JP2011083282A - Method for producing coffee extract - Google Patents
Method for producing coffee extract Download PDFInfo
- Publication number
- JP2011083282A JP2011083282A JP2010210488A JP2010210488A JP2011083282A JP 2011083282 A JP2011083282 A JP 2011083282A JP 2010210488 A JP2010210488 A JP 2010210488A JP 2010210488 A JP2010210488 A JP 2010210488A JP 2011083282 A JP2011083282 A JP 2011083282A
- Authority
- JP
- Japan
- Prior art keywords
- coffee
- extract
- food
- coffee extract
- chlorogenic acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Tea And Coffee (AREA)
- Non-Alcoholic Beverages (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
Description
本発明は、コーヒー抽出物の製造方法に関する。さらに詳述すると、本発明はクロロゲン酸を豊富に含むコーヒー抽出物の製造方法及びコーヒー抽出物を飲食品に添加して該飲食品のクロロゲン酸含有量を高める方法、さらにはコーヒー抽出物を得るためのコーヒー豆加工物、クロロゲン酸を豊富に含むコーヒー飲料を得るためのコーヒー飲料抽出用加工品に関するものである。 The present invention relates to a method for producing a coffee extract. More specifically, the present invention provides a method for producing a coffee extract rich in chlorogenic acid, a method for increasing the chlorogenic acid content of the food and drink by adding the coffee extract to the food and drink, and further obtaining a coffee extract. The present invention relates to a processed coffee bean and a processed product for extracting a coffee beverage for obtaining a coffee beverage rich in chlorogenic acid.
コーヒーは世界中で最も消費されている飲料の一つであり、その香りが持つリラックス効果やカフェインの覚醒作用などから家庭や職場で広く愛好され、日常生活に欠かせないものとなっている。近年ではコーヒーに含まれるクロロゲン酸に血糖値上昇を抑える効果が見出されるなど、コーヒーの生理的な効果も注目され、クロロゲン酸を多く含んだコーヒー飲料なども発売されている。 Coffee is one of the most consumed beverages in the world, and it is widely loved at home and at work because of its relaxing effect and caffeine's awakening action, making it indispensable for daily life. . In recent years, chlorogenic acid contained in coffee has been found to have an effect of suppressing an increase in blood sugar level, and the physiological effects of coffee have attracted attention, and coffee beverages containing a large amount of chlorogenic acid have been released.
クロロゲン酸はコーヒーの生豆に最も多く含まれるが、焙煎するとカフェ酸とキナ酸とに分解されてしまい、その量が大幅に減少してしまう。このため、クロロゲン酸を多く含むコーヒー飲料の製造には、クロロゲン酸が減少しない程度に浅く焙煎したコーヒー豆からクロロゲン酸を多く含んだ抽出液を得る方法が採られており、これまでに通常のコーヒー飲料に用いる浅炒り焙煎よりもさらに浅く焙煎したコーヒー豆を粉砕し、通常の暖かいコーヒー飲料を得るときよりも低温で抽出することにより得られる新規な飲料(特許文献1)、L値60以下40以上のコーヒー生豆加工物とL値30以下の焙煎コーヒー豆を混合した飲料抽出用加工物(特許文献2)などが開示されている。 Chlorogenic acid is most contained in green coffee beans, but when roasted, it is decomposed into caffeic acid and quinic acid, and the amount is greatly reduced. For this reason, in the production of coffee beverages containing a large amount of chlorogenic acid, a method of obtaining an extract containing a large amount of chlorogenic acid from coffee beans roasted so shallow that chlorogenic acid does not decrease has been adopted. A novel beverage obtained by pulverizing coffee beans roasted shallower than the roast roasting used in coffee beverages of the past and extracting them at a lower temperature than when obtaining a normal warm coffee beverage (Patent Document 1), L A beverage extraction processed product (Patent Document 2) in which raw coffee beans with a value of 60 or less and 40 or more and roasted coffee beans with an L value of 30 or less is mixed is disclosed.
しかし、コーヒー豆の焙煎度が低い場合は、コーヒー生豆が有する特有の不快臭(2−イソブチル−3−メトキシピラジン等の香気成分に起因する生豆臭)が焙煎コーヒー豆に残存しており、コーヒー飲料の風味に影響を与えてしまう。 However, when the degree of roasting of coffee beans is low, the unpleasant odor peculiar to green coffee beans (raw bean odor due to aroma components such as 2-isobutyl-3-methoxypyrazine) remains in the roasted coffee beans. Affect the flavor of coffee drinks.
この問題を解決する方法として、クロロゲン酸類の量が低減しない程度の浅い焙煎を行った焙煎コーヒー豆を水または含水水混和性有機溶媒で抽出することを特徴とするコーヒー抽出物の製造方法が提案されている(特許文献3)。 As a method for solving this problem, a method for producing a coffee extract characterized by extracting roasted coffee beans that have been roasted so shallow that the amount of chlorogenic acids is not reduced with water or a water-miscible organic solvent. Has been proposed (Patent Document 3).
しかしながら、特許文献3の方法によっても生豆臭を十分に除去することはできず、得られたコーヒーエキスには生豆臭が残存していた。 However, the green bean odor cannot be sufficiently removed by the method of Patent Document 3, and the green bean odor remains in the obtained coffee extract.
本発明が解決しようとする課題は、2−イソブチル−3−メトキシピラジン等の香気成分に起因する生豆臭が十分に除去され、風味に優れたクロロゲン酸含量の高いコーヒー抽出物を得ること及び該コーヒー抽出物を飲食品に添加して風味の優れたクロロゲン酸含有量の高い飲食品を得ることである。 The problem to be solved by the present invention is to obtain a coffee extract having a high chlorogenic acid content excellent in flavor, in which raw bean odor due to aroma components such as 2-isobutyl-3-methoxypyrazine is sufficiently removed, and The coffee extract is added to a food or drink to obtain a food or drink with an excellent flavor and a high chlorogenic acid content.
また、本発明が解決しようとする課題は、2−イソブチル−3−メトキシピラジン等の香気成分に起因する生豆臭が十分に除去され、風味に優れたクロロゲン酸含量の高いコーヒー抽出物を得るためのコーヒー豆加工品を得ることである。 In addition, the problem to be solved by the present invention is to obtain a coffee extract with a high chlorogenic acid content that is sufficiently flavor-free due to aroma components such as 2-isobutyl-3-methoxypyrazine and is excellent in flavor. To get processed coffee beans.
さらに、本発明が解決しようとする課題は、2−イソブチル−3−メトキシピラジン等の香気成分に起因する生豆臭の無い風味に優れたクロロゲン酸含量の高いコーヒー飲料を得るためのコーヒー飲料抽出用加工品を得ることである。 Furthermore, the problem to be solved by the present invention is to extract a coffee beverage for obtaining a coffee beverage having a high chlorogenic acid content excellent in flavor without raw bean odor caused by aroma components such as 2-isobutyl-3-methoxypyrazine. To obtain a processed product.
