JP2006299360A - Heat treatment method of complex roll for rolling - Google Patents

Heat treatment method of complex roll for rolling Download PDF

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JP2006299360A
JP2006299360A JP2005125049A JP2005125049A JP2006299360A JP 2006299360 A JP2006299360 A JP 2006299360A JP 2005125049 A JP2005125049 A JP 2005125049A JP 2005125049 A JP2005125049 A JP 2005125049A JP 2006299360 A JP2006299360 A JP 2006299360A
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roll
rolling
heating
temperature
outer layer
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JP4410143B2 (en
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Yoshihiro Sakotani
嘉博 佐古谷
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NITTETSU SUMIKIN ROLLS KK
Nippon Steel Corp
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NITTETSU SUMIKIN ROLLS KK
Nippon Steel Corp
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Abstract

<P>PROBLEM TO BE SOLVED: To provide a heat treatment method of a complex roll for rolling with which in the heating to austenizing temperature at the quenching time, the heat-rising of an inner layer is restricted to the minimum at the heating of an outer layer, and the brittleness of the inner layer and the coarsening of crystal grain are prevented and also, only the outer layer can be austenized in a short time and the carbide in the outer layer is sufficiently made to solid-solution in the matrix and thus, the excellent characteristic of a high speed steel can be obtained. <P>SOLUTION: In the heat treatment method of the complex roll for rolling, the heating to austenizing temperature when the quenching is applied to the complex roll for rolling, is performed as the followings, that is; a first process for heating the complex roll for rolling in a first heating furnace at 10-30°C/Hr temperature-rising speed from the room temperature to 600-700°C, after heat-insulating the portion held into a second heating furnace in the inner layer and both end surface parts in the outer layer in the complex roll for rolling; and a second process for heating the outer layer at 300-600°C/Hr temperature-rising speed from 600-700°C to 1050-1150°C, after transporting the complex roll for rolling into the second heating furnace are contained. <P>COPYRIGHT: (C)2007,JPO&INPIT

Description

本発明は,外層にハイス材を用いた熱間圧延または冷間圧延用複合ロールの熱処理方法に関する。   The present invention relates to a heat treatment method of a composite roll for hot rolling or cold rolling using a high-speed material as an outer layer.

一般に,熱間圧延または冷間圧延用複合ロールは,外面側に耐摩耗性,内部側に強靭性が要求されることから,耐摩耗性に優れるハイス系鋳鉄材を遠心力鋳造により形成した外層と,強靭性に優れる鋳鉄もしくは鋳鋼または合金鋼の内層(またはコア)を,冶金的に一体化した複合構造のロールが使用されている。   Generally, composite rolls for hot rolling or cold rolling are required to have wear resistance on the outer surface side and toughness on the inner side. Therefore, an outer layer formed by centrifugal casting of high-speed cast iron material with excellent wear resistance. In addition, a roll having a composite structure in which the inner layer (or core) of cast iron, cast steel or alloy steel having excellent toughness is integrated metallurgically is used.

上述したような複合ロールは,遠心力鋳造法で製造後,外層に高硬度化の特性を付与させるため,ロールを850〜1000℃で2〜10時間,加熱炉中で保持してオーステナイト化温度にした後,噴霧水冷や衝風冷却等によって急冷する焼入れを行い,焼入れ後,硬度調整や残留応力軽減などを目的として500〜650℃で2〜10時間保持する焼き戻しが数回行われている。   The composite roll as described above is manufactured by the centrifugal casting method, and the austenite temperature is maintained by holding the roll in a heating furnace at 850 to 1000 ° C. for 2 to 10 hours in order to give the outer layer high hardness characteristics. After quenching, quenching is performed by quenching by spray water cooling, blast cooling, etc., and after tempering, holding at 500 to 650 ° C. for 2 to 10 hours is performed several times for the purpose of adjusting the hardness and reducing residual stress. Yes.

