JP2011130740A - Raw tea leaf-extracted essence having balanced flavor and easy to drink, and method for producing the same - Google Patents
Raw tea leaf-extracted essence having balanced flavor and easy to drink, and method for producing the same Download PDFInfo
- Publication number
- JP2011130740A JP2011130740A JP2009295163A JP2009295163A JP2011130740A JP 2011130740 A JP2011130740 A JP 2011130740A JP 2009295163 A JP2009295163 A JP 2009295163A JP 2009295163 A JP2009295163 A JP 2009295163A JP 2011130740 A JP2011130740 A JP 2011130740A
- Authority
- JP
- Japan
- Prior art keywords
- tea leaf
- leaf extract
- fresh tea
- producing
- flavor
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000796 flavoring agent Substances 0.000 title claims abstract description 51
- 235000019634 flavors Nutrition 0.000 title claims abstract description 51
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 45
- 241001122767 Theaceae Species 0.000 title abstract 12
- 235000013616 tea Nutrition 0.000 claims abstract description 85
- 238000000034 method Methods 0.000 claims abstract description 52
- 238000007710 freezing Methods 0.000 claims abstract description 25
- 230000008014 freezing Effects 0.000 claims abstract description 25
- 102000004190 Enzymes Human genes 0.000 claims abstract description 19
- 108090000790 Enzymes Proteins 0.000 claims abstract description 18
- 235000013305 food Nutrition 0.000 claims abstract description 15
- 244000269722 Thea sinensis Species 0.000 claims description 93
- 229940092665 tea leaf extract Drugs 0.000 claims description 84
- 238000000605 extraction Methods 0.000 claims description 51
- 230000035622 drinking Effects 0.000 claims description 35
- 235000009569 green tea Nutrition 0.000 claims description 24
- 235000013361 beverage Nutrition 0.000 claims description 15
- 108010059820 Polygalacturonase Proteins 0.000 claims description 10
- 108010093305 exopolygalacturonase Proteins 0.000 claims description 10
- 108010038851 tannase Proteins 0.000 claims description 9
- 235000019606 astringent taste Nutrition 0.000 abstract description 21
- 235000009508 confectionery Nutrition 0.000 abstract description 8
- 230000001747 exhibiting effect Effects 0.000 abstract 1
- 239000002304 perfume Substances 0.000 abstract 1
- 235000019640 taste Nutrition 0.000 description 18
- 238000011156 evaluation Methods 0.000 description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 13
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 10
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 10
- 230000001953 sensory effect Effects 0.000 description 9
- 238000005119 centrifugation Methods 0.000 description 8
- 238000004458 analytical method Methods 0.000 description 7
- 235000019645 odor Nutrition 0.000 description 7
- 239000002994 raw material Substances 0.000 description 7
- 239000007788 liquid Substances 0.000 description 6
- 235000019583 umami taste Nutrition 0.000 description 6
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 description 5
- 229930003268 Vitamin C Natural products 0.000 description 5
- 238000001914 filtration Methods 0.000 description 5
- 239000003205 fragrance Substances 0.000 description 5
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 5
- 235000017557 sodium bicarbonate Nutrition 0.000 description 5
- 235000019154 vitamin C Nutrition 0.000 description 5
- 239000011718 vitamin C Substances 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 4
- 238000002470 solid-phase micro-extraction Methods 0.000 description 4
- 229940098795 (3z)- 3-hexenyl acetate Drugs 0.000 description 3
- 241000745768 Pluchea carolinensis Species 0.000 description 3
- NPFVOOAXDOBMCE-PLNGDYQASA-N cis-3-Hexenyl acetate Natural products CC\C=C/CCOC(C)=O NPFVOOAXDOBMCE-PLNGDYQASA-N 0.000 description 3
- RRGOKSYVAZDNKR-ARJAWSKDSA-M cis-3-hexenylacetate Chemical compound CC\C=C/CCCC([O-])=O RRGOKSYVAZDNKR-ARJAWSKDSA-M 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- 238000005520 cutting process Methods 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000007254 oxidation reaction Methods 0.000 description 3
- 235000018553 tannin Nutrition 0.000 description 3
- 229920001864 tannin Polymers 0.000 description 3
- 239000001648 tannin Substances 0.000 description 3
- NPFVOOAXDOBMCE-UHFFFAOYSA-N trans-3-hexenyl acetate Natural products CCC=CCCOC(C)=O NPFVOOAXDOBMCE-UHFFFAOYSA-N 0.000 description 3
- PFTAWBLQPZVEMU-DZGCQCFKSA-N (+)-catechin Chemical compound C1([C@H]2OC3=CC(O)=CC(O)=C3C[C@@H]2O)=CC=C(O)C(O)=C1 PFTAWBLQPZVEMU-DZGCQCFKSA-N 0.000 description 2
- MBDOYVRWFFCFHM-SNAWJCMRSA-N (2E)-hexenal Chemical compound CCC\C=C\C=O MBDOYVRWFFCFHM-SNAWJCMRSA-N 0.000 description 2
- 244000025254 Cannabis sativa Species 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 235000006468 Thea sinensis Nutrition 0.000 description 2
- 125000003118 aryl group Chemical group 0.000 description 2
- ADRVNXBAWSRFAJ-UHFFFAOYSA-N catechin Natural products OC1Cc2cc(O)cc(O)c2OC1c3ccc(O)c(O)c3 ADRVNXBAWSRFAJ-UHFFFAOYSA-N 0.000 description 2
- 235000005487 catechin Nutrition 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 229950001002 cianidanol Drugs 0.000 description 2
- 235000011850 desserts Nutrition 0.000 description 2
- MTZQAGJQAFMTAQ-UHFFFAOYSA-N ethyl benzoate Chemical compound CCOC(=O)C1=CC=CC=C1 MTZQAGJQAFMTAQ-UHFFFAOYSA-N 0.000 description 2
- 235000019225 fermented tea Nutrition 0.000 description 2
- 230000002401 inhibitory effect Effects 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 230000001954 sterilising effect Effects 0.000 description 2
- 238000004659 sterilization and disinfection Methods 0.000 description 2
- UFLHIIWVXFIJGU-ARJAWSKDSA-N (Z)-hex-3-en-1-ol Chemical compound CC\C=C/CCO UFLHIIWVXFIJGU-ARJAWSKDSA-N 0.000 description 1
- KBPZVLXARDTGGD-UHFFFAOYSA-N 2,3-dihydroxybutanedioic acid;iron Chemical compound [Fe].OC(=O)C(O)C(O)C(O)=O KBPZVLXARDTGGD-UHFFFAOYSA-N 0.000 description 1
- 235000001674 Agaricus brunnescens Nutrition 0.000 description 1
- 239000004382 Amylase Substances 0.000 description 1
- 108010065511 Amylases Proteins 0.000 description 1
- 102000013142 Amylases Human genes 0.000 description 1
- 102100032487 Beta-mannosidase Human genes 0.000 description 1
- 241000209507 Camellia Species 0.000 description 1
- 206010013911 Dysgeusia Diseases 0.000 description 1
- 108090001060 Lipase Proteins 0.000 description 1
- 102000004882 Lipase Human genes 0.000 description 1
- 239000004367 Lipase Substances 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 235000019418 amylase Nutrition 0.000 description 1
- 108010055059 beta-Mannosidase Proteins 0.000 description 1
- 235000019658 bitter taste Nutrition 0.000 description 1
- 239000012267 brine Substances 0.000 description 1
- 238000004737 colorimetric analysis Methods 0.000 description 1
- 235000018597 common camellia Nutrition 0.000 description 1
- 230000002596 correlated effect Effects 0.000 description 1
- 238000003795 desorption Methods 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000000855 fermentation Methods 0.000 description 1
- 230000004151 fermentation Effects 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 235000019609 freshness Nutrition 0.000 description 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- 238000004817 gas chromatography Methods 0.000 description 1
- UFLHIIWVXFIJGU-UHFFFAOYSA-N hex-3-en-1-ol Natural products CCC=CCCO UFLHIIWVXFIJGU-UHFFFAOYSA-N 0.000 description 1
- 238000004128 high performance liquid chromatography Methods 0.000 description 1
- 235000019421 lipase Nutrition 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 238000002414 normal-phase solid-phase extraction Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 238000007873 sieving Methods 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 description 1
- 235000014214 soft drink Nutrition 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 238000001256 steam distillation Methods 0.000 description 1
- 238000000092 stir-bar solid-phase extraction Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- MBDOYVRWFFCFHM-UHFFFAOYSA-N trans-2-hexenal Natural products CCCC=CC=O MBDOYVRWFFCFHM-UHFFFAOYSA-N 0.000 description 1
- 235000019607 umami taste sensations Nutrition 0.000 description 1
- 238000009777 vacuum freeze-drying Methods 0.000 description 1
- 238000009834 vaporization Methods 0.000 description 1
- 230000008016 vaporization Effects 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Landscapes
- Tea And Coffee (AREA)
Abstract
Description
本発明は、生茶葉の急速冷凍処理を用いて、風味バランスと飲みやすさを備えた香味豊かな生茶葉抽出エキスを製造する方法、及び該生茶葉抽出エキスを含有させた飲食品に関する。 The present invention relates to a method for producing a flavorful fresh tea leaf extract having a flavor balance and ease of drinking using a quick freezing treatment of fresh tea leaves, and a food and drink containing the fresh tea leaf extract.
