JP2006280359A - Method for reductive aging of alcoholic beverage and reductively aged alcoholic beverage - Google Patents

Method for reductive aging of alcoholic beverage and reductively aged alcoholic beverage Download PDF

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JP2006280359A
JP2006280359A JP2005158007A JP2005158007A JP2006280359A JP 2006280359 A JP2006280359 A JP 2006280359A JP 2005158007 A JP2005158007 A JP 2005158007A JP 2005158007 A JP2005158007 A JP 2005158007A JP 2006280359 A JP2006280359 A JP 2006280359A
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aging
alcoholic beverage
alcohol
liquor
technique
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Chikashi Kamimura
親士 上村
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JOHO KAGAKU KENKYUSHO KK
Information Science Research Institute
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JOHO KAGAKU KENKYUSHO KK
Information Science Research Institute
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Abstract

<P>PROBLEM TO BE SOLVED: To provide a technique for accelerating aging of alcoholic beverages and a technique for improving quality, and the alcoholic beverage having high functionality. <P>SOLUTION: The alcoholic beverage is continuously treated to be reduced and stored in a storage tank and accelerate aging of the same by using a reduction treatment apparatus for creating a gas-liquid colloidal solution of hydrogen before the aging step by combining a reduction treatment technique and the aging technique. The technique requires short treatment time, accelerates aging of any alcoholic beverages such as brewage, distilled liquor or synthetic liquor, shortens aging time and expresses high economic effects. The finished beverages have antioxidation functions, become to be products which can not easily deteriorate, express improved preservation and are good for health through taking the beverages owing to elimination of active hydrogen in the body, suppression of peroxylipids and the like. <P>COPYRIGHT: (C)2007,JPO&INPIT

Description

発明の詳細な説明Detailed Description of the Invention

本発明は清酒、ブドー酒、果実酒、ビール等の醸造酒、焼酎、泡盛、ウオッカ、ウイスキー、ジン、パイカル等の蒸留酒の製造における、熟成の段階を還元状態に保ち、その熟成を促進し、高品質化することに関する。  The present invention keeps the aging stage in a reduced state and promotes aging in the production of sake, buddo, fruit wine, beer and other brewed sake, shochu, awamori, vodka, whiskey, gin, and baked spirits. , Related to quality improvement.

酒類の熟成は、醸造酒においては醸造の最終段階、蒸留酒においては蒸留貯蔵の最終段階において、低温で酒類を長期寝かせ、それぞれの酒類特徴の色、味、香りを特徴する品質を管理するもので、味をまろやかにすることを目的としている。
熟成は、保蔵し寝かせた年月でまろやかさや旨みに相違があり、原料の善し悪しを表示する生産年と共に保蔵年数が重視されるのである。
熟成期間を短縮することができれば、酒類の生産コストは著しく低下させることができる。
そこで、熟成に関与するのは水の成分や性質であるとの視点から長年にかけて、地下水の特徴を調べたり、電磁的処理、パイウオーターの使用を試みる等多くの試みが成されたが、いずれも不成功に終わり、昔ながらの熟成が行われている。
Alcohol ripening is the final stage of brewing for brewed liquor, and the final stage of distilled storage for distilled liquor. The purpose is to mellow the taste.
Aging is different in mellowness and umami depending on the age of storage and laying down, and the storage age is emphasized along with the production year indicating the quality of the raw material.
If the aging period can be shortened, the production cost of alcoholic beverages can be significantly reduced.
Therefore, from the viewpoint that it is the components and properties of water that are involved in aging, many attempts have been made such as investigating the characteristics of groundwater, trying to use electromagnetic treatment, and using piwater. However, it has been unsuccessful and traditional aging has been carried out.

