JP2009084247A - Combustion composition and method for producing the same - Google Patents
Combustion composition and method for producing the same Download PDFInfo
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Abstract
Description
本発明は燃焼組成物とその製造法に関するものである。その代表的なものは線香であって、これは日用品として幅広く使用されているものである。
The present invention relates to a combustion composition and a method for producing the same. A typical example is an incense stick, which is widely used as a daily necessities.
周知の通り、燃焼組成物は線香のほかに各種お香例えば円錐香（又はコーン）、板状香、円柱香、渦巻き香などが多く知られている。これらの燃焼後の灰分は大きく2種類に分けられ、一方は灰分が燃焼段階でその都度自然落下するか、他方は形状を残したままであるかのどちらかである。一般的には自然落下する燃焼組成物が大半を占めている。しかも灰分量が多く、固定された香炉外に飛び散ったりして汚れが目立っていることが挙げられるのである。また灰分の非常に少ない線香も市販されてはいるが、着色が困難で基材色がやはり黒いという欠点があり、また火の粉が散ったりして市場性が乏しいのが現状である。
しかしながら灰分の非常に少ない燃焼組成物就中線香は脚光を浴びており、本発明者らは着色が容易に出来る燃焼組成物を完成するための研究を続けてきた。
As is well known, various incenses such as conical incense (or cone), plate-like incense, cylindrical incense, and spiral incense are well known in addition to incense. The ash content after combustion is roughly divided into two types, one of which is either the natural fall of ash every time in the combustion stage or the other of which remains in shape. In general, the combustion composition that falls naturally occupies the majority. Moreover, the amount of ash is large, and the dirt is conspicuous due to scattering outside the fixed incense burner. Incense sticks with very little ash are also commercially available, but they have the disadvantages that they are difficult to color and the base color is black, and the market is poor due to the scattering of sparks.
However, burning compositions, especially those with very little ash, are in the limelight, and the inventors have continued research to complete burning compositions that can be easily colored.
本発明における解決しようとする課題は、従来の燃焼組成物について、燃焼中の外観はほとんど灰が目立つことなく、落灰による周囲の汚れなど全く影響を与えないものであって、しかも煙量も極力少なく燃焼組成物の外観上の着色を容易に際立たせることが本発明の解決しょうとする課題である。 The problem to be solved by the present invention is that the appearance during combustion hardly causes ash to stand out, does not affect the surrounding dirt due to falling ash at all, and the amount of smoke is also the problem to be solved in the present invention. The problem to be solved by the present invention is to make the coloring on the appearance of the combustion composition as easily as possible.
そして本発明者の研究により燃焼組成物として、特に粒状活性炭、木粉、水溶性糊料、無機フィラーを有効成分として使用することにより、上記課題が解決出来ることが見出された。 As a result of the inventor's research, it has been found that the above problems can be solved by using granular activated carbon, wood powder, water-soluble paste, and inorganic filler as active ingredients.
本発明は全く新しいタイプの燃焼組成物とその製造法であり、灰分が極端に少なく煙量も少ない事から汚れを防止すると共に、周囲の環境を清浄化できるものである。従って本発明は日常生活において賞用されるものであり、この発明の効果は絶大なものである。 The present invention is a completely new type of combustion composition and a method for producing the same, and is capable of preventing soiling and cleaning the surrounding environment because it has an extremely small amount of ash and a small amount of smoke. Therefore, the present invention is used in daily life and the effect of the present invention is enormous.
