JP2007325537A - Method for producing aqueous suspension of filtration auxiliary - Google Patents

Method for producing aqueous suspension of filtration auxiliary Download PDF

Info

Publication number
JP2007325537A
JP2007325537A JP2006159110A JP2006159110A JP2007325537A JP 2007325537 A JP2007325537 A JP 2007325537A JP 2006159110 A JP2006159110 A JP 2006159110A JP 2006159110 A JP2006159110 A JP 2006159110A JP 2007325537 A JP2007325537 A JP 2007325537A
Authority
JP
Japan
Prior art keywords
gas
suspension
filter aid
filter
aqueous suspension
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
JP2006159110A
Other languages
Japanese (ja)
Inventor
Yoshitaka Kimura
吉孝 木村
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Asahi Breweries Ltd
Original Assignee
Asahi Breweries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Asahi Breweries Ltd filed Critical Asahi Breweries Ltd
Priority to JP2006159110A priority Critical patent/JP2007325537A/en
Publication of JP2007325537A publication Critical patent/JP2007325537A/en
Withdrawn legal-status Critical Current

Links

Images

Landscapes

  • Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)

Abstract

<P>PROBLEM TO BE SOLVED: To provide a method for producing an aqueous suspension of a filtration auxiliary used for the filtration of a fermented drink, wherein the quantity of a deaeration gas is reduced to lower a cost related to the production of the suspension. <P>SOLUTION: The method for producing the aqueous suspension of the filtration auxiliary is characterized in that the quantity of the deaeration gas such as carbon dioxide, nitrogen gas or helium gas, blown in a process for blowing the deaeration gas to remove oxygen gas from the aqueous suspension of the filtration auxiliary in a mixing tank 21 is determined on the basis of the quantity of the suspension. <P>COPYRIGHT: (C)2008,JPO&INPIT

Description

本発明は、発酵飲料の濾過工程で使用する濾過助剤の水懸濁液を製造する方法に関する。   The present invention relates to a method for producing an aqueous suspension of a filter aid used in a filtration process of a fermented beverage.

ビールや麦芽を原料とする発泡酒などの発酵飲料は酵母を使用して製造される。ビールを例にあげると、ビールは、製麦、仕込み、発酵、熟成、濾過、充填の各工程を経て製造される。発酵工程では、麦汁に酵母が加えられ発酵によって若ビールが生成される。熟成工程では、若ビールが貯酒タンク中で熟成される。濾過工程では、熟成工程で得られたビールから酵母や凝固物が濾過される。濾過されたビールはびん、缶、樽に充填されて製品として出荷される。   Fermented beverages such as happoshu made from beer and malt are produced using yeast. Taking beer as an example, beer is produced through the steps of malting, preparation, fermentation, aging, filtration, and filling. In the fermentation process, yeast is added to wort and young beer is produced by fermentation. In the aging process, young beer is aged in a storage tank. In the filtration step, yeast and coagulum are filtered from the beer obtained in the aging step. The filtered beer is filled into bottles, cans and barrels and shipped as products.

