JP2009069261A - Manufacturing device, method and dryer for coating film, and optical film - Google Patents

Manufacturing device, method and dryer for coating film, and optical film Download PDF

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JP2009069261A
JP2009069261A JP2007235195A JP2007235195A JP2009069261A JP 2009069261 A JP2009069261 A JP 2009069261A JP 2007235195 A JP2007235195 A JP 2007235195A JP 2007235195 A JP2007235195 A JP 2007235195A JP 2009069261 A JP2009069261 A JP 2009069261A
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coating film
drying
air supply
side plate
porous member
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Shinji Ota
真司 太田
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Toppan Inc
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Toppan Printing Co Ltd
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<P>PROBLEM TO BE SOLVED: To provide manufacturing device and method, a dryer, and an optical film for maintaining higher drying speed than at least natural drying while preventing the occurrence of even slight unevenness in drying and improving its productivity. <P>SOLUTION: In this manufacturing device, the distance for conveying the coating film from an application part of an applying device to a carrying-in port of a drying furnace is in a range of 0.2 m or more and 0.8 m or less, the inside of the drying furnace is divided into a plurality of drying passages, which are provided with an air intake and exhausting means each, and an air straightening member is provided in a space between the air intake means and a coating film conveying part. Furthermore, the distance between a top plate and a bottom plate is in a range of 10 mm or more and 100 mm or less, and the relationship between the height L1 of the top plate and the coating film and the height L2 of a bottom plate side clearance between the bottom plate and a basic member is L1≤L2. <P>COPYRIGHT: (C)2009,JPO&INPIT

Description

本発明は塗布膜の製造装置および製造方法に関するものである。特に、塗布液に有機溶剤を含み膜厚精度として誤差1%以下の膜厚ムラが製品上欠陥として認識される光学フィルム等の製造において使用される塗布膜の製造装置、製造方法および乾燥装置並びに光学フィルムに関するものである。   The present invention relates to a coating film manufacturing apparatus and manufacturing method. In particular, a coating film manufacturing apparatus, a manufacturing method, and a drying apparatus used in manufacturing an optical film or the like in which an organic solvent is included in the coating liquid and a film thickness unevenness with an error of 1% or less as a film thickness accuracy is recognized as a product defect. The present invention relates to an optical film.

近年ウェットコーティング技術を利用して製造される光学フィルム製品には、膜厚精度として誤差1%以下を要求されるような製品が増えてきている。そのような光学フィルムの製造では、一般的に塗布液の溶媒として有機溶剤を使用することが多いが、有機溶剤は水に比べると蒸発速度が速く、塗布後の乾燥過程において精密に乾燥しないと、風紋のようなムラを生じせしめることが知られている。   In recent years, optical film products manufactured using wet coating technology are increasingly required to have an error of 1% or less in terms of film thickness accuracy. In the production of such an optical film, an organic solvent is generally used as a solvent for a coating solution. However, an organic solvent has a higher evaporation rate than water and must be accurately dried in the drying process after coating. It is known to cause wind-like unevenness.

従来は塗布膜の乾燥効率を上げることを目的とする技術が多く、例えば特許文献1には走行する基材の両面に熱風を当てる方法が提案されているが、この方法では熱風を塗布膜面に当てるためムラが発生し、高い膜厚精度を要求される製品では用いることができない。   Conventionally, there are many techniques aimed at increasing the drying efficiency of a coating film. For example, Patent Document 1 proposes a method in which hot air is applied to both surfaces of a traveling substrate. In this method, hot air is applied to the surface of the coating film. As a result, the film is uneven and cannot be used in products that require high film thickness accuracy.

一方で、精密な塗膜の形成のために乾燥効率よりも精密に乾燥することに重きをおいた技術も提案されている。例えば、特許文献2では乾燥初期に膜面の乾燥風の風速を低くすることが提案されている。
また、特許文献3では乾燥時の雰囲気溶剤濃度を飽和状態にして極力乾燥速度を抑えることで結果的に精密な乾燥を行なうことも提案されている。
しかし、これらの方法は乾燥速度を遅くすることでムラのない面状を達成しようとするものであり、生産性が落ちるという欠点が存在する。
On the other hand, a technique that emphasizes drying more precisely than drying efficiency for the formation of a precise coating film has also been proposed. For example, Patent Document 2 proposes that the speed of the drying air on the film surface be lowered in the initial stage of drying.
Patent Document 3 also proposes that precise drying is performed as a result of suppressing the drying speed as much as possible by saturating the atmosphere solvent concentration during drying.
However, these methods are intended to achieve a uniform surface shape by slowing the drying speed, and have a drawback that productivity is lowered.

そこで、少しでも乾燥速度を上げるために蒸発した溶剤を効率的に除去しながら乾燥する方法として、特許文献4では走行する基材を囲み基材搬送部と溶剤除去部に分割して蒸発した溶剤を溶剤除去部の横風で常に除去しながら乾燥する方法が提案されている。この方法は基材搬送部を基材近傍に狭く区切っていることが特徴である。
また、特許文献5では横風で除去するのではなく、凝縮板に蒸発した溶剤を凝縮させて除去する方法が提案されている。
また、乾燥速度を上げるために乾燥風を整流化しながら横風を直接走行する基材に当てる方法も提案されている。しかし、例えば特許文献6に記載の方法では、特に乾燥初期の塗液粘度が1.5倍まで上昇するまでは風を当てないことを前提としており、乾燥速度を飛躍的に向上させることはできない。
これらの方法は、乾燥速度を大気中に放置したいわゆる自然乾燥の乾燥速度よりも上げることができず、飛躍的な生産性の向上ができないことが問題になる。
特開2002−59074号公報 特開2003−126768号公報 特開2002−320898号公報 特開2003−93954号公報 特表2002−515585号公報 特開2005−81256号公報
Therefore, as a method of drying while efficiently removing the evaporated solvent in order to increase the drying speed as much as possible, Patent Document 4 discloses a solvent that is evaporated by dividing a traveling base material into a base material transport section and a solvent removal section. There has been proposed a method of drying while always removing with a cross wind of the solvent removal section. This method is characterized in that the substrate transport section is narrowly divided in the vicinity of the substrate.
Further, Patent Document 5 proposes a method in which the solvent evaporated on the condensing plate is condensed and removed instead of being removed by cross wind.
In order to increase the drying speed, there has also been proposed a method in which a cross wind is directly applied to a base material while straightening the dry air. However, for example, the method described in Patent Document 6 is based on the premise that no wind is applied until the coating liquid viscosity in the initial stage of drying rises to 1.5 times, and the drying speed cannot be dramatically improved. .
These methods have a problem that the drying rate cannot be increased more than the drying rate of so-called natural drying in which the drying rate is left in the atmosphere, and the productivity cannot be dramatically improved.
JP 2002-59074 A JP 2003-126768 A JP 2002-320898 A JP 2003-93954 A JP 2002-515585 A JP 2005-81256 A

本発明における課題は、わずかな乾燥ムラの発生を抑制しながら少なくとも自然乾燥よりも乾燥速度を早く維持でき、面性と生産性を向上することができる塗布膜の製造装置、製造方法および乾燥装置乾燥装置並びに光学フィルムを提供することである。   An object of the present invention is to provide a coating film manufacturing apparatus, a manufacturing method, and a drying apparatus capable of maintaining a drying speed faster than at least natural drying while suppressing generation of slight drying unevenness, and improving surface properties and productivity. It is to provide a drying device as well as an optical film.