水の還元処理技術については、当発明者が平成3〜4年に研究を行い、平成11年2月26日に特許第890342号として認められた「食品等の還元性水素水とその製造法並びに製造装置」がある。この特許では水素ガスを水に溶解し、還元性を示す水とその製造方法が特許として認められている。
その後、さらに研究を進め、平成13年5月1日に出願した特開2003−19426号「ガス溶存液状媒体の生産方法及びガス溶存液状媒体の生産システム」を提案した。この出願では、流動する液体に対し、水素を添加して液体の酸化還元を一定に調整する技術を提供する技術であった。
さらにその後の研究で、2003年4月28日に出願した特願2003−158698号「水素ガス及び酸素ガスの減圧・加圧溶解方式のコロイド溶液による自動酸化還元処理システム」がある。
この出願では、流動する液体に酸素又は水素を添加して高速に回転する回転子のキャビテーションによりガス気泡を砕き、減圧条件と加圧条件を与えて微細気泡をコロイド状にし、ガスの過飽和状態を作って、液体に強い酸化力、還元力を与える技術である。
これらの技術は何れも水、液体の酸化還元に関与する技術で、酒の熟成を図る技術として提案されたものではない。
Regarding the water reduction treatment technology, the present inventor conducted research in 1991-3, and was recognized as Patent No. 890342 on February 26, 1999, "Reducible hydrogen water for foods and its manufacturing method" As well as manufacturing equipment ". In this patent, water that dissolves hydrogen gas in water and exhibits reducibility and its manufacturing method are recognized as patents.
Thereafter, further research was conducted, and Japanese Patent Application Laid-Open No. 2003-19426 “Production method of gas-dissolved liquid medium and production system of gas-dissolved liquid medium” filed on May 1, 2001 was proposed. In this application, it was a technique that provides a technique for adjusting the oxidation-reduction of a liquid by adding hydrogen to a flowing liquid.
Furthermore, in a later study, there is Japanese Patent Application No. 2003-158698 “Automatic redox treatment system using colloidal solution of hydrogen gas and oxygen gas under reduced pressure and pressure dissolution” filed on April 28, 2003.
In this application, gas bubbles are crushed by cavitation of a rotor that rotates at high speed by adding oxygen or hydrogen to a flowing liquid, and a reduced pressure condition and a pressurized condition are applied to make the fine bubbles colloidal, thereby causing a supersaturated state of the gas. It is a technology that gives strong oxidizing and reducing power to liquids.
These techniques are all related to redox of water and liquid, and are not proposed as techniques for aging alcohol.

問題を解決するための手段Means to solve the problem

このように、酒の熟成を図る手段としては、熟成温度を適温に保ちながら時間の経過をゆっくりと待つのが、良好な熟成法であると言うのが現状である。
そこで、前記問題を解決するために本技術では、当発明者が提案した還元処理技術と酒の熟成技術を組合わせて、酒類生産の最終段階にあたる熟成段階に前記水素の気液コロイド溶液を創出する「還元処理装置」(特願2003−158698)を用い、酒類を連続的に還元処理して貯蔵タンクに貯留し、熟成を速める方法を開発した。
As described above, as a means of aging alcohol, it is the present condition that a good aging method is to wait for the passage of time slowly while keeping the aging temperature at an appropriate temperature.
Therefore, in order to solve the above problems, the present technology creates the gas-liquid colloidal solution of hydrogen in the aging stage, which is the final stage of liquor production, by combining the reduction treatment technique proposed by the inventors and the aging technique of liquor. Using a “reduction treatment device” (Japanese Patent Application No. 2003-158698), a method for continuously reducing and storing alcoholic beverages in a storage tank has been developed.

酒類の熟成には、二つの要素があり、一つの要素は貯蔵中に含まれるアルコールと水の成分が調和することが重要な要素である。この調和は、水が持つ物性の相違が影響し、水によってこの調和し馴染む速度が違うことが経験的に知られている。
あと一つの要素は、熟成中に酒類の中に含まれる成分が酸化によって微妙に変性することである。これを止めるには貯蔵中の酒類の反応系を還元状態に置くことが必要である。
還元処理は、分子運動の激しい水素分子がアルコールと水の分子の間に入り込み、局部的な分子と分子の相互の結び付きをを妨げ、全体として成分が均一に混じり合う作用を促す機能を有している。
また還元処理は前述の通り、酒類の中に含まれる成分の酸化とりわけ香気成分に大きな影響を有する微量に含まれる脂質の酸化を防止する。
There are two factors in the aging of alcoholic beverages, and one factor is that the alcohol and water components contained during storage are in harmony. It is empirically known that this harmony is affected by the difference in physical properties of water, and the speed at which this harmony and conformity varies depending on the water.
Another factor is that the components contained in the liquor during aging are slightly denatured by oxidation. In order to stop this, it is necessary to put the reaction system of the liquor being stored in a reduced state.
The reduction treatment has a function that promotes the action of hydrogen molecules with intense molecular motion entering between alcohol and water molecules, preventing the local molecules from intermingling with each other and mixing the components uniformly as a whole. ing.
Further, as described above, the reduction treatment prevents oxidation of components contained in alcoholic beverages, in particular, oxidation of lipids contained in trace amounts having a great influence on aroma components.

