JP2009298647A5 - - Google Patents

Download PDF

Info

Publication number
JP2009298647A5
JP2009298647A5 JP2008154957A JP2008154957A JP2009298647A5 JP 2009298647 A5 JP2009298647 A5 JP 2009298647A5 JP 2008154957 A JP2008154957 A JP 2008154957A JP 2008154957 A JP2008154957 A JP 2008154957A JP 2009298647 A5 JP2009298647 A5 JP 2009298647A5
Authority
JP
Japan
Prior art keywords
nickel
nickel oxide
aqueous solution
neutralization
treatment
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP2008154957A
Other languages
Japanese (ja)
Other versions
JP2009298647A (en
JP5032400B2 (en
Filing date
Publication date
Application filed filed Critical
Priority to JP2008154957A priority Critical patent/JP5032400B2/en
Priority claimed from JP2008154957A external-priority patent/JP5032400B2/en
Publication of JP2009298647A publication Critical patent/JP2009298647A/en
Publication of JP2009298647A5 publication Critical patent/JP2009298647A5/ja
Application granted granted Critical
Publication of JP5032400B2 publication Critical patent/JP5032400B2/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Description

すなわち、得られたニッケル酸化物では、ニッケル純度が4Nであり、また、カリウム含有量が100ppm以下である。
That is, the obtained nickel oxide has a nickel purity of 4N and a potassium content of 100 ppm or less.

Claims (6)

ニッケル純度が4N以上であり且つナトリウム含有量が100ppm以下であることを特徴とするニッケル酸化物。   A nickel oxide having a nickel purity of 4N or more and a sodium content of 100 ppm or less. ニッケル純度が4N以上であり且つナトリウム含有量が100ppm以下である、ニッケル酸化物を、製造する方法であって、
ニッケルイオンの酸水溶液を水酸化ナトリウム水溶液又は水酸化カリウム水溶液によって中和処理して、ニッケル純度が3N以上であるニッケル化合物を析出させる、中和工程と、
上記ニッケル化合物を加熱処理してニッケル酸化物を生成し、該ニッケル酸化物を水洗処理する、加熱水洗工程と、を有することを特徴とするニッケル酸化物の製造方法。
A method for producing a nickel oxide having a nickel purity of 4N or more and a sodium content of 100 ppm or less,
A neutralization step of neutralizing a nickel ion acid aqueous solution with a sodium hydroxide aqueous solution or a potassium hydroxide aqueous solution to precipitate a nickel compound having a nickel purity of 3N or more;
A heating water washing step of heat-treating the nickel compound to produce nickel oxide and washing the nickel oxide with water.
中和工程の前に、ニッケルイオンの酸水溶液をイオン交換クロマトグラフィーによって処理して、ニッケルイオンの酸水溶液から重金属不純物を除去する、クロマトグラフィー工程、を有する、請求項2記載のニッケル酸化物の製造方法。   The nickel oxide according to claim 2, further comprising a chromatography step of treating an acid aqueous solution of nickel ions by ion exchange chromatography to remove heavy metal impurities from the acid aqueous solution of nickel ions before the neutralization step. Production method. 加熱水洗工程において、加熱処理を、付着水の無い状態のニッケル酸化物の重量減少率が17.0〜23.0重量%となるよう、行う、請求項2又は3に記載のニッケル酸化物の製造方法。 4. The nickel oxide according to claim 2, wherein the heat treatment is performed such that the weight reduction rate of the nickel oxide without adhering water is 17.0 to 23.0 wt% in the heated water washing step. Production method. 中和工程において、pH8.0〜13.0の条件下で、中和処理を行う、請求項2乃至4のいずれか一項に記載のニッケル酸化物の製造方法。 The manufacturing method of the nickel oxide as described in any one of Claims 2 thru | or 4 which performs a neutralization process on the conditions of pH 8.0-13.0 in a neutralization process. 中和工程において、中和処理後に、得られたニッケル化合物を脱水処理又は水洗処理する、請求項2乃至5のいずれか一項に記載のニッケル酸化物の製造方法。 The method for producing nickel oxide according to any one of claims 2 to 5, wherein, in the neutralization step, the obtained nickel compound is subjected to a dehydration treatment or a water washing treatment after the neutralization treatment.
JP2008154957A 2008-06-13 2008-06-13 Nickel oxide Expired - Fee Related JP5032400B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2008154957A JP5032400B2 (en) 2008-06-13 2008-06-13 Nickel oxide