お茶は、世界各地で広く普及した飲料であり、その中でも緑茶は、我が国において古くから、最も人々に親しまれた飲料である。現在、茶の製造には、各種の方法が用いられているが、緑茶の通常の製茶工程は、殺青工程、粗揉工程、揉念工程、中揉工程、精揉工程、乾燥工程からなり、製茶された荒茶を火入れ、篩分け、切断、合組、火入れ等の工程を経て仕上茶に加工し、緑茶として流通させる方法が普通に採られる方法である。また、現在は、緑茶等の茶飲料の原料として、茶抽出エキスの利用も盛んに行なわれている。 Tea is a beverage widely spread all over the world. Among them, green tea has been the most popular beverage in Japan since ancient times. Currently, various methods are used for tea production, but the normal tea making process of green tea consists of a blue-killing process, rough koji process, dedication process, middle mushroom process, refinement process, drying process, A commonly used method is to process the raw tea that has been made into tea, finishing it through sieving, cutting, cutting, assembling, and firing, and then distributing it as finished tea. Currently, tea extract is actively used as a raw material for tea beverages such as green tea.
茶飲料の調製に際しては、上記のとおり生茶葉の採摘後、加熱処理、乾燥を行い茶葉の加工を行なうのが通常の方法であるが、生茶葉の香味をそのまま生かして加工する方法も試みられている。また、その様な場合に、生茶葉を冷凍することで、香味の改善を試みる方法も開示されている。例えば、特開2005−160416号公報には、ツバキ科の常緑樹であるチャ(学名: Camellia sinensis (L) O. Kuntze )の生の葉を摘採後凍結処理し、凍結した茶葉を水蒸気蒸留して得られる留出液を緑茶飲料に配合することにより、フレッシュで耐熱性のある香気・香味が付与された密閉容器入り緑茶飲料を提供する方法が開示されている。 In the preparation of tea beverages, as described above, after picking fresh tea leaves, the usual method is to process the tea leaves by heat treatment and drying, but a method of processing by making use of the flavor of fresh tea leaves is also attempted. ing. In such a case, a method of trying to improve the flavor by freezing fresh tea leaves is also disclosed. For example, Japanese Patent Application Laid-Open No. 2005-160416 discloses that a fresh leaf of tea (Scientific name: Camellia sinensis (L) O. Kuntze), which is an evergreen tree of the camellia family, is picked and frozen, and the frozen tea leaf is subjected to steam distillation. A method for providing a green tea beverage in a sealed container to which a fresh and heat-resistant fragrance / flavor is imparted by blending the resulting distillate into a green tea beverage is disclosed.
また、特開2007−110990号公報には、生茶葉を凍結させる工程と、凍結された生茶葉を水と混合し、粉砕搾汁する工程と、得られた粉砕搾汁液を濾過し、抽出液を得る工程と、得られた抽出液を加熱する工程により、緑茶飲料原料液を製造することにより、加熱処理により香気成分が失われるのを防ぎながらも、酵素活性を抑制することによって、酸化が抑制され、且つ香気に優れた緑茶飲料原料液を製造する方法が開示されている。 Japanese Patent Application Laid-Open No. 2007-110990 discloses a step of freezing fresh tea leaves, a step of mixing frozen fresh tea leaves with water, crushing and squeezing, and filtering the obtained crushed juice and extracting the extract By producing the green tea beverage raw material liquid by the process of obtaining the obtained extract and the process of heating the obtained extract, the oxidation is suppressed by inhibiting the enzyme activity while preventing the loss of aroma components by the heat treatment. A method for producing a green tea beverage raw material liquid that is suppressed and excellent in aroma is disclosed.
更に、特開平11−346702号公報には、生葉を洗浄し水で濡らした状態で真空庫内に入れ、真空引きすることにより前記水の気化熱で前記生葉を凍結させる前処理を施した後、真空凍結乾燥処理により乾燥させることにより、酸化を抑制し、生葉本来の香味と有効成分を変えることなく、長期保存に耐える各種生葉加工品を低コストで製造することが開示されている。 Furthermore, in Japanese Patent Application Laid-Open No. 11-346702, after a fresh leaf is washed and wetted with water, it is put in a vacuum chamber and subjected to a pretreatment for freezing the fresh leaf with the heat of vaporization of water by evacuation. In addition, it is disclosed that, by drying by vacuum freeze-drying, various raw leaf processed products that can withstand long-term storage can be produced at low cost without inhibiting oxidation and changing the original flavor and active ingredients of the raw leaf.
また、特開2004−113090号公報には、破砕処理した萎凋処理前の生茶葉と、茶葉組織破壊酵素の溶解液とを混合し、発酵(タンニン酸化反応)、茶葉組織破壊酵素処理、および抽出処理を単一工程で行うことにより、苦渋味が少なく、コクと旨味を有する発酵茶葉抽出液を効率的に得ることを特徴とする発酵茶葉抽出液の製造方法が開示されている。更に、特開2007−135534号公報には、茶葉の生葉を弱アルカリ性温水に浸漬させた後に、所定の大きさにカットしてペースト状にし、更に真空凍結することにより、生葉の鮮度を極力落とさずに、水への分散性を改善でき、生葉本来の鮮やかな緑色と新鮮な香りと程好い渋味を高いバランスで有する緑茶ペーストを得ることを特徴とする水性の緑茶ペーストの製造方法が開示されている。 Japanese Patent Application Laid-Open No. 2004-113090 mixes a crushed raw tea leaf before wilt treatment with a tea leaf tissue-disrupting enzyme solution, fermentation (tannin oxidation reaction), tea leaf tissue-disrupting enzyme treatment, and extraction. A method for producing a fermented tea leaf extract characterized by efficiently obtaining a fermented tea leaf extract having little bitter and astringent taste and having a rich and umami taste by performing the treatment in a single step is disclosed. Furthermore, Japanese Patent Application Laid-Open No. 2007-135534 discloses that the freshness of fresh leaves is reduced as much as possible by immersing fresh leaves of tea leaves in weak alkaline hot water, cutting them into a predetermined size, pasting them, and further freezing them in a vacuum. A method for producing an aqueous green tea paste characterized in that it can improve the dispersibility in water and obtain a green tea paste with a high balance of vivid green, fresh fragrance and moderate astringency of fresh leaves. Has been.