醸造酒では、熟成中の脂質成分の変性防止が重要な鍵であり、還元処理はタンク内で寝かせている間に、これらが酸化されるのを防ぎ、水の物性が変化してアルコールと水の成分と香気成分に良く馴染み、短い期間ですっきりした感触を醸し出すことを可能としている。
この香気成分が良く馴染み、すっきりした感触を有することが酒の生命である。
In brewing liquor, prevention of denaturation of lipid components during aging is an important key, and reduction treatment prevents them from being oxidized while they are laid in the tank, and the physical properties of water change to change alcohol and water. Familiar with the ingredients and fragrance ingredients, it is possible to create a clean feel in a short period of time.
The life of liquor is that this fragrance component is well-familiar and has a clean feel.

蒸留酒では、酸化されて異臭を放つ成分はないが、蒸留中に微量採取される香気性の揮発成分と水とアルコールの馴染みが熟成の大きな目標である。
この他、ウイスキー等燻煙と樽詰め等により着色、着香を行う蒸留酒においては、熟成は着色、着香成分との馴染みも重要な要素である。
還元処理は上記二種類の馴染みに対する熟成においても、物性的にこれを促進し、速い熟成と芳香を高める効果を有する。
また、還元飲料としての蒸留酒は体内において、活性酸素を消去したり、過酸化脂質の生成を抑制する機能があるので、健康にプラスに働く高品質酒類である。
In distilled liquor, there are no components that oxidize and give off a strange odor, but the familiarity of aroma-based volatile components, water, and alcohol collected in trace amounts during distillation is a major goal of aging.
In addition, in distilled liquor that is colored and flavored by smoking and barreling such as whiskey, aging is also an important factor for familiarity with the coloring and flavoring components.
The reduction treatment promotes the physical properties even in aging for the above two types of familiarity, and has the effect of increasing the aging speed and aroma.
Distilled liquor as a reduced beverage is a high-quality liquor that works positively on health because it has a function of eliminating active oxygen in the body and suppressing the formation of lipid peroxide.

還元処理装置の導入は、酒類の相違によって若干相違する。
醸造酒(第1図)においては、酒、ブドー酒等では発酵終了後搾汁し固液分離する時点と火入れ後貯蔵熟成に入る直前の2回還元処理の適用が可能である。
ビール(第2図)では、発酵終了後貯酒タンクに入れる段階でに還元処理が可能である。蒸留酒(第3図)では、蒸留冷却後貯蔵タンクに入れる直前で還元処理が可能である。
The introduction of the reduction processing device is slightly different depending on the alcoholic beverage.
In brewing liquor (Fig. 1), it is possible to apply a reduction process twice in liquor, budo liquor, etc. at the time of squeezing and solid-liquid separation after completion of fermentation and immediately before storage aging after burning.
In the case of beer (FIG. 2), a reduction process can be performed at the stage where the beer is placed in the storage tank after completion of fermentation. Distilled liquor (FIG. 3) can be reduced immediately before being put into a storage tank after cooling by distillation.