本発明者らはL値25〜40の焙煎コーヒー豆を水蒸気蒸留した後、水、エタノールまたはこれらの混合物で抽出することにより、生豆臭の原因物質である2−イソブチル−3−メトキシピラジン、さらには他の低沸点香気成分の濃度を効果的に低減させて、生豆臭が除去された風味良好なクロロゲン酸高含有コーヒー抽出物を得ることができることを見出し、本発明を完成した。 The present inventors, after steam-distilling roasted coffee beans having an L value of 25 to 40, extract them with water, ethanol or a mixture thereof, thereby producing 2-isobutyl-3-methoxypyrazine which is a causative substance of raw bean odor. Furthermore, the present inventors have found that a coffee extract containing high chlorogenic acid content with good flavor from which raw bean odor is removed can be obtained by effectively reducing the concentration of other low boiling point aroma components.
本発明は以下のように構成される。
(1)L値25以上40以下の焙煎コーヒー豆を水蒸気蒸留により脱臭し、次いで水、エタノールまたはこれらの混合物で抽出することを特徴とするコーヒー抽出物の製造方法。(2)(1)記載の方法で製造したコーヒー抽出物。
(3)クロロゲン酸重量/乾燥固形分重量が少なくとも0.03である(2)記載のコーヒー抽出物。
(4)低沸点香気濃度(質量%)/乾燥固形分含有量(質量%)×100が0.001以下である(2)又は(3)記載のコーヒー抽出物。
(5)(2)〜(4)のいずれか1つに記載のコーヒー抽出物を飲食品に添加することにより該飲食品のクロロゲン酸含有量を高める方法。
(6)飲食品がコーヒー風味の飲食品である(5)記載の方法。
(7)(2)〜(4)のいずれか1つに記載のコーヒー抽出物が添加された飲食品。
(8)飲食品がコーヒー風味の飲食品である(7)記載の飲食品。
(9)L値25以上40以下の焙煎コーヒー豆を水蒸気蒸留により脱臭したコーヒー豆加工品。
(10)(9)に記載のコーヒー豆加工品がL値25未満の焙煎コーヒー豆に配合されているコーヒー飲料抽出用加工品。
(11)(10)に記載のコーヒー飲料抽出用加工品を熱水抽出する工程を含むコーヒー飲料の製造方法。
The present invention is configured as follows.
(1) A method for producing a coffee extract, wherein roasted coffee beans having an L value of 25 or more and 40 or less are deodorized by steam distillation, and then extracted with water, ethanol or a mixture thereof. (2) A coffee extract produced by the method described in (1).
(3) The coffee extract according to (2), wherein the weight of chlorogenic acid / weight of dry solid is at least 0.03.
(4) The coffee extract according to (2) or (3), wherein low boiling point aroma concentration (mass%) / dry solid content (mass%) × 100 is 0.001 or less.
(5) A method for increasing the chlorogenic acid content of a food or drink by adding the coffee extract according to any one of (2) to (4) to the food or drink.
(6) The method according to (5), wherein the food or drink is a coffee-flavored food or drink.
(7) Food / beverage products to which the coffee extract as described in any one of (2) to (4) is added.
(8) The food or drink according to (7), wherein the food or drink is a coffee-flavored food or drink.
(9) A processed coffee bean product obtained by deodorizing roasted coffee beans having an L value of 25 or more and 40 or less by steam distillation.
(10) A processed product for coffee beverage extraction, wherein the processed coffee bean according to (9) is blended with roasted coffee beans having an L value of less than 25.
(11) A method for producing a coffee beverage comprising a step of hot water extraction of the coffee beverage extraction processed product according to (10).
本発明のコーヒー抽出物の製造方法によれば、コーヒー豆から不快な生豆臭が除去され、苦味がなく甘みがあり、クロロゲン酸を豊富に含むコーヒー抽出物が製造できる。さらにこの抽出物を飲食品に添加することにより、クロロゲン酸を多く含み、風味に優れた飲食品を得ることができる。 According to the method for producing a coffee extract of the present invention, an unpleasant raw bean odor is removed from coffee beans, and there is no bitterness and sweetness, and a coffee extract rich in chlorogenic acid can be produced. Furthermore, by adding this extract to foods and drinks, foods and drinks containing a large amount of chlorogenic acid and excellent in flavor can be obtained.
また、本発明のコーヒー豆加工品によれば、コーヒー豆から不快な生豆臭が除去されており、水、エタノールまたはこれらの混合物で抽出することで、生豆臭が無く、苦味がなく甘みがあり、クロロゲン酸を豊富に含むコーヒー抽出物を得ることができる。 Further, according to the processed coffee bean product of the present invention, the unpleasant raw bean odor is removed from the coffee bean, and by extracting with water, ethanol or a mixture thereof, there is no raw bean odor, no bitterness and sweetness A coffee extract rich in chlorogenic acid can be obtained.
また、本発明のコーヒー飲料抽出用加工品によれば、通常のコーヒー飲料を得るための焙煎コーヒー豆に本発明のコーヒー豆加工品が配合されているので、熱水抽出することで、生豆臭が無く、クロロゲン酸を豊富に含むコーヒー飲料を得ることができる。 Further, according to the processed product for coffee beverage extraction of the present invention, the processed coffee bean product of the present invention is blended with roasted coffee beans for obtaining a normal coffee beverage. There is no bean odor, and a coffee beverage rich in chlorogenic acid can be obtained.
[コーヒー豆]
本発明で使用するコーヒー豆は特に制限なく、いずれの品種、産地のコーヒー豆であっても使用できる。コーヒー豆の焙煎方法は特に制限なく、直火焙煎、熱風焙煎、遠赤外線焙煎、マイクロ波焙煎など、種々の焙煎方法を用いることができる。焙煎度はコーヒー豆の風味とクロロゲン酸含量のバランスにより決定されるが、本発明ではコーヒー豆の焙煎度をL値(黒を0、白を100としコーヒー豆の焙煎状態を豆の色で表した値)で表した場合、25未満の中〜深炒り焙煎ではコーヒー豆に含まれるクロロゲン酸がカフェ酸とキナ酸とに分解してクロロゲン酸量が低下する他、苦味が強くなるなど風味の面からも好ましくなく、また40超の浅炒り焙煎では生豆臭が強く、水蒸気蒸留による生豆臭の除去が困難になることから、L値は、25〜40が好ましく、さらに27〜35が好ましい。
[Coffee beans]
The coffee beans used in the present invention are not particularly limited, and any coffee beans of any variety and production area can be used. The method for roasting coffee beans is not particularly limited, and various roasting methods such as direct-fire roasting, hot-air roasting, far-infrared roasting, and microwave roasting can be used. The roasting degree is determined by the balance between the flavor and chlorogenic acid content of the coffee beans. In the present invention, the roasting degree of the coffee beans is L value (black is 0, white is 100, and the roasting state of the coffee beans is In the case of medium to deep roasting less than 25, the chlorogenic acid contained in the coffee beans decomposes into caffeic acid and quinic acid and the amount of chlorogenic acid decreases, and the bitterness is strong. It is not preferable from the aspect of flavor such as, and since the raw bean odor is strong in roast roasting exceeding 40 and removal of the raw bean odor by steam distillation becomes difficult, the L value is preferably 25 to 40, Furthermore, 27-35 are preferable.