本発明は上記各種有効成分を主成分とする燃焼組成物およびこの組成物を水と混練した後成型乾燥してなる燃焼組成物の製造法に係るものである。
本発明においては、上記各種有効成分は下記の割合で使用するのが特に好ましい。すなわち、粒状活性炭50〜70重量％、木粉10〜40重量％、水溶性糊料５〜15重量％、無機フィラー1〜3重量％、その他よりなる燃焼組成物とその製造法である。
そして更に本発明においては、上記各種有効成分としては、特に下記に示す特定の物質を有する成分が夫々使用されることが極めて望ましい。これら各種有効成分について下記に詳しく説明する。
本発明における粒状活性炭は、粒径が0.18〜0.05ｍｍで比表面積が120〜170ｍ２/gであることが極めて好ましい条件であり、また木粉でも常温時の気乾比重が0.4〜0.6で、着火温度が240〜270℃、灰分が0.1〜0.2重量％の条件を満たした木粉が極めて好ましいものである。
The present invention relates to a combustion composition containing the above-mentioned various active ingredients as a main component and a method for producing a combustion composition obtained by kneading this composition with water and then drying it.
In the present invention, the various active ingredients are particularly preferably used in the following proportions. That is, a combustion composition comprising 50 to 70% by weight of granular activated carbon, 10 to 40% by weight of wood flour, 5 to 15% by weight of a water-soluble paste, 1 to 3% by weight of an inorganic filler, and the like, and a production method thereof.
Further, in the present invention, as the various active ingredients, it is extremely desirable to use ingredients having specific substances shown below. These various active ingredients are described in detail below.
The granular activated carbon in the present invention is a very preferable condition that the particle size is 0.18 to 0.05 mm and the specific surface area is 120 to 170 m 2 / g, and even wood powder has an air-drying specific gravity at room temperature of 0.4 to 0.6, Wood flour that satisfies the conditions of an ignition temperature of 240 to 270 ° C. and an ash content of 0.1 to 0.2% by weight is extremely preferable.
本発明にいう粒状活性炭とは、代表的なものはヤシガラ活性炭である。焼成炭化されたヤシガラ炭を破砕、整粒した粒状物または焼成炭化されたヤシガラ炭を、賦活が1〜10％処理後、破砕、整粒した粒状物である。
先ず粒径サイズは0.18〜0.05mm好ましくは0.15〜0.075ｍｍであり、しかも比表面積は120〜170ｍ２/g好ましくは140〜150ｍ２/gである。この範囲外では灰分も多く、また外観の色彩も黒くなる傾向がある。この粒状活性炭の使用量は50〜70重量％好ましくは55〜60重量％がよい。
粒径サイズが0.18ｍｍを超えると燃焼組成物を混練できないばかりか外観上の粒子が粗く製品として好ましくないものとなってしまう傾向があり、また粒径が0.05ｍｍより小さいと着色が出来難く単一黒色しか出ない傾向がある。
本発明にいう粒状活性炭の使用量が50重量％未満では灰分が多くなり、通常のありふれた燃焼組成物になってしまう傾向が強く、また逆に70重量％以上では灰分は少ないが火種が長く、飛び火が発生し危険でもあり着色性が悪くなり用途にそぐわなくなる場合がある。
The typical granular activated carbon referred to in the present invention is coconut shell activated carbon. A granulated product obtained by crushing and sizing calcined coconut shell charcoal, or a granulated product obtained by crushing and sizing calcined coconut husk charcoal after treatment of 1 to 10% of activation.
First, the particle size is 0.18 to 0.05 mm, preferably 0.15 to 0.075 mm, and the specific surface area is 120 to 170 m 2 / g, preferably 140 to 150 m 2 / g. Outside this range, there is a lot of ash and the color of the appearance tends to be black. The amount of the granular activated carbon used is 50 to 70% by weight, preferably 55 to 60% by weight.
If the particle size exceeds 0.18 mm, not only the combustion composition cannot be kneaded, but the appearance particles tend to be coarse and unpreferable as a product, and if the particle size is less than 0.05 mm, coloring is difficult. There tends to be only one black color.
When the amount of granular activated carbon used in the present invention is less than 50% by weight, the ash content increases, and there is a strong tendency to become a normal combustion composition. , Flying fire may occur and it may be dangerous, and coloring may be deteriorated, making it unsuitable for use.