上記のとおり、生茶葉の香味を利用した各種の茶飲料の製造方法が開示されているが、かかる方法を持ってしても、茶葉感が強く、爽やかさ、みずみずしさを有し、渋味や雑味が低減され、全体的な風味バランスや飲みやすさを備えた優れた香味の生茶葉抽出エキスを提供するという観点からは、今までに必ずしも満足のいく方法は開示されていない。 As described above, various methods for producing tea beverages using the flavor of fresh tea leaves are disclosed, but even with such a method, the tea leaves feel strong, refreshing and fresh, and astringent From the standpoint of providing an excellent flavored fresh tea leaf extract with reduced overall taste and taste, and an overall flavor balance and ease of drinking, no satisfactory method has been disclosed so far.
本発明の課題は、茶葉感が強く、爽やかさ、みずみずしさ、甘い香りを有し、渋味や雑味が低減され、全体的な風味・バランスや飲みやすさを備えた優れた香味の生茶葉抽出エキス、該生茶葉抽出エキスを含有させた茶飲料のような飲食品を提供すること、及び、該生茶葉抽出エキスを、複雑な工程を経ることなく、実用的に製造する方法を提供することからなる。 The object of the present invention is to produce an excellent flavor with a strong tea leaf feeling, freshness, freshness, sweet aroma, reduced astringency and miscellaneous taste, and overall flavor / balance and ease of drinking. To provide a tea leaf extract, a food and drink such as a tea beverage containing the fresh tea leaf extract, and a method for practically producing the fresh tea leaf extract without going through complicated steps Made up of.
本発明者は、上記課題を解決すべく鋭意検討する中で、生茶葉抽出エキスの製造方法において、生茶葉を急速冷凍する工程、及び、凍結された不粉砕生茶葉から生茶葉抽出エキスを抽出する工程、による処理を採用することにより、風味バランスと飲みやすさを備えた生茶葉抽出エキスを製造することができることを見い出し、本発明を完成するに至った。すなわち本発明は、生茶葉抽出エキスの製造方法において、(A)生茶葉を急速冷凍する工程、及び(B)凍結された不粉砕生茶葉から生茶葉抽出エキスを抽出する工程、による処理を含むことにより風味バランスと飲みやすさを備えた生茶葉抽出エキスを製造する方法からなる。 The present inventor has intensively studied to solve the above problems, and in the method for producing a fresh tea leaf extract, a step of rapidly freezing fresh tea leaves, and extraction of fresh tea leaf extract from frozen unground green tea leaves It has been found that a raw tea leaf extract having a flavor balance and ease of drinking can be produced by adopting the treatment according to the step, and the present invention has been completed. That is, the present invention includes a process of (A) a step of rapidly freezing fresh tea leaves and (B) a step of extracting a fresh tea leaf extract from frozen unground green tea leaves in a method for producing a fresh tea leaf extract. The method comprises producing a fresh tea leaf extract having a flavor balance and ease of drinking.
本発明の生茶葉抽出エキスの製造方法により、茶葉感が強く、爽やかさ、みずみずしさ、甘い香りを有し、渋味や雑味が低減され、全体的な風味・バランスや飲みやすさの点においても優れた生茶葉抽出エキスを製造することができる。本発明の生茶葉抽出エキスの製造方法においては、上記(A)及び(B)の工程に、更に、(C)生茶葉抽出エキスに酵素を添加する工程を付加することにより、旨味を向上させ、全体的な風味・バランスの良さや飲みやすさを向上させることができる。かかる場合の酵素としては、ぺクチナーゼ及び/又はタンナーゼを挙げることができる。 The method for producing a fresh tea leaf extract of the present invention has a strong tea leaf feeling, refreshingness, freshness, sweet aroma, reduced astringency and miscellaneous taste, and overall flavor / balance and ease of drinking Can also produce an excellent fresh tea leaf extract. In the method for producing a fresh tea leaf extract of the present invention, the process of (A) and (B) is further improved by adding a step of adding an enzyme to the fresh tea leaf extract (C). , Overall flavor, good balance and ease of drinking can be improved. Examples of such enzymes include pectinase and / or tannase.
本発明の生茶葉抽出エキスの製造方法において、凍結された不粉砕生茶葉から生茶葉抽出エキスを抽出する工程は、カラム抽出により行なうことができる。かかる場合のカラム抽出は、抽出温度95〜40℃で行うことが好ましい。本発明の生茶葉抽出エキスの製造方法により、風味バランスと飲みやすさを備えた生茶葉抽出エキスを製造することができ、該生茶葉抽出エキスを含有させた飲食品を調製することができる。かかる飲食品としては、緑茶飲料を挙げることができる。 In the method for producing a fresh tea leaf extract of the present invention, the step of extracting the fresh tea leaf extract from the frozen unground green tea leaf can be performed by column extraction. In this case, the column extraction is preferably performed at an extraction temperature of 95 to 40 ° C. By the method for producing a fresh tea leaf extract of the present invention, a fresh tea leaf extract having a flavor balance and ease of drinking can be produced, and a food and drink containing the fresh tea leaf extract can be prepared. Examples of such foods and drinks include green tea beverages.
すなわち、具体的には本発明は、
(1)生茶葉抽出エキスの製造方法であって、以下の工程:
(A)生茶葉を急速冷凍する工程、
(B)凍結された不粉砕生茶葉から生茶葉抽出エキスを抽出する工程、
による処理を含むことを特徴とする風味バランスと飲みやすさを備えた生茶葉抽出エキスの製造方法や、
(2)生茶葉抽出エキスの製造方法であって、上記(1)記載の(A)及び(B)の工程に、更に、(C)生茶葉抽出エキスに酵素を添加する工程、による処理を含むことを特徴とする上記(1)記載の風味バランスと飲みやすさを備えた生茶葉抽出エキスの製造方法や、
(3)凍結された不粉砕生茶葉から生茶葉抽出エキスを抽出する工程が、カラム抽出により行なわれることを特徴とする上記(1)又は(2)に記載の風味バランスと飲みやすさを備えた生茶葉抽出エキスの製造方法、
からなる。
Specifically, the present invention specifically relates to
(1) A method for producing a fresh tea leaf extract, the following steps:
(A) a process of rapidly freezing fresh tea leaves,
(B) a process of extracting a fresh tea leaf extract from frozen unground green tea leaves,
A method for producing a fresh tea leaf extract having a flavor balance and ease of drinking, characterized by including a treatment by
(2) A method for producing a fresh tea leaf extract, comprising the steps (A) and (B) described in (1) above, and (C) a step of adding an enzyme to the fresh tea leaf extract. A method for producing a fresh tea leaf extract having a flavor balance and ease of drinking as described in (1) above,
(3) The process of extracting a fresh tea leaf extract from frozen unground green tea leaves is performed by column extraction, and has the flavor balance and ease of drinking as described in (1) or (2) above Method for producing fresh tea leaf extract,
Consists of.
また、本発明は、
(4)カラム抽出が、95〜40℃で行われることを特徴とする上記(3)に記載の風味バランスと飲みやすさを備えた生茶葉抽出エキスの製造方法や、
(5)生茶葉抽出エキスに添加する酵素が、ペクチナーゼ及び/又はタンナーゼであることを特徴とする上記(2)〜(4)のいずれかに記載の風味バランスと飲みやすさを備えた生茶葉抽出エキスの製造方法や、
(6)上記(1)〜(5)のいずれかに記載の生茶葉抽出エキスの製造方法により製造された風味バランスと飲みやすさを備えた生茶葉抽出エキスや、
(7)上記(6)記載の生茶葉抽出エキスを含有させたことを特徴とする飲食品や、
(8)飲食品が、緑茶飲料であることを特徴とする上記(7)に記載の飲食品、
からなる。
The present invention also provides:
(4) The method for producing a fresh tea leaf extract having a flavor balance and ease of drinking as described in (3) above, wherein the column extraction is performed at 95 to 40 ° C,
(5) The fresh tea leaves having a flavor balance and ease of drinking according to any one of (2) to (4) above, wherein the enzyme added to the fresh tea leaf extract is pectinase and / or tannase Manufacturing method of extract,
(6) A fresh tea leaf extract having a flavor balance and ease of drinking produced by the method for producing a fresh tea leaf extract according to any one of (1) to (5) above,
(7) A food or drink characterized by containing the fresh tea leaf extract described in (6) above,
(8) The food or drink according to (7) above, wherein the food or drink is a green tea drink,
Consists of.