ここで,上記焼入れにより十分な硬度を得るためには,上記オーステナイト化温度を高くすることが必要であるが,この場合に,上記の内層材として鋳鉄材を用いると内部の偏析部が溶融することがあり,また,内層材として鋼系の材料を用いると結晶粒の粗大化が生じ,ともに靭性が劣化するという問題があった。   Here, in order to obtain sufficient hardness by quenching, it is necessary to increase the austenitizing temperature. In this case, if cast iron material is used as the inner layer material, the internal segregation part melts. In addition, when steel-based materials are used as the inner layer material, there is a problem that the crystal grains become coarse and both the toughness deteriorates.

このような問題を解決する方法として,例えば,特許文献1には,次のような方法が開示されている。すなわち,特許文献1に記載された方法は,予めロール全体を1000℃以下,例えば800℃に均一に予熱した後,ロールを回転させながら,ロールの軸方向に,複数箇所設けたバーナでロールの外層部のみを加熱し,その結果,外層と軸芯部(内層)との境界の温度を1100℃以下の温度とすることにより,上記の鋳鉄材を用いた場合の内部の偏析部の溶融を抑制し,また,鋼系材料による結晶粒の粗大化を抑制し,これにより靭性が劣化するという問題を解決しようとするものである。   As a method for solving such a problem, for example, Patent Document 1 discloses the following method. That is, in the method described in Patent Document 1, the entire roll is preheated uniformly to 1000 ° C. or lower, for example, 800 ° C., and then the roll is rotated by a burner provided at a plurality of locations in the axial direction of the roll while rotating the roll. Only the outer layer part is heated, and as a result, the temperature of the boundary between the outer layer and the shaft core part (inner layer) is set to a temperature of 1100 ° C. or less, so that the inner segregation part is melted when the cast iron material is used. In addition, it is intended to solve the problem that the toughness is deteriorated by suppressing the coarsening of crystal grains by the steel-based material.

特開平4−66619号公報JP-A-4-66619 特許第3230899号公報Japanese Patent No. 3230899

しかしながら,上記特許文献1に記載された方法は,以下のような問題を有しており,実用的な技術ではない。すなわち,特許文献1に記載されている焼入れ時の加熱温度,すなわち1000℃以下,実施例では800℃でロール全体を均一に予熱することが開示されているが,この温度では既に内層がオーステナイト化温度に達しており,内層の脆化や結晶粒の粗大化の防止という観点からは十分ではない。   However, the method described in Patent Document 1 has the following problems and is not a practical technique. That is, it is disclosed that the entire roll is uniformly preheated at the heating temperature described in Patent Document 1 at the time of quenching, that is, 1000 ° C. or less, and in the examples at 800 ° C., but at this temperature, the inner layer is already austenitized. This is not sufficient from the viewpoint of preventing embrittlement of the inner layer and coarsening of crystal grains.

また,特許文献1には,上記ロール全体を均一に予熱した後の加熱方法として,上記複数箇所に設けたバーナでロールの外層部のみを加熱し,外層と軸芯部との境界の温度を1100℃以下の温度とすることが開示されている。しかし,これを加熱炉内で行った場合には,加熱炉内では,
バーナ加熱時の加熱炉内の輻射熱を受けることとなる。したがって,ロール胴部以外のロール軸部および両胴端からの伝熱を受けるため,外層と軸芯部との境界を1100℃以下とすることは困難である。
よって,軸芯部(内層)として鋳鉄材を用いると内部の偏析部が溶融することとなり,また,鋼系の材料を用いると結晶粒の粗大化が生じ,いずれの場合にも靭性が劣化する,という問題もあった。
In Patent Document 1, as a heating method after uniformly preheating the entire roll, only the outer layer portion of the roll is heated by the burners provided at the plurality of locations, and the temperature at the boundary between the outer layer and the shaft core portion is set. It is disclosed that the temperature is 1100 ° C. or lower. However, if this is done in a heating furnace,
It will receive the radiant heat in the heating furnace when the burner is heated. Therefore, it receives heat transfer from the roll shaft part other than the roll body part and both cylinder ends, and it is difficult to set the boundary between the outer layer and the shaft core part to 1100 ° C. or less.
Therefore, if cast iron is used for the shaft core (inner layer), the segregated part inside will melt, and if steel-based materials are used, the grains will become coarser and the toughness will deteriorate in either case. There was also a problem.