ビールは酸化されると製品の老化が進行し、本来の味覚、香りが損なわれ、品質が低下する。したがって、ビールを製造する各工程においてもビールが酸化されないように十分な配慮がなされている。このようなビールの酸化を抑制する技術は、例えば特許文献1に示される。
特開2000−4866号公報 濾過工程では例えば珪藻土、二酸化ケイ素といった濾過助剤の水懸濁液を使用してビールが濾過される。濾過助剤の水懸濁液は濾過機に供給され使用されるが、濾過工程におけるビールの酸化を抑制するために、前記水懸濁液は酸素を含まないものが求められる。濾過助剤と水とをタンク内で混合して濾過助剤の水懸濁液を製造する際に空気(酸素)が混ざり込む。そこで、タンク下部から炭酸ガス、窒素ガス又はヘリウムガスのような酸化作用を有しないガスを吹き込んで、水懸濁液中から酸素を追い出す方法が採られうる。水懸濁液中の酸素を追い出すために水懸濁液に吹き込まれる炭酸ガス、窒素ガス又はヘリウムガスのようなガスを「脱気ガス」と呼ぶ。現状では、脱気ガスをタンク内に吹き込み、その状況のもとで濾過助剤と水とを投入しているために、大量の脱気ガスが消費される。
When beer is oxidized, aging of the product progresses, the original taste and aroma are impaired, and the quality deteriorates. Therefore, sufficient consideration is given so that beer is not oxidized in each process of producing beer. A technique for suppressing such beer oxidation is disclosed in Patent Document 1, for example.
JP, 2000-4866, A In a filtration process, beer is filtered using the water suspension of filter aids, such as diatomaceous earth and silicon dioxide, for example. The aqueous suspension of the filter aid is supplied to the filter and used, but the aqueous suspension is required not to contain oxygen in order to suppress beer oxidation in the filtration step. Air (oxygen) is mixed when the filter aid and water are mixed in a tank to produce a water suspension of the filter aid. Therefore, a method of expelling oxygen from the aqueous suspension by blowing a gas having no oxidizing action such as carbon dioxide, nitrogen gas or helium gas from the lower part of the tank can be employed. A gas such as carbon dioxide, nitrogen gas or helium gas that is blown into the water suspension to drive out oxygen in the water suspension is referred to as “degassing gas”. At present, a large amount of degassed gas is consumed because degassed gas is blown into the tank and the filter aid and water are introduced under this condition.

本発明は、濾過助剤の水懸濁液を製造する際に用いる脱気ガスの消費量を低減し、前記懸濁液製造に係るコストを低減することを目的とする。   An object of the present invention is to reduce the consumption of degassing gas used when producing an aqueous suspension of a filter aid, and to reduce the cost for producing the suspension.

本発明は、発酵飲料の濾過工程で使用する濾過助剤の水懸濁液を製造する方法に関するものであって、タンクに水を供給する第一の工程、前記タンクに濾過助剤を投入する第二の工程、前記タンクに脱気ガスを吹き込む第三の工程を含み、前記脱気ガスは、前記水懸濁液の生成量に基づく量が吹き込まれることを特徴とする。   The present invention relates to a method for producing an aqueous suspension of a filter aid used in a filtration step of a fermented beverage, the first step of supplying water to a tank, and the filter aid is put into the tank. The method includes a second step and a third step of blowing a degassed gas into the tank, wherein the degassed gas is blown in an amount based on the amount of water suspension generated.

本発明の好適な実施の形態では、前記濾過助剤として珪藻土及びニ酸化ケイ素の少なくとも一種が使用される。また、前記第三の工程は、前記第一の工程及び第二の工程の双方が終了した時点以降に開始される。   In a preferred embodiment of the present invention, at least one of diatomaceous earth and silicon dioxide is used as the filter aid. The third step is started after the time point when both the first step and the second step are completed.

本発明によれば、濾過助剤の水懸濁液を製造する際に用いる脱気ガスの消費量を低減することができ、したがって前記水懸濁液製造に係るコストを低減することができる。   According to the present invention, it is possible to reduce the consumption of the degassing gas used when producing the aqueous suspension of the filter aid, and therefore it is possible to reduce the cost associated with the production of the aqueous suspension.