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2008154957A JP5032400B2 (en) 2008-06-13 2008-06-13 Nickel oxide

Related Child Applications (1)

Application Number Title Priority Date Filing Date
JP2011181801A Division JP5373867B2 (en) 2011-08-23 2011-08-23 Method for producing nickel oxide

Publications (3)

Publication Number Publication Date
JP2009298647A JP2009298647A (en) 2009-12-24
JP2009298647A5 true JP2009298647A5 (en) 2010-03-25
JP5032400B2 JP5032400B2 (en) 2012-09-26

Family

ID=41545951

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2008154957A Expired - Fee Related JP5032400B2 (en) 2008-06-13 2008-06-13 Nickel oxide

Country Status (1)

Country Link
JP (1) JP5032400B2 (en)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5168070B2 (en) * 2008-10-08 2013-03-21 住友金属鉱山株式会社 Nickel oxide powder and method for producing the same
JP5862919B2 (en) * 2011-02-10 2016-02-16 住友金属鉱山株式会社 Nickel oxide fine powder and method for producing the same
CN104843806B (en) * 2011-08-06 2018-06-22 住友金属矿山株式会社 NiO fine powder end
JP5733101B2 (en) * 2011-08-11 2015-06-10 住友金属鉱山株式会社 Method for producing nickel oxide powder
JP5834612B2 (en) * 2011-08-13 2015-12-24 住友金属鉱山株式会社 Nickel oxide powder and method for producing the same
JP5790292B2 (en) * 2011-08-13 2015-10-07 住友金属鉱山株式会社 Method for producing nickel oxide powder
JP5867015B2 (en) * 2011-11-24 2016-02-24 住友金属鉱山株式会社 Manufacturing method of high purity nickel sulfate

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0710544A (en) * 1993-06-23 1995-01-13 Tdk Corp Production of nickel oxide powder
JP3676926B2 (en) * 1997-06-04 2005-07-27 株式会社日鉱マテリアルズ Method for recovering and regenerating cobalt, nickel, manganese and lithium from battery cathode waste material and battery cathode material
JPH1179752A (en) * 1997-09-01 1999-03-23 Toda Kogyo Corp Nickel oxide particles and their production

Similar Documents

Publication Publication Date Title
JP2009298647A5 (en)
JP2013047171A5 (en) Method for producing graphite oxide, method for producing graphene oxide, and method for producing graphene
JP2015517595A5 (en)
WO2011035187A3 (en) Selective-cation-removal purification of aluminum source
JP2016053076A5 (en)
CN105568269A (en) Preparation method of cyanide-free gold plating reagent sodium gold sulfite
MX2014007592A (en) Precipitated-silica production method.
JP2014212319A5 (en)
UA113204C2 (en) SELECTIVE EXTRACTION OF POTASSIUM CHLORIDE FROM THE OUTSIDE SHENITA SOLUTION WITH THE USE OF TARTARIC ACID AS A SAFETY SOFT EXTRADENTS
JP2016518821A5 (en)
JP2011518232A5 (en)
RU2015134186A (en) METHOD FOR PRODUCING GALVANIZED STEEL SHEET
WO2013060719A3 (en) Process for preparing a mesopores-containing catalyst, catalyst thus obtained and use thereof in a hydroconversion process.
JP2009511413A5 (en)
CN104030510B (en) A kind of method of acid and heavy metal recovery in gold smelting acid waste water
WO2009080597A3 (en) Process for preparing organically modified layered double hydroxide
RU2015146656A (en) METHOD FOR PROCESSING PURE VANADIUM-TITANO-MAGNETITE ORES WITH APPLICATION OF WET PROCESS
JP2003082003A5 (en)
RU2009145819A (en) METHOD FOR PRODUCING BIOCIDE
JP2016536125A5 (en)
JP2013078725A5 (en)
JP2011042528A5 (en)
MX2018000797A (en) Scale conditioning process for advanced high strength carbon steel alloys.
MD3973B1 (en) Process for obtaining a sorbent on base of diatomite for purification from fluorine ions
CN104588609A (en) Novel precious metal snowflake pattern manufacturing method