第1図に示す通り、清酒、ブドー酒、果実酒等の醸造酒では、熟成促進のための還元処理1の工程は、通常は後発酵工程3、火入れ工程4の後の熟成段階へ移行する時点で連続的に還元処理し熟成させる。
しかし、さらに効果を高めるためには、圧搾ろ過工程の後に後発酵3に入る段階で還元処理し、火入れ4後の貯酒タンク5へ送る前の段階で再度2段階で還元処理1して密閉貯蔵熟成を促進する。
貯酒タンク5以後の工程は、除菌ろ過装置7、容器充填装置8であり、この段階では酒類は還元条件を示している。
還元処理は工程と工程を繋ぐパイプの中間に還元処理装置をINとOUTの方向を確認して、矢印の方向へ繋ぎ、装置のモーターを活用して連続的に処理を行う。
還元貯蔵では、生酒、生ビールの保蔵も可能である。
As shown in FIG. 1, in brewed sakes such as sake, budodo liquor, fruit liquor, etc., the process of reduction treatment 1 for promoting ripening usually shifts to the aging stage after the post-fermentation process 3 and the firing process 4. At the time, it is continuously reduced and aged.
However, in order to further enhance the effect, reduction processing is performed at the stage of entering post-fermentation 3 after the squeezing filtration process, and reduction processing 1 is performed again at two stages before being sent to the storage tank 5 after burning 4 and sealed and stored. Promotes aging.
The steps after the storage tank 5 are a sterilization filtration device 7 and a container filling device 8, and at this stage, the alcoholic beverages indicate the reducing conditions.
In the reduction process, the direction of IN and OUT is confirmed in the middle of the pipe connecting the processes, the direction of IN and OUT is confirmed, the process is continuously performed by utilizing the motor of the apparatus.
In reduced storage, it is also possible to store draft sake and draft beer.

ビール等の醸造酒では、発酵工程2の後の貯酒タンク5へ送る前の段階へ適用する。即ち、熟成段階へ移行する時点で連続的に還元処理1し熟成させる。
貯酒タンク5の後は、サービングタンク6を通過し、除菌ろ過装置7を通過して容器充填装置8に至る。この段階ではビールは還元条件を示し、酸化防止剤を加えなくても酸化防止される。
In the case of brewed liquor such as beer, it is applied to the stage before being sent to the storage tank 5 after the fermentation process 2. That is, the reduction treatment 1 is continuously performed and ripened at the time of transition to the ripening stage.
After the liquor storage tank 5, it passes through the serving tank 6, passes through the sterilization filtration device 7, and reaches the container filling device 8. At this stage, beer exhibits reducing conditions and is oxidized without the addition of antioxidants.

第2図に示す通り、焼酎、泡盛、ウイスキー、ウオッカ、テキーラ、ドライジン、コニャック等の蒸留酒では、熟成促進のための還元処理の工程は、蒸留工程9が終了して冷却段階10に入った段階で、連続的に還元処理1して、貯酒タンク5に入れ、熟成段階に入る。熟成は低温で行う。
蒸留酒の場合も同様に、還元処理は工程と工程を繋ぐパイプの中間に還元処理装置をINとOUTの方向を確認して、矢印の方向に繋ぎ、装置のモーターを活用して連続的に処理を行う。
As shown in FIG. 2, in the distilled liquor such as shochu, awamori, whiskey, vodka, tequila, dry gin, cognac, etc., the reduction process for promoting ripening has completed the distillation process 9 and entered the cooling stage 10. At the stage, continuous reduction treatment 1 is put into the storage tank 5 and the aging stage is entered. Aging is performed at a low temperature.
Similarly, in the case of distilled liquor, the reduction process is performed continuously by checking the direction of IN and OUT in the middle of the pipe connecting the processes, connecting in the direction of the arrow, and using the motor of the apparatus. Process.

いずれの酒類でも、処理終了後時間の経過に伴い、ロット内で発生する酸素の影響と生成物の水素の吸収によって、酸化還元電位は次第に上昇するので、必要によっては再度還元処理を行う。
熟成が終了した段階では、還元処理の繰り返しによって、製品の酒類の酸化還元電位がマイナスになり、成分の酸化や変敗が起り難い製品になっている。
In any liquor, the redox potential gradually rises due to the influence of oxygen generated in the lot and the absorption of hydrogen in the product with the lapse of time after the treatment is completed, so that the reduction treatment is performed again as necessary.
At the stage of ripening, the redox potential of the alcoholic beverages of the product becomes negative due to repetition of the reduction treatment, and the product is difficult to oxidize or deteriorate.