本発明は、茶葉感が強く、爽やかさ、みずみずしさ、甘い香りを有し、渋味や雑味が低減され、全体的な風味・バランスや飲みやすさを備えた優れた香味の生茶葉抽出エキス、及びその製造方法を提供する。本発明の生茶葉抽出エキスの製造方法により、複雑な工程を経ることなく、実用的な方法で風味・バランスや飲みやすさを備えた生茶葉抽出エキスを提供することができる。また、本発明の生茶葉抽出エキスを用いることにより、緑茶飲料のような香味に優れた飲食品を提供することができる。 The present invention has a strong tea leaf feeling, freshness, freshness, sweet scent, reduced astringency and miscellaneous taste, and excellent flavor of fresh tea leaves with overall flavor, balance and ease of drinking An extract and a method for producing the same are provided. By the method for producing a fresh tea leaf extract of the present invention, a fresh tea leaf extract having flavor, balance and ease of drinking can be provided by a practical method without going through complicated steps. Moreover, the food / beverage products excellent in flavor like a green tea drink can be provided by using the raw tea leaf extract of this invention.
本発明は、生茶葉抽出エキスの製造方法において、(A)生茶葉を急速冷凍する工程、及び(B)凍結された不粉砕生茶葉から生茶葉抽出エキスを抽出する工程、或いは、更に、(C)生茶葉抽出エキスに酵素を添加する工程、による処理を採用することにより、風味バランスと飲みやすさを備えた生茶葉抽出エキスを製造する方法からなる。 The present invention provides a method for producing a fresh tea leaf extract, wherein (A) a step of rapidly freezing fresh tea leaves and (B) a step of extracting a fresh tea leaf extract from frozen unground green tea leaves, or C) It comprises a method for producing a fresh tea leaf extract having a flavor balance and ease of drinking by adopting a process of adding an enzyme to the fresh tea leaf extract.
本発明において用いられる茶葉は特に限定されないが、Camellia sinensisに属する茶葉等を用いることができる。 The tea leaves used in the present invention are not particularly limited, and tea leaves belonging to Camellia sinensis can be used.
本発明の生茶葉抽出エキスの製造方法においては、生茶葉を急速冷凍により冷凍処理される。ここで定義する急速冷凍とは、実質的に茶葉の酵素活性がゼロになる0℃以下まで、冷却開始より1時間以内、好ましくは30分以内に冷却することであり、使用する装置としてはIQF凍結装置、ブライン凍結装置、急速冷凍庫などが挙げられる。本発明において好ましくは、IQF凍結装置を用いることができる。緩慢冷凍であると香味上好ましくなく、特に茶葉感が弱く、爽やかさ、みずみずしさ、甘い香りが低くなり、渋味、雑味が強くなる傾向がある。ここで定義する緩慢冷凍とは常温の茶葉を脱気、冷却等の前処理を行わず、−10〜−30℃の雰囲気下の冷凍庫内にて保存し凍結を行うことである。生茶葉を緩慢冷凍すると、自己の酵素活性により発熱し、凍結するまでに長時間要するために品質が劣化する。 In the method for producing a fresh tea leaf extract of the present invention, fresh tea leaves are frozen by quick freezing. Rapid freezing as defined herein means cooling within 1 hour, preferably within 30 minutes from the start of cooling, to 0 ° C. or below at which the enzyme activity of tea leaves becomes substantially zero. A freezing apparatus, a brine freezing apparatus, a quick freezer, etc. are mentioned. In the present invention, preferably, an IQF freezing apparatus can be used. When it is slowly frozen, it is not preferable in terms of flavor, in particular, the tea leaf feeling is weak, freshness, freshness, sweet aroma is lowered, and there is a tendency for astringency and miscellaneous taste to become strong. Slow freezing as defined herein refers to storing and freezing tea leaves at room temperature in a freezer in an atmosphere of −10 to −30 ° C. without pretreatment such as deaeration and cooling. When raw tea leaves are slowly frozen, heat is generated due to their own enzyme activity, and the quality deteriorates because it takes a long time to freeze.
本発明の生茶葉抽出エキスの製造方法においては、凍結された不粉砕生茶葉から生茶葉抽出エキスを抽出する。本発明において、凍結された不粉砕生茶葉から生茶葉抽出エキスを抽出するために用いられる抽出方法は、カラム抽出が好ましい。バッチ抽出では、カラム抽出と比較すると、茶葉感に欠け、渋味、雑味が強くなる傾向があり、全体的な香味バランスや飲みやすさの点においてもカラム抽出の方が好ましい。 In the method for producing a fresh tea leaf extract of the present invention, a fresh tea leaf extract is extracted from frozen unground green tea leaves. In the present invention, the extraction method used for extracting the fresh tea leaf extract from the frozen unground green tea leaves is preferably column extraction. Compared with column extraction, batch extraction lacks the tea leaf feeling and tends to have astringent taste and miscellaneous taste, and column extraction is preferable in terms of overall flavor balance and ease of drinking.
カラム抽出とは、抽出出口にストレーナーを備えた抽出容器に抽出原料を充填し、抽出容器の上部若しくは下部より抽出溶媒を供給し、抽出原料を対流させずに抽出する方法であり、高濃度の抽出液を得ることができる。装置としてはカラム抽出機やドリップ抽出機が挙げられる。本発明において好ましくはカラム抽出機を用いることができる。バッチ抽出とは、抽出容器に抽出原料と抽出溶媒を投入して攪拌抽出を行う方法である。 Column extraction is a method in which an extraction vessel equipped with a strainer at the extraction outlet is filled with an extraction raw material, an extraction solvent is supplied from the upper or lower portion of the extraction vessel, and the extraction raw material is extracted without convection. An extract can be obtained. Examples of the apparatus include a column extractor and a drip extractor. In the present invention, a column extractor can be preferably used. Batch extraction is a method in which an extraction raw material and an extraction solvent are put into an extraction container and agitation extraction is performed.
本発明の生茶葉抽出エキスの製造方法において、生茶葉抽出エキスの抽出時の温度は、95〜40℃が好ましく、更に好ましくは95〜70℃である。95℃を超えると加熱臭や劣化臭が発生し、かつ褐変することにより風味が悪くなるという問題があり、40℃未満であると香味上好ましくなく、特に茶葉感に欠け、渋味、雑味が強くなる傾向がある。本発明においては、凍結された生茶葉は粉砕やこれに類する処理を行わず、生茶葉そのままの形態で用いられる。生茶葉を粉砕すると、爽やかさ、みずみずしさ、甘い香りが低くなり、特に渋味、雑味が強くなる傾向がある。 In the method for producing a fresh tea leaf extract of the present invention, the temperature during the extraction of the fresh tea leaf extract is preferably 95 to 40 ° C, more preferably 95 to 70 ° C. When it exceeds 95 ° C, there is a problem that a heating odor or a deterioration odor is generated and the flavor is deteriorated by browning, and when it is less than 40 ° C, the flavor is not preferred, and particularly the tea leaf feeling is lacking, astringency, miscellaneous taste. Tend to be stronger. In the present invention, the frozen raw tea leaves are used in the form of raw tea leaves as they are without being crushed or similar treatment. When fresh tea leaves are crushed, freshness, freshness and sweet aroma are lowered, and in particular, astringency and miscellaneous taste tend to increase.