したがって,この方法を実施して内層の脆化や結晶粒の粗大化を防止するには,加熱炉外で作業する必要があるため,該作業に伴う排煙により環境が著しく汚染され,また,火災が起こるおそれもあり,作業環境を著しく危険なものにする。   Therefore, in order to prevent embrittlement of the inner layer and coarsening of crystal grains by carrying out this method, it is necessary to work outside the heating furnace, so the environment is significantly polluted by the flue gas accompanying the work, A fire may occur, making the work environment extremely dangerous.

そこで,本発明は,このような問題に鑑みてなされたもので,その目的は,焼入れの際のオーステナイト化温度までの加熱において,外層の加熱時における内層の昇熱を最小限に抑制し,内層の脆化や結晶粒の粗大化を防止するとともに,短時間で外層のみをオーステナイト化でき,外層の炭化物を基地中に十分に固溶させ,ハイスの特性を引き出すことが可能な,新規かつ改良された圧延用複合ロールの熱処理方法を提供することにある。   Therefore, the present invention has been made in view of such problems, and the object thereof is to suppress the heating of the inner layer to a minimum during the heating of the outer layer in the heating up to the austenitizing temperature at the time of quenching, It is a new and capable of preventing embrittlement of the inner layer and coarsening of the crystal grains, as well as being able to austenite only the outer layer in a short time, sufficiently dissolving the carbide of the outer layer in the base, and extracting the characteristics of high speed. An object of the present invention is to provide an improved heat treatment method for a composite roll for rolling.

上記課題を解決するために,本発明のある観点によれば,遠心力鋳造により形成されるハイス材からなる外層に,強靭性を有する材料からなる内層を冶金的に一体化して製造される圧延用複合ロールに対して,オーステナイト化温度まで加熱後に冷却する焼入れ処理を行った後,焼戻し処理を行う圧延用複合ロールの熱処理方法が提供される。   In order to solve the above-mentioned problems, according to one aspect of the present invention, rolling is produced by metallurgically integrating an outer layer made of a high-speed material formed by centrifugal casting with an inner layer made of a material having toughness. A heat treatment method for a rolling composite roll is provided in which the composite roll is subjected to a quenching treatment that is cooled after heating to the austenitizing temperature and then tempered.

上記熱処理方法において,上記オーステナイト化温度までの加熱は,第1加熱炉中で行う第1工程と,第2加熱炉中で行う第2工程とを含むことを特徴としている。具体的には,上記第1工程は,圧延用複合ロールのうち,内層の第2加熱炉に収容される部分と外層の両端面部とを断熱した後,第1加熱炉内にて圧延用複合ロール全体を常温から600〜700℃まで,10〜30℃/Hrの昇温速度で加熱する工程であり,上記第2工程は,第2加熱炉に圧延用複合ロールを移動させた後,外層を600〜700℃から1050〜1150℃まで,300〜600℃/Hrの昇温速度で加熱する工程である。   In the heat treatment method, the heating to the austenitizing temperature includes a first step performed in a first heating furnace and a second step performed in a second heating furnace. Specifically, in the first step, after the part of the composite roll for rolling accommodated in the second heating furnace of the inner layer and the both end face parts of the outer layer are insulated, the composite for rolling is performed in the first heating furnace. The entire roll is heated from room temperature to 600 to 700 ° C. at a heating rate of 10 to 30 ° C./Hr, and the second step is to move the rolling composite roll to the second heating furnace and Is heated from 600 to 700 ° C. to 1050 to 1150 ° C. at a temperature rising rate of 300 to 600 ° C./Hr.