本発明における木粉とは、多くの木材質、例えば針葉樹、広葉樹、常緑樹または外洋材など幅広く使用されるが、木粉の常温時気乾比重が0.4〜0.6好ましくは0.5〜0.55であることが重要である。気乾比重ruは以下の式で算出する。
ru=Gu / Vu（uは含水率を示し、一般的にはu=15%のときの値が用いられる）
Ｇu=気乾材の重量。Ｖu=気乾材の容積である。
そしてその木粉の着火温度が240〜270℃好ましくは250℃近辺、灰分は0.1〜0.2重量％である。この木粉に該当するのは針葉樹マツ科であるツガ属のツガ（トガとも云う）やコメツガ、カナダツガ、米ツガなどがあるが、他の樹木においてもこの条件範囲にあれば良いのは当然である。木粉は10〜40重量％好ましくは15〜30重量％がよい。10重量％未満では組成物として火種が長く、また飛び火が発生する。40重量％以上では燃焼後の灰分が多く本発明に適さないのである。また木粉の気乾比重が0.4〜0.6以外、着火温度が240〜270℃以外、灰分量0.2以上は結果として灰分が多くなることが判明し、本発明においては好ましくないものである。
The wood flour in the present invention is widely used as many wood materials such as conifers, hardwoods, evergreen trees, or open-sea wood, but the wood powder has an air-drying specific gravity at room temperature of 0.4 to 0.6, preferably 0.5 to 0.55. is important. The air-dry specific gravity ru is calculated by the following formula.
ru = Gu / Vu (u indicates water content, generally the value when u = 15% is used)
Gu = weight of air drying material. Vu = volume of air-drying material.
The ignition temperature of the wood powder is 240 to 270 ° C, preferably around 250 ° C, and the ash content is 0.1 to 0.2% by weight. This wood powder includes the coniferous pine family Tsuga genus (also called Toga), rice moth, Canadian eel, and rice tsubo, but it is natural that other trees should be within this range. is there. The wood flour is 10 to 40% by weight, preferably 15 to 30% by weight. If it is less than 10% by weight, the fire type is long as the composition and a spark is generated. If it is 40% by weight or more, the ash content after combustion is large and it is not suitable for the present invention. Further, when the air-drying specific gravity of the wood powder is other than 0.4 to 0.6, the ignition temperature is other than 240 to 270 ° C., and the ash content is 0.2 or more, it is found that the ash content increases as a result.
本発明における水溶性糊料とは、混練した後、任意の形に成型して乾燥し、安定な形を充分保持せしめるために必要な粘結剤であり、また粘着剤も含まれる。代表的なものを示すと、カルボキシメチルセルロースナトリウム塩やグアーガム、キサンタンガム等である。勿論従来公知の各種のものも適宣使用されるのは言うまでもない。使用量は5〜15重量％好ましくは7〜12重量％が最良である。 The water-soluble paste in the present invention is a binder necessary for kneading, molding into an arbitrary shape and drying, and sufficiently maintaining a stable shape, and also includes an adhesive. Typical examples are carboxymethylcellulose sodium salt, guar gum, xanthan gum and the like. Of course, it is needless to say that various conventionally known ones are also properly used. The amount used is 5 to 15% by weight, preferably 7 to 12% by weight.
本発明における無機フィラーとは、軽質で平均粒子径が10〜20μｍであり、燃焼による灰分を凝集させる目的と分散させる目的として使用されるものである。使用量は１〜3重量％で、その代表的なものは珪藻土や水酸化アルミニウムなどが挙げられる。勿論これら以外にも従来公知のものが適宣使用されるのは言うまでもない。 The inorganic filler in the present invention is light and has an average particle diameter of 10 to 20 μm, and is used for the purpose of agglomerating and dispersing ash content from combustion. The amount used is 1 to 3% by weight, and typical examples thereof include diatomaceous earth and aluminum hydroxide. Of course, it goes without saying that conventionally known ones may be appropriately used.
