スクワラン ５
（６）トリイソオクタン酸イソトリデシル ２
合計 １００
製法：成分（１）〜（４）をブレンダーにて混合した後、成分（５）と（６）とを加え、さらに混合する。これを粉砕機で粉砕後ふるいを通し、中皿に圧縮成型した。
<Example 7>
Fragrance substrate (pressed type)
Ingredient Prescription amount (% by weight)
(1) Talc 70
(2) Mica 10
(3) Kaolin 7
(4) Zinc stearate 6
(5) Squalane 5
(6) Isotridecyl triisooctanoate 2
Total 100
Production method: Components (1) to (4) are mixed in a blender, and then components (5) and (6) are added and further mixed. This was pulverized by a pulverizer, passed through a sieve, and compression molded into an intermediate dish.
実施例６、７のフレグランス下地を、片腕の内腕部に塗布し、そこに市販のフレグランス（シトラスノートのコロン）を噴霧（約１００ｍｇ）した。さらにもう片方の内腕部にも同じフレグランスを噴霧し、１時間後香りの評価をしたところ、フレグランス下地を無塗布の内腕部の香りは消失している、一方、フレグランス下地を塗布した内腕部は香りが持続しているという良好な結果を得られた。 The fragrance bases of Examples 6 and 7 were applied to the inner arm portion of one arm, and a commercially available fragrance (colon of citrus note) was sprayed thereon (about 100 mg). Furthermore, when the same fragrance was sprayed on the other inner arm and the scent was evaluated after 1 hour, the scent of the inner arm without the fragrance base disappeared, while the fragrance base was applied. A good result was obtained that the scent of the arm part persisted.
消費者が幅広い香調から選んだ、市販されている通常のフレグランスの、香りの持続性を高めることができるフレグランス用下地を提供できる。 It is possible to provide a base for a fragrance that can increase the scent sustainability of ordinary fragrances on the market selected by consumers from a wide range of fragrances.
Claims (5)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2010060281A JP5661308B2 (en) | 2010-03-17 | 2010-03-17 | Fragrance substrate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2010060281A JP5661308B2 (en) | 2010-03-17 | 2010-03-17 | Fragrance substrate |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2011195454A true JP2011195454A (en) | 2011-10-06 |
| JP5661308B2 JP5661308B2 (en) | 2015-01-28 |
Family
ID=44874111
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2010060281A Active JP5661308B2 (en) | 2010-03-17 | 2010-03-17 | Fragrance substrate |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JP5661308B2 (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2016084316A (en) * | 2014-10-28 | 2016-05-19 | 花王株式会社 | Sheet-type cosmetic |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2002145717A (en) * | 2000-11-01 | 2002-05-22 | Catalysts & Chem Ind Co Ltd | Antimicrobial cosmetic |
| JP2008531724A (en) * | 2005-03-04 | 2008-08-14 | スティーヴン エヌ． ゴードン， | Cosmetic composition, method for applying cosmetic composition, and method for producing cosmetic composition |
-
2010
- 2010-03-17 JP JP2010060281A patent/JP5661308B2/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2002145717A (en) * | 2000-11-01 | 2002-05-22 | Catalysts & Chem Ind Co Ltd | Antimicrobial cosmetic |
| JP2008531724A (en) * | 2005-03-04 | 2008-08-14 | スティーヴン エヌ． ゴードン， | Cosmetic composition, method for applying cosmetic composition, and method for producing cosmetic composition |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2016084316A (en) * | 2014-10-28 | 2016-05-19 | 花王株式会社 | Sheet-type cosmetic |
Also Published As
| Publication number | Publication date |
|---|---|
| JP5661308B2 (en) | 2015-01-28 |
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