JP2009507059A5 - - Google Patents
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- Publication number
- JP2009507059A5 JP2009507059A5 JP2008529589A JP2008529589A JP2009507059A5 JP 2009507059 A5 JP2009507059 A5 JP 2009507059A5 JP 2008529589 A JP2008529589 A JP 2008529589A JP 2008529589 A JP2008529589 A JP 2008529589A JP 2009507059 A5 JP2009507059 A5 JP 2009507059A5
- Authority
- JP
- Japan
- Prior art keywords
- reactor
- zone
- stream
- phosgene
- process according
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 claims 26
- YGYAWVDWMABLBF-UHFFFAOYSA-N Phosgene Chemical compound ClC(Cl)=O YGYAWVDWMABLBF-UHFFFAOYSA-N 0.000 claims 9
- 150000001412 amines Chemical class 0.000 claims 6
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims 3
- 238000006243 chemical reaction Methods 0.000 claims 3
- 239000007789 gas Substances 0.000 claims 3
- 239000012948 isocyanate Substances 0.000 claims 3
- 150000002513 isocyanates Chemical class 0.000 claims 3
- RFFLAFLAYFXFSW-UHFFFAOYSA-N 1,2-dichlorobenzene Chemical compound ClC1=CC=CC=C1Cl RFFLAFLAYFXFSW-UHFFFAOYSA-N 0.000 claims 2
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims 2
- 125000003277 amino group Chemical group 0.000 claims 2
- MVPPADPHJFYWMZ-UHFFFAOYSA-N chlorobenzene Chemical compound ClC1=CC=CC=C1 MVPPADPHJFYWMZ-UHFFFAOYSA-N 0.000 claims 2
- NNBZCPXTIHJBJL-UHFFFAOYSA-N decalin Chemical compound C1CCCC2CCCCC21 NNBZCPXTIHJBJL-UHFFFAOYSA-N 0.000 claims 2
- 239000011541 reaction mixture Substances 0.000 claims 2
- 239000007858 starting material Substances 0.000 claims 2
- JTPNRXUCIXHOKM-UHFFFAOYSA-N 1-chloronaphthalene Chemical compound C1=CC=C2C(Cl)=CC=CC2=C1 JTPNRXUCIXHOKM-UHFFFAOYSA-N 0.000 claims 1
- MKZPMOFOBNHBSL-UHFFFAOYSA-N 1-isocyanato-1-methylcyclohexane Chemical compound O=C=NC1(C)CCCCC1 MKZPMOFOBNHBSL-UHFFFAOYSA-N 0.000 claims 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims 1
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 claims 1
- 229910052786 argon Inorganic materials 0.000 claims 1
- KCXMKQUNVWSEMD-UHFFFAOYSA-N benzyl chloride Chemical compound ClCC1=CC=CC=C1 KCXMKQUNVWSEMD-UHFFFAOYSA-N 0.000 claims 1
- 229910002092 carbon dioxide Inorganic materials 0.000 claims 1
- 239000001569 carbon dioxide Substances 0.000 claims 1
- 229910002091 carbon monoxide Inorganic materials 0.000 claims 1
- JXCHMDATRWUOAP-UHFFFAOYSA-N diisocyanatomethylbenzene Chemical compound O=C=NC(N=C=O)C1=CC=CC=C1 JXCHMDATRWUOAP-UHFFFAOYSA-N 0.000 claims 1
- 239000001307 helium Substances 0.000 claims 1
- 229910052734 helium Inorganic materials 0.000 claims 1
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 claims 1
- RRAMGCGOFNQTLD-UHFFFAOYSA-N hexamethylene diisocyanate Chemical compound O=C=NCCCCCCN=C=O RRAMGCGOFNQTLD-UHFFFAOYSA-N 0.000 claims 1
- NIMLQBUJDJZYEJ-UHFFFAOYSA-N isophorone diisocyanate Chemical compound CC1(C)CC(N=C=O)CC(C)(CN=C=O)C1 NIMLQBUJDJZYEJ-UHFFFAOYSA-N 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 239000000203 mixture Substances 0.000 claims 1
- 229910052757 nitrogen Inorganic materials 0.000 claims 1
- 239000008096 xylene Substances 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102005042392.2 | 2005-09-06 | ||
| DE102005042392A DE102005042392A1 (de) | 2005-09-06 | 2005-09-06 | Verfahren zur Herstellung von Isocyanaten |
| PCT/EP2006/065593 WO2007028715A1 (de) | 2005-09-06 | 2006-08-23 | Verfahren zur herstellung von isocyanaten |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2009507059A JP2009507059A (ja) | 2009-02-19 |