本発明の生茶葉抽出エキスの製造方法において、生茶葉抽出エキスに酵素を添加して処理することができる。用いられる酵素としては、ぺクチナーゼ、タンナーゼ、アミラーゼ、リパーゼ、マンナナーゼが挙げられ、これらを1種又は2種以上を組み合わせて用いることができる。好ましくは、ぺクチナーゼ又はタンナーゼであり、特に、好ましくはペクチナーゼとタンナーゼを併用することである。このような酵素処理を行うことにより、旨味が向上し、特に全体的な風味・バランスの良さや飲みやすさが向上する。 In the method for producing a fresh tea leaf extract of the present invention, the fresh tea leaf extract can be treated by adding an enzyme. Examples of the enzyme used include pectinase, tannase, amylase, lipase, and mannanase, and these can be used alone or in combination of two or more. Pectinase or tannase is preferable, and pectinase and tannase are particularly preferably used in combination. By performing such an enzyme treatment, the umami is improved, and in particular, the overall flavor and balance and the ease of drinking are improved.
本発明の生茶葉抽出エキスは様々な飲食品に含有させ、香味豊かな飲食品を製造することができる。例えば、清涼飲料、冷菓・デザート類である。中でも、緑茶飲料に含有させることが好ましい。飲料においては、本発明の生茶葉抽出エキスを飲料原料に含有させて、そのまま飲用する場合はもちろん、UHT殺菌やレトルト殺菌を施した容器詰め飲料に含有させることもできる。 The raw tea leaf extract of the present invention can be contained in various foods and drinks to produce flavorful foods and drinks. For example, soft drinks, frozen desserts and desserts. Especially, it is preferable to make it contain in a green tea drink. In beverages, the raw tea leaf extract of the present invention can be contained in a beverage raw material and used as it is, as well as in a container-packed beverage subjected to UHT sterilization or retort sterilization.
本発明の生茶葉エキスやこれを含有させた飲食品においては渋味が低減されているが、渋味の原因の一つにタンニン、カテキンが挙げられる。タンニンの測定は、酒石酸鉄比色法、フォーリンチオカルト法などの方法で測定することができる。本発明においてカテキンの測定は、HPLC法で測定することができる。本発明において香気成分の測定は、香気成分の抽出濃縮操作を行なった上でGC法で測定することができる。抽出濃縮操作としてはヘッドスペース法、固相抽出法、固相マイクロ抽出(SPME)法、溶剤抽出法、スターバー抽出(SBSE)法などの方法が挙げられる。 In the fresh tea leaf extract of the present invention and foods and drinks containing the same, astringency is reduced, but tannin and catechin are one of the causes of astringency. Tannin can be measured by methods such as iron tartrate colorimetric method and foreign thiocult method. In the present invention, catechin can be measured by the HPLC method. In the present invention, the aromatic component can be measured by the GC method after extracting and concentrating the aromatic component. Examples of the extraction and concentration operation include methods such as a head space method, a solid phase extraction method, a solid phase micro extraction (SPME) method, a solvent extraction method, and a star bar extraction (SBSE) method.
本発明の官能評価に用いられている評価項目において、「茶葉感」とは生葉から感じる滋味を表現し、「爽やかさ」とは生葉のもつ新鮮香や軽い青さを表し、「青臭さ」とは好ましくない草様の青臭を意味し、「みずみずしさ」とはみる芽香があり後味がスッキリしていることであり、「甘い香り」とは華やかで蜜のような香りがすることであり、「渋味」とは飲んだ後に舌に残る渋みを指し、「旨味」とは飲んだ後に感じる旨味のことで、「雑味」とは舌にざらつきを伴う収斂味のことで、「風味・バランスの良さ」とは香りと呈味の一体感を指し、「飲みやすさ」とは喉越しよく飲める感覚を評価する項目である。 In the evaluation items used in the sensory evaluation of the present invention, “tea leaf feeling” expresses the taste felt from fresh leaves, “freshness” represents the fresh aroma and light blueness of fresh leaves, and “blue smell” Means an unpleasant grass-like blue odor, `` Mizumizushi '' means that there is a scented scent and a refreshing aftertaste. Yes, `` Astringency '' refers to the astringency that remains on the tongue after drinking, `` Umami '' refers to the umami that you feel after drinking, and `` Misami taste '' refers to the astringent taste with a rough texture on the tongue, “Flavor / balance” refers to a sense of unity between fragrance and taste, and “ease of drinking” is an item that evaluates the sense of being able to drink well over the throat.
以下、実施例によって本発明をより具体的に説明するが、本発明はこれらに制限されるものではない。 Hereinafter, the present invention will be described more specifically with reference to examples, but the present invention is not limited thereto.
[冷凍方法について(急速冷凍、緩慢冷凍)条件No.1,2]
<No.1>:洗浄した生茶葉をIQF凍結装置にて20分間処理し、生茶葉の温度を0℃に冷却した後、−20℃の冷凍庫で1ヶ月保存した。次にこの凍結生茶葉400gをカラム抽出機に充填し、カラム抽出を行った。90℃の熱水をカラム下部より通液し、カラム上部より抽出液を得、生茶葉の3倍量である1200gの抽出液を得た。次に、液量に対して0.03%(w/w)のビタミンCを加え、3000rpm、10分間の遠心分離を行った。遠心分離後、濾紙(アドバンテック東洋株式会社製No.2)で濾過を行なった。得られた抽出液を重曹でpH6.0に調整したのち、80℃ 10分間の殺菌を行い、生茶葉抽出エキスを得た。
[Regarding the freezing method (rapid freezing, slow freezing) 1, 2]
<No. 1>: Washed fresh tea leaves were treated with an IQF freezer for 20 minutes, the temperature of the fresh tea leaves was cooled to 0 ° C, and then stored in a freezer at -20 ° C for 1 month. Next, 400 g of the frozen fresh tea leaves were packed into a column extractor, and column extraction was performed. Hot water at 90 ° C. was passed from the lower part of the column, and an extract was obtained from the upper part of the column to obtain 1200 g of extract that was three times the amount of fresh tea leaves. Next, 0.03% (w / w) of vitamin C was added to the liquid volume, and centrifugation was performed at 3000 rpm for 10 minutes. After centrifugation, filtration was performed with a filter paper (No. 2 manufactured by Advantech Toyo Co., Ltd.). The obtained extract was adjusted to pH 6.0 with sodium bicarbonate and then sterilized at 80 ° C. for 10 minutes to obtain a fresh tea leaf extract.
<No.2>:実施例1において、IQF凍結装置を使用せず、洗浄後−20℃の冷凍庫にて保存した。生茶葉の温度は冷凍開始より36時間後に0℃に達した。そのまま−20℃の冷凍庫で1ヶ月保存した。以降は実施例1と同様にして生茶葉抽出エキスを得た。得られた抽出液をBrix 0.2に希釈し、ビタミンC、重曹を用いてpH6.0になるように調整した飲料を作成し、官能評価を行った。官能評価は、7人の専門パネルにより以下の要領にて行った。 <No. 2>: In Example 1, the IQF freezing apparatus was not used, and the sample was stored in a freezer at −20 ° C. after washing. The temperature of the fresh tea leaves reached 0 ° C. 36 hours after the start of freezing. It was stored for one month in a -20 ° C freezer. Thereafter, a raw tea leaf extract was obtained in the same manner as in Example 1. The obtained extract was diluted with Brix 0.2, a beverage adjusted to pH 6.0 with vitamin C and sodium bicarbonate was prepared, and sensory evaluation was performed. Sensory evaluation was carried out by the following 7 points using 7 expert panels.
<茶葉感、爽やかさ、青臭さ、みずみずしさ、甘い香り、渋味、旨味および雑味は>:1点が弱い、2点は少し弱い、3点は普通、4点は少し強い、5点は強い、で評価した。<風味・バランスの良さ、飲みやすさは>:1点が悪い、2点が少し悪い、3点がどちらでもない、4点が少し良い、5点が良い、で評価した。 <Tea leaf feeling, freshness, blue odor, freshness, sweet aroma, astringency, umami and miscellaneous taste>: 1 point is weak, 2 points are slightly weak, 3 points are normal, 4 points are slightly strong, 5 points Was strong, evaluated. <Flavor, good balance and ease of drinking> Evaluation was made with 1 point being bad, 2 points being slightly bad, 3 points being neither, 4 points being good, and 5 points being good.