図面を用いて本発明の実施の形態を説明する。図1は、代表的な発酵飲料であるビールの濾過工程で使用する濾過装置1の全体構成を示すものである。濾過装置1は、濾過助剤の水懸濁液製造装置2、貯酒タンクから供給される未濾過のビールを濾過し酵母や凝固物を除去する濾過機本体3、未濾過のビール及び濾過助剤の水懸濁液を濾過機本体1に供給する供給管4、濾過後のビールを回収し、瓶、缶、樽詰め工程に送る回収管5を含みうる。濾過機本体3は略円筒状の缶体31を備え、缶体31はその上部に隔壁32が設けられ、隔壁32の下方が未濾過側34、上方が濾過側35に構成される。隔壁32には多数の円筒状の濾過担体33が略鉛直に吊り下げられる。供給管4は、濾過機本体1と接続される側と反対側で、貯酒タンクに接続される管路と濾過助剤の水懸濁液製造装置2に接続される管路とに分岐している。供給管4の分岐点と貯酒タンク及び濾過助剤の水懸濁液製造装置2との間には、バルブV1,V2とポンプP1,P2とがそれぞれ設けられる。   Embodiments of the present invention will be described with reference to the drawings. FIG. 1 shows an overall configuration of a filtration device 1 used in a filtration process of beer, which is a typical fermented beverage. The filtration device 1 includes a filter aid water suspension production device 2, a filter body 3 that filters unfiltered beer supplied from a storage tank to remove yeast and coagulum, unfiltered beer, and filter aid. Supply pipe 4 for supplying the aqueous suspension of the filter to the filter body 1, and a recovery pipe 5 for recovering the filtered beer and sending it to a bottle, can, and barreling step. The filter main body 3 includes a substantially cylindrical can body 31, and the can body 31 is provided with a partition wall 32 at an upper portion thereof. A large number of cylindrical filter carriers 33 are suspended substantially vertically on the partition wall 32. The supply pipe 4 is branched on the side opposite to the side connected to the filter body 1 into a pipe connected to the liquor storage tank and a pipe connected to the filter suspension water suspension production apparatus 2. Yes. Valves V1 and V2 and pumps P1 and P2 are respectively provided between the branch point of the supply pipe 4 and the storage tank 2 and the water suspension manufacturing apparatus 2 for the filter aid.

ビールを濾過する際の手順の一例を示すと、貯酒タンクに接続する管路のバルブV1を閉じ、濾過助剤の水懸濁液製造装置2に接続する管路のバルブV2を開ける。そしてポンプP2を駆動して濾過助剤の水懸濁液をその製造装置2から供給管4を介して濾過機本体3へ供給する。供給された濾過助剤の水懸濁液は濾過担体33に堆積し、濾過助剤の濾過層(プレコート層)を形成する。濾過担体33としては、その表面に濾過助剤の濾過層を形成させることができる濾過層保持体であればなんでもよく、例えば金属製の網、厚手の濾紙、セラミックの筒を使用しうる。また、濾過助剤としては、珪藻土、二酸化ケイ素が使用されうる。   An example of the procedure for filtering beer is to close the valve V1 of the pipe line connected to the liquor storage tank and open the valve V2 of the pipe line connected to the water suspension production apparatus 2 for the filter aid. And the pump P2 is driven and the aqueous suspension of the filter aid is supplied from the manufacturing apparatus 2 to the filter main body 3 through the supply pipe 4. The supplied aqueous suspension of the filter aid is deposited on the filter carrier 33 to form a filter layer (precoat layer) of the filter aid. Any filter carrier can be used as the filter carrier 33 as long as it can form a filter layer of a filter aid on the surface thereof. For example, a metal net, thick filter paper, or a ceramic tube can be used. Moreover, diatomaceous earth and silicon dioxide can be used as a filter aid.

次いで、バルブV2を閉じ、バルブV1を開ける。その状態でポンプP1を駆動し、貯酒タンクに貯蔵される未濾過のビールを供給管4を介して濾過機本体3へ供給する。
供給された未濾過のビールは、濾過機本体3の未濾過側34に流入し、濾過担体33に形成された濾過助剤の濾過層で酵母、凝固物等が除去される。濾過によって清澄とされたビールは濾過機本体3の濾過側35から回収管5を介して次工程へ送られる。
Next, the valve V2 is closed and the valve V1 is opened. In this state, the pump P1 is driven to supply unfiltered beer stored in the storage tank to the filter main body 3 through the supply pipe 4.
The supplied unfiltered beer flows into the unfiltered side 34 of the filter body 3, and yeast, coagulum and the like are removed by the filter layer of the filter aid formed on the filter carrier 33. The beer clarified by filtration is sent from the filtration side 35 of the filter body 3 to the next process through the recovery pipe 5.

次に、図2を用いて濾過助剤の水懸濁液の製造について説明する。   Next, production of an aqueous suspension of the filter aid will be described with reference to FIG.

