JP2008035741A - Method and device for producing fruit/vegetable freshness preservative using phytoncide gas extracted from hiba - Google Patents

Method and device for producing fruit/vegetable freshness preservative using phytoncide gas extracted from hiba Download PDF

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JP2008035741A
JP2008035741A JP2006211876A JP2006211876A JP2008035741A JP 2008035741 A JP2008035741 A JP 2008035741A JP 2006211876 A JP2006211876 A JP 2006211876A JP 2006211876 A JP2006211876 A JP 2006211876A JP 2008035741 A JP2008035741 A JP 2008035741A
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JP4368366B2 (en
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Kingo Yamada
金伍 山田
Kazuyuki Kumazawa
和之 熊澤
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KASHIMO SHINRIN KUMIAI
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Abstract

<P>PROBLEM TO BE SOLVED: To provide a method for producing a fruit/vegetable freshness preservative using phytoncide gas extracted from Hiba comprising making zeolite efficiently adsorb, with no loss, biogas of phytoncide gas extracted from Hiba charged in a steaming pod via supply of steam. <P>SOLUTION: The method for producing a fruit/vegetable freshness preservative using phytoncide gas extracted from Hiba comprises the following process: collecting phytoncide gas generated by charging the Hiba in the steaming pod and supply steam to the pod in a bag-like body 5 which is joined to the steaming pod and whose inner capacity increases or reduces so as to stick the collected phytoncide gas in the bag-like body 5; connecting the opening 50 of the bag-like body 5 to the connection port 70 of a pressure vessel 7 charged with a net bag in which zeolite stone grains are stuck, and deaerated by a vacuum pump P to be evacuated; making the connection port 70 communicate with the inside of the bag-like body 5 and the inside of the pressure vessel 7 while opening its auxiliary valve; and sending the gas in the bag-like body 5 to the pressure vessel 7 by negative pressure in the pressure vessel 7 so as to make the zeolite stone grains in the vessel 7 adsorb the gas. <P>COPYRIGHT: (C)2008,JPO&INPIT

Description

本発明は檜葉から抽出した芳香物質のバイオガス(フィトンチッドガス)を、粉末状または小塊状のゼオライトに吸着保持せしめて、このバイオガスを吸着させたゼオライトを、果実・野菜類の貯蔵に際して装填しておくようにすることで、果実・野菜類の鮮度を保持せしめるように用いる鮮度保持剤の製造方法と製造装置についての改良に関する。   In the present invention, a biogas (phytoncide gas) of an aromatic substance extracted from a bamboo leaf is adsorbed and held in a powdery or small block of zeolite, and the zeolite adsorbed with the biogas is loaded when storing fruits and vegetables. It is related with the improvement about the manufacturing method and manufacturing apparatus of the freshness-keeping agent used so that the freshness of fruit and vegetables may be kept.

松・杉のような針葉樹の葉から、水蒸気の供給で抽出されるガス状の芳香物質を、ゼオライト(沸石)に吸着させて、その吸着体であるゼオライトをもって、果実・野菜類の貯蔵・保存に際し、鮮度保持剤として用いる手段は、特公平7−25647号公報により知られている。   Gaseous aromatic substances extracted by supplying steam from pine and cedar leaves are adsorbed to zeolite (zeolite), and the adsorbent zeolite is used to store and preserve fruits and vegetables. In this case, means used as a freshness-preserving agent is known from Japanese Patent Publication No. 7-25647.

この手段に用いる鮮度保持剤は、蒸し釜に装入した針葉樹の葉に対し、ボイラーで発生させた水蒸気を供給して、それにより抽出されて水蒸気とともに蒸し釜から排出されるガス状の芳香物質(バイオガス)を、気液分離装置に導き冷却することで、混在している水蒸気を除去して、バイオガスだけに分離し、これを、ゼオライトを装入しておくゼオライトタンク内に供給することで、そのタンク内のゼオライトに吸着させることで造られる鮮度保持剤である。   The freshness-preserving agent used in this means is a gaseous fragrance that is extracted from the steamer with the steam by supplying steam generated by the boiler to the leaves of the conifers charged in the steamer. (Biogas) is guided to the gas-liquid separator and cooled to remove the mixed water vapor and separate only into the biogas, and this is supplied into the zeolite tank in which the zeolite is charged. Therefore, it is a freshness-preserving agent produced by adsorbing to the zeolite in the tank.

この手段により得られる鮮度保持剤は、果実・野菜類の鮮度の保持に効果のあるものであるが、その得られる鮮度保持の効果が製造された鮮度保持剤の製品によりバラツキがある問題がある。これは製品のゼオライトに吸着させたバイオガスのゼオライトに対する吸着量にバラツキがある、ということである。   The freshness-preserving agent obtained by this means is effective in maintaining the freshness of fruits and vegetables, but there is a problem that the freshness-retaining effect obtained varies with the product of the freshness-preserving agent produced. . This means that there is variation in the amount of biogas adsorbed on the zeolite of the product.