[結果]
結果を、表1に示す。本発明の製造方法において、急速冷凍を採用して他の工程と組み合わせることにより、緩慢な冷凍を行った場合と比較して、特に茶葉感に富み、爽やかさ、みずみずしさ、甘い香りの評価が高くなり、渋味、雑味が抑えられる。また、全体的な風味・バランスや飲みやすさの点においても優れている結果であった。
[result]
The results are shown in Table 1. In the manufacturing method of the present invention, by adopting quick freezing and combining with other processes, compared with the case where slow freezing is performed, the tea leaf feeling is particularly rich, and refreshing, freshness, and sweet aroma are evaluated. It becomes high and astringency and miscellaneous taste are suppressed. In addition, the results were excellent in terms of overall flavor and balance and ease of drinking.
[抽出方法について(カラム抽出、バッチ抽出)条件No.1,8]
<No.8>:洗浄した生茶葉をIQF凍結装置にて20分間処理し、0℃に冷却した後、−20℃の冷凍庫で1ヶ月保存した。この凍結生茶葉 200gに対し、3倍量である600gの90℃の熱水に入れ、時々攪拌しながら1分間バッチ抽出を行った。次に、液量に対して0.03%(w/w)のビタミンCを加え、3000rpm、10分間の遠心分離を行った。遠心分離後、濾紙(アドバンテック東洋株式会社製No.2)で濾過を行なった。得られた抽出液を重曹でpH6.0に調整したのち、80℃10分間の殺菌を行い、生茶葉抽出エキスを得た。官能評価は、実施例1と同様に実施した。
[Extraction method (column extraction, batch extraction) Condition No. 1,8]
<No. 8>: Washed fresh tea leaves were treated with an IQF freezer for 20 minutes, cooled to 0 ° C., and stored in a freezer at −20 ° C. for 1 month. 200 g of this frozen fresh tea leaf was placed in 600 g of 90 ° C. hot water, which is three times the amount, and batch extraction was performed for 1 minute with occasional stirring. Next, 0.03% (w / w) of vitamin C was added to the liquid volume, and centrifugation was performed at 3000 rpm for 10 minutes. After centrifugation, filtration was performed with a filter paper (No. 2 manufactured by Advantech Toyo Co., Ltd.). The obtained extract was adjusted to pH 6.0 with sodium bicarbonate and then sterilized at 80 ° C. for 10 minutes to obtain a fresh tea leaf extract. The sensory evaluation was performed in the same manner as in Example 1.
[結果]
結果を表2に示す。本発明の製造方法において、カラム抽出を採用して他の工程と組み合わせることにより、バッチ抽出を行った場合と比較して、茶葉感に富み、特に渋味、雑味が非常に低く抑えられる。また、全体的な風味・バランスや飲みやすさの点においても優れている結果であった。また、香気成分の分析の結果を以下に示す。
[result]
The results are shown in Table 2. In the production method of the present invention, by adopting column extraction and combining with other steps, it is rich in tea leaf feeling, especially astringency and miscellaneous taste, compared to the case where batch extraction is performed. In addition, the results were excellent in terms of overall flavor and balance and ease of drinking. Moreover, the result of the analysis of an aroma component is shown below.
<香気の分析条件>
生茶葉抽出エキスをBrix 0.2になるように希釈し、サンプルとした。サンプル10mlに対し、内部標準として10ppbのEthyl Benzoate溶液を10μl添加した。塩化ナトリウムを3g添加したあと、固相マイクロ抽出(SPME)法を用いて抽出し、GC/MSにて分析を行った。抽出条件:60℃、30分;脱着温度:240℃;GC:Agilent6890N;検出器:Agilent5973;カラム:TC−WAX 60m×0.25μm×I.D.0.25mm;温度:70℃(1分)→240℃ 昇温 4℃/分
<Aroma analysis conditions>
The fresh tea leaf extract was diluted to Brix 0.2 and used as a sample. 10 μl of 10 ppb Ethyl Benzoate solution was added to 10 ml of sample as an internal standard. After adding 3 g of sodium chloride, extraction was performed using a solid phase microextraction (SPME) method, and analysis was performed by GC / MS. Extraction conditions: 60 ° C., 30 minutes; Desorption temperature: 240 ° C .; GC: Agilent 6890N; Detector: Agilent 5973; Column: TC-WAX 60 m × 0.25 μm × I. D. 0.25 mm; Temperature: 70 ° C. (1 minute) → 240 ° C. Temperature rise 4 ° C./min
結果を、表3に示す。下記の香気成分の分析結果より、カラム抽出を採用して他の工程と組み合わせることにより、野草臭であり低級茶葉の指標となるtrans-2-hexenalやcis-3-hexenyl acetateは低く抑えられており、官能評価の茶葉感が高くなる点、青臭さが低くなる点と相関していることがわかる。 The results are shown in Table 3. From the analysis results of the following fragrance components, trans-2-hexenal and cis-3-hexenyl acetate, which are wild grass odors and indicators of lower tea leaves, are kept low by adopting column extraction and combining with other processes. Thus, it can be seen that this is correlated with the point that the sense of tea leaves in sensory evaluation is high and the point that blue odor is low.
[抽出方法について(カラム抽出)条件No.1、3、4,5,6]
<No.3>:No.1において、抽出を70℃の熱水で行う以外は同様にして生茶葉抽出エキスを得た。
<No.4>:No.1において、抽出を55℃の温水で行う以外は同様にして生茶葉抽出エキスを得た。
<No.5>:No.1において、抽出を40℃の温水で行う以外は同様にして生茶葉抽出エキスを得た。
<No.6>:No.1において、抽出を10℃の冷水で行う以外は同様にして生茶葉抽出エキスを得た。
官能評価は、実施例1と同様に実施した。
[Extraction method (column extraction) Condition No. 1, 3, 4, 5, 6]
<No. 3>: No. In Example 1, a fresh tea leaf extract was obtained in the same manner except that extraction was performed with hot water at 70 ° C.
<No. 4>: No. In Example 1, a fresh tea leaf extract was obtained in the same manner except that the extraction was performed with hot water at 55 ° C.
<No. 5>: No. In Example 1, a fresh tea leaf extract was obtained in the same manner except that the extraction was performed with warm water at 40 ° C.
<No. 6>: No. In Example 1, a fresh tea leaf extract was obtained in the same manner except that extraction was performed with cold water at 10 ° C.
The sensory evaluation was performed in the same manner as in Example 1.
[結果]
結果を表4に示す。本発明の製造方法において、抽出温度を比較的高くして他の工程と組み合わせることにより、特に茶葉感に富み、爽やかさ、みずみずしさ、甘い香りの評価が高くなり、渋味、雑味が抑えられる。また、全体的な風味・バランスや飲みやすさの点においても優れている結果であった。以上の結果から、抽出温度は95〜40℃が好ましく、95〜70℃が更に好ましい。
[result]
The results are shown in Table 4. In the production method of the present invention, by combining the extraction temperature with other processes at a relatively high temperature, the tea leaf feeling is particularly rich and the evaluation of freshness, freshness and sweet aroma is enhanced, and astringency and miscellaneous taste are suppressed. It is done. In addition, the results were excellent in terms of overall flavor and balance and ease of drinking. From the above results, the extraction temperature is preferably 95 to 40 ° C, more preferably 95 to 70 ° C.
香気成分の分析結果を表5に示す。表5の香気成分の分析結果より、カラム抽出による抽出温度を高くするほど、野草臭であり低級茶葉の指標となるcis-3-hexenyl acetateは低く抑えられ、フレッシュな爽やかさの指標となるcis-3-hexenolは概ね高くなり、cis-3-hexenol/cis-3-hexenyl acetateの値は高くなることがわかる。以上の香気分析結果は、官能評価の爽やかさ、みずみずしさが高い点と相関していることがわかる。 Table 5 shows the analysis results of the aroma components. From the results of analysis of aroma components in Table 5, the higher the extraction temperature by column extraction, the lower the cis-3-hexenyl acetate, which is a wild grass odor and is an indicator of lower tea leaves, and a cis that is an indicator of fresh freshness. It can be seen that -3-hexenol is generally high, and that cis-3-hexenol / cis-3-hexenyl acetate is high. It can be seen that the above fragrance analysis results correlate with the freshness and freshness of sensory evaluation.
