JP2010233497A - Extract from soybean curd refuse - Google Patents
Extract from soybean curd refuse Download PDFInfo
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- JP2010233497A JP2010233497A JP2009085066A JP2009085066A JP2010233497A JP 2010233497 A JP2010233497 A JP 2010233497A JP 2009085066 A JP2009085066 A JP 2009085066A JP 2009085066 A JP2009085066 A JP 2009085066A JP 2010233497 A JP2010233497 A JP 2010233497A
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- extract
- okara
- ethanol
- soybean curd
- curd refuse
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
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- Non-Alcoholic Beverages (AREA)
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Abstract
Description
本発明は、オカラからの抽出物に関し、特に、産業廃棄物としてのオカラの廃棄コストを削減し、バイオディーゼル燃料への転用の可能性、化粧品、飲料などへの混入にて様々な効果を図ることが可能な、オカラからの抽出物に関する。 The present invention relates to an extract from okara, and in particular, reduces the disposal cost of okara as industrial waste, and aims at various effects in the possibility of diversion to biodiesel fuel, mixing in cosmetics, beverages, and the like. It relates to an extract from Okara.
オカラは、それ自体が食用に供されるものであるが、豆腐製造の際に大量に発生する産業廃棄物としての性格も有しており、現在国内で年間約70万トン(未乾燥の状態で)の廃棄物としてのオカラが発生している。オカラの廃棄物としての処理コストは、現在1トン当たり約2万円の負担が生じており、オカラの有効活用についても、種々検討がなされている。例えば特許文献1には、オカラと油とを混合して水性溶媒中に分散し、溶媒を除去して油含有おからを製造する方法が開示されている。 Okara itself is used for food, but it also has the character of industrial waste generated in large quantities during the production of tofu. Okara is generated as waste. The cost of disposal of Okara as waste currently costs about 20,000 yen per ton, and various studies have been conducted on the effective use of Okara. For example, Patent Document 1 discloses a method for producing an oil-containing okara by mixing okara and oil, dispersing the mixture in an aqueous solvent, and removing the solvent.
特許文献1に記載の技術では、オカラに飽和脂肪酸、不飽和脂肪酸などを混入する必要があり、コスト的に見合わないという問題がある。 In the technique described in Patent Document 1, it is necessary to mix saturated fatty acid, unsaturated fatty acid, and the like into okara, and there is a problem that it is not commensurate with cost.
本発明は上記の点に鑑みてなされたものであって、産業廃棄物としてのオカラの廃棄コストを削減し、バイオディーゼル燃料への転用の可能性、飲料、化粧品などへの混入にて様々な効果を図ることが可能な、オカラからの抽出物を提供することを目的としている。 The present invention has been made in view of the above points, and reduces the cost of disposal of okara as industrial waste, which can be diverted to biodiesel fuel, mixed in beverages, cosmetics, and the like. The object is to provide an extract from Okara that can be effective.
上記の問題点を解決するために、本発明に係るオカラからの抽出物は、オカラにエタノールを加え、可溶分を抽出した後にろ過し、エタノールを除去して得られることを特徴としている。 In order to solve the above-mentioned problems, the extract from okara according to the present invention is characterized in that it is obtained by adding ethanol to okara, extracting a soluble component, and filtering to remove ethanol.
本発明においては、オカラにエタノールを加えて、可溶分を抽出し、エタノールを除去して抽出物を得る。この抽出物には、オカラに含有される脂肪分やたんぱく質が含まれており、さらに脂肪分を取り出せば、バイオディーゼル燃料の原料となり得るし、イソフラボンなども含まれているとすれば、飲料への混入、化粧品への混入など、様々な効果を得る可能性が期待できる。一方、抽出物を得た後は、産業廃棄物が減少するため、産業廃棄物としてのオカラの廃棄コスト削減を図ることもできる。 In the present invention, ethanol is added to okara to extract soluble components, and ethanol is removed to obtain an extract. This extract contains fat and protein contained in okara, and if the fat is further extracted, it can be used as a raw material for biodiesel fuel. The possibility of obtaining various effects such as contamination of cosmetics and cosmetics can be expected. On the other hand, after the extract is obtained, industrial waste is reduced, so that the cost of discarding Okara as industrial waste can be reduced.