また、抽出してゼオライトが装入されているゼオライトタンクに送給するバイオガスの、ゼオライトに対する吸着のロスが多く、鮮度保持剤の生産の効率が悪い問題がある。これは、抽出してゼオライトタンクに供給するバイオガスの、タンク内のゼオライトに対する接触が、連続して行なわれていくように、ゼオライトタンクに排気口を設けておくと、バイオガスが吸着したゼオライトに、引き続き送給されてくるバイオガスが接触していくときに、排気口からバイオガスの一部が外部に放出されて飛散するようになることでロスが多くなり、また、排出口をなくして、ゼオライトタンクを密閉しておくと、抽出されて、ゼオライトタンク内に送給されるバイオガスの、ゼオライトタンク内におけるガス圧が高くなってきたときに、蒸し釜の側に逆流するようになって、ゼオライトタンクに対するバイオガスの供給を阻害し、蒸し釜からの外部飛散を生ぜしめ、ゼオライトに対するバイオガスの吸着の効率を低下させるようになることによる。
特公平7−25647号公報
In addition, there is a problem that the biogas fed to the zeolite tank extracted and fed to the zeolite tank has a large adsorption loss to the zeolite and the production efficiency of the freshness-preserving agent is poor. This is because, if an exhaust port is provided in the zeolite tank so that the biogas extracted and supplied to the zeolite tank is continuously contacted with the zeolite in the tank, the zeolite adsorbed with the biogas In addition, when biogas that is continuously fed comes into contact, a part of the biogas is released from the exhaust port and scattered, increasing the loss and eliminating the exhaust port. If the zeolite tank is sealed, the biogas extracted and fed into the zeolite tank will flow back to the steamer when the gas pressure in the zeolite tank increases. This hinders the supply of biogas to the zeolite tank, causes external scattering from the steamer, and reduces the efficiency of biogas adsorption on zeolite. According to the to become that allow.
Japanese Patent Publication No. 7-25647

本発明において解決しようとする課題は、蒸し釜に装入した檜葉から水蒸気の供給により抽出したフィトンチッドガスのバイオガスを、ロスがなく効率よくゼオライトに吸着させるようにするとともに、そのフィトンチッドガスを吸着させたゼオライトにより調整する鮮度保持剤の製品に、鮮度保持能力・機能にバラツキが無いものとすることにある。   The problem to be solved in the present invention is to allow the biogas of phytoncide gas extracted by supplying steam from the koji leaves charged in the steamer to be efficiently adsorbed to the zeolite without loss, and to adsorb the phytoncide gas. The product of the freshness-keeping agent that is adjusted by the zeolite that has been made is to have no variation in freshness-holding ability and function.

本発明においては、上述の課題を解決するための手段として、
蒸し釜に、檜葉を充填し水蒸気を供給して生成せしめるフィトンチッドガスを、その蒸し釜に接続せしめた内容積が拡縮する袋状体(5)内に収集せしめ、その収集したフィトンチッドガスを、袋状体5に填めた状態として、その袋状体(5)の口(50)を、ゼオライト石粒を填めた網目袋を装入して真空ポンプ(P)により真空に脱気した圧力釜(7)の接続口(70)に接続し、その接続口(70)に付設のバルブを開いて袋状体(5)内と圧力釜(7)内とを連通させ、袋状体(5)内のガスを圧力釜(7)内の負圧によりその釜(7)内に送給して、その釜(7)内のゼオライト石粒に吸着させる工程を行ない、この工程を終えたところで、圧力釜(7)を開き、ゼオライト石粒を網目袋ごと取り出して、気密性のガスバリヤ袋に装入し、その袋を密封して鮮度保持剤の製品とすることを特徴とする檜葉から抽出したフィトンチッドガスを用いる果実・野菜類の鮮度保持剤の製造方法。
蒸し釜に、檜葉を充填し水蒸気を供給して生成せしめるフィトンチッドガスを、その蒸し釜に接続する抽出管の先端側に設けた接続口に対し吐出口を接続せしめた内容積が拡縮する袋状体(5)内に収集せしめ、その袋状体(5)内に収集せしめた前記ガスを真空ポンプ(P)で引き出してボンベ(B)に詰め換えて保存しておき、別に、焼成して小粒に造成したゼオライト鉱石を、所定単位重量に計量して、その単位重量ごとに対応する容量の網目袋に充填して多数袋用意しておき、このゼオライト石粒を填めた網目袋を、圧力釜(7)の中に適宜数積み重ねて装入し、その圧力釜(7)の蓋を閉じ、その釜(7)内を真空ポンプ(P)により真空に脱気し、次いで、前記ボンベ(B)に填めておいたフィトンチッドガスを袋状体(5)に詰め替えて、その袋状体(5)の口(50)を、この真空に脱気した圧力釜(7)の接続口(70)に、接続し、その接続口(70)に付設のバルブを開いて袋状体(5)内と圧力釜(7)内とを連通させ、袋状体(5)内のガスを圧力釜(7)内の負圧によりその釜(7)内に送給して、その釜(7)内のゼオライト石粒に吸着させる工程を行ない、この工程を終えたところで、圧力釜(7)を開き、ゼオライト石粒を網目袋ごと取り出して、気密性のガスバリヤ袋に装入し、その袋を密封して鮮度保持剤の製品とすることを特徴とする檜葉から抽出したフィトンチッドガスを用いる果実・野菜類の鮮度保持剤の製造方法を提起するものである。
また、これに併せて、上記鮮度保持剤の製造方法の実施に用いる鮮度保持剤の製造装置として、
檜葉を詰めて供給する水蒸気によりフィトンチッドガスを生成せしめる蒸し釜(2)と、蒸し釜(2)に水蒸気を供給するボイラー(1)と、蒸し釜(2)に接続してその釜(2)内に生成してくるフィトンチッドガスを抽き出す抽出管(3)と、その抽出管(3)の先端側に設けた接続口(30)に、口(50)を装脱自在に接続しておく大径の袋状体(5)と、調整して粒状に造成したゼオライト石粒を装填して内部を真空に脱気する圧力釜(7)と、内部を真空に脱気した圧力釜(7)に、フィトンチッドガスが填められた袋状体(5)の口(50)を接続するよう設けておく接続口(70)と、からなる檜葉から抽出したフィトンチッドガスを用いる果実・野菜類の鮮度保持剤の製造装置を提起するものである。
In the present invention, as means for solving the above-described problems,
The phytoncide gas, which is generated by filling the steamed leaves and supplying water vapor to the steamer, is collected in the bag-like body (5) connected to the steamer, and the collected phytoncide gas is collected in the bag. In the state of being packed in the body 5, the mouth (50) of the bag-like body (5) is inserted into a mesh bag filled with zeolite stone particles and depressurized to vacuum by a vacuum pump (P) ( 7) is connected to the connection port (70), and a valve attached to the connection port (70) is opened so that the inside of the bag-like body (5) communicates with the inside of the pressure hook (7). The gas inside was fed into the kettle (7) by the negative pressure in the pressure kettle (7) and adsorbed on the zeolite stone particles in the kettle (7). Open the pressure cooker (7) and remove the zeolite stone particles together with the mesh bag into an airtight gas barrier bag. Input, and method for producing freshness retaining agent for fruit and vegetables using phytoncide gas extracted from hiba, characterized in that the product freshness keeping agent was sealed the bag.
A phytoncide gas that is generated by filling the steamed leaves and supplying water vapor to the steaming pot, and the inner volume of the extraction port connected to the steaming pot connected to the tip of the extraction pipe is expanded and contracted. Collect the gas in the body (5), draw out the gas collected in the bag-like body (5) with a vacuum pump (P), refill it into a cylinder (B), store it, and fire it separately. Zeolite ore formed into small grains is weighed to a predetermined unit weight, filled into a mesh bag with a capacity corresponding to each unit weight, and a large number of bags are prepared. An appropriate number of stacks are inserted into the hook (7), the lid of the pressure hook (7) is closed, the inside of the pot (7) is evacuated to vacuum by a vacuum pump (P), and then the cylinder ( B) The phytoncide gas filled in B) into the bag-like body (5) Instead, the port (50) of the bag-like body (5) is connected to the connection port (70) of the pressure cooker (7) deaerated to this vacuum, and a valve attached to the connection port (70). Is opened to allow the inside of the bag-like body (5) to communicate with the inside of the pressure hook (7), and the gas in the bag-like body (5) is fed into the hook (7) by the negative pressure in the pressure hook (7). And the adsorption stone particles in the kettle (7) are adsorbed, and when this process is completed, the pressure kettle (7) is opened, the zeolite stone particles are taken out together with the mesh bag, and an airtight gas barrier is formed. The present invention proposes a method for producing a freshness-keeping agent for fruits and vegetables using phytoncide gas extracted from bamboo leaves, which is inserted into a bag and sealed to produce a freshness-keeping product.
In addition, in addition to this, as a manufacturing apparatus for a freshness-keeping agent used in the implementation of the method for producing the freshness-keeping agent,
Steamer (2) for generating phytoncide gas by steam supplied after filling with straw leaves, boiler (1) for supplying steam to steamer (2), and steamer (2) connected to steamer (2) The mouth (50) is detachably connected to the extraction pipe (3) for extracting the phytoncide gas generated inside and the connection port (30) provided on the distal end side of the extraction pipe (3). A large-diameter bag-like body (5) to be placed, a pressure cooker (7) that is charged with zeolite stones that have been adjusted to be granulated and the inside is evacuated to a vacuum, and a pressure cooker that is evacuated to a vacuum ( 7) a connection port (70) provided to connect the mouth (50) of the bag-like body (5) filled with phytoncide gas, and a fruit / vegetables using phytoncide gas extracted from the bamboo leaf An apparatus for producing a freshness-preserving agent is proposed.