濾過助剤の水懸濁液製造装置2は、濾過助剤と水とを混合撹拌する混合タンク21、混合タンク21に投入する濾過助剤を計量する濾過助剤計量タンク22、混合タンク21に所定量の水を供給する水供給管23、混合タンク21に炭酸ガス、窒素ガス又はヘリウムガスのような酸化作用を有しない脱気ガスを供給するガス吹き込み管24、混合タンク25から脱気ガスと置換された酸素を含む空気、脱気ガスを放出するガス放出管25を含みうる。また、混合タンク21には、その中で生成された濾過助剤の水懸濁液を排出し、濾過機本体34に供給するための供給管4の分岐管が接続される。   The filter aid water suspension manufacturing apparatus 2 includes a mixing tank 21 for mixing and stirring the filter aid and water, a filter aid measuring tank 22 for measuring the filter aid to be added to the mixing tank 21, and a mixing tank 21. A water supply pipe 23 for supplying a predetermined amount of water, a gas blowing pipe 24 for supplying a degassing gas such as carbon dioxide, nitrogen gas or helium gas to the mixing tank 21 and a degassing gas from the mixing tank 25 Further, air containing oxygen substituted for gas and a gas discharge pipe 25 for releasing degassing gas can be included. The mixing tank 21 is connected to a branch pipe of the supply pipe 4 for discharging the aqueous suspension of the filter aid produced therein and supplying it to the filter main body 34.

濾過助剤の水懸濁液を製造する際、まず供給管4の分岐管に配置されるバルブV2が閉じられる。次いで、第一工程として、所定量の水が水供給管23から混合タンク21内へ供給される。そして、第二工程として濾過助剤計量タンク22で所定量に調整された濾過助剤が混合タンク21に投入される。第一工程における水の供給、第二工程における濾過助剤の投入によって、濾過助剤の水懸濁液中に酸素が混ざり込む。第一工程及び第二工程は、そのいずれかの工程を先に行ってもよい。また、第一、第二工程を同時に行うこともできる。   When the aqueous suspension of the filter aid is produced, the valve V2 disposed in the branch pipe of the supply pipe 4 is first closed. Next, as a first step, a predetermined amount of water is supplied from the water supply pipe 23 into the mixing tank 21. Then, as a second step, the filter aid adjusted to a predetermined amount in the filter aid metering tank 22 is charged into the mixing tank 21. Oxygen is mixed into the aqueous suspension of the filter aid by supplying water in the first step and introducing the filter aid in the second step. In the first step and the second step, any one of the steps may be performed first. Also, the first and second steps can be performed simultaneously.

懸濁液中の酸素を除去するために、第三工程で脱気ガスがガス吹き込み管24を介して混合タンク21の懸濁液内に吹き込まれる。脱気ガスは懸濁液内に溶存する酸素を追い出し、追い出される酸素とともにガス放出管25から放出される。第三工程を経ることで、混合タンク21内の濾過助剤の水懸濁液は酸素を含まないものとされる。第三工程で使用する脱気ガスとしては、例えば酸化作用を有さない炭酸ガス、窒素ガス、ヘリウムガスが使用されうる。その中では、醸造の際に副生する炭酸ガスを使用することが、入手の容易性の点から好適である。   In order to remove oxygen in the suspension, degassed gas is blown into the suspension of the mixing tank 21 through the gas blowing pipe 24 in the third step. The degassed gas expels oxygen dissolved in the suspension, and is released from the gas discharge pipe 25 together with the expelled oxygen. By passing through the third step, the aqueous suspension of the filter aid in the mixing tank 21 does not contain oxygen. As the degassing gas used in the third step, for example, carbon dioxide gas, nitrogen gas, or helium gas that does not have an oxidizing action can be used. Among them, it is preferable to use carbon dioxide gas produced as a by-product during brewing from the viewpoint of availability.