本発明におけるその他の成分としては香料又は香料化合物、着色料、消臭剤、防腐剤などが含まれ、それらは少なくとも一つ以上添加され、その添加量は合算して２〜10重量％である。
本発明にいう香料とは動・植物より抽出された天然香料、石油化学より合成された香料、天然香料や合成香料よりなる調合香料等である。香料化合物とはこれらの香料に付加された増粘剤、乳化剤、分散剤、有機・無機粉末、溶剤等を含む香料化合物を示す。これらの使用形態としては単独もしくは少なくともひとつ以上の形で用いられるのである。
Other components in the present invention include a fragrance or a fragrance compound, a colorant, a deodorant, a preservative, and the like, and at least one of them is added, and the addition amount is 2 to 10% by weight in total. .
The fragrances referred to in the present invention include natural fragrances extracted from animals and plants, fragrances synthesized from petrochemicals, blended fragrances composed of natural fragrances and synthetic fragrances, and the like. A fragrance compound refers to a fragrance compound containing a thickener, an emulsifier, a dispersant, an organic / inorganic powder, a solvent and the like added to these fragrances. These usage forms are used alone or in at least one form.
香料又は香料化合物を燃焼組成物に配合されて水と混練して得られた成型乾燥製品の場合と香料又は香料化合物を無添加での同成型乾燥製品に、後で賦香させて用いうる場合がある。この賦香させて用いうる場合には香りの好みに合わせたり、香りの濃度を自ら調製したりすることができるのである。
本発明にいう着色料とは塩基性・酸性・直接染料や有機または無機顔料などである。これら染・顔料は通常少なくともひとつ以上で単独または混合した形で用いられる。但し、白色無機顔料使用に当たっては、燃焼組成物の灰分を白くさせる目的と落灰性を高める目的の為に使用されるのである。
本発明にいう消臭剤とは、主に植物から抽出されたものであり、例えば大豆抽出消臭剤、緑茶抽出消臭剤、ヒノキ抽出消臭剤等がある。形態としては溶液状、粉末状、顆粒状として適宣用いられる。
本発明にいう防腐剤とは、食品添加物に規定されているものを使用するものとする。例えばソルビン酸やデハイドロ酢酸などである。
In the case of a molded dry product obtained by blending a fragrance or a fragrance compound in a combustion composition and kneading with water, and in the case where the fragrance or fragrance compound can be used after being perfumed to the same molded dry product without addition There is. When this fragrance can be used, it can be adjusted to the taste of the scent or the concentration of the scent can be adjusted by itself.
The colorants referred to in the present invention are basic, acidic, direct dyes, organic or inorganic pigments, and the like. These dyes / pigments are usually used alone or in a mixed form. However, when the white inorganic pigment is used, it is used for the purpose of making the ash content of the combustion composition white and for improving the ash fall off property.
The deodorant referred to in the present invention is mainly extracted from plants, such as soybean extract deodorant, green tea extract deodorant, hinoki extract deodorant and the like. As the form, it is suitably used as a solution, a powder, or a granule.
What is prescribed | regulated to the food additive shall be used with the antiseptic | preservative said to this invention. For example, sorbic acid or dehydroacetic acid.