[水蒸気蒸留]
焙煎したコーヒー豆は適度な粒度、例えば0.2〜3.0mm程度に粉砕した後、水蒸気蒸留により脱臭して生豆臭を除去する。水蒸気蒸留は本来香気成分を精油として抽出する方法であるが、本発明では焙煎コーヒー豆に残存する不快な生豆臭を除去する方法として用いる。水蒸気蒸留方法は特に制限がなく、加圧水蒸気蒸留、常圧水蒸気蒸留、減圧水蒸気蒸留のいずれの方法もとることができる。水蒸気の温度や蒸気流量、蒸留液の留出液量などは原料の生豆臭の強さなどに応じて任意に設定することができる。具体的には、生豆臭の脱臭度を考慮すると、蒸留温度80〜100℃、蒸気流量は空間速度(蒸気流量(m3/hr)/コーヒー豆仕込量(m3))100〜600(1/hr)、蒸留液の留出液量はコーヒー豆に対して重量で0.5〜1.5倍量とすることが好適であるが、この範囲に限定されるものではない。
[Steam distillation]
The roasted coffee beans are pulverized to an appropriate particle size, for example, about 0.2 to 3.0 mm, and then deodorized by steam distillation to remove raw bean odor. Steam distillation is originally a method for extracting an aromatic component as an essential oil, but in the present invention, it is used as a method for removing an unpleasant raw bean odor remaining in roasted coffee beans. The steam distillation method is not particularly limited, and any of pressurized steam distillation, atmospheric steam distillation, and reduced pressure steam distillation can be used. The temperature of steam, the flow rate of steam, the amount of distillate distillate, etc. can be arbitrarily set according to the strength of raw bean odor. Specifically, considering the deodorization degree of raw bean odor, the distillation temperature is 80 to 100 ° C., the steam flow rate is the space velocity (steam flow rate (m 3 / hr) / coffee bean charge (m 3 )) 100 to 600 ( 1 / hr), the amount of distillate distillate is preferably 0.5 to 1.5 times the weight of coffee beans, but is not limited to this range.
[抽出]
次いで水蒸気蒸留により生豆臭を除去したコーヒー豆から抽出により、クロロゲン酸を多く含むコーヒー抽出物を得る。抽出方法としては従来から使用されている方法を特に制限なく用いることができ、例としてドリップ抽出、浸漬抽出などを挙げることができる。抽出溶媒としては水、エタノール又はエタノール水溶液を用いることができ、水を用いる場合は冷水、温水、熱水いずれでもよいが、クロロゲン酸の抽出効率を考慮すると、一般に90℃以上の熱水が好ましい。エタノール又はエタノール水溶液を用いる場合は抽出温度、エタノール濃度に特に制限はなく任意に設定できるが、クロロゲン酸の抽出効率を考慮すると、一般に抽出温度は40〜90℃、好ましくは80〜90℃、エタノール水溶液の濃度は一般に30〜80質量%、好ましくは40〜60質量%である。抽出時間については特に制限なく、任意に設定することができるが、クロロゲン酸の抽出効率を考慮すると30〜180分が好ましい。また、コーヒー豆に対する抽出溶媒の量についても特に制限はないが、抽出溶媒の回収率を考慮するとコーヒー豆に対して重量で3〜30倍の抽出溶媒量が好適である。得られた抽出液はそのままコーヒー抽出物として用いることもできるが、必要に応じて活性炭や多孔性のスチレン−ジビニルベンゼン共重合体からなる合成樹脂吸着剤などを用いた精製処理を行うことができる。
[Extract]
Next, a coffee extract rich in chlorogenic acid is obtained by extraction from the coffee beans from which the green bean odor has been removed by steam distillation. As the extraction method, a conventionally used method can be used without particular limitation, and examples thereof include drip extraction and immersion extraction. As the extraction solvent, water, ethanol, or an aqueous ethanol solution can be used. When water is used, any of cold water, hot water, and hot water may be used, but in consideration of the extraction efficiency of chlorogenic acid, hot water of 90 ° C. or higher is generally preferable. . In the case of using ethanol or ethanol aqueous solution, the extraction temperature and ethanol concentration are not particularly limited and can be arbitrarily set. However, considering the extraction efficiency of chlorogenic acid, the extraction temperature is generally 40 to 90 ° C, preferably 80 to 90 ° C. The concentration of the aqueous solution is generally 30 to 80% by mass, preferably 40 to 60% by mass. The extraction time is not particularly limited and can be arbitrarily set. However, considering the extraction efficiency of chlorogenic acid, 30 to 180 minutes is preferable. Moreover, there is no restriction | limiting in particular also about the quantity of the extraction solvent with respect to coffee beans, but when the recovery rate of an extraction solvent is considered, the amount of extraction solvents 3-30 times by weight with respect to coffee beans is suitable. The obtained extract can be used as a coffee extract as it is, but can be purified using a synthetic resin adsorbent made of activated carbon or a porous styrene-divinylbenzene copolymer, if necessary. .
