JP2006336164A - Method for dyeing fabric by using seaweeds and leaves of chestnut tree - Google Patents
Method for dyeing fabric by using seaweeds and leaves of chestnut tree Download PDFInfo
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- JP2006336164A JP2006336164A JP2005163698A JP2005163698A JP2006336164A JP 2006336164 A JP2006336164 A JP 2006336164A JP 2005163698 A JP2005163698 A JP 2005163698A JP 2005163698 A JP2005163698 A JP 2005163698A JP 2006336164 A JP2006336164 A JP 2006336164A
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Abstract
Description
本発明は自然界に在る海藻類および栗の葉の色素を抽出し、布地ヘ染色する事に関する。 The present invention relates to the extraction of the pigments of seaweeds and chestnut leaves that exist in nature and dyeing them on fabrics.
従来の木綿を始めセルロース繊維ヘ染色する場合は、合成染料を使用し多量の中性塩もしくは中性塩と共にアルカリを使用している。また羊毛を始め動物性蛋白繊維用染料の染色物の一部には重金属であるクロームが含まれている場合がある。特に木綿の場合、アルカリが染色物へ残留した場合は、人体の肌あれとなり、またある種の反応性染色による染色物の場合、未反応の合成染料が残留し、染料による塩酸が繊維上に生成され、人体および繊維製品へ悪影響を及ぼすことになる。そこで現在行われている反応染料による染色方法について図1を参照しながら説明する。まず精練・漂白は、木綿の原糸にたんぱく質・ペクチン質・脂肪酸・ろう質などの不純物が含まれているので、これらを取り除き、白く晒す。
工程は、精練釜に軟水・木綿・精練安定剤・苛性ソーダ・過酸化水素を入れて常圧処方の場合は90℃、高温処方の場合は120℃で30分かけて精練漂白す る。次に、染色には、反応染料が多く使用されている。反応染料は、色相が鮮明で洗濯、日光には強い染料であるが塩素に弱い欠点がある。工程は、染色釜に軟水、精練漂白した木綿をいれて40℃まで昇温して、反応染料を入れて10分後に芒硝1/10・4/10・5/10と5分おきに入れる。その後60℃まで昇温して10分後にアルカリ剤を1/10・4/10・5/10と5分おきに入れて、淡色の場合は30分、濃色の場合は50分間染色する。その後、排水して水洗する。洗浄は、染色後に未反応染料、分解染料を除去し染料堅牢度を高めるため、洗浄を行う。工程は、水洗後に一旦排水して、軟水を設定された量入れた後、洗浄剤を入れて、90℃まで昇温して15分間洗浄する。その後、排水して水洗するがこの洗浄工程が不充分の場合に布地へアルカリ等が残り人体の肌荒れが起こる。(例えば、特許文献1、2参照)
In the process, soft water, cotton, scouring stabilizer, caustic soda, and hydrogen peroxide are placed in a scouring pot, and scouring bleaching is performed at 90 ° C for normal pressure formulation and 120 ° C for high temperature formulation over 30 minutes. Next, reactive dyes are often used for dyeing. Reactive dyes have a clear hue and are resistant to washing and sunlight, but are weak against chlorine. In the process, put soft water and scoured and bleached cotton in a dyeing pot, raise the temperature to 40 ° C, add the reactive dye, and after 10 minutes, add it every 5 minutes, 1/10, 4/10, 5/10. Then, raise the temperature to 60 ° C, and after 10 minutes, add the alkaline agent every 5 minutes, 1/10, 4/10, 5/10, and dye for 30 minutes for light colors and 50 minutes for dark colors. Then drain and wash. Washing is performed after dyeing in order to remove unreacted dyes and decomposing dyes to increase dye fastness. In the process, the water is once drained after washing with water, and after adding a set amount of soft water, a cleaning agent is added, the temperature is raised to 90 ° C., and washing is performed for 15 minutes. After that, drain and wash with water, but when this washing process is insufficient, alkali or the like remains on the fabric, causing rough skin. (For example, see Patent Documents 1 and 2)
本発明は、合成染料で染色した布地を肌着として使用した場合、人の体質により肌あれ現象が起こり、人体へ悪影響を及ぼす。そこで人体にやさしい自然界に在る海藻や栗の葉の色素を抽出し、布地へ染色を行う。 In the present invention, when a fabric dyed with a synthetic dye is used as an undergarment, a rough skin phenomenon occurs depending on the human constitution, which adversely affects the human body. Therefore, we extract the pigments of seaweed and chestnut leaves that are natural to the human body and dye them on the fabric.
人体にやさしい自然界に在る海藻類特にホンダワラ類や栗の葉を乾燥後、粉砕加工を行ったものを軟水中に投入し90〜100℃で長時間加熱し色素を所定の濃度まで抽出したものを染料とし布地ヘ染色を行う。 Natural algae that are kind to the human body, especially hondawalas and chestnut leaves, dried and then pulverized into soft water and heated at 90-100 ° C for a long time to extract the pigment to the specified concentration Dye the fabric with the dye.
海藻類、特にホンダワラ類を抽出した染料はカルシウム、鉄、マグネシウム、が多く含有されているため人体の肌にはやさしく、汗疹、かぶれ等の肌荒れ防止効果がある。また栗の葉のせんじた液の薬効は古くから、漆かぶれ、ぎんなんかぶれ、汗疹等の肌荒れ防止に使用されている。この栗の葉を抽出した染料を布地へ染色したものを肌着として使用すれば肌荒れ防止効果がある。 Dye extracted from seaweeds, especially Honda Walla, is rich in calcium, iron, and magnesium, so it is gentle on human skin and has the effect of preventing rough skin such as sweats and rashes. In addition, the medicinal effects of chestnut leaves are used to prevent rough skin such as lacquer rashes, rashes, and rashes. If the chestnut leaf-extracted dye is used as an underwear, there is an effect of preventing rough skin.
人体にやさしい自然界に在る海藻類特にホンダワラ類や栗の葉を乾燥後、粉砕加工を行ったものを軟水中に投入し90〜100℃で長時間加熱し色素を所定の濃度まで抽出したものを染料とし布地ヘ染色を行う。 Natural algae that are kind to the human body, especially hondawalas and chestnut leaves, dried and then pulverized into soft water and heated at 90-100 ° C for a long time to extract the pigment to the specified concentration Dye the fabric with the dye.
以下、本発明の実施例を用いて説明する。まず染料の製造方法について説明する。染料の原料は、海藻類のホンダワラ又は栗の葉を使用し、採取後、表面へ付着しているゴミや不燃物を水洗にて取り除き、その後100℃の乾燥機内へ入れ完全に乾くまで乾燥する。乾燥されたホンダワラ又は栗の葉は色素の抽出を容易にする目的で、粉砕機で2mmアンダーまで粉末化を行う。次に色素の抽出方法は、粉末化された粉末100gと軟水1Lを染色機へ投入し、95℃で60分間加熱を行い色素の抽出を行い、ガーゼ等で濾し、染料液を取り出し染料とする。 The present invention will be described below with reference to examples. First, a method for producing a dye will be described. The raw material for the dye is the seaweed Honda Walla or chestnut leaves. After collection, remove dust and incombustible material adhering to the surface by washing with water, and then put it in a dryer at 100 ° C to dry it completely. . For the purpose of facilitating the extraction of the pigment, dried Honda Walla or chestnut leaves are pulverized to 2 mm or less with a pulverizer. Next, the pigment is extracted by adding 100 g of powdered powder and 1 L of soft water to a dyeing machine, heating at 95 ° C. for 60 minutes, extracting the pigment, filtering with gauze, etc., taking out the dye solution and using it as a dye .
次に染料前の前処理方法について説明する。染色物の木綿などの植物繊維はセルロースでできている為シルクやウールなどの動物繊維に比べて染色があまり良くない。本特許の特徴である前処理へ使用する大豆タンパク質を加工して繊維につけることにより、染色が大幅に改善される。大豆タンパク質の前処理工程は、大豆100gに対して水を10倍量の1000gを入れ半日ぐらい漬けておく。その後大豆を水ごとミキサーにかけて潰す。ミキサーから取り出し、ガーゼで濾して、豆乳を作る。次に、被染物が木綿10gの場合、豆乳200gを染色機に豆乳、木綿の順に投入し、30℃で30分間処理し、大豆タンパク質を木綿へ付着させる。次に染色機から取り出した木綿を脱水機で30秒間して乾燥機の温度30℃で120分間乾燥して前処理工程を終える。本前処理工程は図2を参照下さい。また、豆乳に代えカチオン化剤で綿繊維へ付けることも出来る。被染物が木綿10gの場合、カチオン化剤2g(第4級アンモニウム塩を含むポリカチオン性物質)、アルカリ4g、軟水200gを染色機へ、カチオン化剤、アルカリ、軟水、木綿、の順に投入し、80℃で30分間加熱し、カチオン化剤を木綿へ付着させた後処理液を染色機より排出する。次に被染物を中和させる為、酢酸0.2gと軟水200gを染色機へ入れ、40℃で10分間中和処理を行い、その後水洗し、前処理工程を終える。 Next, a pretreatment method before dye will be described. Plant fibers such as dyed cotton are made of cellulose and are not dyed much better than animal fibers such as silk and wool. Dyeing is greatly improved by processing soy protein used in the pretreatment characteristic of this patent and attaching it to the fiber. In the soy protein pretreatment process, 1000 grams of water is added to 100 grams of soybeans and soaked for about half a day. Then mash the soybeans with water in a mixer. Remove from the mixer and filter with gauze to make soy milk. Next, when the material to be dyed is 10 g of cotton, 200 g of soy milk is put into the dyeing machine in the order of soy milk and cotton, and treated at 30 ° C. for 30 minutes to attach the soy protein to the cotton. Next, the cotton taken out from the dyeing machine is dried with a dehydrator for 30 seconds and at a dryer temperature of 30 ° C. for 120 minutes to complete the pretreatment process. See Fig. 2 for the pretreatment process. Moreover, it can replace with soybean milk and can attach to cotton fiber with a cationizing agent. If the material to be dyed is 10 g of cotton, add 2 g of cationizing agent (polycationic substance containing a quaternary ammonium salt), 4 g of alkali and 200 g of soft water to the dyeing machine in the order of cationizing agent, alkali, soft water and cotton. After heating at 80 ° C. for 30 minutes to attach the cationizing agent to cotton, the treatment solution is discharged from the dyeing machine. Next, in order to neutralize the object to be dyed, 0.2 g of acetic acid and 200 g of soft water are put into the dyeing machine, neutralized at 40 ° C. for 10 minutes, then washed with water, and the pretreatment process is completed.
前処理を終えた木綿へ染色を行う方法について説明する。例えばらくだ色の中色程度の色へ染色する場合、木綿10gに対して染料を50ccと軟水150ccを染色機へ投入し、よく攪拌してから木綿を投入し染料機で攪拌を行う。その後徐々に昇温を行い80℃で30分間染色処理を行う。染色後染色機より木綿を取り出し、水槽で水洗を3回程度行い、脱水機で脱水し、乾燥機で100℃で20分間乾燥を行うと、人体にやさしい自然界の染料で染色された布地を提供することができる。また羊毛および絹等動物性蛋白繊維の場合は、大豆蛋白処理は必要とせず、木綿と同様の染色処理により自然界の染料で染色されて、肌にやさしい布地ができる。染色の濃度は染料の量により自由に調整できる。
A method for dyeing cotton after pretreatment will be described. For example, when dyeing to a neutral color of camel, add 50cc of dye and 150cc of soft water to 10g of cotton, stir well, add cotton and stir in the dye machine. Thereafter, the temperature is gradually raised and dyeing is performed at 80 ° C. for 30 minutes. After dyeing, the cotton is taken out from the dyeing machine, washed in the water tank about 3 times, dehydrated with a dehydrator, and dried at 100 ° C for 20 minutes with a dryer to provide a fabric dyed with natural dyes that are gentle to the human body. can do. In the case of animal protein fibers such as wool and silk, soy protein treatment is not required, and the fabric is gentle to the skin by being dyed with natural dyes by the same dyeing treatment as cotton. The concentration of dyeing can be freely adjusted by the amount of dye.
Claims (3)
A method in which chestnut leaves are dried and pulverized, put into soft water, heated at 90 to 100 ° C. for a long time, and dyed to extract a dye having a predetermined concentration to fabric.
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR101183958B1 (en) | 2012-06-21 | 2012-09-19 | 한밭대학교 산학협력단 | Dyeing method using algae extract and textile products and algae dyed textile products |
KR101239350B1 (en) | 2010-12-14 | 2013-03-05 | 전라남도 | Dyeing method using enteromorpha extracts |
JP2018009163A (en) * | 2011-06-30 | 2018-01-18 | イー アンド ジェイ ガロ ワイネリイE. & J. Gallo Winery | Natural crystalline coloring agent and production method |
KR101895730B1 (en) * | 2017-09-06 | 2018-09-05 | 남옥선 | Manufacturing method of natural dye having excellent light-fastness using chestnut bur and dyeing method using thereof |
JP2021105114A (en) * | 2019-12-26 | 2021-07-26 | 和文 金子 | Fabric printing ink |
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2005
- 2005-06-03 JP JP2005163698A patent/JP2006336164A/en active Pending
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR101239350B1 (en) | 2010-12-14 | 2013-03-05 | 전라남도 | Dyeing method using enteromorpha extracts |
JP2018009163A (en) * | 2011-06-30 | 2018-01-18 | イー アンド ジェイ ガロ ワイネリイE. & J. Gallo Winery | Natural crystalline coloring agent and production method |
KR101183958B1 (en) | 2012-06-21 | 2012-09-19 | 한밭대학교 산학협력단 | Dyeing method using algae extract and textile products and algae dyed textile products |
KR101895730B1 (en) * | 2017-09-06 | 2018-09-05 | 남옥선 | Manufacturing method of natural dye having excellent light-fastness using chestnut bur and dyeing method using thereof |
JP2021105114A (en) * | 2019-12-26 | 2021-07-26 | 和文 金子 | Fabric printing ink |
JP7373844B2 (en) | 2019-12-26 | 2023-11-06 | 和文 金子 | ink for fabric printing |
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