[生茶葉の粉砕処理の有無 条件No.1、7、8、9]
[方法]:
<No.7>:No.1において、凍結生茶葉400gをミキサー(パナソニック株式会社製ミキサーMX−X57)にて粉砕してからカラム抽出した以外はNo.1と同様にし、生茶葉抽出エキスを得た。
<N0.9>:No.1において得られた凍結生茶葉200gに対し、3倍量である600gの90℃の熱水に入れミキサー(パナソニック株式会社製ミキサーMX−X57)にて1分間粉砕し、バッチ抽出した。次に、液量に対して0.03%(w/w)のビタミンCを加え、3000rpm、10分間の遠心分離を行った。遠心分離後、濾紙(アドバンテック東洋株式会社製No.2)で濾過を行なった。得られた抽出液を重曹でpH6.0に調整したのち、80℃、10分間の殺菌を行い、生茶葉抽出エキスを得た。(No.8は実施例2にて記載)官能評価は、実施例1と同様に実施した。
[Presence / absence of crushed raw tea leaves Condition No. 1, 7, 8, 9]
[Method]:
<No. 7>: No. No. 1 except that 400 g of frozen fresh tea leaves were crushed with a mixer (Mixer MX-X57 manufactured by Panasonic Corporation) and then extracted with a column. In the same manner as in No. 1, a fresh tea leaf extract was obtained.
<N0.9>: No. 200 g of the frozen fresh tea leaves obtained in 1 were placed in 600 g of 90 ° C. hot water, which is three times the volume, and pulverized for 1 minute with a mixer (Mixer MX-X57 manufactured by Panasonic Corporation), and batch extracted. Next, 0.03% (w / w) of vitamin C was added to the liquid volume, and centrifugation was performed at 3000 rpm for 10 minutes. After centrifugation, filtration was performed with a filter paper (No. 2 manufactured by Advantech Toyo Co., Ltd.). The obtained extract was adjusted to pH 6.0 with sodium bicarbonate and then sterilized at 80 ° C. for 10 minutes to obtain a fresh tea leaf extract. (No. 8 is described in Example 2) Sensory evaluation was performed in the same manner as in Example 1.
[結果]
結果を、表6(カラム抽出)及び表7(バッチ抽出)に示す。本発明の製造方法において、生茶葉を粉砕処理に供さず、生茶葉そのままの形態で用いて他の工程と組み合わせることにより、爽やかさ、みずみずしさ、甘い香りの評価が高くなり、特に渋味、雑味が抑えられる。
[result]
The results are shown in Table 6 (column extraction) and Table 7 (batch extraction). In the production method of the present invention, fresh tea leaves are not subjected to pulverization treatment, but are used in the form of fresh tea leaves as they are, and combined with other processes, the evaluation of freshness, freshness, sweet scent becomes high, especially astringency The miscellaneous taste is suppressed.
[生茶葉の酵素処理の有無 条件No.1、12、13、14]
<No.12>:No.1において得られた凍結生茶葉400gをカラム抽出機に充填し、カラム抽出を行った。90℃の熱水をカラム下部より通液し、カラム上部より抽出液を得、生茶葉の3倍量である1200gの抽出液を得た。次に、液量に対して0.03%(w/w)のビタミンC、0.005%(w/w)のペクチナーゼG「アマノ」(天野エンザイム株式会社製)を加え、40℃で1時間攪拌反応させた。反応の後、3000rpm、10分間の遠心分離を行った。遠心分離後、濾紙(アドバンテック東洋株式会社製No.2)で濾過を行なった。得られた抽出液を重曹でpH6.0に調整したのち、80℃、10分間の殺菌を行い、生茶葉抽出エキスを得た。
[Presence or absence of enzyme treatment of fresh tea leaves Condition No. 1, 12, 13, 14]
<No. 12>: No. A column extractor was filled with 400 g of the frozen fresh tea leaves obtained in 1, and column extraction was performed. Hot water at 90 ° C. was passed from the lower part of the column, and an extract was obtained from the upper part of the column to obtain 1200 g of extract that was three times the amount of fresh tea leaves. Next, 0.03% (w / w) of vitamin C and 0.005% (w / w) of pectinase G “Amano” (manufactured by Amano Enzyme Co., Ltd.) are added to the liquid volume, and 1 at 40 ° C. The reaction was stirred for an hour. After the reaction, centrifugation was performed at 3000 rpm for 10 minutes. After centrifugation, filtration was performed with a filter paper (No. 2 manufactured by Advantech Toyo Co., Ltd.). The obtained extract was adjusted to pH 6.0 with sodium bicarbonate and then sterilized at 80 ° C. for 10 minutes to obtain a fresh tea leaf extract.
<No.13>:No.12において、ペクチナーゼG「アマノ」の代わりに0.0003%(w/w)のタンナーゼFKT50(キッコーマン株式会社製)を使用した以外は同様にして生茶葉抽出エキスを得た。
<No.14>No.12においてペクチナーゼG「アマノ」に加え0.0003%(w/w)のタンナーゼFTK50(キッコーマン株式会社製)を使用した以外は同様にして生茶葉抽出エキスを得た。
官能評価は、実施例1と同様に実施した。
<No. 13>: No. In Example 12, a fresh tea leaf extract was obtained in the same manner except that 0.0003% (w / w) tannase FKT50 (manufactured by Kikkoman Corporation) was used instead of pectinase G “Amano”.
<No. 14> No. In Example 12, a fresh tea leaf extract was obtained in the same manner except that 0.0003% (w / w) tannase FTK50 (manufactured by Kikkoman Corporation) was used in addition to pectinase G “Amano”.
The sensory evaluation was performed in the same manner as in Example 1.
[結果]
結果を表8に示す。本発明の製造方法において、酵素処理工程を他の工程と組み合わせることにより、旨味の評価が高くなり、特にぺクチナーゼとタンナーゼを併用することにより、全体的な風味・バランスや飲みやすさの点において優れた生茶葉抽出エキスを製造できることがわかった。
[result]
The results are shown in Table 8. In the production method of the present invention, the evaluation of umami is enhanced by combining the enzyme treatment step with other steps, and particularly in combination with pectinase and tannase, in terms of overall flavor / balance and ease of drinking. It was found that an excellent fresh tea leaf extract can be produced.
本発明は、茶葉感が強く、爽やかさ、みずみずしさ、甘い香りを有し、渋味や雑味が低減され、全体的な風味・バランスや飲みやすさを備えた優れた香味の生茶葉抽出エキス、及びその製造方法を提供する。本発明の生茶葉抽出エキスの製造方法により、複雑な工程を経ることなく、実用的な方法で風味・バランスや飲みやすさを備えた生茶葉抽出エキスを提供することができる。
The present invention has a strong tea leaf feeling, freshness, freshness, sweet scent, reduced astringency and miscellaneous taste, and excellent flavor of fresh tea leaves with overall flavor, balance and ease of drinking An extract and a method for producing the same are provided. By the method for producing a fresh tea leaf extract of the present invention, a fresh tea leaf extract having flavor, balance and ease of drinking can be provided by a practical method without going through complicated steps.
Claims (8)
(A)生茶葉を急速冷凍する工程、
(B)凍結された不粉砕生茶葉から生茶葉抽出エキスを抽出する工程、
による処理を含むことを特徴とする風味バランスと飲みやすさを備えた生茶葉抽出エキスの製造方法。 A method for producing a fresh tea leaf extract comprising the following steps:
(A) a process of rapidly freezing fresh tea leaves,
(B) a process of extracting a fresh tea leaf extract from frozen unground green tea leaves,
A method for producing a fresh tea leaf extract having a flavor balance and ease of drinking, characterized in that it comprises a treatment according to claim 1.