抽出により得られた抽出液は、クロロゲン酸重量/乾燥固形分重量が少なくとも0.03であり生豆臭がほとんど感じられず、甘味のある好ましい風味を有する。尚、乾燥固形分とは、コーヒー抽出液を乾燥して得られる固形分を意味している。抽出液はそのままあるいは濃縮した抽出物として飲食品に添加することにより、該飲食品のクロロゲン酸含有量を高めることができ、抽出物が有する風味が飲食品の風味を損なわない限り、各種飲食品に特に制限なく使用することができる。飲食品としてはコーヒー、ココア、茶飲料などの各種飲料や、チョコレート、焼き菓子、キャンディー、チューイングガム、ゼリー、アイスクリームなどの菓子、冷菓類を挙げることができるが、抽出物自体の風味が飲食品の風味に与える影響を考慮すると、コーヒー風味を有する飲食品が好ましく、特にコーヒー飲料への使用が最も適している。抽出液はそのまま本発明のコーヒー抽出物としてコーヒー飲料に添加してもよいが、適当な濃度に濃縮して使用することが好ましい。この場合には、飲食物のクロロゲン酸含有量を少ない添加量で高めることができる。抽出液を濃縮する場合、抽出溶媒として水を用いた場合は、例えばBrix5〜50まで濃縮したコーヒー抽出物として使用することが好適であり、抽出溶媒としてエタノールまたはエタノール水溶液を用いた場合は、例えば乾燥固形分が10〜60質量%になるように濃縮したコーヒー抽出物とすることが好適である。また、必要に応じて、一度濃縮した抽出液を再度溶媒で希釈して用いるようにしてもよい。例えば乾燥固形分が10〜60質量%になるように濃縮したコーヒー抽出物を再度エタノール水溶液で希釈して乾燥固形分を5〜30質量%に調整したコーヒー抽出物として使用するようにしてもよい。なお、本発明におけるコーヒー飲料とは、公正競争規約に定義されたコーヒー、コーヒー飲料、コーヒー入り清涼飲料の他、乳固形分を3%以上含み、乳等省令で乳飲料として扱われるミルク入りコーヒーやカフェオレなども含む。コーヒー飲料は原料のコーヒー豆の品種、産地、焙煎度、抽出方法等は特に制限なく、通常の方法で得られるコーヒー飲料に本発明のコーヒー抽出物を添加することができ、さらに必要に応じて糖類などの甘味料や、ミルクなどの乳、乳製品を加えることができる。本発明のコーヒー抽出物は不快な生豆臭が少なく、コーヒー飲料の風味に影響を及ぼさないことから、コーヒー飲料への添加量は特に制限はないが、一般的にはコーヒー飲料に対し0.01〜1.0質量%添加することが好ましい。 The extract obtained by the extraction has a weight of chlorogenic acid / weight of dry solids of at least 0.03, almost no raw bean odor, and has a sweet and desirable flavor. The dry solid content means a solid content obtained by drying the coffee extract. By adding the extract as it is or as a concentrated extract to a food or drink, the chlorogenic acid content of the food or drink can be increased, and as long as the flavor of the extract does not impair the taste of the food or drink, It can be used without any particular restrictions. Examples of foods and beverages include various beverages such as coffee, cocoa and tea beverages, chocolates, baked confectionery, candy, chewing gum, jelly, ice cream and other confectionery, and frozen desserts. In view of the influence on the flavor of food, foods and beverages having a coffee flavor are preferable, and use in coffee beverages is most suitable. The extract may be added as it is to the coffee beverage as a coffee extract of the present invention, but it is preferably used after being concentrated to an appropriate concentration. In this case, the chlorogenic acid content of food and drink can be increased with a small addition amount. When concentrating the extract, when water is used as the extraction solvent, it is preferable to use it as a coffee extract concentrated to, for example, Brix 5 to 50. When using ethanol or an aqueous ethanol solution as the extraction solvent, for example, It is preferable that the coffee extract is concentrated so that the dry solid content is 10 to 60% by mass. If necessary, the extract once concentrated may be diluted with a solvent again and used. For example, a coffee extract concentrated to have a dry solid content of 10 to 60% by mass may be diluted again with an aqueous ethanol solution and used as a coffee extract having a dry solid content adjusted to 5 to 30% by mass. . The coffee beverage in the present invention includes coffee, coffee beverages, soft drinks with coffee as defined in the fair competition rules, and milk-containing coffee that contains 3% or more of milk solids and is treated as a milk beverage by a ministerial ordinance such as milk. Including cafe au lait. There are no particular restrictions on the type, origin, roasting degree, extraction method, etc. of the coffee beans used as the raw material for the coffee beverage, and the coffee extract of the present invention can be added to the coffee beverage obtained by a conventional method, and if necessary Sweeteners such as sugar, milk such as milk, and dairy products can be added. Since the coffee extract of the present invention has less unpleasant green bean odor and does not affect the flavor of the coffee beverage, the amount added to the coffee beverage is not particularly limited. It is preferable to add 01-1.0 mass%.
上述の形態は本発明の好適な形態の一例ではあるがこれに限定されるものではなく本発明の要旨を逸脱しない範囲において種々変形実施可能である。例えば、水蒸気蒸留により脱臭したL値25以上40以下の焙煎コーヒー豆をL値25未満の焙煎コーヒー豆(例えば、ライトロースト、シナモンロースト、ミディアムロースト、ハイロースト、シティロースト、フルシティロースト、フレンチロースト、イタリアンローストといった通常のコーヒー飲料を得るための焙煎状態にあるコーヒー豆)に一定量配合してコーヒー飲料抽出用加工品とし、このコーヒー飲料抽出加工品をドリップ抽出に供して、クロロゲン酸を豊富に含むコーヒー飲料を製造するようにしてもよい。 The above-described embodiment is an example of a preferred embodiment of the present invention, but is not limited thereto, and various modifications can be made without departing from the gist of the present invention. For example, roasted coffee beans having an L value of 25 or more and 40 or less deodorized by steam distillation are roasted coffee beans having an L value of less than 25 (for example, light roast, cinnamon roast, medium roast, high roast, city roast, full city roast, A certain amount of coffee beans in a roasted state to obtain a normal coffee drink such as French roast or Italian roast) is blended into a coffee beverage extraction processed product, and this coffee beverage extracted processed product is subjected to drip extraction to produce chlorogen. An acid-rich coffee drink may be produced.
以下に実施例を挙げて本発明を具体的に説明するが、本発明は実施例の記載に限定されるものではない。 EXAMPLES The present invention will be specifically described below with reference to examples, but the present invention is not limited to the description of the examples.
[実施例1]
L値35に焙煎したブラジル産コーヒー豆2000gを0.2〜1.0mmに粉砕し、常圧下で水蒸気蒸留(蒸留温度100℃、空間速度300(1/h)、蒸留液の留出液量2000g)して生豆臭を除去した後、95℃の熱水でドリップ抽出を行ってコーヒー抽出物10000gを得た。
[Example 1]
2000g of Brazilian coffee beans roasted to L value 35 is crushed to 0.2-1.0mm and steam distilled under normal pressure (distillation temperature 100 ° C, space velocity 300 (1 / h), distillate distillate 2,000 g) to remove the green bean odor, followed by drip extraction with hot water at 95 ° C. to obtain 10,000 g of coffee extract.
[実施例2]
実施例1で得たコーヒー抽出液をBrix30まで濃縮し、0.45μmのメンブランフィルターにより除菌濾過を行ってコーヒー抽出物を得た。
[Example 2]
The coffee extract obtained in Example 1 was concentrated to Brix 30, and sterilized by a 0.45 μm membrane filter to obtain a coffee extract.
[実施例3]
L値35に焙煎したブラジル産コーヒー豆2000gを0.2〜1.0mmに粉砕し、常圧下で水蒸気蒸留(蒸留温度100℃、空間速度600(1/h)、蒸留液の留出液量2000g)して生豆臭を除去した。この生豆臭を除去したコーヒー豆200gに対し10倍量(質量)の50質量%エタノール水溶液を加え、加熱還流を2時間行った後、コーヒー豆を分離すると抽出液が1970g得られた。この抽出液に、生豆臭を除去したコーヒー豆をさらに200g加え、加熱還流を2時間行った。コーヒー豆を分離後、得られた抽出液を−15℃で一晩冷却し、ろ過することで、コーヒー抽出物1930gを得た。
[Example 3]
2000g of Brazilian coffee beans roasted to L value 35 is crushed to 0.2-1.0mm and steam distilled under normal pressure (distillation temperature 100 ° C, space velocity 600 (1 / h), distillate distillate The amount of raw bean odor was removed by 2000 g). A 10-fold amount (mass) of a 50% by weight ethanol aqueous solution was added to 200 g of coffee beans from which the green bean odor was removed, and after heating and refluxing for 2 hours, the coffee beans were separated to obtain 1970 g of an extract. To this extract, 200 g of coffee beans from which the green bean odor was removed was added and heated under reflux for 2 hours. After separating the coffee beans, the obtained extract was cooled at −15 ° C. overnight and filtered to obtain 1930 g of a coffee extract.