請求項1に記載の発明は、搬送中の帯状の基材に溶剤を含む塗布液を塗布し塗布膜を形成する塗布装置と、前記基材に形成した塗布膜を搬送しながら乾燥させる乾燥装置とを有する塗布膜の製造装置において、前記乾燥装置は、少なくとも、乾燥路と、給気口と、給気手段と、排気口と、排気手段と、整風部材とを備え、前記乾燥路は、前記塗布膜をその厚さ方向で挟んで対向する天板および底板と、前記塗布膜をその幅方向で挟んで対向し前記天板と前記底板の両側を接続する右側板および左側板とを含んで構成され、前記乾燥路の前記塗布膜の搬送方向の上流端に搬入口が設けられ、前記乾燥路の前記塗布膜の搬送方向の下流端に搬出口が設けられ、前記給気口は、前記乾燥路の右側板または左側板の一方に配置され、前記給気手段は、前記給気口を介して前記乾燥路内に空気を給気し、前記排気口は、前記左側板または右側板の他方に配置され、前記排気手段は、前記排気口を介して前記乾燥路内から空気を排気し、前記整風部材は、前記給気口に配置され、前記整風部材は、前記右側板または左側板に沿って延在し互いに対向する面状の第1の多孔部材と第2の多孔部材とを含んで構成され、前記第1の多孔部材は前記給気口に臨むように配置され、前記第2の多孔部材は前記塗布膜に臨むように配置され、前記第1の多孔部材は、孔径が2mm以上10mm以下、開口率が10%以上30%以下の面状の部材を1枚以上備えてなり、前記第2の多孔部材は、孔径が0.1mm以上2mm未満、開口率が40%以上99%以下の面状の部材を1枚以上備えてなることを特徴とする塗布膜の製造装置である。   The invention according to claim 1 is a coating apparatus that forms a coating film by applying a coating solution containing a solvent to a belt-shaped substrate being transported, and a drying apparatus that dries while transporting the coating film formed on the substrate. The drying apparatus includes at least a drying path, an air supply port, an air supply unit, an exhaust port, an exhaust unit, and an air conditioning member, and the drying path includes: A top plate and a bottom plate facing each other with the coating film sandwiched in its thickness direction; and a right side plate and a left side plate facing each other with the coating film sandwiched in the width direction and connecting both sides of the top plate and the bottom plate. A carry-in port is provided at the upstream end of the drying path in the conveyance direction of the coating film, a carry-out port is provided at the downstream end of the drying path in the conveyance direction of the coating film, Arranged on one of the right side plate or left side plate of the drying path, the air supply means, Air is supplied into the drying path through the air supply port, the exhaust port is disposed on the other of the left side plate or the right side plate, and the exhaust means is provided in the dry path through the exhaust port. The air conditioning member is disposed at the air supply port, and the air conditioning member extends along the right side plate or the left side plate and faces the first porous member and the second porous member. The first porous member is disposed so as to face the air supply port, the second porous member is disposed so as to face the coating film, and the first porous member is disposed. The member includes one or more planar members having a hole diameter of 2 mm to 10 mm and an opening ratio of 10% to 30%. The second porous member has a hole diameter of 0.1 mm to less than 2 mm, an opening It is characterized by comprising one or more planar members having a rate of 40% or more and 99% or less. An apparatus for producing a coating film.

請求項2に記載の発明は、前記塗布装置は前記基材に前記塗布液を塗布し前記塗布膜を形成する塗布部を有し、前記塗布部から該塗布部に臨む前記搬入口までの塗布膜搬送距離が0.2m以上0.8m以下の範囲であることを特徴とする請求項1に記載の塗布膜の製造装置である。   According to a second aspect of the present invention, the coating apparatus includes a coating unit that applies the coating solution to the base material to form the coating film, and coating from the coating unit to the carry-in port facing the coating unit. 2. The coating film manufacturing apparatus according to claim 1, wherein the film transport distance is in a range of 0.2 m to 0.8 m.

請求項3に記載の発明は、前記天板が前記基材の塗布膜を形成した側に位置し、前記底板が前記基材の塗布膜を形成した側と反対側に位置し、前記天板と前記塗布膜との距離を天板側間隙の高さL1とし、前記底板と前記基材との距離を底板側間隙の高さL2としたときに、前記高さL1と高さL2が、L1≦L2の関係を満たすことを特徴とする請求項1または2に記載の塗布膜の製造装置である。   According to a third aspect of the present invention, the top plate is located on the side of the base material on which the coating film is formed, and the bottom plate is located on the opposite side of the base material on which the coating film is formed. When the distance between the top plate side gap is the height L1 of the top plate side gap and the distance between the bottom plate and the base material is the height L2 of the bottom plate side gap, the height L1 and the height L2 are: 3. The coating film manufacturing apparatus according to claim 1, wherein a relationship of L1 ≦ L2 is satisfied.

請求項4に記載の発明は、前記天板と底板との距離が10mm以上100mm以下の範囲であることを特徴とする請求項1〜3のいずれかに記載の塗布膜の製造装置である。   The invention according to claim 4 is the coating film manufacturing apparatus according to any one of claims 1 to 3, wherein a distance between the top plate and the bottom plate is in a range of 10 mm to 100 mm.

請求項5に記載の発明は、前記給気口は前記右側板または左側板の一方に開口された給気口用開口部を有し、前記排気口は前記右側板または左側板の他方に開口された排気口用開口部を有し、前記天板と前記底板とが対向する方向に沿った前記給気口用開口部および前記排気口用開口部の高さは、前記天板と前記底板との距離とほぼ一致していることを特徴とする請求項1〜4のいずれかに記載の塗布膜の製造装置である。   According to a fifth aspect of the present invention, the air supply port has an air supply port opening opened in one of the right side plate and the left side plate, and the exhaust port opens in the other side of the right side plate or the left side plate. The height of the opening for the air supply port and the opening for the exhaust port along the direction in which the top plate and the bottom plate face each other is the height of the top plate and the bottom plate. 5. The coating film manufacturing apparatus according to claim 1, wherein the coating film manufacturing apparatus is substantially equal to a distance between

請求項6に記載の発明は、請求項1〜5のいずれかに記載の製造装置を用いて形成したことを特徴とする光学フィルムである。   The invention according to claim 6 is an optical film formed using the manufacturing apparatus according to any one of claims 1 to 5.

請求項7に記載の発明は、搬送中の帯状の基材に溶剤を含む塗布液を塗布し塗布膜を形成する塗布工程と、次に、前記基材に形成した塗布膜を乾燥路中で搬送しつつ乾燥させる乾燥工程とを含む塗布膜の製造方法において、前記乾燥路に給気口と整風部材を配置し、
前記整風部材を、前記搬送される前記基材の塗布膜の延長面に対して交差する面上を延在し互いに対向する面状の第1の多孔部材と第2の多孔部材とを含んで構成し、前記第1の多孔部材を前記給気口に臨ませて配置し、前記第2の多孔部材を前記塗布膜に臨むように配置し、前記第1の多孔部材を、孔径が2mm以上10mm以下、開口率が10%以上30%以下の面状の部材を1枚以上含んで構成し、前記第2の多孔部材を、孔径が0.1mm以上2mm未満、開口率が40%以上99%以下の面状の部材を1枚以上含んで構成し、前記給気口から前記整風部材を通して前記塗布膜上に空気を流すようにしたことを特徴とする塗布膜の製造方法である。
The invention according to claim 7 is a coating step in which a coating liquid containing a solvent is applied to a belt-shaped substrate being conveyed to form a coating film, and then the coating film formed on the substrate is dried in a drying path. In a manufacturing method of a coating film including a drying step of drying while transporting, an air supply port and a wind regulating member are disposed in the drying path,
The air conditioning member includes a planar first porous member and a second porous member that extend on a surface intersecting with an extended surface of the coating film of the substrate to be conveyed and face each other. And the first porous member is disposed facing the air supply port, the second porous member is disposed facing the coating film, and the first porous member has a pore diameter of 2 mm or more. The second porous member has a pore diameter of 0.1 mm to less than 2 mm and an opening ratio of 40% to 99. % Or less of a planar member, and air is allowed to flow over the coating film from the air supply port through the air conditioning member.