本発明手段においては、果実・野菜類の鮮度保持に効果のある針葉樹の葉から抽出するバイオガスのフィトンチッドガスを収集するのに、蒸し釜に檜葉を填めて水蒸気を供給して生成せしめる蒸し釜に接続したバイオガスの抽出管の先端側に、大径の風船状に成形した袋状体の口を接続しておいて、この袋状体内に生成してくるバイオガスを収集せしめて、これをボンベに移し換えて保存しておき、このバイオガスを吸着させて、芳香物質の担体とするゼオライトは、その鉱石を、焼成して小径のゼオライト石粒に調整して、これを単位重量に計量して網目袋に装填しておき、これを圧力釜に詰めて、その釜内を真空に脱気したところに、ボンベからバイオガスを移し換えた袋状体を接続して、その袋状体内のバイオガスを、時間をかけてゼオライト石粒に吸着させ、このガスの吸着を終えたゼオライト石粒を網目袋ごと圧力釜から取り出して、その袋ごと気密性の袋に詰めて密封しておき、使用するときに、密封袋から取出し、野菜・果実類を詰めた箱の中に、網目袋ごと装入するようにしていることから、檜葉から抽出したバイオガスを、ロスがなく収集でき、かつ、そのガスをロスのない状態で、担体のゼオライト石粒に対しそれの吸着能力の限度まで吸着させるようになるので、鮮度保持の機能を充分に発揮する鮮度保持剤を、その鮮度保持の機能にバラツキのない製品として製造し得るようになる。   In the means of the present invention, in order to collect phytoncide gas of biogas extracted from the leaves of coniferous trees effective in maintaining the freshness of fruits and vegetables, a steaming pot is formed by filling a steaming pot and supplying steam to supply steam. The mouth of the bag-shaped body shaped like a large balloon is connected to the tip of the biogas extraction tube connected to the tube, and the biogas generated in this bag-shaped body is collected, The zeolite used as an aromatic substance carrier by adsorbing this biogas and storing it in a cylinder is calcined to adjust the ore to small-diameter zeolite stones. Weigh and load it into a mesh bag, pack it in a pressure cooker, degas the inside of the kettle to a vacuum, connect a bag-like body to which biogas has been transferred from the cylinder, and Take the biogas in your body over time The zeolite stone particles that have been adsorbed on the light stone particles and have been adsorbed on the gas are taken out from the pressure kettle together with the mesh bag, packed in an airtight bag together with the bag, and sealed from the sealed bag when used. Since the whole mesh bag is placed in a box filled with vegetables and fruits, the biogas extracted from the bamboo leaves can be collected without loss and the gas is not lost. Therefore, it will be adsorbed to the limit of the adsorption capacity of the zeolite stone particles of the carrier, so a freshness-keeping agent that fully exhibits the freshness-keeping function is manufactured as a product that does not vary in the freshness-keeping function. To get.