[比較例1]
L値35に焙煎したブラジル産コーヒー豆200gを0.2〜1.0mmに粉砕し、95℃の熱水でドリップ抽出を行ってコーヒー抽出物1000gを得た。
[Comparative Example 1]
200 g of Brazilian coffee beans roasted to L value 35 were pulverized to 0.2 to 1.0 mm, and drip extraction was performed with hot water at 95 ° C. to obtain 1000 g of coffee extract.
[比較例2]
L値35に焙煎したブラジル産コーヒー豆200gを0.2〜1.0mmに粉砕し、30℃の水でドリップ抽出を行ってコーヒー抽出物1000gを得た。
[Comparative Example 2]
200 g of Brazilian coffee beans roasted to L value 35 were pulverized to 0.2 to 1.0 mm, and drip extraction was performed with water at 30 ° C. to obtain 1000 g of coffee extract.
[比較例3]
L値16に焙煎したブラジル産コーヒー豆200gを0.2〜1.0mmに粉砕し、95℃の熱水でドリップ抽出を行ってコーヒー抽出物1000gを得た。
[Comparative Example 3]
200 g of Brazilian coffee beans roasted to L value 16 were pulverized to 0.2 to 1.0 mm, and drip extraction was performed with hot water at 95 ° C. to obtain 1000 g of coffee extract.
[比較例4]
L値22に焙煎したブラジル産コーヒー豆200gを0.2〜1.0mmに粉砕し、95℃の熱水でドリップ抽出を行ってコーヒー抽出物1000gを得た。
[Comparative Example 4]
200 g of Brazilian coffee beans roasted to L value 22 were pulverized to 0.2 to 1.0 mm, and drip extraction was performed with hot water at 95 ° C. to obtain 1000 g of coffee extract.
[比較例5]
L値27に焙煎したブラジル産コーヒー豆200gを0.2〜1.0mmに粉砕し、95℃の熱水でドリップ抽出を行ってコーヒー抽出物1000gを得た。
[Comparative Example 5]
200 g of Brazilian coffee beans roasted to L value 27 were pulverized to 0.2 to 1.0 mm, and drip extraction was performed with hot water at 95 ° C. to obtain 1000 g of coffee extract.
[比較例6]
L値45に焙煎したブラジル産コーヒー豆2000gを0.2〜1.0mmに粉砕し、常圧下で水蒸気蒸留(蒸留温度100℃、空間速度300(1/h)、蒸留液の留出液量2000g)して生豆臭を除去した後、95℃の熱水でドリップ抽出を行ってコーヒー抽出物10000gを得た。
[Comparative Example 6]
2000g of Brazilian coffee beans roasted to L value 45 is crushed to 0.2-1.0mm and steam distilled under normal pressure (distillation temperature 100 ° C, space velocity 300 (1 / h), distillate of distillate 2,000 g) to remove the green bean odor, followed by drip extraction with hot water at 95 ° C. to obtain 10,000 g of coffee extract.
[実施例4] コーヒー飲料
表1の処方のように配合(質量比)を行った後、190g缶に充填し、121℃10分間レトルト殺菌を行ってコーヒー飲料を得た。
[Example 4] Coffee beverage After blending (mass ratio) as shown in Table 1, it was filled in a 190 g can and sterilized at 121 ° C for 10 minutes to obtain a coffee beverage.
[実施例5] コーヒーゼリー
表2の処方のように各原料を配合(質量比)し加温溶解させた後、ゼリーカップに充填し、85℃20分間殺菌を行ってコーヒーゼリーを得た。
[Example 5] Coffee jelly After blending each raw material (mass ratio) as shown in Table 2 and dissolving by heating, the jelly cup was filled and sterilized at 85 ° C for 20 minutes to obtain coffee jelly.
[実施例6] 黒糖キャンディー
表3の配合量(質量比)に基づき、砂糖、水飴、水を配合して155℃まで加温した後、120℃まで急冷し、実施例2のコーヒー抽出物および黒糖フレーバーを添加後、成型、冷却して黒糖キャンディーを得た。
[Example 6] Brown sugar candy Based on the blending amount (mass ratio) of Table 3, sugar, starch syrup, and water were mixed and heated to 155 ° C, then rapidly cooled to 120 ° C, and the coffee extract of Example 2 and After adding the brown sugar flavor, it was molded and cooled to obtain a brown sugar candy.
[実施例7]
L値25に焙煎したブラジル産コーヒー豆2000gを0.2〜1.0mmに粉砕し、常圧下で水蒸気蒸留(蒸留温度100℃、空間速度300(1/h)、蒸留液の留出液量2000g)して生豆臭を除去した後、95℃の熱水でドリップ抽出を行ってコーヒー抽出物10000gを得た。
[Example 7]
2000g of Brazilian coffee beans roasted to L value 25 are crushed to 0.2-1.0mm and steam distilled under normal pressure (distillation temperature 100 ° C, space velocity 300 (1 / h), distillate distillate 2,000 g) to remove the green bean odor, followed by drip extraction with hot water at 95 ° C. to obtain 10,000 g of coffee extract.
[実施例8]
L値40に焙煎したブラジル産コーヒー豆2000gを0.2〜1.0mmに粉砕し、常圧下で水蒸気蒸留(蒸留温度100℃、空間速度300(1/h)、蒸留液の留出液量2000g)して生豆臭を除去した後、95℃の熱水でドリップ抽出を行ってコーヒー抽出物10000gを得た。
[Example 8]
2000g of Brazilian coffee beans roasted to L value 40 is ground to 0.2-1.0mm and steam distilled under normal pressure (distillation temperature 100 ° C, space velocity 300 (1 / h), distillate distillate 2,000 g) to remove the green bean odor, followed by drip extraction with hot water at 95 ° C. to obtain 10,000 g of coffee extract.
[試験例1]
実施例1、比較例1、比較例2で得られたコーヒー抽出物を乾燥固形分1質量%になるように調整し、7名のパネルにより官能評価を行った。官能評価は以下の評価基準により生豆臭、甘味に関する各項目を点数で評価し、各パネルの評価点を平均した。結果を表4に示す。
(評価基準)
5点:非常に強い
4点:強い
3点:中程度
2点:弱い
1点:非常に弱い
[Test Example 1]
The coffee extracts obtained in Example 1, Comparative Example 1 and Comparative Example 2 were adjusted so as to have a dry solid content of 1% by mass, and sensory evaluation was performed by a panel of seven persons. Sensory evaluation evaluated each item regarding raw bean odor and sweetness by the score according to the following evaluation criteria, and averaged the evaluation points of each panel. The results are shown in Table 4.