本発明者らは多数の実験を行なって、本発明の優秀性を明らかにしたのであるが、さらに本発明の技術的内容を説明する為に多数の実験例より代表的な数例を選んで以下に実施例として示すことにする。従って本発明は単に実施例のみに限定されるべきではなく、本発明の趣旨と精神を逸脱せざる限り任意のその実施形態を変更して実施しうることは当然である。
[実施例１]
粒径0.12〜0.06ｍｍの粒状活性炭（二村化学工業製）56.0重量％、気乾比重（常温）0.5で平均200メッシュのカナダツガ粉29.0重量％、カルボキシメチルセルロース-Na 5.0重量％、グアーガム2.9重量％、無機フィラー（ラジオライトF600 昭和化学工業（株）製）1.3重量％、バラ調合香料2.0重量％、大豆抽出消臭剤2.0重量％を均一に混合し燃焼組成物を得る。これに食用赤色3号0.３重量％と白色顔料（二酸化チタン40重量％含有）1.5重量％を水に溶解分散させ燃焼組成物と共に混練する。充分に混練されたものを圧縮させて空気を抜き、これを押出し成型機にて線状に押出し、乾燥後必要な長さにカットした。ここに得られた線香は赤桃色のきれいなバラの香りを放ち、しかも灰分が極端に少なく美麗な製品であった。
[実施例２〜４]
粒径0.14〜0.08ｍｍの粒状活性炭（二村化学工業製）６５．０重量％、気乾比重（常温）0.5で平均150メッシュのツガ粉２０重量％、カルボキシメチルセルロース-Na 3.0重量％、キサンタンガム4.0重量％、無機フィラー（ラジオライトF600昭和化学工業（株）製）1.0重量％、緑茶カテキン３．０重量％、白色顔料（亜鉛華３０重量％含有）2.0重量％を均一に混合した後、これに下記の表１に記載の香料化合物および色素量の条件下（数値は全て重量％とする）で夫々水と混練、夫々の形状に成型乾燥させて製造した。燃焼中は夫々の香りを揮散し、灰の少ない環境に適したものであった。
The present inventors conducted a number of experiments to clarify the superiority of the present invention. In order to further explain the technical contents of the present invention, several representative examples were selected from a number of experimental examples. Examples will be shown below. Therefore, the present invention should not be limited only to the examples, and it is obvious that any of the embodiments can be modified without departing from the spirit and spirit of the present invention.
[Example 1]
Granular activated carbon with a particle size of 0.12 to 0.06 mm (made by Futamura Chemical Co., Ltd.) 56.0% by weight, air dry specific gravity (room temperature) 0.5 and average 200 mesh Canadian tsuga powder 29.0% by weight, carboxymethylcellulose-Na 5.0% by weight, guar gum 2.9% by weight, An inorganic filler (Radiolite F600, manufactured by Showa Chemical Industry Co., Ltd.) 1.3% by weight, rose blended fragrance 2.0% by weight, and soybean extract deodorant 2.0% by weight are uniformly mixed to obtain a combustion composition. To this, 0.3% by weight of Edible Red No. 3 and 1.5% by weight of white pigment (containing 40% by weight of titanium dioxide) are dissolved and dispersed in water and kneaded with the combustion composition. The fully kneaded product was compressed to release air, extruded into a linear shape by an extrusion molding machine, and cut to the required length after drying. The incense sticks obtained here gave off a beautiful red peach-colored rose scent and had a very low ash content and was a beautiful product.
[Examples 2 to 4]
Granular activated carbon with a particle size of 0.14-0.08 mm (made by Futamura Chemical Co., Ltd.) 65.0% by weight, air dry specific gravity (room temperature) 0.5, average 150 mesh hull powder 20% by weight, carboxymethylcellulose-Na 3.0% by weight, xanthan gum 4.0% by weight %, Inorganic filler (Radiolight F600 manufactured by Showa Chemical Industry Co., Ltd.) 1.0% by weight, green tea catechin 3.0% by weight, white pigment (containing 30% by weight of zinc white) 2.0% by weight, The fragrance compounds and pigment amounts shown in Table 1 below were prepared by kneading with water and molding and drying into respective shapes under the conditions of the amounts of the fragrance compounds and pigments (all numerical values are given by weight). During combustion, each fragrance was volatilized and it was suitable for an environment with little ash.
［表１］
実施例 香料化合物 色素 形状
２ ヒノキ粉末香料1.7 シルクスカーレット 0.3 木片
３ ピーチフレーバ粉末1.5 レッド有機顔料 0.5 棒
４ 森林浴香料含浸粉末1.8 ダイヤモンドグリーン 0.2 葉
[実施例5〜８]
実施例１と同様な方法で下記に示した木粉種類および木粉量の条件下で製造した。夫々の結果を表２中に示した。尚、実施例5および６は、本発明の木粉条件範囲外のものを使用して比較例とした。
[Table 1]
Examples Fragrance compounds Dye Shape 2 Cypress powder fragrance 1.7 Silk Scarlet 0.3 Wood chips 3 Peach flavor powder 1.5 Red organic pigment 0.5 Bar 4 Forest bath fragrance impregnated powder 1.8 Diamond green 0.2 Leaf
[Examples 5 to 8]
The same method as in Example 1 was used to produce the following types of wood flour and wood flour. The respective results are shown in Table 2. In addition, Examples 5 and 6 were used as comparative examples using those outside the wood powder condition range of the present invention.
［表２］
実施例 木粉種類 外観色彩 外観灰分状態
５ クス心材 ○ 多い
６ タブ心材 ○ やや多い
７ シオジ心材 ◎ ほぼ良好
８ バルサ材 ◎ 良好
[Table 2]
Examples Wood flour type Appearance color Appearance ash condition 5 Cushion heartwood ○ Many 6 Tab heartwood ○ Slightly much 7 Sojiji heartwood ◎ Almost good
8 Balsa wood ◎ Good
Claims (7)
その製造法。
The composition according to any one of claims 1 to 5, and the method for producing the composition, wherein the combustion composition is an incense composition.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2019081714A (en) * | 2017-10-30 | 2019-05-30 | 雄悟 池田 | Incense stick |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5058245A (en) * | 1973-09-27 | 1975-05-21 | ||
| JPS5916815A (en) * | 1982-07-20 | 1984-01-28 | Koukandou:Kk | Preparation of fragrant incenser stick |
| JPS5920215A (en) * | 1982-07-21 | 1984-02-01 | Koukandou:Kk | Preparation of fragrant incense stick |
| JPH0881347A (en) * | 1994-09-14 | 1996-03-26 | Yagiken:Kk | Smokeless odorless stick of incense |
| JP2002046107A (en) * | 2000-07-31 | 2002-02-12 | National Institute Of Advanced Industrial & Technology | Apparatus and method for forming wood |
| JP2003024425A (en) * | 2001-07-19 | 2003-01-28 | Dai Ichi Kogyo Seiyaku Co Ltd | Deodorant and low smell incense stick blended therewith |
| JP2005008544A (en) * | 2003-06-18 | 2005-01-13 | Kunjudo:Kk | Incense and method for producing the same |
| JP2007070242A (en) * | 2005-09-05 | 2007-03-22 | Kunjudo:Kk | Slimming-assisting fragrance |
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- 2007-10-02 JP JP2007258909A patent/JP5403384B2/en active Active
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5058245A (en) * | 1973-09-27 | 1975-05-21 | ||
| JPS5916815A (en) * | 1982-07-20 | 1984-01-28 | Koukandou:Kk | Preparation of fragrant incenser stick |
| JPS5920215A (en) * | 1982-07-21 | 1984-02-01 | Koukandou:Kk | Preparation of fragrant incense stick |
| JPH0881347A (en) * | 1994-09-14 | 1996-03-26 | Yagiken:Kk | Smokeless odorless stick of incense |
| JP2002046107A (en) * | 2000-07-31 | 2002-02-12 | National Institute Of Advanced Industrial & Technology | Apparatus and method for forming wood |
| JP2003024425A (en) * | 2001-07-19 | 2003-01-28 | Dai Ichi Kogyo Seiyaku Co Ltd | Deodorant and low smell incense stick blended therewith |
| JP2005008544A (en) * | 2003-06-18 | 2005-01-13 | Kunjudo:Kk | Incense and method for producing the same |
| JP2007070242A (en) * | 2005-09-05 | 2007-03-22 | Kunjudo:Kk | Slimming-assisting fragrance |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2019081714A (en) * | 2017-10-30 | 2019-05-30 | 雄悟 池田 | Incense stick |
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| JP5403384B2 (en) | 2014-01-29 |
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