| JP2009507059A5 true JP2009507059A5 (enExample) | 2012-10-04 |
| JP5264489B2 JP5264489B2 (ja) | 2013-08-14 |
Family
ID=37459369
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2008529589A Active JP5264489B2 (ja) | 2005-09-06 | 2006-08-23 | イソシアネートの製造方法 |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US8258337B2 (enExample) |
| EP (1) | EP1924552B1 (enExample) |
| JP (1) | JP5264489B2 (enExample) |
| KR (1) | KR101339601B1 (enExample) |
| CN (1) | CN101258127B (enExample) |
| DE (1) | DE102005042392A1 (enExample) |
| HU (1) | HUE042073T2 (enExample) |
| SG (1) | SG166091A1 (enExample) |
| WO (1) | WO2007028715A1 (enExample) |
Families Citing this family (36)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2049675A1 (de) | 2006-08-01 | 2009-04-22 | Basf Se | Verfahren zur herstellung von pentamethylen-1,5-diisocyanat |
| CN101583594B (zh) * | 2006-11-07 | 2013-06-19 | 巴斯夫欧洲公司 | 生产异氰酸酯的方法 |
| DE102006058633A1 (de) | 2006-12-13 | 2008-06-19 | Bayer Materialscience Ag | Verfahren zur Herstellung von Isocyanaten in der Gasphase |
| WO2009027234A1 (de) * | 2007-08-30 | 2009-03-05 | Basf Se | Verfahren zur herstellung von isocyanaten |
| US8558026B2 (en) | 2007-08-30 | 2013-10-15 | Basf Se | Method for producing isocyanates |
| DE102007056511A1 (de) | 2007-11-22 | 2009-05-28 | Bayer Materialscience Ag | Verfahren zur Herstellung aromatischer Diisocyanate in der Gasphase |
| CN102317254B (zh) * | 2008-07-23 | 2014-11-19 | 巴斯夫欧洲公司 | 制备异氰酸酯的方法 |
| KR20110084922A (ko) | 2008-10-15 | 2011-07-26 | 바스프 에스이 | 이소시아네이트의 제조 방법 |
| US8916725B2 (en) | 2008-11-07 | 2014-12-23 | Basf Se | Process for preparing isocyanates |
| CN102239143B (zh) | 2008-12-03 | 2014-02-12 | 巴斯夫欧洲公司 | 制备异氰酸酯的方法 |
| DE102008061686A1 (de) | 2008-12-11 | 2010-06-17 | Bayer Materialscience Ag | Verfahren zur Herstellung von Isocyanaten in der Gasphase |
| DE102008063991A1 (de) | 2008-12-19 | 2010-06-24 | Bayer Materialscience Ag | Verfahren zur Herstellung von Isocyanaten in der Gasphase |
| KR20110135937A (ko) | 2009-03-06 | 2011-12-20 | 바스프 에스이 | 이소시아네이트를 제조하기 위한 방법 및 장치 |
| WO2010115908A2 (de) | 2009-04-08 | 2010-10-14 | Basf Se | Verfahren zur herstellung von isocyanaten |
| DE102009032414A1 (de) | 2009-07-09 | 2011-01-13 | Bayer Materialscience Ag | Verfahren zur Herstellung von Isocyanaten in der Gasphase |
| DE102010019342A1 (de) | 2010-05-05 | 2011-11-10 | Bayer Materialscience Ag | Verfahren zur Herstellung von Isocyanaten in der Gasphase |
| US9321720B2 (en) * | 2010-10-14 | 2016-04-26 | Basf Se | Process for preparing isocyanates |
| WO2012049158A1 (de) | 2010-10-14 | 2012-04-19 | Basf Se | Verfahren zur herstellung von isocyanaten |
| US8816126B2 (en) | 2011-09-02 | 2014-08-26 | Basf Se | Process for preparing isocyanates |
| CN110511164A (zh) | 2011-09-02 | 2019-11-29 | 巴斯夫欧洲公司 | 制备异氰酸酯的方法 |
| US9932299B2 (en) * | 2013-02-08 | 2018-04-03 | Covestro Deutschland Ag | Process for separating an isocyanate prepared by phosgenation of a primary amine in the gas phase from the gaseous crude product of the phosgenation |
| JP6621759B2 (ja) | 2014-03-27 | 2019-12-18 | コベストロ、ドイチュラント、アクチエンゲゼルシャフトＣｏｖｅｓｔｒｏ Ｄｅｕｔｓｃｈｌａｎｄ Ａｇ | 気相ホスゲン化プラントの運転方法 |
| WO2015144681A1 (de) | 2014-03-27 | 2015-10-01 | Bayer Material Science Ag | Verfahren zum betreiben einer gasphasenphosgenierungsanlage |