(Evaluation criteria)
5 points: very strong 4 points: strong 3 points: moderate 2 points: weak 1 point: very weak
表4に示したように、実施例1のコーヒー抽出物は比較例1及び2のコーヒー抽出物に比べ、生豆臭が非常に弱く、甘味が強かった。 As shown in Table 4, the coffee extract of Example 1 had a very weak raw bean odor and a strong sweetness as compared with the coffee extracts of Comparative Examples 1 and 2.
[試験例2]
実施例1、比較例1、比較例2で得られたコーヒー抽出物の乾燥固形分測定、香気成分測定を行った。
[Test Example 2]
Measurement of dry solid content and aroma component of the coffee extracts obtained in Example 1, Comparative Example 1, and Comparative Example 2 were performed.
<乾燥固形分の測定方法>
海砂20gを入れた蒸発皿と攪拌棒を十分に乾燥し、冷却した後、試料2gを添加して秤量した。攪拌して海砂と試料を十分に混合し、オーブンで105℃2時間乾燥後、デシケーター内で冷却し、乾燥後の試料重量を秤量し、乾燥固形分を以下の数式で算出した。
乾燥固形分(質量%)=(乾燥後の試料重量(g))/(乾燥前の試料重量(g))×100
<Method for measuring dry solid content>
The evaporating dish and stirring bar containing 20 g of sea sand were sufficiently dried and cooled, and then 2 g of a sample was added and weighed. After stirring, the sea sand and the sample were sufficiently mixed, dried in an oven at 105 ° C. for 2 hours, cooled in a desiccator, the weight of the dried sample was weighed, and the dry solid content was calculated by the following formula.
Dry solid content (% by mass) = (Sample weight after drying (g)) / (Sample weight before drying (g)) × 100
<香気成分の測定方法>
試料調製
試料5gを精秤後、内部標準物質(フェニルイソチオシアネート)を試料中の濃度が20ppm(0.002質量%)になるように添加し、合成吸着樹脂を充填したカラムに通し、香気成分を吸着させた。蒸留水でカラムを洗浄後、ジエチルエーテル60mlで香気成分を回収し、濃縮して分析サンプル100μlを調製した。各分析サンプルは、各試料(実施例1、比較例1、比較例2)の持つ香りの特徴を維持していた。
<Measurement method of aroma components>
Sample preparation After accurately weighing 5 g of the sample, an internal standard substance (phenyl isothiocyanate) was added so that the concentration in the sample was 20 ppm (0.002% by mass), passed through a column packed with a synthetic adsorption resin, and aroma components. Was adsorbed. After washing the column with distilled water, aroma components were collected with 60 ml of diethyl ether and concentrated to prepare 100 μl of an analytical sample. Each analysis sample maintained the scent characteristics of each sample (Example 1, Comparative Example 1, Comparative Example 2).
測定法
下記条件により、各分析サンプルの香気成分分析を行い、低沸点香気濃度と、生豆臭の寄与成分である2−イソブチル−3−メトキシピラジン濃度を算出した。下記条件で香気成分分析を行った際に、リテンションタイムが20分未満の香気成分濃度の合計値を低沸点香気濃度の値とした。各香気成分の濃度は以下の数式で算出した。
香気成分濃度(質量%)=(内部標準物質の試料中濃度(質量%))×(各成分のピーク面積値)/(内部標準物質のピーク面積値)
結果を表5A及び5Bに示す。
装置:GC−MS(Agilent Technoligies社製 7890A(GC)5975C(MS))
カラム:DB−WAX(内径0.25mm×長さ60m、膜厚0.25μm)
キャリアガス:He(1.0ml/min)
オーブン温度:80→230℃、3℃/min
注入条件:250℃、スプリット比30:1
注入量:1μl
Measurement method Aroma component analysis of each analysis sample was performed under the following conditions, and a low-boiling-point aroma concentration and a 2-isobutyl-3-methoxypyrazine concentration, which is a contributing component of green bean odor, were calculated. When the aroma component analysis was performed under the following conditions, the total value of the aroma component concentrations with a retention time of less than 20 minutes was taken as the value of the low boiling point aroma concentration. The concentration of each aroma component was calculated by the following formula.
Aroma component concentration (mass%) = (concentration of internal standard substance in sample (mass%)) × (peak area value of each component) / (peak area value of internal standard substance)
The results are shown in Tables 5A and 5B.
Apparatus: GC-MS (manufactured by Agilent Technologies 7890A (GC) 5975C (MS))
Column: DB-WAX (inner diameter 0.25 mm × length 60 m, film thickness 0.25 μm)
Carrier gas: He (1.0 ml / min)
Oven temperature: 80 → 230 ° C, 3 ° C / min
Injection conditions: 250 ° C., split ratio 30: 1
Injection volume: 1 μl
表5A及び表5Bより、実施例のコーヒー抽出物は比較例1および比較例2のコーヒー抽出物と比べ、生豆臭の寄与成分である2−イソブチル−3−メトキシピラジン量および低沸点香気濃度/乾燥固形分が低かった。実施例の脱臭効果が高いことを示す結果となった。また、表5Bに示される結果から、生豆臭が十分に除去されたコーヒー抽出物の2−イソブチル−3−メトキシピラジン濃度(質量%)/乾燥固形分(質量%)×109は、4.5であることが明らかとなった。したがって、2−イソブチル−3−メトキシピラジン濃度(質量%)/乾燥固形分(質量%)×109が10以下、好適には7.5以下、より好適には5以下であれば、コーヒー抽出物の生豆臭が十分に除去されているものと推定された。また、表5Aに示される結果から、生豆臭が十分に除去されたコーヒー抽出物の低沸点香気濃度(質量%)/乾燥固形分(質量%)×100は、0.000014以下であることが明らかとなった。したがって、低沸点香気濃度(質量%)/乾燥固形分(質量%)×100が0.001以下、好適には0.0001以下、より好適には0.00005以下、さらに好適には0.00002以下であれば、コーヒー抽出物の生豆臭が十分に除去されているものと推定された。 From Table 5A and Table 5B, compared with the coffee extract of the comparative example 1 and the comparative example 2, the coffee extract of an Example has the amount of 2-isobutyl-3-methoxypyrazine which is a contribution component of a green bean smell, and a low boiling point aromatic concentration. / The dry solid content was low. It became the result which shows that the deodorizing effect of an Example is high. Further, from the results shown in Table 5B, 2-isobutyl-3-methoxy pyrazine concentration of coffee extract beans odor is sufficiently removed (wt%) / dry solids (wt%) × 10 9, the 4 It became clear that it was .5. Therefore, if 2-isobutyl-3-methoxypyrazine concentration (% by mass) / dry solid content (% by mass) × 10 9 is 10 or less, preferably 7.5 or less, more preferably 5 or less, coffee extraction It was estimated that the raw bean odor was sufficiently removed. From the results shown in Table 5A, the low boiling point aroma concentration (mass%) / dry solid content (mass%) × 100 of the coffee extract from which the green bean odor has been sufficiently removed is 0.000014 or less. Became clear. Therefore, low boiling point aroma concentration (% by mass) / dry solid content (% by mass) × 100 is 0.001 or less, preferably 0.0001 or less, more preferably 0.00005 or less, and further preferably 0.00002. If it was below, it was estimated that the green bean odor of coffee extract was fully removed.