このように,本発明に係る圧延用複合ロールの熱処理方法においては,まず,第2工程で使用する第2加熱炉に収容される圧延用複合ロールのロール軸部およびロール胴部の両端面部のみを断熱処理した圧延用複合ロールを,第1加熱炉内で,均一に600℃以上700℃以下の温度範囲,すなわち,内層がオーステナイト化しない範囲で最大限加熱しておく(第1工程)。次いで,第2加熱炉に上記ロールを移動させる。ここで,この第2加熱炉において,上記ロールの両端部にある上記断熱処理がされていないロール軸部は,炉殻および外気に接触している。また,第2加熱炉内に収容されたロール軸部およびロール胴部の両端面部は,上記の通り断熱処理されている。かかる状態で,最短時間で,1050〜1150℃へ昇熱させること(第2工程)で,内層の昇熱を最小限に抑制し,内層の脆化や結晶粒の粗大化を防止するとともに,短時間で外層のみをオーステナイト化でき,外層の炭化物を基地中に十分に固溶させ,ハイスの特性を引き出すことが可能となる。   Thus, in the heat treatment method for a composite roll for rolling according to the present invention, first, only the roll shaft portion of the composite roll for rolling housed in the second heating furnace used in the second step and both end portions of the roll body portion are used. Is heated to the maximum within a temperature range of 600 ° C. or higher and 700 ° C. or lower, that is, a range in which the inner layer does not become austenite, in the first heating furnace (first step). Next, the roll is moved to the second heating furnace. Here, in this 2nd heating furnace, the roll axial part which is not the said heat insulation process in the both ends of the said roll is contacting the furnace shell and external air. Further, both end surfaces of the roll shaft portion and the roll body portion accommodated in the second heating furnace are heat-insulated as described above. In such a state, by raising the temperature to 1050 to 1150 ° C. in the shortest time (second step), the temperature rise of the inner layer is minimized, and the embrittlement of the inner layer and the coarsening of crystal grains are prevented. Only the outer layer can be converted to austenite in a short time, and the carbides of the outer layer can be sufficiently dissolved in the matrix to bring out the characteristics of high speed steel.

本発明によれば,焼入れの際のオーステナイト化温度までの加熱において,外層の加熱時における内層の昇熱を最小限に抑え,内層の脆化,結晶粒の粗大化を防止するとともに,短時間で外層のみをオーステナイト化でき,外層の炭化物を基地中に十分固溶させ,ハイスの特性を引き出すことが可能な圧延用複合ロールの熱処理方法を提供することができる。   According to the present invention, in heating up to the austenitizing temperature at the time of quenching, the temperature rise of the inner layer during the heating of the outer layer is minimized, and the embrittlement of the inner layer and the coarsening of the crystal grains are prevented. Thus, it is possible to provide a method for heat treatment of a composite roll for rolling, in which only the outer layer can be austenitized, carbides in the outer layer can be sufficiently dissolved in the matrix, and high speed properties can be obtained.

以下に添付図面を参照しながら,本発明の好適な実施の形態について詳細に説明する。なお,本明細書および図面において,実質的に同一の機能構成を有する構成要素については,同一の符号を付することにより重複説明を省略する。   Hereinafter, preferred embodiments of the present invention will be described in detail with reference to the accompanying drawings. In the present specification and drawings, components having substantially the same functional configuration are denoted by the same reference numerals, and redundant description is omitted.

本発明の一実施形態に係る圧延用複合ロールの熱処理方法は,遠心力鋳造により形成されるハイス材からなる外層に,強靭性を有する材料からなる内層を冶金的に一体化して製造される圧延用複合ロールに対して,オーステナイト化温度まで加熱後に冷却する焼入れ処理を行った後,焼戻し処理を行うものである。   A heat treatment method for a composite roll for rolling according to an embodiment of the present invention includes a rolling process in which an inner layer made of a material having toughness is integrated metallurgically with an outer layer made of a high-speed material formed by centrifugal casting. The composite roll is subjected to a tempering treatment after being quenched to austenitizing temperature and then cooled.