| CN106715384B (zh) * | 2014-09-19 | 2022-07-08 | 科思创德国股份有限公司 | 在气相中制备1,5-戊二异氰酸酯的方法 |
| KR102540646B1 (ko) | 2015-03-16 | 2023-06-08 | 코베스트로 도이칠란트 아게 | 1,5-펜타메틸렌 디이소시아네이트를 기재로 하는 폴리이소시아네이트 조성물 |
| JP7486914B2 (ja) | 2015-04-21 | 2024-05-20 | コベストロ、ドイチュラント、アクチエンゲゼルシャフト | １，５－ジイソシアナトペンタンを基礎とするポリイソシアネート混合物 |
| WO2016198404A1 (de) | 2015-06-12 | 2016-12-15 | Covestro Deutschland Ag | Verfahren zur herstellung von diisocyanaten in der gasphase |
| CN108137782B (zh) * | 2015-10-16 | 2021-01-05 | 亨茨曼国际有限公司 | 控制制造异氰酸酯的工艺的方法 |
| WO2017093215A1 (de) | 2015-12-03 | 2017-06-08 | Covestro Deutschland Ag | Verfahren zur herstellung von isocyanaten |
| WO2018184980A1 (de) | 2017-04-03 | 2018-10-11 | Covestro Deutschland Ag | Reinigungsvorrichtung für gasströme aus der isocyanatherstellung |
| CN110105248B (zh) * | 2019-05-31 | 2021-07-20 | 上海应用技术大学 | 一种甲苯二异氰酸酯的制备方法 |
| US20240059648A1 (en) | 2020-11-23 | 2024-02-22 | Base Se | Process for producing isocyanates |
| JP7602926B2 (ja) * | 2021-02-09 | 2024-12-19 | 旭化成株式会社 | オキシメチレン重合体の製造方法 |
| EP4442859A1 (de) | 2023-04-06 | 2024-10-09 | Covestro Deutschland AG | Nachhaltige herstellung von hexamethylendiisocyanat für die produktion von polyurethan |
| EP4480944A1 (de) | 2023-06-20 | 2024-12-25 | Covestro Deutschland AG | Verfahren zur herstellung von aliphatischen diisocyanaten in der gasphase |
| EP4545579A1 (de) | 2023-10-24 | 2025-04-30 | Covestro Deutschland AG | Verfahren zur herstellung eines polyisocyanats auf basis von 1,5-pentamethylendiisocyanat |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10032269A1 (de) | 2000-07-03 | 2002-01-31 | Basf Ag | Verfahren und Vorrichtung zur Verringerung von Nebenprodukten bei der Vermischung von Eduktströmen |
| DE10133728A1 (de) | 2001-07-11 | 2003-01-23 | Bayer Ag | Verfahren zur Herstellung von (cyclo)aliphatischen Diisocyanaten |
| DE10133729A1 (de) * | 2001-07-11 | 2003-01-23 | Bayer Ag | Verfahren zur Herstellung von (cyclo)aliphatischen Diisocyanaten |
| DE10158160A1 (de) * | 2001-11-28 | 2003-06-12 | Basf Ag | Herstellung von Isocyanaten in der Gasphase |
| DE10222968A1 (de) * | 2002-05-23 | 2003-12-04 | Basf Ag | Verfahren zur Herstellung von Isocyanaten |
| DE10307141A1 (de) * | 2003-02-20 | 2004-09-02 | Bayer Ag | Verfahren zur Herstellung von (Poly)isocyanaten in der Gasphase |
| DE10349504A1 (de) * | 2003-10-23 | 2005-05-25 | Bayer Technology Services Gmbh | Verfahren zur Herstellung von Isocyanaten in der Gasphase |
| DE10359627A1 (de) * | 2003-12-18 | 2005-07-21 | Bayer Materialscience Ag | Verfahren zur Herstellung von Diisocyanaten |
| US7961724B2 (en) * | 2005-03-18 | 2011-06-14 | Qualcomm Incorporated | Dynamic media access control (MAC) address assignment |
-
2005
- 2005-09-06 DE DE102005042392A patent/DE102005042392A1/de not_active Withdrawn
-
2006
- 2006-08-23 SG SG201006422-8A patent/SG166091A1/en unknown
- 2006-08-23 CN CN2006800326067A patent/CN101258127B/zh active Active
- 2006-08-23 US US12/065,964 patent/US8258337B2/en active Active
- 2006-08-23 WO PCT/EP2006/065593 patent/WO2007028715A1/de not_active Ceased
- 2006-08-23 JP JP2008529589A patent/JP5264489B2/ja active Active
- 2006-08-23 HU HUE06792972A patent/HUE042073T2/hu unknown
- 2006-08-23 EP EP06792972.9A patent/EP1924552B1/de active Active
- 2006-08-23 KR KR1020087008183A patent/KR101339601B1/ko active Active
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