[試験例3]
実施例2、実施例3、実施例7、実施例8、比較例3、比較例4、比較例5、比較例6で得られたコーヒー抽出物の官能評価、乾燥固形分測定、クロロゲン酸測定を行った。
[Test Example 3]
Example 2, Example 3, Example 7, Example 8, Comparative Example 3, Comparative Example 4, Comparative Example 5, Comparative Example 6, sensory evaluation, dry solid content measurement, chlorogenic acid measurement of coffee extract obtained in Comparative Example 6 Went.
<官能評価>
実施例2、実施例3、実施例7、実施例8、比較例3、比較例4、比較例5、比較例6で得られたコーヒー抽出物を乾燥固形分1質量%になるように調整し、7名のパネルにより匂いのみの官能評価を行った。評価は以下の評価基準により、生豆臭に関する各項目を点数で評価し、各パネルの評価点を平均した。結果を表7に示した。
評価基準
5点:非常に強い
4点:強い
3点:中程度
2点:弱い
1点:非常に弱い
<Sensory evaluation>
The coffee extracts obtained in Example 2, Example 3, Example 7, Example 8, Comparative Example 3, Comparative Example 4, Comparative Example 5, and Comparative Example 6 were adjusted to have a dry solid content of 1% by mass. Then, sensory evaluation of only smell was performed by a panel of seven people. Evaluation evaluated each item regarding raw bean smell by the following evaluation criteria, and averaged the evaluation score of each panel. The results are shown in Table 7.
Evaluation criteria 5 points: very strong 4 points: strong 3 points: moderate 2 points: weak 1 point: very weak
<乾燥固形分の測定>
実施例2、実施例3、実施例7、実施例8、比較例3、比較例4、比較例5、比較例6で得られたコーヒー抽出物を試験例2と同様の方法で乾燥固形分測定を行った。結果を表7に示した。
<Measurement of dry solid content>
The coffee extracts obtained in Example 2, Example 3, Example 7, Example 8, Comparative Example 3, Comparative Example 4, Comparative Example 5, and Comparative Example 6 were dried in the same manner as in Test Example 2. Measurements were made. The results are shown in Table 7.
<クロロゲン酸の測定方法>
実施例2、実施例3、実施例7、実施例8、比較例3、比較例4、比較例5、比較例6で得られたコーヒー抽出物のクロロゲン酸の測定を行った。結果を表7に示した。
<Measurement method of chlorogenic acid>
The coffee extracts obtained in Example 2, Example 3, Example 7, Example 8, Comparative Example 3, Comparative Example 4, Comparative Example 5, and Comparative Example 6 were measured for chlorogenic acid. The results are shown in Table 7.
試料調整
希釈後の乾燥固形分が1質量%になるように試料を精秤、水で希釈し、0.45μmメンブランフィルターを通して測定試料を得た。
Sample preparation The sample was precisely weighed so that the dry solid content after dilution was 1% by mass, diluted with water, and a measurement sample was obtained through a 0.45 μm membrane filter.
測定法
装置:HPLC(Agilent Technoligies社製 1100)
カラム:CAPCELL Pak C18 MG
(内径4.6mm×長さ250mm、充填剤5μm)
溶離液:A液、B液のグラジエント
A液:アセトニトリル/水=10/90(pH2.5)
B液:アセトニトリル
表6にグラジエント条件を示した。
流速:1ml/min
オーブン温度:25℃
検出:UV324nm
試料注入量:10μl
Measuring apparatus: HPLC (manufactured by Agilent Technologies 1100)
Column: CAPCELL Pak C18 MG
(Inner diameter 4.6 mm x length 250 mm, filler 5 μm)
Eluent: A liquid, B liquid gradient A liquid: acetonitrile / water = 10/90 (pH 2.5)
Liquid B: acetonitrile Table 6 shows the gradient conditions.
Flow rate: 1 ml / min
Oven temperature: 25 ° C
Detection: UV324nm
Sample injection volume: 10 μl
実施例2、実施例3、実施例7、実施例8、のコーヒー抽出物は、生豆臭が非常に弱く、クロロゲン酸/乾燥固形分は高かった。比較例3、比較例4のコーヒー抽出物は、生豆臭は弱かったが、クロロゲン酸/乾燥固形分は低かった。比較例5のコーヒー抽出物はクロロゲン酸/乾燥固形分はやや高かったが、生豆臭は強かった。比較例6のコーヒー抽出物は、クロロゲン酸/乾燥固形分は高かったが、生豆臭は非常に強かった。 The coffee extracts of Example 2, Example 3, Example 7, and Example 8 had a very weak green bean odor and a high chlorogenic acid / dry solid content. The coffee extracts of Comparative Examples 3 and 4 had a weak green bean odor but a low chlorogenic acid / dry solid content. The coffee extract of Comparative Example 5 had a slightly higher chlorogenic acid / dry solid content but a strong green bean odor. The coffee extract of Comparative Example 6 had a high chlorogenic acid / dry solid content, but the raw bean odor was very strong.
[試験例4]
実施例4、実施例5、実施例6の食品を、7名のパネルで以下の評価基準をもとに官能評価(嗜好性)を行った。あわせて、試験例3と同様の方法で官能評価(生豆臭の強さ)、クロロゲン酸測定を行った。結果を表8に示す。
評価基準(嗜好性)
5点:非常に高い
4点:高い
3点:中程度
2点:低い
1点:非常に低い
[Test Example 4]
The food of Example 4, Example 5, and Example 6 was subjected to sensory evaluation (preference) using seven panels based on the following evaluation criteria. In addition, sensory evaluation (raw bean odor intensity) and chlorogenic acid measurement were performed in the same manner as in Test Example 3. The results are shown in Table 8.
Evaluation criteria (preference)
5 points: very high 4 points: high 3 points: moderate 2 points: low 1 point: very low
実施例4、実施例5、実施例6の食品はすべて嗜好性が高く、生豆臭が弱く、クロロゲン酸を豊富に含んでいた。 The foods of Example 4, Example 5, and Example 6 were all highly palatable, had a weak raw bean odor, and were rich in chlorogenic acid.