次に本発明手段の実施の態様を実施例につき図面に従い詳述する。   Next, embodiments of the means of the present invention will be described in detail with reference to the drawings.

図1は、本発明手段の実施に用いるフィトンチッドガスの製造装置の概要を示す展開図で、同図において、1は水蒸気を発生させるボイラー、2は檜葉を釜内に詰め込んで前記ボイラー1から供給する水蒸気により檜葉からフィトンチッドガスを抽出する蒸し釜、3はこの蒸し釜2内に発生する水蒸気およびフィトンチッドガスを抽き出す抽出管、4はその抽出管3の中間部に設けた蛇管状部を包み込んで冷却する冷却器、5は前記抽出管3の先端側に設けた接続口30に接続した大径の風船状の袋状体を示す。   FIG. 1 is a developed view showing an outline of a phytoncide gas production apparatus used for implementing the means of the present invention. In the figure, 1 is a boiler for generating water vapor, 2 is packed with straw leaves in a kettle, and is supplied from the boiler 1. 3 is an extraction pipe for extracting steam and phytoncide gas generated in the steamer 2, and 4 is a serpentine tubular portion provided in the middle of the extraction pipe 3. A cooler 5 for wrapping and cooling indicates a large-sized balloon-like bag-like body connected to a connection port 30 provided on the distal end side of the extraction tube 3.

ボイラー1は焚口に設けたバーナーによりタンク内の水を沸かして発生させる水蒸気を蒸気導出管10から噴出させる通常のものである。   The boiler 1 is a normal one in which water vapor generated by boiling water in a tank is ejected from a steam outlet pipe 10 by a burner provided at a mouth.

蒸し釜2は、蓋20を取り外すことで上方に開放するドラム状の胴部内に、檜葉を積み重ねて装入し、蓋20を閉じた状態で、底部から供給する高圧の水蒸気により詰め込んで檜葉からフィトンチッドガスのバイオガスを抽出する通常の蒸し釜であり、発生させたバイオガスおよび水蒸気を抽き出す抽出管3が、蓋20の頂部に接続させてある。   In the steamer 2, the cocoon leaves are stacked and loaded in a drum-shaped body part that opens upward by removing the lid 20, and the lid 20 is closed and packed with the high-pressure steam supplied from the bottom, It is a normal steamer for extracting biogas of phytoncide gas, and an extraction pipe 3 for extracting the generated biogas and water vapor is connected to the top of the lid 20.

冷却器4は、前記抽出管3により抽き出されるバイオガス及び水蒸気を、冷却によって、バイオガスと凝結してくる水蒸気とに分ける冷却手段であり、抽出管3の途中に設けた蛇管状部を包み込む水槽に形成してあって、底部には、抽出管3の中間の蛇管状部に凝縮して捕集される凝縮水を抽出管3から取り出し分離する水受け40が装設してある。   The cooler 4 is a cooling means that divides the biogas and water vapor extracted by the extraction pipe 3 into biogas and water vapor condensed by cooling, and is a serpentine tubular portion provided in the middle of the extraction pipe 3. The bottom is provided with a water receiver 40 for extracting and separating condensed water collected and condensed in a meander-shaped tubular portion in the middle of the extraction pipe 3 from the extraction pipe 3. .

抽出管3の先端側に設けた接続口30は、袋状体5の口50を、装脱自在に接続するニップル状のもので、抽出管3に対する連通をオン・オフするバルブ31が装備され、かつ、多連に並設してある。   The connection port 30 provided on the distal end side of the extraction pipe 3 is a nipple-like one that detachably connects the port 50 of the bag-like body 5, and is equipped with a valve 31 that turns on and off communication with the extraction pipe 3. And it is arranged in parallel.

袋状体5は、畳まれた状態の周壁が、外側に張り出すことで膨らむ気密な袋であり、この例においては、合成樹脂材のシートを所定形状に型どりして、それらを、はぎ合わせて接着することで、大径の風船状に成形し、それに管状の口50を付設して構成してあり、内容が空のときは、周壁が平らに畳まれて平板状となり、管状の口50から内部に気体を注入すると、畳まれていた周壁が張り出して風船状に膨らむようになる。   The bag-like body 5 is an air-tight bag in which a folded peripheral wall bulges by projecting to the outside. In this example, a sheet of synthetic resin material is shaped into a predetermined shape, and they are joined together. It is formed by bonding to form a large-diameter balloon, and a tubular port 50 is attached thereto. When the content is empty, the peripheral wall is flatly folded into a flat plate shape. When the gas is injected from the inside, the folded peripheral wall protrudes and expands like a balloon.