第三工程において、脱気ガスの無駄な吹き込みを行わないように、脱気ガスの吹き込み量は製造すべき懸濁液の量に基づいて決定される。第一工程で供給される水の量及び第二工程で投入される濾過助剤の量の合計量すなわち製造すべき懸濁液の量が決定されれば、懸濁液中に混ざり込む酸素の量が定まり、その酸素の量に対応して脱気ガスの吹き込み量が決定される。脱気ガスの吹き込み量は、製造すべき濾過助剤の水懸濁液の量に比例する量である。したがって、第三工程における脱気ガスの吹き込みは、吹き込み量が製造すべき懸濁液の量に基づいて決定される所定値に達する時点で停止される。   In the third step, the amount of degassed gas blown is determined based on the amount of suspension to be manufactured so as not to wastefully blow out the degassed gas. If the total amount of water supplied in the first step and the amount of filter aid added in the second step, that is, the amount of the suspension to be produced is determined, the amount of oxygen mixed in the suspension is determined. The amount is determined, and the amount of degassed gas blown is determined in accordance with the amount of oxygen. The amount of degassed gas blown is an amount proportional to the amount of the filter aid water suspension to be produced. Accordingly, the blowing of the degassing gas in the third step is stopped when the blowing amount reaches a predetermined value determined based on the amount of the suspension to be manufactured.

脱気ガスの吹き込み量は脱気ガスの吹き込み時間として表現されうる。例えば脱気ガスの単位時間当たりにガス供給管24を介して吹き込まれる量が一定である場合には、脱気ガスの吹き込み時間は製造すべき懸濁液の量に基づいて定められうる。この場合、脱気ガスの吹き込み時間が製造すべき懸濁液の量に基づいて決定される所定時間に到達すると、脱気ガスの吹き込みは自動的に停止されうる。   The blowing amount of the degassing gas can be expressed as the blowing time of the degassing gas. For example, when the amount of degassing gas blown through the gas supply pipe 24 per unit time is constant, the degassing gas blowing time can be determined based on the amount of suspension to be manufactured. In this case, when the degassing gas blowing time reaches a predetermined time determined based on the amount of suspension to be produced, the degassing gas blowing can be automatically stopped.

第一、第二工程が開始されるときから第三工程を開始すると脱気ガスが無駄に消費される。したがって、第三工程は第一工程及び第二工程の双方が終了した時点以降に開始されるのが好ましい。   When the third step is started from the time when the first and second steps are started, degassed gas is wasted. Therefore, the third step is preferably started after the time point when both the first step and the second step are completed.

前記の実施の形態では、濾過助剤の水懸濁液に使用する水は脱気されていないものとしたが、脱気された水を使用することもできる。その場合、脱気ガスの吹き込み量に対する製造すべき懸濁液の量の比例定数は変更される必要がある。   In the above embodiment, the water used for the aqueous suspension of the filter aid is not degassed, but degassed water can also be used. In that case, the proportionality constant of the amount of suspension to be produced with respect to the amount of degassed gas must be changed.

本発明で使用しうる濾過装置の全体構成を示す図である。It is a figure which shows the whole structure of the filtration apparatus which can be used by this invention. 本発明で使用しうる濾過助剤の水懸濁液製造装置を示す図である。It is a figure which shows the water suspension manufacturing apparatus of the filter aid which can be used by this invention.

符号の説明Explanation of symbols

1 濾過装置
2 濾過助剤の水懸濁液製造装置
21 混合タンク
22 濾過助剤計量タンク
23 水供給管
24 ガス吹き込み管
25 ガス放出管
3 濾過機本体
31 缶体
32 隔壁
33 濾過担体
34 未濾過側
35 濾過側
4 供給管
5 回収管
V1,V2 バルブ
P1,P2 ポンプ
DESCRIPTION OF SYMBOLS 1 Filtration apparatus 2 Water suspension manufacturing apparatus 21 of a filter aid 21 Mixing tank 22 Filtration aid metering tank 23 Water supply pipe 24 Gas blowing pipe 25 Gas discharge pipe 3 Filter body 31 Can body 32 Partition 33 Filter carrier 34 Unfiltered Side 35 Filtration side 4 Supply pipe 5 Recovery pipe V1, V2 Valve P1, P2 Pump

Claims (3)

発酵飲料の濾過工程で使用する濾過助剤の水懸濁液を製造する方法であって、
タンクに水を供給する第一工程と、
前記タンクに濾過助剤を投入する第二工程と、
前記タンクに脱気ガスを吹き込む第三工程とを含み、
前記第三工程において前記タンクに吹き込むべき前記脱気ガスの量は、製造すべき前記水懸濁液の量に基づいて決定されることを特徴とする方法。
A method for producing an aqueous suspension of a filter aid used in a filtration process of a fermented beverage,
A first step of supplying water to the tank;
A second step of adding a filter aid to the tank;
A third step of blowing degassing gas into the tank,
The method according to claim 3, wherein the amount of the degassing gas to be blown into the tank in the third step is determined based on the amount of the water suspension to be produced.
前記濾過助剤は、珪藻土及び二酸化ケイ素の少なくとも一種が使用されることを特徴とする請求項1に記載の方法。   The method according to claim 1, wherein at least one of diatomaceous earth and silicon dioxide is used as the filter aid. 前記第三工程は、前記第一工程及び第二工程の双方が終了する時点以降に開始されることを特徴とする請求項1又は請求項2に記載の方法。   The method according to claim 1 or 2, wherein the third step is started after the time point when both the first step and the second step are finished.
JP2006159110A 2006-06-07 2006-06-07 Method for producing aqueous suspension of filtration auxiliary Withdrawn JP2007325537A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2006159110A JP2007325537A (en) 2006-06-07 2006-06-07 Method for producing aqueous suspension of filtration auxiliary

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2006159110A JP2007325537A (en) 2006-06-07 2006-06-07 Method for producing aqueous suspension of filtration auxiliary

Publications (1)

Publication Number Publication Date
JP2007325537A true JP2007325537A (en) 2007-12-20

Family

ID=38926482

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2006159110A Withdrawn JP2007325537A (en) 2006-06-07 2006-06-07 Method for producing aqueous suspension of filtration auxiliary

Country Status (1)

Country Link
JP (1) JP2007325537A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2018198519A1 (en) * 2017-04-28 2018-11-01 アサヒビール株式会社 Method for predicting gushing properties of malt

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2018198519A1 (en) * 2017-04-28 2018-11-01 アサヒビール株式会社 Method for predicting gushing properties of malt

Similar Documents

Publication Publication Date Title
JP5120723B2 (en) Beer production method
JP4838248B2 (en) Reduction of backwash liquid waste
JPH0760005A (en) Dearation of liquid product
JP4112607B1 (en) Process for producing sparkling sake
JPH08276121A (en) Method and apparatus for controlling dissolved gas in liquidand gas/liquid contact body module and usage thereof
CN115667484A (en) Device for preparing and dispensing reconstituted beer
US20160201019A1 (en) Wine packaged in aluminium containers
JPH0768139A (en) Method for backwashing hollow-fiber membrane module
AU2012372142B2 (en) Packaging wine in aluminium containers
JP2007325537A (en) Method for producing aqueous suspension of filtration auxiliary
JP2023527139A (en) Single-serve capsules for the production of alcoholic beer
JP3260940B2 (en) Beverage package
RU2740478C2 (en) Kit for in situ obtaining the fermented beverage by adding a liquid solvent
US20100068360A1 (en) Method of operating a container filling plant for filling containers with filtered liquid, such as beer
JP2006280359A (en) Method for reductive aging of alcoholic beverage and reductively aged alcoholic beverage
JP4246618B2 (en) Fermentation apparatus, fermentation method, and fermented beverage production method
TW201925451A (en) Improved beer drink and method for improving beer drink
JP6979556B1 (en) Residual and deterioration control system for naturally effervescent carbon dioxide in alcoholic beverages
JP6726157B2 (en) Sake, its manufacturing method, and its manufacturing apparatus
US20230167388A1 (en) System for accelerating the aging of beer and method of use thereof
WO2002028994A1 (en) Method of removing carbon dioxide from fermenting medium using a polymeric membrane
US20210348092A1 (en) Method of Producing Beer or a Beer-Like Beverage and a Beer Concentrate
WO2018002704A1 (en) Draught beer with a high c02 content
JP2022092198A (en) Method for producing alcoholic beverage
JP2001206490A (en) Method and device for feeding pressurized gas

Legal Events

Date Code Title Description
A300 Withdrawal of application because of no request for examination

Free format text: JAPANESE INTERMEDIATE CODE: A300

Effective date: 20090901