Claims (11)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2010210488A JP2011083282A (en) | 2009-09-18 | 2010-09-21 | Method for producing coffee extract |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2009218063 | 2009-09-18 | ||
JP2010210488A JP2011083282A (en) | 2009-09-18 | 2010-09-21 | Method for producing coffee extract |
Publications (1)
Publication Number | Publication Date |
---|---|
JP2011083282A true JP2011083282A (en) | 2011-04-28 |
Family
ID=44076735
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2010210488A Pending JP2011083282A (en) | 2009-09-18 | 2010-09-21 | Method for producing coffee extract |
Country Status (1)
Country | Link |
---|---|
JP (1) | JP2011083282A (en) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2601844A1 (en) * | 2011-12-05 | 2013-06-12 | Plantextrakt GmbH&Co. Kg | Method of producing an extract enriched with trigonelline (TRIG) and/or chlorogenic acids (CQA), extract enriched with trigonelline (TRIG) and/or chlorogenic acids (CQA) and the use of same |
JP2014150780A (en) * | 2013-02-13 | 2014-08-25 | Nisshin Foods Kk | Method for producing vegetable or fruit paste |
JP2018050535A (en) * | 2016-09-29 | 2018-04-05 | キーコーヒー株式会社 | Modified coffee raw bean, modification method of coffee raw bean, roasted coffee bean, production method thereof, and production method of coffee extract |
CN112640981A (en) * | 2020-12-03 | 2021-04-13 | 东莞波顿香料有限公司 | Coffee heat treatment liquid, coffee heat treatment liquid extract, preparation method and application of coffee heat treatment liquid and coffee heat treatment liquid extract |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2000342182A (en) * | 1999-06-01 | 2000-12-12 | Pokka Corp | Modification of coffee bean |
WO2005011396A1 (en) * | 2003-07-31 | 2005-02-10 | Suntory Limited | Method of treating roasted coffee beans and vapor-treated roasted coffee beans |
JP2006081451A (en) * | 2004-09-15 | 2006-03-30 | Key Coffee Inc | Coffee raw bean-processed material, processed material for extracting beverage, and beverage using the processed material |
JP2006191925A (en) * | 2004-12-14 | 2006-07-27 | T Hasegawa Co Ltd | Method for producing coffee extract |
JP2007181406A (en) * | 2005-12-30 | 2007-07-19 | Ito En Ltd | Packaged coffee beverage and method for producing the same |
-
2010
- 2010-09-21 JP JP2010210488A patent/JP2011083282A/en active Pending
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2000342182A (en) * | 1999-06-01 | 2000-12-12 | Pokka Corp | Modification of coffee bean |
WO2005011396A1 (en) * | 2003-07-31 | 2005-02-10 | Suntory Limited | Method of treating roasted coffee beans and vapor-treated roasted coffee beans |
JP2006081451A (en) * | 2004-09-15 | 2006-03-30 | Key Coffee Inc | Coffee raw bean-processed material, processed material for extracting beverage, and beverage using the processed material |
JP2006191925A (en) * | 2004-12-14 | 2006-07-27 | T Hasegawa Co Ltd | Method for producing coffee extract |
JP2007181406A (en) * | 2005-12-30 | 2007-07-19 | Ito En Ltd | Packaged coffee beverage and method for producing the same |
Non-Patent Citations (2)
Title |
---|
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, vol. 48, no. 3, JPN6015022235, 2000, US, pages 868 - 872, ISSN: 0003087425 * |
コーヒー用語辞典, JPN6014032488, 2009, JP, ISSN: 0002868368 * |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2601844A1 (en) * | 2011-12-05 | 2013-06-12 | Plantextrakt GmbH&Co. Kg | Method of producing an extract enriched with trigonelline (TRIG) and/or chlorogenic acids (CQA), extract enriched with trigonelline (TRIG) and/or chlorogenic acids (CQA) and the use of same |
JP2014150780A (en) * | 2013-02-13 | 2014-08-25 | Nisshin Foods Kk | Method for producing vegetable or fruit paste |
JP2018050535A (en) * | 2016-09-29 | 2018-04-05 | キーコーヒー株式会社 | Modified coffee raw bean, modification method of coffee raw bean, roasted coffee bean, production method thereof, and production method of coffee extract |
CN112640981A (en) * | 2020-12-03 | 2021-04-13 | 东莞波顿香料有限公司 | Coffee heat treatment liquid, coffee heat treatment liquid extract, preparation method and application of coffee heat treatment liquid and coffee heat treatment liquid extract |
CN112640981B (en) * | 2020-12-03 | 2023-11-10 | 东莞波顿香料有限公司 | Coffee heat treatment liquid, extracting solution, preparation method and application thereof |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
ES2441450T3 (en) | Method to produce a green coffee extract | |
RU2709654C2 (en) | Method of powdered coffee drink production | |
JP4568490B2 (en) | Method for producing volatile component, food and drink containing volatile component, and method for producing coffee beverage or tea beverage | |
WO2010124936A1 (en) | Food or beverage composition comprising unroasted coffee solids | |
JP2008543336A (en) | Method for isolating bitter compounds for use in food and beverage products | |
JP6778994B2 (en) | Tea extract manufacturing method | |
JP5872215B2 (en) | Coffee extract composition | |
JP5622451B2 (en) | Tea extract | |
JP2009219488A (en) | Coffee caramel, food containing coffee caramel and method for producing coffee caramel | |
WO2007077746A1 (en) | Container-packed coffee beverage and process for production thereof | |
JP2011083282A (en) | Method for producing coffee extract | |
TWI674316B (en) | Process for producing enzymatically treated plant extract | |
JP4679362B2 (en) | Preparation method of tea extract | |
JP2020072665A (en) | Method of producing tea extract | |
JP6212675B1 (en) | Tea drink | |
WO2016189888A1 (en) | Method for producing roasted-aroma recovered material | |
JPH0334896B2 (en) | ||
JP7578210B1 (en) | Coffee drink and composition for instant coffee drink | |
JP4871010B2 (en) | Method for producing chlorogenic acid-containing material | |
JP5992765B2 (en) | Coffee flavor, its production method and its use | |
CN104039160B (en) | Coffee beverage, the extracting method of coffee liquid and the Extraction solvent for extracting coffee liquid | |
JP7150691B2 (en) | METHOD FOR IMPROVING FLAVOR OF COFFEE BEVERAGE | |
Fardenan et al. | Effect of acetic acid immersion on the taste and aroma quality of immature Robusta coffee beans. | |
JP2024062565A (en) | Coffee beverage and composition for instant coffee beverage | |
JP2020174637A (en) | Flavor expression enhancer containing 3-mercaptohexanal as active ingredient |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
A621 | Written request for application examination |
Free format text: JAPANESE INTERMEDIATE CODE: A621 Effective date: 20130726 |
|
A977 | Report on retrieval |
Free format text: JAPANESE INTERMEDIATE CODE: A971007 Effective date: 20140718 |
|
A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20140805 |
|
A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20141002 |
|
A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20141209 |
|
A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20150130 |
|
A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20150306 |
|
A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A821 Effective date: 20150309 |
|
A02 | Decision of refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A02 Effective date: 20150609 |