図2は、上述の製造装置により生成したバイオガスを、ゼオライト石粒に吸着させる装置の概要の展開図で、Wは、前記フィトンチッドガスの製造装置で生成して袋状体5に収集したフィトンチッドガスを、袋状体5に詰め込まれた状態で一時貯留しておく貯留室、Yはフィトンチッドガスのバイオガスを、前述の網目袋に填めたゼオライト石粒に吸着させる作業室、aは貯留室Wに付設の温度計、bは貯留室Wに付設せるヒータ、cは貯留室Wと作業室Yとを仕切る隔壁、dは作業室Yに装備せる換気扇、eは貯留室W内に設置せる袋状体5の懸架用の架枠、5…はこの架枠eに吊り下げたバイオガスが詰められた袋状体、Cは袋状体5に填められたバイオガスをボンベBに填め替えるよう作業室に設置したコンプレッサ、60はそのコンプレッサCの抽き口、61は吐出口、7は、網目袋に詰め込まれたゼオライト石粒を、網目袋ごと詰め込んで、真空状態に曝らすようにするために作業室Yに設置した圧力釜、Pはその圧力釜7内を真空に脱気する真空ポンプ、70はその圧力釜7の接続口、vはその接続口70に付設の開閉バルブ、5’は前記ボンベBからバイオガスが詰め替えられた袋状体を示している。   FIG. 2 is a development view of the outline of an apparatus for adsorbing biogas generated by the above-described manufacturing apparatus to zeolite stone particles. W is a phytoncide generated by the phytoncide gas manufacturing apparatus and collected in the bag-like body 5. A storage chamber for temporarily storing gas in a state packed in the bag-like body 5, Y is a working chamber for adsorbing the biogas of phytoncide gas to the zeolite stone particles packed in the mesh bag, and a is a storage chamber A thermometer attached to W, b is a heater attached to the storage chamber W, c is a partition wall that partitions the storage chamber W and the work chamber Y, d is a ventilation fan installed in the work chamber Y, and e is installed in the storage chamber W. A suspension frame of the bag-like body 5, 5... Is a bag-like body filled with biogas suspended on this frame e, and C is refilled with the cylinder B with the biogas filled in the bag-like body 5. The compressor installed in the work room, 60 Lessa C extraction port, 61 is the discharge port, 7 is the pressure installed in the working chamber Y so that the zeolite stone particles packed in the mesh bag are packed together and exposed to a vacuum state. A pot, P is a vacuum pump for evacuating the pressure pot 7 to a vacuum, 70 is a connection port of the pressure pot 7, v is an open / close valve attached to the connection port 70, 5 'is biogas from the cylinder B The refilled bag-like body is shown.

貯留室Wは、温度計aにより検出される室温に制御されて作動するヒータにより、室温が常時36度C〜28度Cの範囲の夏の状態に保持されている。また、作業室Yは、温度計aにより検出される温度によって制御される換気扇dの作動で、室温が20度C前後の常温に保持されている。   The storage room W is kept in a summer state where the room temperature is always in the range of 36 degrees C to 28 degrees C by a heater that is controlled to operate at the room temperature detected by the thermometer a. Further, the working room Y is kept at a room temperature of about 20 degrees C by the operation of the ventilation fan d controlled by the temperature detected by the thermometer a.

架枠eは、バイオガスの製造装置により生成したバイオガスを収集せしめた袋状体5を、懸架して貯留・保存しておく架台であり、バイオガスが詰められた袋状体5を、それの口50を緊縛した状態で、ハンガーfにより、この架枠eに吊り下げられる。   The frame e is a frame for suspending and storing and storing the bag-like body 5 in which the biogas generated by the biogas production apparatus is collected, and the bag-like body 5 packed with biogas, With its mouth 50 tightly bound, it is suspended from the frame e by a hanger f.

コンプレッサCは、袋状体5に詰められたバイオガスをボンベBに詰め替えて、そのボンベBにより保存しておくためのもので、作業室Yに設置してある。そして、それの抽き口70は、隔壁cに設けた窓孔を介して貯留室W内に突出させてあり、貯留室Wにおいて、そこに貯留してある袋状体5の口50が接続するようにしてある。また吐出口61は、作業室YにおいてボンベBに接続するようにしている。   The compressor C is for refilling the biogas packed in the bag-like body 5 into the cylinder B and storing it in the cylinder B, and is installed in the working chamber Y. And the extraction port 70 is protruded in the storage chamber W through the window hole provided in the partition wall c, and the port 50 of the bag-like body 5 stored therein is connected in the storage chamber W. I have to do it. Further, the discharge port 61 is connected to the cylinder B in the working chamber Y.

圧力釜7は、ゼオライト鉱石を約400度C程度に焼成して10ミリ〜5ミリ程の小粒に調整しておいたゼオライト石粒に、バイオガスを吸着させるときに、そのゼオライト石粒を、その周面に接触している機体を除去した状態にしておくためのもので、網目袋に計量して充填しておいたゼオライト石粒を堆積状態に詰め込むドラム状の胴部には、真空ポンプPに接続する抽き口70が付設され、上面には開閉する蓋板71が装着されている通常のものであり、蓋板71を開放して、内部に網目袋に填めたゼオライト石粒を網目袋ごと詰め込み、蓋板71を閉じ密閉して抽き口70に接続した真空ポンプPの作動により内部を真空に脱気して、ゼオライト石粒に接触している空気を排除しておくように使用する。   When the pressure stoner 7 adsorbs the biogas to the zeolite stone particles that have been baked to about 400 degrees C and adjusted to a small particle size of about 10 mm to 5 mm, A vacuum pump is installed in the drum-shaped body to pack the zeolite stone particles weighed and packed in the mesh bag into a piled state. A drawing port 70 connected to P is attached, and a lid plate 71 that opens and closes is mounted on the upper surface. The lid plate 71 is opened, and the zeolite stone particles filled in the mesh bag are inside. The mesh bag is packed together, the lid 71 is closed and sealed, and the vacuum pump P connected to the extraction port 70 is evacuated to evacuate the inside so as to eliminate the air in contact with the zeolite stone particles. Used for.

袋状体5’は、脱気した圧力釜7内にバイオガスを注入して、その釜内のゼオライト石粒に接触させるためのもので、ボンベBに詰められているバイオガスを填め替えたものであり、この袋状体5’の口50を抽き口70に嵌着して、抽き口70に設けた開閉バルブvを開放することで、この袋状体5’内のバイオガスを圧力釜7内に送り込み、ゼオライト石粒に吸着させるように用いられる。   The bag-like body 5 ′ is for injecting biogas into the degassed pressure kettle 7 and bringing it into contact with the zeolite stone grains in the kettle, and the biogas filled in the cylinder B is refilled. By inserting the opening 50 of the bag-like body 5 ′ into the extraction port 70 and opening the opening / closing valve v provided in the extraction port 70, the biogas in the bag-like body 5 ′ is opened. Is fed into the pressure cooker 7 and used to adsorb to the zeolite stone particles.

次に、上述の装置を用いて行うバイオガスの生成・収集およびそれをゼオライト石粒に吸着させて鮮度保持剤を造成する実施例を説明する。   Next, an example of producing and collecting biogas using the above-described apparatus and adsorbing it to zeolite stone particles to create a freshness-keeping agent will be described.

まず、採取してきた檜葉を蒸し釜2に詰める。次いで、蒸し釜2の蓋20を閉め、蒸し釜2内に、ボイラー1で生成した高圧の水蒸気を、その蒸し釜2の底から送り込み、蒸し釜2内の檜葉を徐々に蒸す。   First, the collected koji leaves are packed in the steaming pot 2. Next, the lid 20 of the steamer 2 is closed, and high-pressure steam generated by the boiler 1 is fed into the steamer 2 from the bottom of the steamer 2, and the straw leaves in the steamer 2 are gradually steamed.

これにより蒸し釜2の蓋20の頂部に接続した抽管3から噴き出してくる水蒸気および檜葉から生成してくるフィトンチッドガスを、抽出管3の中間部を包み込む冷却器4により冷却して、凝縮してくる水および蒸留液は、抽出管3から引き抜いて分離し、凝縮しないフィトンチッドガスを、抽出管3の先端側に導き、その先端側に接続しておく袋状体5内に詰め込み、これに収集させる。   As a result, the water vapor ejected from the extraction pipe 3 connected to the top of the lid 20 of the steamer 2 and the phytoncide gas generated from the bamboo leaf are cooled and condensed by the cooler 4 enclosing the middle part of the extraction pipe 3. The incoming water and distillate are extracted from the extraction tube 3 and separated, and the phytoncide gas that does not condense is guided to the distal end side of the extraction tube 3 and packed into the bag-like body 5 that is connected to the distal end side. Let them collect.

この袋状体5は、周壁が折り畳まれて平らに潰れた状態から、注入されてくるフィトンチッドガスのガス圧で、周壁がひらき、大径の風船状に一杯に膨らんだところで、抽出管3の接続口30から外し、これを真空ポンプPで引き出し、コンプレッサCによりボンベB内に加圧して填め込み、ボンベに移し替えて保存しておく。   This bag-like body 5 is formed in a state in which the peripheral wall is folded and flattened from the state where the peripheral wall is folded flat, and the peripheral wall is opened by the gas pressure of the injected phytoncide gas. It is removed from the connection port 30, pulled out by the vacuum pump P, pressurized and packed in the cylinder B by the compressor C, transferred to the cylinder and stored.

次にフィトンチッドガスを吸着させるゼオライト石粒を調整する工程について説明する。
400度C程度に焼成して直径5ミリ程度の小粒に造成したゼオライト鉱石を、篩別・精選して石粉・屑を除き、所定の単位重量(約50g)に計量する。ゼオライト鉱石は、焼成により吸着の機能が著しく向上する。このゼオライト鉱石の粒状化は、小径のものほど良いが、取り扱い上5ミリ程度が望ましい。
Next, the process of adjusting the zeolite stone particles to adsorb the phytoncide gas will be described.
Zeolite ore that has been baked to about 400 ° C and formed into small granules with a diameter of about 5 mm is sieved and carefully selected to remove stone dust and debris and weighed to a predetermined unit weight (about 50 g). Zeolite ore is remarkably improved in adsorption function by firing. As for the granulation of the zeolite ore, the smaller the diameter, the better, but about 5 mm is desirable for handling.

計量した単位重量のゼオライト石粒を、網目袋に装填する。網目袋の網目は、填め込んだゼオライト石粒が流出しない程度とし、出来るだけ通気性のよいものとする。ゼオライトは、この網目袋に詰め込んだ状態として多数袋用意しておく。   A weighed unit weight of zeolite stone is loaded into a mesh bag. The mesh of the mesh bag should be such that the filled zeolite stone particles do not flow out and be as breathable as possible. A large number of zeolites are prepared as packed in the mesh bag.

次に、このゼオライトに対しフィトンチッドガスを吸着させる工程について説明する。   Next, the process of adsorbing phytoncide gas to this zeolite will be described.

上述の如く調整したゼオライト石粒を詰めた網目袋を、所定数束にまとめ、その束を、別に用意しておく圧力釜(真空釜)7の内部に、適宜段数に重ねて填めこみ、圧力釜7を密封する。   The mesh bags packed with zeolite stone particles adjusted as described above are collected into a predetermined number of bundles, and the bundles are packed in a pressure cooker (vacuum cooker) 7 prepared separately and stacked in an appropriate number of stages. The kettle 7 is sealed.

次に、圧力釜7内を、真空ポンプPにより真空に脱気し、減圧状態にする。この真空びきは、40分以上続け、これにより、ゼオライトの吸着面の全てが、真空の脱気した減圧状態の雰囲気に曝されるようにする。   Next, the inside of the pressure cooker 7 is evacuated to a reduced pressure state by the vacuum pump P. This vacuuming lasts for more than 40 minutes, so that all of the zeolite adsorption surface is exposed to a vacuum degassed and depressurized atmosphere.

この所定時間の真空びきが終了したところで、圧力釜7に、フィトンチッドガスを供給する。この供給は、檜葉から抽出してボンベに填め込んで保存しておいたフィトンチッドガスを、ボンベBから畳まれた状態の袋状体5に移し換え、その移し換えた袋状体5の口50を、圧力釜7に設けておく接続口70に接続し、その接続口70に設けておくバルブを開いて、袋状体5を圧力釜7に連通させる。この圧力釜7の接続口70に接続する袋状体5は、収集したガスをボンベBに移し換える前の、袋状体5をそのまま接続してもよい。   When this predetermined period of time is over, phytoncide gas is supplied to the pressure cooker 7. In this supply, the phytoncide gas extracted from the bamboo leaf and stored in the cylinder is transferred from the cylinder B to the folded bag 5 and the mouth 50 of the transferred bag 5 is transferred. Is connected to a connection port 70 provided in the pressure cooker 7, and a valve provided in the connection port 70 is opened to allow the bag-like body 5 to communicate with the pressure cooker 7. The bag-like body 5 connected to the connection port 70 of the pressure cooker 7 may be directly connected to the bag-like body 5 before the collected gas is transferred to the cylinder B.

これにより、袋状体5内のフィトンチッドガスは圧力釜7内の負圧より吸引されてその釜7内に送り込まれ、その送り込まれたガスは、圧力釜7内に填め込んでおいたゼオライト石粒に接触して吸着されていく。   As a result, the phytoncide gas in the bag-like body 5 is sucked in from the negative pressure in the pressure cooker 7 and is sent into the kettle 7, and the fed-in gas is the zeolite stone that is filled in the pressure cooker 7. It is adsorbed in contact with the grains.

このゼオライト石粒に対するフィトンチッドガスの吸着が充分に行われるようにするために、圧力釜にフィトンチッドガスが填められた袋状体5を接続してしておく工程は、約1時間程度続け、ゆっくりと時間をかけて充分に吸着させる。   In order to sufficiently absorb the phytoncide gas to the zeolite stone particles, the step of connecting the bag-like body 5 filled with the phytoncide gas to the pressure kettle is continued for about 1 hour, and slowly And take sufficient time to adsorb.

この吸着工程が終えたところで、圧力釜を開き、素早くゼオライト石粒を、網目袋ごとに取り出し、束ねた網目袋ごとに、気密性のガスバリア袋に装入し、そのガスバリア袋の口をシーラーによりシール密封し、これにより鮮度保持剤の製品とする。   When this adsorption process is completed, the pressure cooker is opened, and the zeolite stone particles are quickly taken out for each mesh bag, and each bundled mesh bag is inserted into an airtight gas barrier bag, and the mouth of the gas barrier bag is sealed with a sealer. Seal and seal to make a product of freshness-preserving agent.

この鮮度保持剤を使用するとき、例えば、果実・野菜類の生産者が、果実等を箱詰めして出荷する際に、その箱詰めした果実類の鮮度を保持させるために用いる場合にあっては、上述のガスバリア袋を開封して、フィトンチッドガスを吸着させたゼオライト石粒が填められている網目袋を取りだし、その網目袋ごと果実類を詰めた箱内に入れ込み、その箱の外周を気密性の強い包装紙で包み込み密封するように使用する。   When using this freshness-keeping agent, for example, when the producer of fruits and vegetables is used to hold the freshness of the boxed fruits when shipping the boxed fruits, etc. Open the gas barrier bag mentioned above, take out the mesh bag filled with zeolite stone particles adsorbed with phytoncide gas, put the mesh bag into a box filled with fruits, and seal the outer periphery of the box with airtightness. Wrap with strong wrapping paper and use to seal.

本発明手段の実施に使用するフィトンチッドガスの製造装置の概要を示す展開図である。It is an expanded view which shows the outline | summary of the manufacturing apparatus of the phytoncide gas used for implementation of the means of this invention. 本発明手段の実施に用いる鮮度保持剤の製造装置の概要を示す展開図である。It is an expanded view which shows the outline | summary of the manufacturing apparatus of the freshness-keeping agent used for implementation of this invention means.

符号の説明Explanation of symbols

B…ボンベ、C…コンプレッサ、P…真空ポンプ、W…貯留室、Y…作業室、a…温度計、b…ヒータ、c…隔壁、d…換気扇、e…架枠、f…ハンガー、v…開閉バルブ、1…ボイラー、10…蒸気導出管、2…蒸し釜、20…蓋、3…抽出管、30…接続口、31…バルブ、4…冷却器、40…水受け、5・5’…袋状体、50…袋状体の口、60…抽き口、61…吐出口、7…圧力釜、70…接続口・抽き口、71…蓋板。   B ... cylinder, C ... compressor, P ... vacuum pump, W ... storage chamber, Y ... work chamber, a ... thermometer, b ... heater, c ... partition, d ... ventilation fan, e ... frame, f ... hanger, v Open / close valve, 1 boiler, 10 steam outlet pipe, 2 steamer, 20 lid, 3 extraction pipe, 30 connection port, 31 valve, 4 cooler, 40 water receptacle, 5/5 '... bag-like body, 50 ... bag-like body opening, 60 ... extraction port, 61 ... discharge port, 7 ... pressure cooker, 70 ... connection port / extraction port, 71 ... lid plate.

Claims (3)

蒸し釜に、檜葉を充填し水蒸気を供給して生成せしめるフィトンチッドガスを、その蒸し釜に接続せしめた内容積が拡縮する袋状体(5)内に収集せしめ、その収集したフィトンチッドガスを、袋状体5に填めた状態として、その袋状体(5)の口(50)を、ゼオライト石粒を填めた網目袋を装入して真空ポンプ(P)により真空に脱気した圧力釜(7)の接続口(70)に接続し、その接続口(70)に付設のバルブを開いて袋状体(5)内と圧力釜(7)内とを連通させ、袋状体(5)内のガスを圧力釜(7)内の負圧によりその釜(7)内に送給して、その釜(7)内のゼオライト石粒に吸着させる工程を行ない、この工程を終えたところで、圧力釜(7)を開き、ゼオライト石粒を網目袋ごと取り出して、気密性のガスバリヤ袋に装入し、その袋を密封して鮮度保持剤の製品とすることを特徴とする檜葉から抽出したフィトンチッドガスを用いる果実・野菜類の鮮度保持剤の製造方法。   The phytoncide gas, which is formed by filling the steamed leaves and supplying water vapor to the steaming pot, is collected in the bag-like body (5) connected to the steaming pot, and the collected phytoncide gas is collected in the bag. In the state of being packed in the body 5, the mouth (50) of the bag-like body (5) is inserted into a mesh bag filled with zeolite stone particles and depressurized to vacuum by a vacuum pump (P) ( 7) is connected to the connection port (70), and a valve attached to the connection port (70) is opened so that the inside of the bag-like body (5) communicates with the inside of the pressure hook (7). The gas inside was fed into the kettle (7) by the negative pressure in the pressure kettle (7) and adsorbed on the zeolite stone particles in the kettle (7). Open the pressure cooker (7) and remove the zeolite stone particles together with the mesh bag into an airtight gas barrier bag. Input, and method for producing freshness retaining agent for fruit and vegetables using phytoncide gas extracted from hiba, characterized in that the product freshness keeping agent was sealed the bag. 蒸し釜に、檜葉を充填し水蒸気を供給して生成せしめるフィトンチッドガスを、その蒸し釜に接続する抽出管の先端側に設けた接続口に対し吐出口を接続せしめた内容積が拡縮する袋状体(5)内に収集せしめ、その袋状体(5)内に収集せしめた前記ガスを真空ポンプ(P)で引き出してボンベ(B)に詰め換えて保存しておき、別に、焼成して小粒に造成したゼオライト鉱石を、所定単位重量に計量して、その単位重量ごとに対応する容量の網目袋に充填して多数袋用意しておき、このゼオライト石粒を填めた網目袋を、圧力釜(7)の中に適宜数積み重ねて装入し、その圧力釜(7)の蓋を閉じ、その釜(7)内を真空ポンプ(P)により真空に脱気し、次いで、前記ボンベ(B)に填めておいたフィトンチッドガスを袋状体(5)に詰め替えて、その袋状体(5)の口(50)を、この真空に脱気した圧力釜(7)の接続口(70)に、接続し、その接続口(70)に付設のバルブを開いて袋状体(5)内と圧力釜(7)内とを連通させ、袋状体(5)内のガスを圧力釜(7)内の負圧によりその釜(7)内に送給して、その釜(7)内のゼオライト石粒に吸着させる工程を行ない、この工程を終えたところで、圧力釜(7)を開き、ゼオライト石粒を網目袋ごと取り出して、気密性のガスバリヤ袋に装入し、その袋を密封して鮮度保持剤の製品とすることを特徴とする檜葉から抽出したフィトンチッドガスを用いる果実・野菜類の鮮度保持剤の製造方法。   A phytoncide gas that is generated by filling the steamed leaves and supplying water vapor to the steaming pot, and the inner volume of the extraction port connected to the steaming pot connected to the tip of the extraction pipe is expanded and contracted. Collect the gas in the body (5), draw out the gas collected in the bag-like body (5) with a vacuum pump (P), refill it into a cylinder (B), store it, and fire it separately. Zeolite ore formed into small grains is weighed to a predetermined unit weight, filled into a mesh bag with a capacity corresponding to each unit weight, and a large number of bags are prepared. An appropriate number of stacks are inserted into the hook (7), the lid of the pressure hook (7) is closed, the inside of the pot (7) is evacuated to vacuum by a vacuum pump (P), and then the cylinder ( B) The phytoncide gas filled in B) into the bag-like body (5) Instead, the port (50) of the bag-like body (5) is connected to the connection port (70) of the pressure cooker (7) deaerated to this vacuum, and a valve attached to the connection port (70). Is opened to allow the inside of the bag-like body (5) to communicate with the inside of the pressure hook (7), and the gas in the bag-like body (5) is fed into the hook (7) by the negative pressure in the pressure hook (7). And the adsorption stone particles in the kettle (7) are adsorbed, and when this process is completed, the pressure kettle (7) is opened, the zeolite stone particles are taken out together with the mesh bag, and an airtight gas barrier is formed. A method for producing a freshness-keeping agent for fruits and vegetables using phytoncide gas extracted from bamboo leaves, wherein the bag is sealed and the bag is sealed to obtain a freshness-keeping product. 檜葉を詰めて供給する水蒸気によりフィトンチッドガスを生成せしめる蒸し釜(2)と、蒸し釜(2)に水蒸気を供給するボイラー(1)と、蒸し釜(2)に接続してその釜(2)内に生成してくるフィトンチッドガスを抽き出す抽出管(3)と、その抽出管(3)の先端側に設けた接続口(30)に、口(50)を装脱自在に接続しておく大径の袋状体(5)と、調整して粒状に造成したゼオライト石粒を装填して内部を真空に脱気する圧力釜(7)と、内部を真空に脱気した圧力釜(7)に、フィトンチッドガスが填められた袋状体(5)の口(50)を接続するよう設けておく接続口(70)と、からなる檜葉から抽出したフィトンチッドガスを用いる果実・野菜類の鮮度保持剤の製造装置。   Steamer (2) for generating phytoncide gas by steam supplied after filling with straw leaves, boiler (1) for supplying steam to steamer (2), and steamer (2) connected to steamer (2) The mouth (50) is detachably connected to the extraction pipe (3) for extracting the phytoncide gas generated inside and the connection port (30) provided on the distal end side of the extraction pipe (3). A large-sized bag-like body (5) to be placed, a pressure cooker (7) that is charged with zeolite stone particles that have been adjusted to be granulated and the inside is evacuated to a vacuum, 7) a connection port (70) provided to connect the mouth (50) of the bag-like body (5) filled with phytoncide gas, and a fruit / vegetables using phytoncide gas extracted from cocoon leaves A device for producing a freshness-preserving agent.
JP2006211876A 2006-08-03 2006-08-03 A method and apparatus for producing a freshness-preserving agent for fruits and vegetables using phytoncide gas extracted from bamboo leaves. Active JP4368366B2 (en)

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Publication number Priority date Publication date Assignee Title
CZ303593B6 (en) * 2010-04-12 2013-01-02 Ceská zemedelská univerzita v Praze Device to measure composition and volume of gas and method of making the same

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CZ303593B6 (en) * 2010-04-12 2013-01-02 Ceská zemedelská univerzita v Praze Device to measure composition and volume of gas and method of making the same

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