まず,本実施形態に係る熱処理方法の熱処理の対象となる圧延用複合ロールについて説明する。この圧延用複合ロールの外層は,公知の材料であるハイス材で形成される。かかるハイス材の代表的な成分としては,例えば,上記特許文献1または特許文献2に開示されているように,C:1.2〜2.5%,Si:0.3〜1.5%,Mn:0.3〜1.5%,Cr:4.0〜10.0%,Mo:3.0〜10.0%,W:0.5〜10.0%,V:2.0〜10.0%から構成されている。また,適用の対象となるロールのサイズ,要求されるロールの使用特性等により,その他の化学成分として,上記の成分に加えて,さらに,例えば,Ni:0.1〜3.0%,Co:0.1〜10.0%,Nb:0.1〜3.0%を適宜選択して含有させてもよい。本実施形態に係る圧延用複合ロールの外層は,例えば,上記のようなハイス系化学成分で構成される溶湯を用いて,遠心鋳造法により形成することができる。   First, a rolling composite roll that is a target of heat treatment of the heat treatment method according to the present embodiment will be described. The outer layer of the composite roll for rolling is formed of a high speed material which is a known material. As typical components of the high-speed material, for example, as disclosed in Patent Document 1 or Patent Document 2, C: 1.2 to 2.5%, Si: 0.3 to 1.5% , Mn: 0.3 to 1.5%, Cr: 4.0 to 10.0%, Mo: 3.0 to 10.0%, W: 0.5 to 10.0%, V: 2.0 It is comprised from -10.0%. In addition to the above components, other chemical components, for example, Ni: 0.1 to 3.0%, Co, depending on the size of the roll to be applied, required usage characteristics of the roll, and the like. : 0.1 to 10.0%, Nb: 0.1 to 3.0% may be appropriately selected and contained. The outer layer of the rolling composite roll according to the present embodiment can be formed by, for example, a centrifugal casting method using a molten metal composed of the high-speed chemical components as described above.

また,本実施形態に係る圧延用複合ロールの内層は,例えば,公知のダクタイル鋳鉄,高級鋳鉄,黒鉛鋼などの強靭性を有する材料により形成することができる。さらに,この内層を上述したような外層に,例えば遠心鋳造法等により冶金的に一体化することで,本実施形態に係る圧延用複合ロールが形成される。   Moreover, the inner layer of the composite roll for rolling according to the present embodiment can be formed of a material having toughness such as known ductile cast iron, high-grade cast iron, and graphite steel. Furthermore, this inner layer is integrated with the outer layer as described above by metallurgical integration, for example, by a centrifugal casting method or the like, whereby the rolling composite roll according to this embodiment is formed.

次に,本実施形態に係る圧延用複合ロールの熱処理方法について詳細に説明する。本実施形態に係る熱処理方法においては,上述したように,焼入れの際にオーステナイト化温度までの加熱を行うが,この加熱は,第1加熱炉中で行う工程1と,第2加熱炉中で行う工程2とを含む。   Next, the heat treatment method for the rolling composite roll according to this embodiment will be described in detail. In the heat treatment method according to this embodiment, as described above, heating to the austenitizing temperature is performed during quenching, and this heating is performed in the first heating furnace and in the second heating furnace. And performing step 2.

まず,図1に基づいて,本実施形態に係る圧延用複合ロール5の熱処理方法の工程1に使用する第1加熱炉の構成について説明する。なお,図1は,本実施形態に係る工程1に使用する第1加熱炉の概略的な構成を示す説明図である。   First, based on FIG. 1, the structure of the 1st heating furnace used for the process 1 of the heat processing method of the composite roll 5 for rolling which concerns on this embodiment is demonstrated. In addition, FIG. 1 is explanatory drawing which shows schematic structure of the 1st heating furnace used for the process 1 which concerns on this embodiment.