前記可溶分の抽出に際して、試料を50℃から60℃とすることができるが、抽出条件は、これに限定されず、より高温にて加熱還流すれば、より多くの有効成分が抽出されることも期待できる。抽出時間は、例えば1時間とすることができる。エタノールを用いた場合、比較的短時間で有効成分の抽出ができると思われるためであるが、より長時間としてもよいことは勿論である。 When extracting the soluble component, the sample can be set to 50 ° C. to 60 ° C. However, the extraction conditions are not limited to this, and more effective components can be extracted by heating and refluxing at a higher temperature. I can also expect that. The extraction time can be, for example, 1 hour. This is because when ethanol is used, it is considered that the active ingredient can be extracted in a relatively short time, but it is needless to say that a longer time may be used.
さらに、水分を除去すると、飲料、化粧品への混入の他、健康食品としての活用も図ることが可能である。さらに、脂肪分を溶解する有機溶剤により抽出を行えば、バイオディーゼル燃料の原料としても好適なものとなり得る。 Furthermore, when moisture is removed, it can be used as a health food as well as mixed into beverages and cosmetics. Furthermore, extraction with an organic solvent that dissolves fat can be a suitable raw material for biodiesel fuel.
なお、本発明に係るオカラからの抽出物の製造方法は、オカラにエタノールを加え、可溶分を抽出する抽出工程と、抽出工程で得られた物をろ過するろ過工程と、ろ過した後に得られたろ液からエタノールを除去するエタノール除去工程とを含むことを特徴としている。 The method for producing an extract from okara according to the present invention is obtained by adding ethanol to okara and extracting a soluble component, a filtration step for filtering the product obtained in the extraction step, and filtering. And an ethanol removal step of removing ethanol from the filtrate.
本発明に係るオカラからの抽出物によると、産業廃棄物としてのオカラの廃棄コストを削減し、様々な効果を図ることが可能であるといった効果が奏される。 According to the extract from Okara according to the present invention, the cost of discarding Okara as industrial waste can be reduced, and various effects can be achieved.
以下、本発明の実施の形態について、図面を参照しながら説明する。 Hereinafter, embodiments of the present invention will be described with reference to the drawings.
図1は、本実施の形態におけるオカラからの抽出物の取得について説明するための図である。本実施の形態では、ビーカー101にオカラ102を100グラム入れて、エタノール103を500ml加えた。溶媒としてエタノールを用いたのは、毒性が低いこと、試験的な実施の結果、短時間でエタノールが着色し、オカラ中の有効成分を比較的短い時間で抽出することが可能であると考えられたことによる。
FIG. 1 is a diagram for explaining acquisition of an extract from okara in the present embodiment. In this embodiment, 100 grams of
そして、図1には不図示の水浴中で50℃から60℃とし、ときどきガラス棒104を用いて、試料をよく撹拌しつつ、約1時間有効成分の抽出を行った。
Then, the active ingredient was extracted for about 1 hour while thoroughly stirring the sample using a
その後、図2に示されるように、ろ紙105を設置した漏斗106を用いてオカラの粒をこし取り、ビーカー107中にオカラからの抽出物108を得た。その後、ガスコンロでの湯煎によってエタノールを除去して分析用の抽出物試料を得た。ろ過は、図2に示したような通常の漏斗106を用いる方法に限定されず、減圧ろ過とすれば、より多くの有効成分が抽出され得るし、残渣をエタノールで洗浄し、さらに抽出物を得ても良いことは勿論である。
Thereafter, as shown in FIG. 2, the particles of okara were scraped using a
次に得られた抽出物試料の分析結果について説明する。本実施の形態では、脂肪含有量の測定、及びたんぱく質含有量の測定を行った。脂肪含有量の測定には、一般に大豆、大豆加工食品に適するといわれるクロロホルム・メタノール混液抽出法を用いた。たんぱく質含有量の測定には、食品全般に用いられるマクロ改良ケルダール法を用いた。 Next, the analysis result of the obtained extract sample will be described. In the present embodiment, measurement of fat content and measurement of protein content were performed. For the measurement of the fat content, a chloroform / methanol mixed liquid extraction method, which is generally said to be suitable for soybeans and processed soybean foods, was used. For the measurement of protein content, the macro modified Kjeldahl method used for all foods was used.
分析の結果、オカラ100gから採れた脂肪分の量は最大で0.79gであり、オカラ100gから採れたたんぱく質は最大で0.089gであった。なお、脂肪含有量測定用試料とたんぱく質含有量測定用試料は個別に作製したものであり、また、オカラの種類の相違(主として原料大豆の相違、豆腐の製造方法の相違)などによっても、脂肪含有量、たんぱく質含有量は異なる可能性がある。従って、本願発明の範囲が、上記に説明する測定結果に限定されないことは当然であることは念のために付記する。 As a result of analysis, the maximum amount of fat extracted from 100 g of okara was 0.79 g, and the maximum amount of protein extracted from 100 g of okara was 0.089 g. Note that the fat content measurement sample and the protein content measurement sample were prepared separately, and also due to differences in the types of okara (mainly differences in raw soybeans and differences in the production method of tofu) Content and protein content may vary. Therefore, it should be noted that the scope of the present invention is not limited to the measurement results described above.
なお、オカラのエタノール抽出物に含まれる脂肪分、たんぱく質などは、抽出時間、抽出条件(例えば加熱還流)によっても変化する可能性もあり、より高温、長時間とすれば、有効成分の抽出量は増加し、結果としてオカラの廃棄コスト削減に資する可能性も高い。エタノールは毒性が低く、抽出物は、飲料、化粧品など、種々の製品に混入して、効果を図ることが可能である。また、脂肪分を溶解する有機溶剤で、さらに抽出処理を行えば、バイオディーゼル燃料の原料とすることもできる。 In addition, fat content, protein, etc. contained in Okara's ethanol extract may change depending on the extraction time and extraction conditions (for example, heating and refluxing). As a result, there is a high possibility that it will contribute to the reduction of Okara disposal costs. Ethanol has low toxicity, and the extract can be mixed with various products such as beverages and cosmetics to achieve an effect. Further, if extraction processing is further performed with an organic solvent that dissolves fat, it can be used as a raw material for biodiesel fuel.
本発明は、例えば、オカラからの抽出物の活用に適用することができる。 The present invention can be applied to, for example, utilization of an extract from okara.
101、107 ビーカー
102 オカラ
103 エタノール
104 ガラス棒
105 ろ紙
106 漏斗
108 オカラからの抽出物
101, 107 Beaker 102 Okara 103
Claims (11)
ことを特徴とする請求項1に記載のオカラからの抽出物。 The extract from okara according to claim 1, wherein the temperature during extraction of the soluble component is set to 50 to 60 ° C.
ことを特徴とする請求項1又は2に記載のオカラからの抽出物。 Furthermore, the water | moisture content was removed, The extract from the okara of Claim 1 or 2 characterized by the above-mentioned.
ことを特徴とする請求項1から3のいずれかに記載のオカラからの抽出物。 The extract from okara according to any one of claims 1 to 3, further extracted with an organic solvent that dissolves fat.
ことを特徴とするバイオディーゼル燃料。 A biodiesel fuel produced from the extract from okara according to any one of claims 1 to 4.
ことを特徴とする飲料。 A beverage comprising the extract from okara according to any one of claims 1 to 4.
ことを特徴とする化粧品。 A cosmetic product comprising the extract from okara according to any one of claims 1 to 4.
抽出工程で得られた物をろ過するろ過工程と、
ろ過した後に得られたろ液からエタノールを除去するエタノール除去工程とを含む
ことを特徴とするオカラからの抽出物の製造方法。 An extraction step of adding ethanol to okara and extracting soluble components;
A filtration step of filtering the product obtained in the extraction step;
And an ethanol removal step of removing ethanol from the filtrate obtained after filtration. A method for producing an extract from okara.
ことを特徴とする請求項8に記載のオカラからの抽出物の製造方法。 In the said extraction process, temperature is 50 to 60 degreeC. The manufacturing method of the extract from the okara of Claim 8 characterized by the above-mentioned.
ことを特徴とする請求項8又は9に記載のオカラからの抽出物の製造方法。 Furthermore, the water removal process which removes a water | moisture content is included. The manufacturing method of the extract from the okara of Claim 8 or 9 characterized by the above-mentioned.
ことを特徴とする請求項8から10のいずれかに記載のオカラからの抽出物の製造方法。 Furthermore, the fat content extraction process which extracts a fat content with the organic solvent which melt | dissolves a fat content is included. The manufacturing method of the extract from the okara in any one of Claim 8 to 10 characterized by the above-mentioned.
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN115343428A (en) * | 2022-08-02 | 2022-11-15 | 山东金胜粮油食品有限公司 | Method for measuring residual quantity of fat in oil residue or soap residue |
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JPS58187155A (en) * | 1982-04-26 | 1983-11-01 | Meiji Milk Prod Co Ltd | Food raw material and its preparation |
JPH0376551A (en) * | 1989-08-16 | 1991-04-02 | Raifu Eng Kk | Preparation of food raw material from bean curd refuse |
JPH04114653A (en) * | 1990-09-06 | 1992-04-15 | Toppan Printing Co Ltd | Deodorant and manufacture thereof |
JPH04359993A (en) * | 1991-06-06 | 1992-12-14 | Daiki:Kk | Fuel |
JPH0748403A (en) * | 1993-06-03 | 1995-02-21 | Nippon Chem Res Kk | Polysaccharide originated from 'tanjin', production and use thereof |
JP2005179226A (en) * | 2003-12-18 | 2005-07-07 | Shiseido Co Ltd | Method for extracting skin-whitening ingredient from hakushinin |
JP2005298400A (en) * | 2004-04-12 | 2005-10-27 | Bernet International:Kk | Cosmetic |
WO2008018785A1 (en) * | 2006-08-07 | 2008-02-14 | Universiti Sains Malaysia | Polar organic extract of eurycoma longifolia |
JP2008214215A (en) * | 2007-03-01 | 2008-09-18 | Mitsukan Group Honsha:Kk | Composition having apoptosis induction ability |
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2009
- 2009-03-31 JP JP2009085066A patent/JP2010233497A/en active Pending
Patent Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
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JPS58187155A (en) * | 1982-04-26 | 1983-11-01 | Meiji Milk Prod Co Ltd | Food raw material and its preparation |
JPH0376551A (en) * | 1989-08-16 | 1991-04-02 | Raifu Eng Kk | Preparation of food raw material from bean curd refuse |
JPH04114653A (en) * | 1990-09-06 | 1992-04-15 | Toppan Printing Co Ltd | Deodorant and manufacture thereof |
JPH04359993A (en) * | 1991-06-06 | 1992-12-14 | Daiki:Kk | Fuel |
JPH0748403A (en) * | 1993-06-03 | 1995-02-21 | Nippon Chem Res Kk | Polysaccharide originated from 'tanjin', production and use thereof |
JP2005179226A (en) * | 2003-12-18 | 2005-07-07 | Shiseido Co Ltd | Method for extracting skin-whitening ingredient from hakushinin |
JP2005298400A (en) * | 2004-04-12 | 2005-10-27 | Bernet International:Kk | Cosmetic |
WO2008018785A1 (en) * | 2006-08-07 | 2008-02-14 | Universiti Sains Malaysia | Polar organic extract of eurycoma longifolia |
JP2008214215A (en) * | 2007-03-01 | 2008-09-18 | Mitsukan Group Honsha:Kk | Composition having apoptosis induction ability |
Non-Patent Citations (3)
Title |
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JPN6013004888; Bioresource Technol. vol.97, 2006, p.1509-14 * |
JPN6013004889; 玉川大学学術研究紀要 第6号, 2000, p.73-80 * |
JPN6013047988; New Food Industry Vol.54,No.3, 2012, P.59-63 * |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN115343428A (en) * | 2022-08-02 | 2022-11-15 | 山东金胜粮油食品有限公司 | Method for measuring residual quantity of fat in oil residue or soap residue |
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