第4図に示したように、清酒等醸造酒の全工程は、原料調整工程、仕込み工程、醪仕込工程、発酵工程、しぼり工程、後発酵工程、熟成工程、成品工程の順に作業が進む。その工程への還元処理装置の導入は、通常は火入れの後の貯蔵タンクへ入れる段階で還元処理することが最も容易である。
しかし、火入れは温度を高めるために、火入れの段階で溶解している可変性成分が、酸化され品質低下の原因になる場合がある。そう言う場合は、後発酵槽への発酵生成物の送入に際し還元処理を加えるのが安全である。その場合はアルコールの回収率も高まる。
ビールの全工程は、原料調整工程、仕込工程、冷却工程、発酵工程、貯酒工程、熟成工程、成品工程の順に作業が進む。その工程への還元処理装置の導入は、通常は発酵工程の後の貯酒工程の前の段階で還元処理することが最も容易である。
As shown in FIG. 4, the whole process of brewing sake such as sake is proceeded in the order of raw material adjustment process, preparation process, koji preparation process, fermentation process, squeezing process, post-fermentation process, aging process, and product process. Introducing the reduction treatment apparatus into the process is usually the easiest to carry out the reduction treatment at the stage of entering the storage tank after the firing.
However, in order to raise the temperature of the firing, the variable components dissolved at the stage of the firing may be oxidized and cause a deterioration in quality. In that case, it is safe to add a reduction treatment when the fermentation product is fed into the post-fermentor. In that case, the alcohol recovery rate also increases.
The whole process of beer proceeds in the order of raw material adjustment process, preparation process, cooling process, fermentation process, liquor storage process, aging process, and product process. In general, the reduction treatment apparatus is most easily introduced into the process at the stage before the liquor storage process after the fermentation process.

発明の効果The invention's effect

以上説明したように本発明では、醸造酒、蒸留酒各々の生産工程へ還元処理装置を用いて、アルコール溶液へ水素を溶解させ、酒類の熟成を促進するもので、熟成期間の短縮による経済効果と酒類の高品質化を図るものである。
また、還元の酒は生体内に吸収された段階で活性酸素の消去を行ったり、過酸化脂質の生成を抑制したりするなど、健康にも良い効果を有していると考えられ、本装置を用いた水ではアトピー性皮膚炎の快癒等の現象も観察されている。
As described above, in the present invention, the reduction treatment device is used for each production process of brewed liquor and distilled liquor, hydrogen is dissolved in the alcohol solution, and the aging of the liquor is promoted. Economic effect by shortening the aging period And to improve the quality of liquors.
In addition, reduced liquor is thought to have a good effect on health, such as eliminating active oxygen when it is absorbed in the body and suppressing the formation of lipid peroxide. Phenomena such as pleasant healing of atopic dermatitis have been observed in water using water.


還元処理装置の清酒醸造工程への通常の適用例Example of normal application of reduction processing equipment to sake brewing process 還元処理装置のビール醸造工程への通常の適用例Example of normal application of reduction processing equipment to beer brewing process 還元処理装置の蒸留酒製造工程への通常の適用例Example of normal application of reduction processing equipment to the spirits manufacturing process 醸造酒の全工程と熟成における還元処理の適用事例Application examples of reduction treatment in all processes and aging of brewed sake 蒸留酒の全工程と熟成における還元処理の適用事例Application examples of reduction treatment in all processes and aging of distilled spirits

符号の説明Explanation of symbols

1 還元処理装置
2 発酵タンク
3 後発酵タンク
4 火入れ
5 貯酒タンク
6 サービングタンク
7 除菌ろ過装置
8 容器充填機
9 蒸留装置
10 冷却装置
DESCRIPTION OF SYMBOLS 1 Reduction processing apparatus 2 Fermentation tank 3 Post-fermentation tank 4 Burning 5 Storage tank 6 Serving tank 7 Sterilization filtration apparatus 8 Container filling machine 9 Distillation apparatus 10 Cooling apparatus

Claims (7)