による処理を含むことを特徴とする請求項1記載の風味バランスと飲みやすさを備えた生茶葉抽出エキスの製造方法。 A method for producing a fresh tea leaf extract, wherein (C) a step of adding an enzyme to the fresh tea leaf extract, in addition to the steps (A) and (B) according to claim 1,
The method for producing a fresh tea leaf extract having a flavor balance and ease of drinking according to claim 1.
The food / beverage product according to claim 7, wherein the food / beverage product is a green tea beverage.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2009295163A JP5144638B2 (en) | 2009-12-25 | 2009-12-25 | Fresh tea leaf extract with flavor balance and ease of drinking, and method for producing the same |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2009295163A JP5144638B2 (en) | 2009-12-25 | 2009-12-25 | Fresh tea leaf extract with flavor balance and ease of drinking, and method for producing the same |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2011130740A true JP2011130740A (en) | 2011-07-07 |
JP5144638B2 JP5144638B2 (en) | 2013-02-13 |
Family
ID=44344143
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2009295163A Active JP5144638B2 (en) | 2009-12-25 | 2009-12-25 | Fresh tea leaf extract with flavor balance and ease of drinking, and method for producing the same |
Country Status (1)
Country | Link |
---|---|
JP (1) | JP5144638B2 (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103704423A (en) * | 2014-01-02 | 2014-04-09 | 绿锦发展(福建)有限公司 | Preparation method for tea extract |
Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2000050798A (en) * | 1998-08-05 | 2000-02-22 | Hisashi Takeuchi | Frozen tea leaf and its production |
JP2001258477A (en) * | 2000-03-16 | 2001-09-25 | Kirin Beverage Corp | Green tea beverage in sealed container and method for producing the same |
JP2003111558A (en) * | 2001-10-03 | 2003-04-15 | T Hasegawa Co Ltd | Method for producing tea extract |
JP2004321105A (en) * | 2003-04-25 | 2004-11-18 | Kao Corp | Green tea extract treated with tannase |
JP2005137265A (en) * | 2003-11-06 | 2005-06-02 | Kirin Beverage Corp | New oolong tea beverage and method for producing the same |
JP2005168426A (en) * | 2003-12-12 | 2005-06-30 | Kao Corp | Method for producing tea extract solution |
JP2007110990A (en) * | 2005-10-21 | 2007-05-10 | Ito En Ltd | Green tea drink raw material liquid |
JP2008220202A (en) * | 2007-03-09 | 2008-09-25 | T Hasegawa Co Ltd | Method for producing tea extraction-treated matter with modified flavor |
JP2009082110A (en) * | 2007-10-03 | 2009-04-23 | Kao Corp | Method of producing tea extract solution |
-
2009
- 2009-12-25 JP JP2009295163A patent/JP5144638B2/en active Active
Patent Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2000050798A (en) * | 1998-08-05 | 2000-02-22 | Hisashi Takeuchi | Frozen tea leaf and its production |
JP2001258477A (en) * | 2000-03-16 | 2001-09-25 | Kirin Beverage Corp | Green tea beverage in sealed container and method for producing the same |
JP2003111558A (en) * | 2001-10-03 | 2003-04-15 | T Hasegawa Co Ltd | Method for producing tea extract |
JP2004321105A (en) * | 2003-04-25 | 2004-11-18 | Kao Corp | Green tea extract treated with tannase |
JP2005137265A (en) * | 2003-11-06 | 2005-06-02 | Kirin Beverage Corp | New oolong tea beverage and method for producing the same |
JP2005168426A (en) * | 2003-12-12 | 2005-06-30 | Kao Corp | Method for producing tea extract solution |
JP2007110990A (en) * | 2005-10-21 | 2007-05-10 | Ito En Ltd | Green tea drink raw material liquid |
JP2008220202A (en) * | 2007-03-09 | 2008-09-25 | T Hasegawa Co Ltd | Method for producing tea extraction-treated matter with modified flavor |
JP2009082110A (en) * | 2007-10-03 | 2009-04-23 | Kao Corp | Method of producing tea extract solution |
Non-Patent Citations (1)
Title |
---|
JPN6011056835; 五十嵐脩 他 編: '冷凍食品' 丸善食品総合辞典 , 1998, p.1159 * |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103704423A (en) * | 2014-01-02 | 2014-04-09 | 绿锦发展(福建)有限公司 | Preparation method for tea extract |
Also Published As
Publication number | Publication date |
---|---|
JP5144638B2 (en) | 2013-02-13 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
JP4680062B2 (en) | Fresh tea leaf powder, extract obtained from fresh tea leaf powder, and method for producing aroma component-containing material | |
JP5658918B2 (en) | Green tea extract | |
JP2011103901A (en) | Method for producing roast coffee bean, method for producing coffee extract liquid and method for producing coffee drink packed in container | |
JP2008237066A (en) | Packaged mixed tea beverage | |
JPH119189A (en) | Milk-containing coffee beverage and its production | |
JP2019180291A (en) | Production method of aromatic coffee beans, aromatic coffee beans and coffee extract | |
JP5642976B2 (en) | Coffee aroma-containing composition | |
JP2010268765A (en) | Roasted oolong tea and tea beverage using the same | |
JP2017006020A (en) | Process for preparing tea extract | |
JP2007110990A (en) | Green tea drink raw material liquid | |
JP2010207216A (en) | Method for producing new fermented coffee and fermented coffee produced thereby | |
JP2012187051A (en) | Wine like beverage and food and drink containing the same | |
JP5517349B2 (en) | Tea extract production method and tea extract | |
AU2021295085A1 (en) | Fermented beverage composition | |
JP2020072665A (en) | Method of producing tea extract | |
JP5144638B2 (en) | Fresh tea leaf extract with flavor balance and ease of drinking, and method for producing the same | |
JP3720171B2 (en) | Method for producing coffee-flavored sparkling liquor | |
JP4111414B2 (en) | Green tea beverage in sealed container and method for producing the same | |
WO2019142729A2 (en) | Production method for extract of green coffee beans | |
JP2000083587A (en) | Production of extract of favorite beverage | |
JP2019062755A (en) | Method for improving taste and flavor of semi-fermented tea, and method for producing semi-fermented tea | |
JP2006187253A (en) | Tencha beverage | |
JP6775317B2 (en) | Manufacturing method of packaged coffee beverages and packaged coffee beverages | |
JPH0870775A (en) | Preparation of highly palatable extracted liquid | |
JP7150691B2 (en) | METHOD FOR IMPROVING FLAVOR OF COFFEE BEVERAGE |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
A977 | Report on retrieval |
Free format text: JAPANESE INTERMEDIATE CODE: A971007 Effective date: 20111024 |
|
A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20111031 |
|
A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20111221 |
|
A02 | Decision of refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A02 Effective date: 20120611 |
|
A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20120905 |
|
A911 | Transfer to examiner for re-examination before appeal (zenchi) |
Free format text: JAPANESE INTERMEDIATE CODE: A911 Effective date: 20120912 |
|
TRDD | Decision of grant or rejection written | ||
A01 | Written decision to grant a patent or to grant a registration (utility model) |
Free format text: JAPANESE INTERMEDIATE CODE: A01 Effective date: 20121112 |
|
A01 | Written decision to grant a patent or to grant a registration (utility model) |
Free format text: JAPANESE INTERMEDIATE CODE: A01 |
|
A61 | First payment of annual fees (during grant procedure) |
Free format text: JAPANESE INTERMEDIATE CODE: A61 Effective date: 20121122 |
|
FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20151130 Year of fee payment: 3 |
|
R150 | Certificate of patent or registration of utility model |
Ref document number: 5144638 Country of ref document: JP Free format text: JAPANESE INTERMEDIATE CODE: R150 Free format text: JAPANESE INTERMEDIATE CODE: R150 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |