JP2009510261A5 - Electrochemical deposition of selenium in ionic liquids - Google Patents

Electrochemical deposition of selenium in ionic liquids Download PDF

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JP2009510261A5
JP2009510261A5 JP2008532621A JP2008532621A JP2009510261A5 JP 2009510261 A5 JP2009510261 A5 JP 2009510261A5 JP 2008532621 A JP2008532621 A JP 2008532621A JP 2008532621 A JP2008532621 A JP 2008532621A JP 2009510261 A5 JP2009510261 A5 JP 2009510261A5
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imidazolium
hydroxypropyl
hydroxyethyl
methyl
hydroxybutyl
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１，１−ジヘキシルピロリジニウム、１−ヘキシル−１−ヘプチルピロリジニウム、１−ヘキシル−１−オクチルピロリジニウム、１−ヘキシル−１−ノニルピロリジニウム、１−ヘキシル−１−デシルピロリジニウム、１，１−ジヘキシルピロリジニウム、１−ヘキシル−１−ヘプチルピロリジニウム、１−ヘキシル−１−オクチルピロリジニウム、１−ヘキシル−１−ノニルピロリジニウム、１−ヘキシル−１−デシルピロリジニウム、１，１−ジヘプチルピロリジニウム、１−ヘプチル−１−オクチルピロリジニウム、１−ヘプチル−１−ノニルピロリジニウム、１−ヘプチル−１−デシルピロリジニウム、１，１−ジオクチルピロリジニウム、１−オクチル−１−ノニルピロリジニウム、１−オクチル−１−デシルピロリジニウム、１，１−ジノニルピロリジニウム、１−ノニル−１−デシルピロリジニウム、または１，１−ジデシルピロリジニウム、 1,1-dihexylpyrrolidinium, 1-hexyl-1-heptylpyrrolidinium, 1-hexyl-1-octylpyrrolidinium, 1-hexyl-1-nonylpyrrolidinium, 1-hexyl-1-decylpyrrole Dinium, 1,1-dihexylpyrrolidinium, 1-hexyl-1-heptylpyrrolidinium, 1-hexyl-1-octylpyrrolidinium, 1-hexyl-1-nonylpyrrolidinium, 1-hexyl-1 -Decylpyrrolidinium, 1,1-diheptylpyrrolidinium, 1-heptyl-1-octylpyrrolidinium, 1-heptyl-1-nonylpyrrolidinium, 1-heptyl-1-decylpyrrolidinium, , 1-dioctylpyrrolidinium, 1-octyl-1-nonylpyrrolidinium, 1-octyl-1-decylpyrrolidinium, 1-dinonyl pyrrolidinium, 1-nonyl-1-decyl pyrrolidinium or 1,1 didecyl pyrrolidinium,

Claims (2)

イオン性液体が、少なくとも１つのテトラアルキルアンモニウム、テトラアルキルホスホニウム−、１，１−ジアルキルピロリジニウム、１−ヒドロキシアルキル−１−アルキルピロリジニウム、１−ヒドロキシアルキル−３−アルキルイミダゾリウム、または１，３−ビス（ヒドロキシアルキル）イミダゾリウムのカチオンを含有し、アルキル基またはヒドロキシアルキル基のアルキレン鎖は、各々互いに独立して、１〜１０個のＣ原子を有してもよい、請求項１または２に記載の方法。 The ionic liquid is at least one tetraalkylammonium, tetraalkylphosphonium-, 1,1-dialkylpyrrolidinium, 1-hydroxyalkyl-1-alkylpyrrolidinium, 1-hydroxyalkyl-3-alkylimidazolium, or containing 1,3-bis (hydroxyalkyl) imidazolium cation, a alkylene chain alkyl or hydroxyalkyl groups are each independently of one another, may have a 1 to 10 C atoms, wherein Item 3. The method according to Item 1 or 2. カチオンが、以下の群より選択される、請求項１〜５のいずれかに記載の方法：直鎖または分枝状の、テトラメチルアンモニウム、テトラエチルアンモニウム、テトラプロピルアンモニウム、テトラブチルアンモニウム、テトラペンチルアンモニウム、テトラヘキシルアンモニウム、テトラヘプチルアンモニウム、テトラオクチルアンモニウム、テトラノニルアンモニウム、テトラデシルアンモニウム、トリメチルアルキルアンモニウム、トリメチル（エチル）アンモニウム、トリエチル（メチル）アンモニウム、トリヘキシルアンモニウム、メチル（トリオクチル）アンモニウム、テトラメチルホスホニウム、テトラエチルホスホニウム、テトラプロピルホスホニウム、テトラブチルホスホニウム、テトラペンチルホスホニウム、テトラヘキシルホスホニウム、テトラヘプチルホスホニウム、テトラオクチルホスホニウム、テトラノニルホスホニウム、テトラデシルホスホニウム、トリヘキシルテトラデシルホスホニウム、トリイソブチル（メチル）ホスホニウム、トリブチル（エチル）ホスホニウム、トリブチル（メチル）ホスホニウム、１，１−ジメチルピロリジニウム、１−メチル−１−エチルピロリジニウム、１−メチル−１−プロピルピロリジニウム、１−メチル−１−ブチルピロリジニウム、１−メチル−１−ペンチルピロリジニウム、１−メチル−１−ヘキシルピロリジニウム、１−メチル−１−ヘプチルピロリジニウム、１−メチル−１−オクチルピロリジニウム、１−メチル−１−ノニルピロリジニウム、１−メチル−１−デシルピロリジニウム、１，１−ジエチルピロリジニウム、１−エチル−１−プロピルピロリジニウム、１−エチル−１−ブチルピロリジニウム、１−エチル−１−ペンチルピロリジニウム、１−エチル−１−ヘキシルピロリジニウム、１−エチル−１−ヘプチルピロリジニウム、１−エチル−１−オクチルピロリジニウム、１−エチル−１−ノニルピロリジニウム、１−エチル−１−デシルピロリジニウム、１，１−ジプロピルピロリジニウム、１−プロピル−１−ブチルピロリジニウム、１−プロピル−１−ペンチルピロリジニウム、１−プロピル−１−ヘキシルピロリジニウム、１−プロピル−１−ヘプチルピロリジニウム、１−プロピル−１−オクチルピロリジニウム、１−プロピル−１−ノニルピロリジニウム、１−プロピル−１−デシルピロリジニウム、１，１−ジブチルピロリジニウム、１−ブチル−１−ペンチルピロリジニウム、１−ブチル−１−ヘキシルピロリジニウム、１−ブチル−１−ヘプチルピロリジニウム、１−ブチル−１−オクチルピロリジニウム、１−ブチル−１−ノニルピロリジニウム、１−ブチル−１−デシルピロリジニウム、１，１−ジペンチルピロリジニウム、１−ペンチル−１−ヘキシルピロリジニウム、１−ペンチル−１−ヘプチルピロリジニウム、１−ペンチル−１−オクチルピロリジニウム、１−ペンチル−１−ノニルピロリジニウム、１−ペンチル−１−デシルピロリジニウム、１，１−ジヘキシルピロリジニウム、１−ヘキシル−１−ヘプチルピロリジニウム、１−ヘキシル−１−オクチルピロリジニウム、１−ヘキシル−１−ノニルピロリジニウム、１−ヘキシル−１−デシルピロリジニウム、１，１−ジヘキシルピロリジニウム、１−ヘキシル−１−ヘプチルピロリジニウム、１−ヘキシル−１−オクチルピロリジニウム、１−ヘキシル−１−ノニルピロリジニウム、１−ヘキシル−１−デシルピロリジニウム、１，１−ジヘプチルピロリジニウム、１−ヘプチル−１−オクチルピロリジニウム、１−ヘプチル−１−ノニルピロリジニウム、１−ヘプチル−１−デシルピロリジニウム、１，１−ジオクチルピロリジニウム、１−オクチル−１−ノニルピロリジニウム、１−オクチル−１−デシルピロリジニウム、１，１−ジノニルピロリジニウム、１−ノニル−１−デシルピロリジニウム、または１，１−ジデシルピロリジニウム、１−ヒドロキシメチル−１−メチルピロリジニウム、１−ヒドロキシメチル−１−エチルピロリジニウム、１−ヒドロキシメチル−１−プロピルピロリジニウム、１−ヒドロキシメチル−１−ブチルピロリジニウム、１−（２−ヒドロキシエチル）−１−メチルピロリジニウム、１−（２−ヒドロキシエチル）−１−エチルピロリジニウム、１−（２−ヒドロキシエチル）−１−プロピルピロリジニウム、１−（２−ヒドロキシエチル）−１−ブチルピロリジニウム、１−（３−ヒドロキシプロピル）−１−メチルピロリジニウム、１−（３−ヒドロキシプロピル）−１−エチルピロリジニウム、１−（３−ヒドロキシプロピル）−１−プロピルピロリジニウム、１−（３−ヒドロキシプロピル）−１−ブチルピロリジニウム、１−（４−ヒドロキシブチル）−１−メチルピロリジニウム、１−（４−ヒドロキシブチル）−１−エチルピロリジニウム、１−（４−ヒドロキシブチル）−１−プロピルピロリジニウム、または１−（４−ヒドロキシブチル）−１−ブチルピロリジニウム、１−（１−ヒドロキシメチル）−３−メチルイミダゾリウム、１−（１−ヒドロキシメチル）−３−エチルイミダゾリウム、１−（１−ヒドロキシメチル）−３−プロピルイミダゾリウム、１−（１−ヒドロキシメチル）−３−ブチルイミダゾリウム、１−（２−ヒドロキシエチル）−３−メチルイミダゾリウム、１−（２−ヒドロキシエチル）−３−エチルイミダゾリウム、１−（２−ヒドロキシエチル）−３−プロピルイミダゾリウム、１−（２−ヒドロキシエチル）−３−ブチルイミダゾリウム、１−（３−ヒドロキシプロピル）−３−メチルイミダゾリウム、１−（３−ヒドロキシプロピル）−３−エチルイミダゾリウム、１−（３−ヒドロキシプロピル）−３−プロピルイミダゾリウム、１−（３−ヒドロキシプロピル）−３−ブチルイミダゾリウム、１−（４−ヒドロキシブチル）−３−メチルイミダゾリウム、１−（４−ヒドロキシブチル）−３−エチルイミダゾリウム、１−（４−ヒドロキシブチル）−３−プロピルイミダゾリウム、１−（４−ヒドロキシブチル）−３−ブチルイミダゾリウム、１，３−ビス（１−ヒドロキシメチル）イミダゾリウム、１，３−ビス（２−ヒドロキシエチル）イミダゾリウム、１，３−ビス（３−ヒドロキシプロピル）イミダゾリウム、１，３−ビス（４−ヒドロキシブチル）イミダゾリウム、１−（２−ヒドロキシエチル）−３−（１−ヒドロキシメチル）イミダゾリウム、１−（２−ヒドロキシエチル）−３−（３−ヒドロキシプロピル）イミダゾリウム、１−（２−ヒドロキシエチル）−３−（４−ヒドロキシブチル）イミダゾリウム、１−（３−ヒドロキシプロピル）−３−（１−ヒドロキシメチル）イミダゾリウム、１−（３−ヒドロキシプロピル）−３−（２−ヒドロキシエチル）イミダゾリウム、１−（３−ヒドロキシプロピル）−３−（４−ヒドロキシブチル）イミダゾリウム、１−（４−ヒドロキシブチル）−３−（１−ヒドロキシメチル）イミダゾリウム、１−（４−ヒドロキシブチル）−３−（２−ヒドロキシエチル）イミダゾリウム、または１−（４−ヒドロキシブチル）−３−（３−ヒドロキシプロピル）イミダゾリウム。 6. The method according to any of claims 1 to 5, wherein the cation is selected from the following group: linear or branched tetramethylammonium, tetraethylammonium, tetrapropylammonium, tetrabutylammonium, tetrapentylammonium , Tetrahexylammonium, tetraheptylammonium, tetraoctylammonium, tetranonylammonium, tetradecylammonium, trimethylalkylammonium, trimethyl (ethyl) ammonium, triethyl (methyl) ammonium, trihexylammonium, methyl (trioctyl) ammonium, tetramethylphosphonium Tetraethylphosphonium, tetrapropylphosphonium, tetrabutylphosphonium, tetrapentylphosphonium, tetra Silphosphonium, tetraheptylphosphonium, tetraoctylphosphonium, tetranonylphosphonium, tetradecylphosphonium, trihexyltetradecylphosphonium, triisobutyl (methyl) phosphonium, tributyl (ethyl) phosphonium, tributyl (methyl) phosphonium, 1,1-dimethylpyrroline Dinium, 1-methyl-1-ethylpyrrolidinium, 1-methyl-1-propylpyrrolidinium, 1-methyl-1-butylpyrrolidinium, 1-methyl-1-pentylpyrrolidinium, 1-methyl -1-hexylpyrrolidinium, 1-methyl-1-heptylpyrrolidinium, 1-methyl-1-octylpyrrolidinium, 1-methyl-1-nonylpyrrolidinium, 1-methyl-1-decylpyrrolidi Ni, 1,1-di Tilpyrrolidinium, 1-ethyl-1-propylpyrrolidinium, 1-ethyl-1-butylpyrrolidinium, 1-ethyl-1-pentylpyrrolidinium, 1-ethyl-1-hexylpyrrolidinium, 1 - ethyl-1-heptyl pyrrolidinium, 1 - ethyl-1-octyl pyrrolidinium, 1-ethyl-1-nonyl pyrrolidinium, 1-ethyl-1-decyl pyrrolidinium, 1,1-di-propyl pylori Dinium, 1-propyl-1-butylpyrrolidinium, 1-propyl-1-pentylpyrrolidinium, 1-propyl-1-hexylpyrrolidinium, 1-propyl-1-heptylpyrrolidinium, 1-propyl -1-octylpyrrolidinium, 1-propyl-1-nonylpyrrolidinium, 1-propyl-1-decylpyrrolidinium, 1,1- Butylpyrrolidinium, 1-butyl-1-pentylpyrrolidinium, 1-butyl-1-hexylpyrrolidinium, 1-butyl-1-heptylpyrrolidinium, 1-butyl-1-octylpyrrolidinium, 1 -Butyl-1-nonylpyrrolidinium, 1-butyl-1-decylpyrrolidinium, 1,1-dipentylpyrrolidinium, 1-pentyl-1-hexylpyrrolidinium, 1-pentyl-1-heptylpyrrolidi 1-pentyl-1-octylpyrrolidinium, 1-pentyl-1-nonylpyrrolidinium, 1-pentyl-1-decylpyrrolidinium, 1,1-dihexylpyrrolidinium, 1-hexyl-1- Heptylpyrrolidinium, 1-hexyl-1-octylpyrrolidinium, 1-hexyl-1-nonylpyrrolidinium, 1-hexyl Ru-1-decylpyrrolidinium, 1,1-dihexylpyrrolidinium, 1-hexyl-1-heptylpyrrolidinium, 1-hexyl-1-octylpyrrolidinium, 1-hexyl-1-nonylpyrrolidinium 1 - hexyl-1-decylpyrrolidinium, 1,1-diheptylpyrrolidinium, 1-heptyl-1-octylpyrrolidinium, 1-heptyl-1-nonylpyrrolidinium, 1-heptyl-1- decyl pyrrolidinium, 1,1 dioctyl pyrrolidinium, 1-octyl-1-nonyl pyrrolidinium, 1-octyl-1-decyl pyrrolidinium, 1, 1-di-nonyl pyrrolidinium, 1-nonyl - 1-decylpyrrolidinium, or 1,1-didecylpyrrolidinium, 1-hydroxymethyl-1-methylpyrrolidinium, 1-hydro Cimethyl-1-ethylpyrrolidinium, 1-hydroxymethyl-1-propylpyrrolidinium, 1-hydroxymethyl-1-butylpyrrolidinium, 1- (2-hydroxyethyl) -1-methylpyrrolidinium, -(2-hydroxyethyl) -1-ethylpyrrolidinium, 1- (2-hydroxyethyl) -1-propylpyrrolidinium, 1- (2-hydroxyethyl) -1-butylpyrrolidinium, 1- ( 3-hydroxypropyl) -1-methylpyrrolidinium, 1- (3-hydroxypropyl) -1-ethylpyrrolidinium, 1- (3-hydroxypropyl) -1-propylpyrrolidinium, 1- (3- Hydroxypropyl) -1-butylpyrrolidinium, 1- (4-hydroxybutyl) -1-methylpyrrolidinium, 