酒類の熟成段階において、溶液への水素の加圧・減圧溶解方式による還元コロイド生成装置を用い、酒類を水素ガス添加による気液コロイド溶液に保ち、貯酒タンク内での熟成を速め、保蔵期間の短縮を可能とし、香気の高い芳香性の酒類を生成することを特徴とする、酒類の還元熟成方法。  In the aging stage of alcoholic beverages, a reduced colloid generation device that uses hydrogen under pressure and dissolution under reduced pressure is used to keep the alcoholic beverage in a gas-liquid colloidal solution by adding hydrogen gas, speeding aging in the storage tank, A method for reducing and ripening alcoholic beverages, characterized in that the alcoholic beverages can be shortened and produce fragrant and highly aromatic alcoholic beverages. 請求項1において、貯酒タンクが0.0001〜0.1トールの減圧状態であることを特徴とする酒類の熟成方法。  The method for aging alcohol according to claim 1, wherein the storage tank is in a reduced pressure state of 0.0001 to 0.1 Torr. 請求項1において、貯酒タンク内の圧力が常圧〜10パスカルの加圧状態であることを特徴とする酒類の熟成方法。According to claim 1, liquor way ripening, wherein the pressure in the alcohol storage tank is pressurized state of normal pressure to 105 Pa. 請求項1の熟成促進方法によって生成される酒で、酸化還元電位=ORPがマイナスを示すことを特徴とする還元熟成酒。  A reduced aging liquor produced by the aging promotion method according to claim 1, wherein the redox potential = ORP is negative. 請求項1において、熟成される酒の種類が醸造酒であることを特徴とする酒類。  2. The alcoholic beverage according to claim 1, wherein the type of sake to be aged is brewed sake. 請求項1において、熟成される酒の種類が蒸留酒であることを特徴とする酒類。  2. The alcoholic beverage according to claim 1, wherein the type of alcohol to be aged is distilled alcohol. 請求項1において、熟成される酒の種類が合成酒であることを特徴とする酒類。  2. The alcoholic beverage according to claim 1, wherein the type of alcohol to be aged is synthetic alcohol.
JP2005158007A 2005-04-04 2005-04-04 Method for reductive aging of alcoholic beverage and reductively aged alcoholic beverage Pending JP2006280359A (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009044988A (en) * 2007-08-18 2009-03-05 Yukinori Itokazu Method for modifying liquors, modifying apparatus, and liquors obtained thereby
WO2016121542A1 (en) * 2015-01-26 2016-08-04 有限会社情報科学研究所 Alcoholic beverage having antioxidative function, method for removing acetaldehyde from alcoholic beverage at low temperature, reductive fermentation method, and oxidative/reductive brewing method and apparatus therefor
CN108410683A (en) * 2018-04-16 2018-08-17 广东省九江酒厂有限公司 A kind of Spirit aging device and ageing method using sunlight
PL127073U1 (en) * 2018-02-27 2019-09-09 Tomasz Szloser Device for processing alcohol-containing fluids
CN111133092A (en) * 2017-08-08 2020-05-08 直会株式会社 Method for distilling brewed liquor under reduced pressure, method for aging brewed liquor, and alcoholic beverage

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009044988A (en) * 2007-08-18 2009-03-05 Yukinori Itokazu Method for modifying liquors, modifying apparatus, and liquors obtained thereby
WO2016121542A1 (en) * 2015-01-26 2016-08-04 有限会社情報科学研究所 Alcoholic beverage having antioxidative function, method for removing acetaldehyde from alcoholic beverage at low temperature, reductive fermentation method, and oxidative/reductive brewing method and apparatus therefor
EP3252135A4 (en) * 2015-01-26 2018-11-07 Johokagaku Kenkyusyo Co. Ltd. Alcoholic beverage having antioxidative function, method for removing acetaldehyde from alcoholic beverage at low temperature, reductive fermentation method, and oxidative/reductive brewing method and apparatus therefor
CN111133092A (en) * 2017-08-08 2020-05-08 直会株式会社 Method for distilling brewed liquor under reduced pressure, method for aging brewed liquor, and alcoholic beverage
EP3666877A4 (en) * 2017-08-08 2020-08-19 Naorai Inc. Method for vacuum-distilling and aging brewage, and alcoholic beverage
PL127073U1 (en) * 2018-02-27 2019-09-09 Tomasz Szloser Device for processing alcohol-containing fluids
CN108410683A (en) * 2018-04-16 2018-08-17 广东省九江酒厂有限公司 A kind of Spirit aging device and ageing method using sunlight

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