請求項8に記載の発明は、基材に形成した塗布膜を搬送しながら乾燥させる塗布物の乾燥装置において、少なくとも、乾燥路と、給気口と、給気手段と、排気口と、排気手段と、整風部材とを備え、前記乾燥路は、前記塗布膜をその厚さ方向で挟んで対向する天板および底板と、前記塗布膜をその幅方向で挟んで対向し前記天板と前記底板の両側を接続する右側板および左側板とを含んで構成され、前記乾燥路の前記塗布膜の搬送方向の上流端に搬入口が設けられ、前記乾燥路の前記塗布膜の搬送方向の下流端に搬出口が設けられ、前記給気口は、前記乾燥路の右側板または左側板の一方に配置され、前記給気手段は、前記給気口を介して前記乾燥路内に空気を給気し、前記排気口は、前記左側板または右側板の他方に配置され、前記排気手段は、前記排気口を介して前記乾燥路内から空気を排気し、
前記整風部材は、前記給気口に配置され、前記整風部材は、前記右側板または左側板に沿って延在し互いに対向する面状の第1の多孔部材と第2の多孔部材とを含んで構成され、
前記第1の多孔部材は前記給気口に臨むように配置され、前記第2の多孔部材は前記塗布膜に臨むように配置され、前記第1の多孔部材は、孔径が2mm以上10mm以下、開口率が10%以上30%以下の面状の部材を1枚以上備えてなり、前記第2の多孔部材は、孔径が0.1mm以上2mm未満、開口率が40%以上99%以下の面状の部材を1枚以上備えてなることを特徴とする塗布膜の乾燥装置である。
The invention according to claim 8 is an apparatus for drying a coated product that is dried while transporting a coating film formed on a substrate, and includes at least a drying path, an air supply port, an air supply means, an exhaust port, and an exhaust gas. Means and an air conditioning member, the drying path is opposed to the top and bottom plates sandwiching the coating film in its thickness direction, and opposed to the top plate and the top plate sandwiching the coating film in its width direction. A right side plate and a left side plate that connect both sides of the bottom plate, a transport port is provided at an upstream end in the transport direction of the coating film of the drying path, and a downstream side of the drying path in the transport direction of the coating film A carry-out port is provided at the end, the air supply port is disposed on one of the right side plate and the left side plate of the drying path, and the air supply means supplies air into the drying path through the air supply port. The exhaust port is disposed on the other of the left side plate or the right side plate, and the exhaust hand Exhausts air from the drying passage through the exhaust port,
The air conditioning member is disposed at the air supply port, and the air conditioning member includes a planar first porous member and a second porous member that extend along the right side plate or the left side plate and face each other. Consists of
The first porous member is arranged to face the air supply port, the second porous member is arranged to face the coating film, and the first porous member has a pore diameter of 2 mm or more and 10 mm or less, One or more planar members having an opening ratio of 10% or more and 30% or less are provided, and the second porous member has a hole diameter of 0.1 mm or more and less than 2 mm and an opening ratio of 40% or more and 99% or less. A coating film drying apparatus comprising at least one sheet-shaped member.

本発明における塗布膜の製造装置、製造方法および乾燥装置を使用することにより、わずかな乾燥ムラの発生をも抑制しながら少なくとも自然乾燥よりも乾燥速度を早く維持でき、塗布膜の面性と生産性を向上することができる。   By using the coating film manufacturing apparatus, manufacturing method and drying apparatus of the present invention, it is possible to maintain at least a drying speed faster than natural drying while suppressing the occurrence of slight drying unevenness. Can be improved.

以下、本発明の一実施形態について、図面を参照して説明する。
図1は、本発明における塗布物の製造装置を側面から見たときの側面概略図である。
塗布装置1aの塗布部1bにおいて基材4上に塗布膜が塗布される。
塗布膜が形成された基材4は乾燥装置2に搬送される。
乾燥装置2は乾燥路(乾燥ゾーン)3a〜3dの4ゾーンを備え、各乾燥路3a〜3dは、乾燥路の塗布膜5の搬送方向の上流端に設けられた搬入口と乾燥路の塗布膜5の搬送方向の下流端に設けられた搬出口とを有し、塗布膜を搬送し、給気口9を介して、整風部材を通り塗布膜搬送部6に空気を強制的に給気する給気手段と、同じく図示していないが排気口10を介して塗布膜搬送部6から空気を強制的に排気する排気手段と、塗布膜が最初に搬送される乾燥路3aの搬入口13から構成されている。
Hereinafter, an embodiment of the present invention will be described with reference to the drawings.
FIG. 1 is a schematic side view of a coated product manufacturing apparatus according to the present invention as viewed from the side.
A coating film is applied on the base material 4 in the coating unit 1b of the coating apparatus 1a.
The substrate 4 on which the coating film is formed is conveyed to the drying device 2.
The drying apparatus 2 includes four zones, ie, drying paths (drying zones) 3a to 3d, and each of the drying paths 3a to 3d is applied to a carry-in port provided at the upstream end in the transport direction of the coating film 5 on the drying path and the drying path. A transport outlet provided at the downstream end in the transport direction of the film 5, transports the coating film, and forcibly supplies air to the coating film transport unit 6 through the air conditioning port 9 through the air supply port 9. An air supply means for carrying out the process, an exhaust means for forcibly exhausting air from the coating film transport section 6 through the exhaust port 10 (not shown), and an inlet 13 of the drying path 3a through which the coating film is transported first. It is composed of

図2は、図1に示された乾燥装置のA−A’断面概略図である。
給気手段を用いて塗布膜搬送部6内へ空気を給気し、排気手段を用いて塗布膜搬送部6内から空気を排気することで、塗布膜搬送部6内に空気の流れ18を発生させている。
塗布膜搬送部6内では給気口9から排気口10に向って空気の流れ15が発生しており、塗布膜搬送部6内を搬送される塗布膜5から蒸発した有機溶剤は、空気の流れ15とともに排気口10を介して塗布膜搬送部6内から排気される。
FIG. 2 is a schematic cross-sectional view taken along line AA ′ of the drying apparatus shown in FIG.
Air is supplied into the coating film transport section 6 using the air supply means, and air is exhausted from the coating film transport section 6 using the exhaust means, whereby an air flow 18 is generated in the coating film transport section 6. Is generated.
In the coating film transport unit 6, an air flow 15 is generated from the air supply port 9 toward the exhaust port 10, and the organic solvent evaporated from the coating film 5 transported in the coating film transport unit 6 The air is exhausted from the coating film transport unit 6 through the exhaust port 10 together with the flow 15.

このとき、基材4に形成した塗布膜5と天板11の高さL1と、基材4と底板12との底板側間隙の高さL2が、L1≦L2の関係になっていることが好ましい。
詳細に説明すると、図2に示すように、各乾燥路3a〜3dは、塗布膜5をその厚さ方向で挟んで対向する天板11および底板12と、塗布膜5をその幅方向で挟んで対向し天板11と底板12の両側を接続する右側板および左側板とを含んで構成され、天板11が基材4の塗布膜5を形成した側に位置し、底板12が基材4の塗布膜5を形成した側と反対側に位置し、天板11と塗布膜5との距離を天板11側間隙の高さL1とし、底板12と基材4との距離を底板12側間隙の高さL2としたときに、高さL1と高さL2が、L1≦L2の関係を満たすことが好ましい。
L1≦L2の関係を満たすとき、外乱となる風は基材4と底板12との間に流れ込むのが主流になるため、塗布膜面に外乱となる風が当たり難く、面性と生産性を向上することができる。
At this time, the height L1 of the coating film 5 and the top plate 11 formed on the substrate 4 and the height L2 of the bottom plate side gap between the substrate 4 and the bottom plate 12 are in a relationship of L1 ≦ L2. preferable.
More specifically, as shown in FIG. 2, each of the drying paths 3a to 3d sandwiches the coating film 5 in the thickness direction and the top plate 11 and the bottom plate 12 that face each other and the coating film 5 in the width direction. And the right side plate and the left side plate that connect both sides of the top plate 11 and the bottom plate 12, the top plate 11 is located on the side of the base material 4 on which the coating film 5 is formed, and the bottom plate 12 is the base material. 4, the distance between the top plate 11 and the coating film 5 is the height L1 of the gap on the top plate 11 side, and the distance between the bottom plate 12 and the substrate 4 is the bottom plate 12. When the side gap height L2 is set, it is preferable that the height L1 and the height L2 satisfy the relationship of L1 ≦ L2.
When the relationship of L1 ≦ L2 is satisfied, wind that becomes a disturbance mainly flows between the base material 4 and the bottom plate 12, so that the wind that becomes a disturbance hardly hits the coating film surface, and the surface property and productivity are reduced. Can be improved.