1- (4-hydride) Xylbutyl) -1-ethylpyrrolidinium, 1- (4-hydroxybutyl) -1-propylpyrrolidinium, or 1- (4-hydroxybutyl) -1-butylpyrrolidinium, 1- (1-hydroxymethyl) ) -3-Methylimidazolium, 1- (1-hydroxymethyl) -3-ethylimidazolium, 1- (1-hydroxymethyl) -3-propylimidazolium, 1- (1-hydroxymethyl) -3-butyl Imidazolium, 1- (2-hydroxyethyl) -3-methylimidazolium, 1- (2-hydroxyethyl) -3-ethylimidazolium, 1- (2-hydroxyethyl) -3-propylimidazolium, 1- (2-hydroxyethyl) -3-butylimidazolium, 1- (3-hydroxypropyl) -3-methylimidazolium 1- (3-hydroxypropyl) -3-ethylimidazolium, 1- (3-hydroxypropyl) -3-propylimidazolium, 1- (3-hydroxypropyl) -3-butylimidazolium, 1- ( 4-hydroxybutyl) -3-methylimidazolium, 1- (4-hydroxybutyl) -3-ethylimidazolium, 1- (4-hydroxybutyl) -3-propylimidazolium, 1- (4-hydroxybutyl) -3-butylimidazolium, 1,3-bis (1-hydroxymethyl) imidazolium, 1,3-bis (2-hydroxyethyl) imidazolium, 1,3-bis (3-hydroxypropyl) imidazolium, 1 , 3-bis (4-hydroxybutyl) imidazolium, 1- (2-hydroxyethyl) -3- (1-hydroxy Til) imidazolium, 1- (2-hydroxyethyl) -3- (3-hydroxypropyl) imidazolium, 1- (2-hydroxyethyl) -3- (4-hydroxybutyl) imidazolium, 1- (3- Hydroxypropyl) -3- (1-hydroxymethyl) imidazolium, 1- (3-hydroxypropyl) -3- (2-hydroxyethyl) imidazolium, 1- (3-hydroxypropyl) -3- (4-hydroxy) Butyl) imidazolium, 1- (4-hydroxybutyl) -3- (1-hydroxymethyl) imidazolium, 1- (4-hydroxybutyl) -3- (2-hydroxyethyl) imidazolium, or 1- (4 -Hydroxybutyl) -3- (3-hydroxypropyl) imidazolium.
JP2008532621A 2005-09-30 2006-09-05 Electrochemical deposition of selenium in ionic liquids Pending JP2009510261A (en)

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DE102005046908A DE102005046908A1 (en) 2005-09-30 2005-09-30 Electrochemical deposition of gray selenium on substrate e.g. non-metal, metalloid, metal, alloy or conductive and metallized ceramic or plastics for use as photosemiconductor in photovoltaics or electronics is carried out from ionic liquid
PCT/EP2006/008631 WO2007039035A1 (en) 2005-09-30 2006-09-05 Electrochemical deposition of selenium in ionic liquids

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