また、天板11と底板12との距離が10mm未満であると、基材4が搬送されたとき、天板11もしくは底板12に接触するなどのトラブルの原因となる不利があり、天板11と底板12との距離が100mmより大きいと、乾燥速度を維持するために給気量と排気量とを増加させる必要があることから、給気手段と排気手段の増設やエネルギー量の増加などコスト面での不利があり、天板11と底板12との距離が10mm以上100mm以下の範囲であることが安定生産とコストの面で好ましい。   Further, if the distance between the top plate 11 and the bottom plate 12 is less than 10 mm, there is a disadvantage that causes a trouble such as contact with the top plate 11 or the bottom plate 12 when the base material 4 is conveyed. If the distance between the bottom plate 12 and the bottom plate 12 is larger than 100 mm, it is necessary to increase the air supply amount and the exhaust amount in order to maintain the drying speed. In terms of stable production and cost, it is preferable that the distance between the top plate 11 and the bottom plate 12 is in the range of 10 mm or more and 100 mm or less.

また、給気口9は右側板または左側板の一方に開口された給気口用開口部を有し、排気口10は右側板または左側板の他方に開口された排気口用開口部を有している。
天板11と底板12とが対向する方向に沿った給気口用開口部および排気口用開口部の高さが天板11と底板12との距離とほぼ一致していると、給気口用開口部と排気口用開口部の間に発生する空気の流れが天板11と底板12との間で一様に発生し、基材4を搬送する高さにブレが生じにくくなり、基材4の搬送時の安定性が確保されるため好ましい。
In addition, the air supply port 9 has an air supply port opening which is opened in one of the right side plate and the left side plate, and the exhaust port 10 has an air outlet opening which is opened in the other side of the right side plate or the left side plate. is doing.
When the heights of the opening for the air supply port and the opening for the exhaust port along the direction in which the top plate 11 and the bottom plate 12 face each other substantially coincide with the distance between the top plate 11 and the bottom plate 12, The air flow generated between the opening for the exhaust and the opening for the exhaust port is uniformly generated between the top plate 11 and the bottom plate 12, and the height at which the substrate 4 is conveyed is less likely to be blurred. Since stability at the time of conveyance of the material 4 is ensured, it is preferable.

本構成を塗布装置1aと乾燥装置2を0.2m以上〜0.8m以下の範囲で連結することが望ましい。言い換えると、塗布部1bから該塗布部1bに臨む搬入口13までの塗布膜搬送距離8が0.2m以上0.8m以下の範囲であることが望ましい。
塗布膜搬送距離8が0.8mより離れると自然に乾燥していく領域が無視できなくなり、自然乾燥によるムラが生じるため好ましくない。また、0.2m未満であると基材4を搬入する搬入口13において外気を遮断してしまうため好ましくない。
In this configuration, it is desirable to connect the coating device 1a and the drying device 2 within a range of 0.2 m to 0.8 m. In other words, it is desirable that the coating film transport distance 8 from the coating unit 1b to the carry-in port 13 facing the coating unit 1b is in the range of 0.2 m to 0.8 m.
If the coating film conveyance distance 8 is longer than 0.8 m, the naturally drying region cannot be ignored, and unevenness due to natural drying occurs, which is not preferable. Moreover, since outside air will be interrupted | blocked in the entrance 13 which carries in the base material 4 as it is less than 0.2 m, it is unpreferable.

図3は、整風部材22の一例を側面から見たときの側面概略図である。
整風部材22は、吸気口側に開口率が小さく、孔径の大きな板状の部材をいれ吸気される気流をわざと乱すことにより速度分布を打ち消し、その後開口率が大きく、孔径の小さな板状の部材をいれ気流を整流化する構成を有する機構である。
ここで、孔の開口率とは、(孔の開口部の面積/整風部材の面積)×100(%)で表される値である。
詳細に説明すると、給気口9は、乾燥路の右側板または左側板の一方に配置され、排気口10は、乾燥路の右側板または左側板の他方に配置されている。
整風部材22は給気口9に配置されている。
整風部材22は、右側板または左側板に沿って延在し互いに対向する面状の第1の多孔部材24と第2の多孔部材23とを含んで構成されている。
第1の多孔部材24は給気口9に臨むように配置され、第2の多孔部材23は塗布膜5に臨むように配置されている。
言い換えると、整風部材22は、搬送される基材4の塗布膜5の延長面に対して交差する面上(または直交する面上)を延在し互いに対向する面状の第1の多孔部材24と第2の多孔部材23とを含んで構成されている。
FIG. 3 is a schematic side view of the air conditioning member 22 as viewed from the side.
The air conditioning member 22 is a plate-like member having a small opening ratio on the side of the air inlet and canceling the velocity distribution by intentionally disturbing the airflow that is sucked by inserting a plate-like member having a large hole diameter and then having a large opening ratio and a small hole diameter. This is a mechanism having a configuration that rectifies the airflow.
Here, the aperture ratio of the hole is a value represented by (area of the opening of the hole / area of the air conditioning member) × 100 (%).
More specifically, the air supply port 9 is disposed on one of the right side plate and the left side plate of the drying path, and the exhaust port 10 is disposed on the other side of the right side plate or the left side plate of the drying path.
The air conditioning member 22 is disposed in the air supply port 9.
The air conditioning member 22 includes a planar first porous member 24 and a second porous member 23 that extend along the right side plate or the left side plate and face each other.
The first porous member 24 is disposed so as to face the air supply port 9, and the second porous member 23 is disposed so as to face the coating film 5.
In other words, the air conditioning member 22 is a planar first porous member that extends on a surface that intersects (or is perpendicular to) the extended surface of the coating film 5 of the substrate 4 to be conveyed and faces each other. 24 and the 2nd porous member 23 are comprised.

第1の多孔部材24は速度分布を打ち消す部材であり、第1の多孔部材24としては、金網、パンチングメタル等、複数の孔を形成した板状部材を用いることができる。
好ましい構成としては孔径2〜10mm、開口率10〜30%程度の条件になる。ただし、枚数を重ねれば塗布膜搬送部内の空気の流れ、および、蒸発した有機溶剤の流れを制御する機能を有するものであれば、孔の開口形状や孔の開口率等は特に制限されるものではない。また、部材の材質としては、耐溶剤性を有するものであればよく、特に限定されるものではない。
言い換えると、第1の多孔部材24は、孔径が2mm以上10mm以下、開口率が10%以上30%以下の面状の部材を1枚以上備えて構成されている。
The first porous member 24 is a member that cancels the velocity distribution. As the first porous member 24, a plate-like member in which a plurality of holes are formed, such as a wire mesh or a punching metal, can be used.
A preferable configuration is such that the hole diameter is 2 to 10 mm and the aperture ratio is about 10 to 30%. However, as long as the number is increased, the shape of the hole, the hole opening ratio, etc. are particularly limited as long as it has a function of controlling the flow of air in the coating film transport unit and the flow of the evaporated organic solvent. It is not a thing. The material of the member is not particularly limited as long as it has solvent resistance.
In other words, the first porous member 24 includes one or more planar members having a hole diameter of 2 mm to 10 mm and an aperture ratio of 10% to 30%.

第2の多孔部材23は整流化させる部材であり、第2の多孔部材23としては、金網、メッシュ、ハニカム等、複数の孔を形成した板状部材を用いることができる。好ましい構成としては孔径0.1〜2mm、開口率40〜99%程度の条件になる。この条件の部材の枚数を重ねるごとにムラを抑える効果は大きくなる。また、部材の材質としては、耐溶剤性を有するものであればよく、特に限定されるものではない。
言い換えると、第2の多孔部材23は、孔径が0.1mm以上2mm未満、開口率が40%以上99%以下の面状の部材を1枚以上備えて構成されている。
The second porous member 23 is a member to be rectified. As the second porous member 23, a plate-like member having a plurality of holes, such as a wire net, a mesh, and a honeycomb, can be used. A preferable configuration is that the hole diameter is 0.1 to 2 mm and the aperture ratio is about 40 to 99%. The effect of suppressing unevenness increases as the number of members having this condition is increased. The material of the member is not particularly limited as long as it has solvent resistance.
In other words, the second porous member 23 includes one or more planar members having a hole diameter of 0.1 mm to less than 2 mm and an opening ratio of 40% to 99%.

図1において、基材4に形成された塗布膜5は、最初に搬入する乾燥路3aの搬入口13から最初の乾燥路3a内へ搬入され、最後に搬出する乾燥路3dの搬出口14から乾燥路3d外へ搬出される。図1では、乾燥路3a〜3dの4ゾーンが直線的に配置されているが、これは本発明の一実施形態を表したものであり、これに限定されるものではない。また、隣接する各乾燥路は直線的に配置されていても、屈折して配置されていてもよい。   In FIG. 1, the coating film 5 formed on the substrate 4 is carried into the first drying path 3a from the carry-in port 13 of the drying path 3a that is first carried in, and from the carry-out port 14 of the drying path 3d that is finally carried out. It is carried out of the drying path 3d. In FIG. 1, the four zones of the drying paths 3 a to 3 d are linearly arranged. However, this represents one embodiment of the present invention, and the present invention is not limited to this. Moreover, each adjacent drying path may be arrange | positioned linearly, or may be arrange | positioned refractingly.

また、図1では、各乾燥路(3a〜3d)に給気口9と排気口10が1個ずつ配置されているが、これは本発明の一実施形態を表したものであり、これに限定されるものではなく、各乾燥路に対して配置される給気口9および排気口10の個数に制限はない。   Further, in FIG. 1, one air supply port 9 and one exhaust port 10 are arranged in each drying path (3 a to 3 d), but this represents one embodiment of the present invention. There is no limitation, and the number of air supply ports 9 and exhaust ports 10 arranged for each drying path is not limited.

本発明における塗布装置1aは、グラビア、ワイヤーバー、ダイ等を用いることができるが、これらに限定されるものではない。   The coating apparatus 1a in the present invention can use a gravure, a wire bar, a die or the like, but is not limited to these.

本発明における乾燥路は、乾燥路外から吹き込む風や塵等の外乱を防止するためにある程度密封された箱型の形状をしている。塗布膜5を搬入する搬入口と、塗布膜5を搬出し搬入口に対向して設置された搬出口と、基材4の塗布膜5を形成した側に設置された天板11と、基材4を挟んで天板11と対向して設置された底板12と、塗布膜5の搬送方向に向って右側であり、塗布膜5の幅方向に設置された右側板と、右側板と対向して設置された左側板とで構成されている。ここで、搬送される基材4に対し、重力方向上面側に塗布膜5が形成されているか、下面側に塗布膜5が形成されているかは関係ない。   The drying path in the present invention has a box shape that is sealed to some extent in order to prevent disturbances such as wind and dust blown from outside the drying path. A carry-in port for carrying in the coating film 5, a carry-out port installed opposite to the carry-in port, the top plate 11 installed on the side of the substrate 4 on which the coating film 5 is formed, A bottom plate 12 placed opposite to the top plate 11 across the material 4, a right side facing the conveying direction of the coating film 5, and a right side plate placed in the width direction of the coating film 5, and facing the right side plate And the left side plate installed. Here, it does not matter whether the coating film 5 is formed on the upper surface side in the gravity direction or the coating film 5 is formed on the lower surface side of the substrate 4 to be conveyed.

本発明における給気手段、または、排気手段、または、その両方、のいずれかより選ばれる気流発生手段としては、給気手段および排気手段の出力(給気出力D1および排気出力D2)に応じて、塗布膜搬送部内の空気の流れを調節することができるブロアを用いることができるが、これに限定されるものではない。   As the air flow generation means selected from either the air supply means and / or the exhaust means in the present invention, depending on the outputs (supply air output D1 and exhaust output D2) of the air supply means and the exhaust means. A blower capable of adjusting the flow of air in the coating film transport unit can be used, but is not limited thereto.

本発明における乾燥装置2の長さ(基材の搬送方向)は、特に制約すべき事項ではない。乾燥装置2の長さは塗布膜が乾燥するかどうかで決定されるものであり、製品によって異なるものである。ただし、本発明では、50cm以上100m以下程度の一般的な長さの乾燥装置2を用いている。
また、本発明における乾燥路の長さ(基材の搬送方向)としては、30cm以上30m以下程度のものを用いている。
The length of the drying device 2 in the present invention (base material transport direction) is not particularly limited. The length of the drying device 2 is determined by whether or not the coating film is dried, and varies depending on the product. However, in the present invention, the drying apparatus 2 having a general length of about 50 cm to 100 m is used.
In addition, the length of the drying path (the conveyance direction of the substrate) in the present invention is about 30 cm to 30 m.

本発明における基材4の搬送速度は制約すべき事項ではないが、10m/min以上100m/min以下程度の一般的な速度が好ましい。   Although the conveyance speed of the base material 4 in this invention is not a matter which should be restrict | limited, the general speed of about 10 m / min or more and 100 m / min or less is preferable.

本発明における乾燥装置2は、塗布膜中の有機溶剤の蒸発速度を安定化し、わずかな乾燥ムラの発生を抑制することができるため、その効果が最も現れるのは乾燥初期である。乾燥装置の全長すべてが本発明の乾燥装置2によるものではなく、基材に形成された塗布膜を最初に搬入する乾燥路の搬入口を含む乾燥初期段階のみに本発明の乾燥装置2を導入することも可能である。その場合、図1に示すように、前半部に第一乾燥装置として本発明の乾燥装置2を導入し、後半部に第二乾燥装置21として公知の乾燥装置を導入してもよい。   Since the drying apparatus 2 in the present invention can stabilize the evaporation rate of the organic solvent in the coating film and suppress the occurrence of slight drying unevenness, the effect is most apparent in the initial stage of drying. The entire length of the drying apparatus is not based on the drying apparatus 2 of the present invention, and the drying apparatus 2 of the present invention is introduced only in the initial stage of drying including the inlet of the drying path for first carrying the coating film formed on the substrate. It is also possible to do. In that case, as shown in FIG. 1, the drying apparatus 2 of the present invention may be introduced as the first drying apparatus in the first half, and a known drying apparatus may be introduced as the second drying apparatus 21 in the second half.

第二乾燥装置21としては、スリットノズルやパンチングメタルから基材に形成された塗布膜に温度を上昇させた噴流を当てるような方式を導入しても良いし、クイックリターン方式のノズルや基材の搬送方向に平行流を流す方式のノズルから熱風を噴出する方式でも良い。また、片面だけでなく両面から加熱手段を設けても良い。市販されているいかなる乾燥装置を使用しても本発明の効果をさまたげるものではない。   As the second drying device 21, a method of applying a jet flow with increased temperature to a coating film formed on a base material from a slit nozzle or punching metal may be introduced, or a quick return type nozzle or base material A system in which hot air is ejected from a nozzle of a system in which a parallel flow is made in the transport direction may be used. Moreover, you may provide a heating means not only from one side but from both sides. The use of any commercially available drying apparatus does not interfere with the effects of the present invention.

さらに、図1には本発明の乾燥装置2と公知の第二乾燥装置21をそれぞれの装置として独立させる場合を示しているが、一つの乾燥装置の中で、前半部が本発明の乾燥装置による方式をとり、後半部が公知の乾燥装置に基づく方式をとる場合でも本発明の効果は変わらない。   Further, FIG. 1 shows a case where the drying device 2 of the present invention and the known second drying device 21 are independent from each other, but the first half of one drying device is the drying device of the present invention. The effect of the present invention remains the same even when the latter part is based on a known drying apparatus.

本発明の塗布膜の乾燥装置および乾燥方法、これらを用いた塗布物の製造装置および製造方法は、様々な製品に対して用いることができるが、近年需要が伸びている光学フィルムのようなこれまで以上にムラに対する許容余地の少ない製品に効果的である。   The coating film drying apparatus and drying method of the present invention, and the coated product manufacturing apparatus and manufacturing method using these can be used for various products. It is effective for products with less tolerance for unevenness.

ここで、光学フィルムとは、透過光や反射光の方向、位相、偏光面等を制御するフィルムであり、例えば、液晶やプラズマディスプレイなどの表示装置の最表面またはその内側に使用されるフィルムであり、反射防止フィルム、防眩性フィルム、光学補償フィルム、光拡散フィルムなどが挙げられる。   Here, the optical film is a film that controls the direction, phase, polarization plane, and the like of transmitted light and reflected light, and is, for example, a film used on the outermost surface of a display device such as a liquid crystal or a plasma display or on the inside thereof. Yes, examples thereof include an antireflection film, an antiglare film, an optical compensation film, and a light diffusion film.

また、本発明に用いられる有機溶剤としては、メタノール、エタノール、イソプロパノール、ブタノール、2−メトキシエタノール等のアルコール類、アセトン、メチルエチルケトン、メチルイソブチル等のケトン類、酢酸メチル、酢酸エチル、酢酸ブチル等のエステル類、ジイソプロピルエーテル等のエーテル類、エチレングリコール、プロピレングリコール、ヘキシレングリコール等のグリコール類、エチルセロソルブ、ブチルセロソルブ、エチルカルビトール・ブチルカルビトール等のグリコールエーテル類、ヘキサン、ヘプタン・オクタン等の脂肪族炭化水素類、ハロゲン化炭化水素、ベンゼン、トルエン、キシレン等の芳香族炭化水素、N−メチルピロリドン、ジメチルホルムアミド等が挙げられ、1種、または、2種類以上の混合物として用いてよいが、これらに限定されるものではない。   Examples of the organic solvent used in the present invention include alcohols such as methanol, ethanol, isopropanol, butanol and 2-methoxyethanol, ketones such as acetone, methyl ethyl ketone and methyl isobutyl, methyl acetate, ethyl acetate and butyl acetate. Esters, ethers such as diisopropyl ether, glycols such as ethylene glycol, propylene glycol, hexylene glycol, glycol ethers such as ethyl cellosolve, butyl cellosolve, ethyl carbitol / butyl carbitol, fats such as hexane, heptane / octane, etc. Aromatic hydrocarbons such as aromatic hydrocarbons, halogenated hydrocarbons, benzene, toluene and xylene, N-methylpyrrolidone, dimethylformamide and the like, and one kind or a mixture of two or more kinds It may be used as an object, but is not limited thereto.

本発明の塗布液に用いられるバインダーとしては、紫外線硬化性樹脂、電子線硬化性樹脂などの電離放射線硬化性樹脂や熱硬化性樹脂等が挙げられ、電離放射線硬化性樹脂等には光重合開始剤が含まれる。   Examples of the binder used in the coating liquid of the present invention include ionizing radiation curable resins and thermosetting resins such as ultraviolet curable resins and electron beam curable resins. Agent is included.

電離放射線硬化性樹脂としては、多価アルコールのアクリル酸またはメタクリル酸エステルのような多官能性のアクリレート樹脂、ジイソシアネート、多価アルコール及びアクリル酸またはメタクリル酸のヒドロキシエステル等から合成されるような多官能のウレタンアクリレート樹脂等が挙げられる。またこれらの他にも、アクリレート系の官能基を有するポリエーテル樹脂、ポリエステル樹脂、エポキシ樹脂、アルキッド樹脂、スピロアセタール樹脂、ポリブタジエン樹脂、ポリチオールポリエン樹脂等も使用することができる。   Examples of the ionizing radiation curable resin include polyfunctional acrylate resins such as polyhydric alcohol acrylic acid or methacrylic acid ester, diisocyanate, polyhydric alcohol and acrylic acid or methacrylic acid hydroxy ester. Examples include functional urethane acrylate resins. Besides these, polyether resins having an acrylate functional group, polyester resins, epoxy resins, alkyd resins, spiroacetal resins, polybutadiene resins, polythiol polyene resins, and the like can also be used.

熱硬化性樹脂としては、熱硬化型ウレタン樹脂、フェノール樹脂、尿素メラミン樹脂、エポキシ樹脂、不飽和ポリエステル樹脂、シリコーン樹脂等が挙げられる。   Examples of the thermosetting resin include thermosetting urethane resins, phenol resins, urea melamine resins, epoxy resins, unsaturated polyester resins, and silicone resins.

光重合開始剤としては、活性エネルギー線が照射された際にラジカルを発生するものであればよく、例えば、1−ヒドロキシシクロヘキシルフェニルケトン、2−ヒドロキシ−2−メチル−1−フェニルプロパン−1−オン、2−メチル[4−(メチルチオ)フェニル]モルフォリノプロパン−1−オン、2,2−ジメトキシ−1,2−ジフェニルエタン−1−オン、ベンゾフェノン、1−[4−(2−ヒドロキシエトキシ)フェニル]−2−ヒドロキシ−2−メチル−1−プロパン−1−オン、2−ベンジル−2−ジメチルアミノ−1−(4−モルフォリノフェニル)ブタン−1−オン、ビス(2,6−ジメトキシベンゾイル)−2,4,4−トリメチルペンチルフォスフィンオキサイド等が挙げられる。光重合開始剤の添加量は、活性エネルギー線硬化単量体10〜80質量部に対して、0.1〜10質量部が好ましく、1〜7質量部がより好ましく、1〜5質量部がさらに好ましくい。   Any photopolymerization initiator may be used as long as it generates radicals when irradiated with active energy rays. For example, 1-hydroxycyclohexyl phenyl ketone, 2-hydroxy-2-methyl-1-phenylpropane-1- ON, 2-methyl [4- (methylthio) phenyl] morpholinopropan-1-one, 2,2-dimethoxy-1,2-diphenylethane-1-one, benzophenone, 1- [4- (2-hydroxyethoxy) ) Phenyl] -2-hydroxy-2-methyl-1-propan-1-one, 2-benzyl-2-dimethylamino-1- (4-morpholinophenyl) butan-1-one, bis (2,6- And dimethoxybenzoyl) -2,4,4-trimethylpentylphosphine oxide. 0.1-10 mass parts is preferable with respect to 10-80 mass parts of active energy ray hardening monomers, and, as for the addition amount of a photoinitiator, 1-7 mass parts is more preferable, and 1-5 mass parts is. Further preferred.

本発明に用いられる基材としては、用途によって様々なものを使用することができる。基材を構成する成分としては、例えば、アセチルセルロース、トリアセチルセルロース等のセルロース系フィルム、ポリエチレンテレフタレート、ポリエチレンナフタレート等のポリエステル系フルイム、ポリメチルメタクリレート等のアクリル系フィルム等が挙げられるが、これらに限定されるものではない。また、基材は、単層からなっていても複数層からなっていてもよい。なお、基材の厚さは一般的に10μm以上500μm以下のものが用いられる。   As the base material used in the present invention, various materials can be used depending on applications. Examples of the component constituting the substrate include cellulose films such as acetyl cellulose and triacetyl cellulose, polyester films such as polyethylene terephthalate and polyethylene naphthalate, acrylic films such as polymethyl methacrylate, and the like. It is not limited to. Further, the substrate may be composed of a single layer or a plurality of layers. In general, a substrate having a thickness of 10 μm or more and 500 μm or less is used.

(実施例)
次に実施例について説明する。
幅1000mm、厚み80μmのトリアセチルセルロース(TAC)基材に、溶剤として酢酸エチル、バインダーとしてアクリル樹脂を用い、固形分濃度50wt%からなる塗布液をエクストルージョン方式のダイヘッドで塗布し、長さ8.0mの乾燥装置2内に、搬送速度30m/minで塗布膜5を搬送した。
基材4と天板側間隙の高さL1と、基材と底板側間隙の高さL2はともに15mmである。ここで用いた乾燥装置2は、長さ1.0mの乾燥路を8ゾーン配置したものであった。
(Example)
Next, examples will be described.
A triacetyl cellulose (TAC) substrate having a width of 1000 mm and a thickness of 80 μm is coated with an extrusion type die head using an extrusion type die head using ethyl acetate as a solvent and an acrylic resin as a binder and a solid content concentration of 50 wt%. The coating film 5 was conveyed in a drying apparatus 2 of 0.0 m at a conveyance speed of 30 m / min.
Both the height L1 of the base material 4 and the top plate side gap and the height L2 of the base material and the bottom plate side gap are 15 mm. The drying device 2 used here was one in which eight zones of 1.0 m long drying paths were arranged.

整風部材22としては、第1の多孔部材24として開口率20%、孔径3mm、厚さ2mmのパンチングメタルを2枚、給気口9に臨ませて設け、第2の多孔部材23として開口率60%、孔径1mm、厚さ1mmの金網を1枚、塗布膜5に臨ませて設ける構成とした。   As the air conditioning member 22, two punching metals having an opening ratio of 20%, a hole diameter of 3 mm, and a thickness of 2 mm are provided facing the air supply port 9 as the first porous member 24, and the opening ratio is provided as the second porous member 23. One sheet of wire net having 60%, a hole diameter of 1 mm, and a thickness of 1 mm is provided facing the coating film 5.

この時、乾燥後の塗布膜には風紋のようなムラは見つからなかった。   At this time, no unevenness such as wind ripples was found on the coating film after drying.

一方、整風部材22無しでそれ以外の条件は同様にしたところ、乾燥後の塗布膜5上にはっきりとしたムラが確認された。   On the other hand, when the air conditioning member 22 was not used and the other conditions were the same, clear unevenness was confirmed on the coating film 5 after drying.

また、上記とは別の条件で整風部材22を作成した。
この整風部材22としては、第1の多孔部材24として開口率20%、孔径3mm、厚さ2mmのパンチングメタルを2枚、給気口9に臨ませて設け、第2の多孔部材23として開口率30%、孔径1mm、厚さ1mmの金網を1枚、塗布膜5に臨ませて設ける構成とした。
この場合には整風部材22がない状態よりは改善するが、供給側の一部に風紋のようなムラが生じる。
Moreover, the air conditioning member 22 was created on the conditions different from the above.
As the air conditioning member 22, two punching metals having an opening ratio of 20%, a hole diameter of 3 mm, and a thickness of 2 mm are provided facing the air supply port 9 as the first porous member 24, and the opening is provided as the second porous member 23. A wire net having a rate of 30%, a hole diameter of 1 mm, and a thickness of 1 mm was provided facing the coating film 5.
In this case, the condition is improved as compared with the case where the air conditioning member 22 is not provided, but unevenness such as a wind pattern occurs in a part on the supply side.

乾燥後の塗布膜のムラ状況を比較した結果から本発明はムラの低減の効果を有する。   From the result of comparing the unevenness of the coating film after drying, the present invention has an effect of reducing unevenness.

塗布物の製造装置を側面から見たときの側面概略図である。It is the side surface schematic when the manufacturing apparatus of a coated material is seen from the side. 乾燥装置のA−A’断面概略図である。It is A-A 'cross-sectional schematic of a drying apparatus. 整風部材の一例を側面から見たときの側面概略図である。It is a side schematic diagram when an example of a wind regulation member is seen from the side.

符号の説明Explanation of symbols

1a……塗布装置、1b……塗布部、2……乾燥装置、3a〜3c……乾燥路、4……基材、5……塗布膜、6……塗布膜搬送部、9……給気口、10……排気口、11……天板、12……底板、13……最初に搬入する乾燥路の搬入口、14……最後に搬出する乾燥路の搬出口、15……空気の流れ、18……空気の流れ、21……第二乾燥装置、22……整風部材、23……第2の多孔部材、24……第2の多孔部材。   DESCRIPTION OF SYMBOLS 1a ... Coating apparatus, 1b ... Coating part, 2 ... Drying apparatus, 3a-3c ... Drying path, 4 ... Base material, 5 ... Coating film, 6 ... Coating film conveyance part, 9 ... Supply Air port, 10 ... Exhaust port, 11 ... Top plate, 12 ... Bottom plate, 13 ... Inlet for the first drying path, 14 ... Exit for the last drying path, 15 ... Air 18 ... Air flow, 21 ... Second drying device, 22 ... Air conditioning member, 23 ... Second porous member, 24 ... Second porous member.

Claims (8)

搬送中の帯状の基材に溶剤を含む塗布液を塗布し塗布膜を形成する塗布装置と、前記基材に形成した塗布膜を搬送しながら乾燥させる乾燥装置とを有する塗布膜の製造装置において、
前記乾燥装置は、少なくとも、乾燥路と、給気口と、給気手段と、排気口と、排気手段と、整風部材とを備え、
前記乾燥路は、前記塗布膜をその厚さ方向で挟んで対向する天板および底板と、前記塗布膜をその幅方向で挟んで対向し前記天板と前記底板の両側を接続する右側板および左側板とを含んで構成され、
前記乾燥路の前記塗布膜の搬送方向の上流端に搬入口が設けられ、
前記乾燥路の前記塗布膜の搬送方向の下流端に搬出口が設けられ、
前記給気口は、前記乾燥路の右側板または左側板の一方に配置され、
前記給気手段は、前記給気口を介して前記乾燥路内に空気を給気し、
前記排気口は、前記左側板または右側板の他方に配置され、
前記排気手段は、前記排気口を介して前記乾燥路内から空気を排気し、
前記整風部材は、前記給気口に配置され、
前記整風部材は、前記右側板または左側板に沿って延在し互いに対向する面状の第1の多孔部材と第2の多孔部材とを含んで構成され、
前記第1の多孔部材は前記給気口に臨むように配置され、
前記第2の多孔部材は前記塗布膜に臨むように配置され、
前記第1の多孔部材は、孔径が2mm以上10mm以下、開口率が10%以上30%以下の面状の部材を1枚以上備えてなり、
前記第2の多孔部材は、孔径が0.1mm以上2mm未満、開口率が40%以上99%以下の面状の部材を1枚以上備えてなる、
ことを特徴とする塗布膜の製造装置。
In an apparatus for manufacturing a coating film, comprising: a coating apparatus that forms a coating film by applying a coating solution containing a solvent to a belt-shaped substrate being transported; and a drying apparatus that dries while transporting the coating film formed on the substrate. ,
The drying apparatus includes at least a drying path, an air supply port, an air supply unit, an exhaust port, an exhaust unit, and an air conditioning member.
The drying path includes a top plate and a bottom plate that are opposed to each other with the coating film sandwiched in a thickness direction thereof, a right side plate that is opposed to the coating film in a width direction and that connects both sides of the top plate and the bottom plate, and Comprising a left side plate,
A carry-in entrance is provided at an upstream end of the drying path in the transport direction of the coating film,
A carry-out port is provided at the downstream end of the drying path in the transport direction of the coating film,
The air supply port is disposed on one of the right side plate and the left side plate of the drying path,
The air supply means supplies air into the drying path through the air supply port,
The exhaust port is disposed on the other of the left side plate or the right side plate,
The exhaust means exhausts air from the inside of the drying path through the exhaust port,
The air conditioning member is disposed in the air supply port,
The air conditioning member includes a planar first porous member and a second porous member that extend along the right side plate or the left side plate and face each other.
The first porous member is disposed so as to face the air supply port,
The second porous member is disposed so as to face the coating film,
The first porous member comprises one or more planar members having a hole diameter of 2 mm to 10 mm and an aperture ratio of 10% to 30%,
The second porous member comprises one or more planar members having a hole diameter of 0.1 mm or more and less than 2 mm and an aperture ratio of 40% or more and 99% or less.
An apparatus for producing a coating film, comprising:
前記塗布装置は前記基材に前記塗布液を塗布し前記塗布膜を形成する塗布部を有し、
前記塗布部から該塗布部に臨む前記搬入口までの塗布膜搬送距離が0.2m以上0.8m以下の範囲である、
ことを特徴とする請求項1に記載の塗布膜の製造装置。
The coating apparatus includes a coating unit that coats the coating liquid on the substrate to form the coating film,
The coating film transport distance from the coating unit to the carry-in port facing the coating unit is in the range of 0.2 m or more and 0.8 m or less.
The manufacturing apparatus of the coating film of Claim 1 characterized by the above-mentioned.
前記天板が前記基材の塗布膜を形成した側に位置し、前記底板が前記基材の塗布膜を形成した側と反対側に位置し、前記天板と前記塗布膜との距離を天板側間隙の高さL1とし、前記底板と前記基材との距離を底板側間隙の高さL2としたときに、前記高さL1と高さL2が、L1≦L2の関係を満たす、
ことを特徴とする請求項1または2に記載の塗布膜の製造装置。
The top plate is located on the side of the substrate on which the coating film is formed, the bottom plate is located on the side opposite to the side on which the coating film of the substrate is formed, and the distance between the top plate and the coating film is measured on the ceiling. The height L1 and the height L2 satisfy the relationship of L1 ≦ L2 when the height L1 of the plate-side gap and the distance between the bottom plate and the base material is the height L2 of the bottom-plate-side gap.
The coating film manufacturing apparatus according to claim 1, wherein the coating film manufacturing apparatus is a coating film manufacturing apparatus.
前記天板と底板との距離が10mm以上100mm以下の範囲であることを特徴とする請求項1〜3のいずれかに記載の塗布膜の製造装置。   The apparatus for producing a coating film according to any one of claims 1 to 3, wherein a distance between the top plate and the bottom plate is in a range of 10 mm to 100 mm. 前記給気口は前記右側板または左側板の一方に開口された給気口用開口部を有し、
前記排気口は前記右側板または左側板の他方に開口された排気口用開口部を有し、
前記天板と前記底板とが対向する方向に沿った前記給気口用開口部および前記排気口用開口部の高さは、前記天板と前記底板との距離とほぼ一致している、
ことを特徴とする請求項1〜4のいずれかに記載の塗布膜の製造装置。
The air supply port has an air supply port opening which is opened in one of the right side plate or the left side plate,
The exhaust port has an exhaust port opening opened to the other of the right side plate or the left side plate,
The heights of the air supply opening and the exhaust opening along the direction in which the top plate and the bottom plate face each other substantially coincide with the distance between the top plate and the bottom plate.
The manufacturing apparatus of the coating film in any one of Claims 1-4 characterized by the above-mentioned.
請求項1〜5のいずれかに記載の製造装置を用いて形成したことを特徴とする光学フィルム。   An optical film formed using the manufacturing apparatus according to claim 1. 搬送中の帯状の基材に溶剤を含む塗布液を塗布し塗布膜を形成する塗布工程と、次に、前記基材に形成した塗布膜を乾燥路中で搬送しつつ乾燥させる乾燥工程とを含む塗布膜の製造方法において、
前記乾燥路に給気口と整風部材を配置し、
前記整風部材を、前記搬送される前記基材の塗布膜の延長面に対して交差する面上を延在し互いに対向する面状の第1の多孔部材と第2の多孔部材とを含んで構成し、
前記第1の多孔部材を前記給気口に臨ませて配置し、
前記第2の多孔部材を前記塗布膜に臨むように配置し、
前記第1の多孔部材を、孔径が2mm以上10mm以下、開口率が10%以上30%以下の面状の部材を1枚以上含んで構成し、
前記第2の多孔部材を、孔径が0.1mm以上2mm未満、開口率が40%以上99%以下の面状の部材を1枚以上含んで構成し、
前記給気口から前記整風部材を通して前記塗布膜上に空気を流すようにした、
ことを特徴とする塗布膜の製造方法。
A coating step of applying a coating solution containing a solvent to the belt-shaped substrate being transported to form a coating film, and a drying step of drying the coating film formed on the substrate while being transported in a drying path In the manufacturing method of the coating film containing,
An air supply port and an air conditioning member are arranged in the drying path,
The air conditioning member includes a planar first porous member and a second porous member that extend on a surface intersecting with an extended surface of the coating film of the substrate to be conveyed and face each other. Configure
Arranging the first porous member facing the air supply port;
Arranging the second porous member so as to face the coating film,
The first porous member comprises one or more planar members having a hole diameter of 2 mm or more and 10 mm or less and an aperture ratio of 10% or more and 30% or less,
The second porous member comprises one or more planar members having a pore diameter of 0.1 mm or more and less than 2 mm and an aperture ratio of 40% or more and 99% or less,
Air was allowed to flow on the coating film from the air supply port through the air conditioning member.
The manufacturing method of the coating film characterized by the above-mentioned.
基材に形成した塗布膜を搬送しながら乾燥させる塗布物の乾燥装置において、
少なくとも、乾燥路と、給気口と、給気手段と、排気口と、排気手段と、整風部材とを備え、
前記乾燥路は、前記塗布膜をその厚さ方向で挟んで対向する天板および底板と、前記塗布膜をその幅方向で挟んで対向し前記天板と前記底板の両側を接続する右側板および左側板とを含んで構成され、
前記乾燥路の前記塗布膜の搬送方向の上流端に搬入口が設けられ、
前記乾燥路の前記塗布膜の搬送方向の下流端に搬出口が設けられ、
前記給気口は、前記乾燥路の右側板または左側板の一方に配置され、
前記給気手段は、前記給気口を介して前記乾燥路内に空気を給気し、
前記排気口は、前記左側板または右側板の他方に配置され、
前記排気手段は、前記排気口を介して前記乾燥路内から空気を排気し、
前記整風部材は、前記給気口に配置され、
前記整風部材は、前記右側板または左側板に沿って延在し互いに対向する面状の第1の多孔部材と第2の多孔部材とを含んで構成され、
前記第1の多孔部材は前記給気口に臨むように配置され、
前記第2の多孔部材は前記塗布膜に臨むように配置され、
前記第1の多孔部材は、孔径が2mm以上10mm以下、開口率が10%以上30%以下の面状の部材を1枚以上備えてなり、
前記第2の多孔部材は、孔径が0.1mm以上2mm未満、開口率が40%以上99%以下の面状の部材を1枚以上備えてなる、
ことを特徴とする塗布膜の乾燥装置。
In a drying apparatus for a coated product that is dried while transporting a coating film formed on a substrate,
At least a drying path, an air supply port, an air supply unit, an exhaust port, an exhaust unit, and a wind control member,
The drying path includes a top plate and a bottom plate that are opposed to each other with the coating film sandwiched in a thickness direction thereof, a right side plate that is opposed to the coating film in a width direction and that connects both sides of the top plate and the bottom plate, and Comprising a left side plate,
A carry-in entrance is provided at an upstream end of the drying path in the transport direction of the coating film,
A carry-out port is provided at the downstream end of the drying path in the transport direction of the coating film,
The air supply port is disposed on one of the right side plate and the left side plate of the drying path,
The air supply means supplies air into the drying path through the air supply port,
The exhaust port is disposed on the other of the left side plate or the right side plate,
The exhaust means exhausts air from the inside of the drying path through the exhaust port,
The air conditioning member is disposed in the air supply port,
The air conditioning member includes a planar first porous member and a second porous member that extend along the right side plate or the left side plate and face each other.
The first porous member is disposed so as to face the air supply port,
The second porous member is disposed so as to face the coating film,
The first porous member comprises one or more planar members having a hole diameter of 2 mm to 10 mm and an aperture ratio of 10% to 30%,
The second porous member comprises one or more planar members having a hole diameter of 0.1 mm or more and less than 2 mm and an aperture ratio of 40% or more and 99% or less.
An apparatus for drying a coating film, comprising:
JP2007235195A 2007-09-11 2007-09-11 Manufacturing device, method and dryer for coating film, and optical film Pending JP2009069261A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111167683A (en) * 2018-11-13 2020-05-19 耿晋 Air inlet device and drying unit

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111167683A (en) * 2018-11-13 2020-05-19 耿晋 Air inlet device and drying unit

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