図1に示すように,第1加熱炉の炉殻1は,耐火材料からなっており,その一側面が炉扉2,その下面がロール載置台3として構成されている。炉扉2を開閉することにより,第1加熱炉に対して圧延用複合ロール5を搬入および搬出することができる。また,ロール載置台3の下面側には,移動手段として,例えば複数のコロ4が設けられており,このコロ4により,略平坦な床面FL上に載置された第1加熱炉を圧延用複合ロール5の軸方向に移動させることができる。一方,第1加熱炉の内部には,ロール載置台3の上面側に,圧延用複合ロール5(具体的には,後述するロール胴部54)を支持するための第1ロール支持部6が設けられており,また,圧延用ロールを加熱する加熱手段としてバーナ7(図1では2箇所)が設けられている。第1ロール支持部6には,次工程の工程2で使用する第2加熱炉に搬入する圧延用複合ロール5が設置されている。圧延用複合ロール5は,内層としてのロール軸部52と,外層としてのロール胴部54とからなり,ロール軸部52のうち第2加熱炉内に収容される部分とロール胴部54の両端面部とを,例えばセラミックファイバー56などの断熱材で覆うことにより,これらを断熱施工している。   As shown in FIG. 1, the furnace shell 1 of the first heating furnace is made of a refractory material, and one side surface thereof is configured as a furnace door 2, and the lower surface thereof is configured as a roll mounting table 3. By opening and closing the furnace door 2, the rolling composite roll 5 can be carried into and out of the first heating furnace. Further, on the lower surface side of the roll mounting table 3, for example, a plurality of rollers 4 are provided as moving means, and the first heating furnace mounted on the substantially flat floor surface FL is rolled by the rollers 4. The composite roll 5 can be moved in the axial direction. On the other hand, in the first heating furnace, a first roll support portion 6 for supporting a rolling composite roll 5 (specifically, a roll body portion 54 to be described later) is provided on the upper surface side of the roll mounting table 3. In addition, burners 7 (two locations in FIG. 1) are provided as heating means for heating the roll for rolling. The first roll support portion 6 is provided with a rolling composite roll 5 that is carried into a second heating furnace used in the next step 2. The rolling composite roll 5 includes a roll shaft portion 52 as an inner layer and a roll barrel portion 54 as an outer layer, and a portion of the roll shaft portion 52 accommodated in the second heating furnace and both ends of the roll barrel portion 54. These are heat-insulated by covering the surface part with a heat insulating material such as ceramic fiber 56, for example.

このような第1加熱炉内に圧延用複合ロール5を設置した後,バーナ7を点火し,後述する工程1による加熱が実施される。   After the rolling composite roll 5 is installed in such a first heating furnace, the burner 7 is ignited, and heating in Step 1 described later is performed.

次に,図2および図3に基づいて,本実施形態に係る圧延用複合ロール5の熱処理方法の工程2に使用する第2加熱炉の構成について説明する。なお,図2は,本実施形態に係る工程2に使用する第2加熱炉の概略的な構成を示す説明図であり,図3は,図2のA−A矢視図である。   Next, based on FIG. 2 and FIG. 3, the structure of the 2nd heating furnace used for the process 2 of the heat processing method of the composite roll 5 for rolling which concerns on this embodiment is demonstrated. FIG. 2 is an explanatory diagram showing a schematic configuration of the second heating furnace used in step 2 according to the present embodiment, and FIG. 3 is a view taken along the line AA of FIG.

図2および図3に示すように,第2加熱炉の本体は,耐火材料からなる略半筒状の形状をした2個の炉殻10から構成される。この炉殻10は開閉可能に構成されており,図3に示したように,閉塞位置10aで接触している2個の炉殻10が,それぞれ水平方向逆向き(図の矢印の向き)に,開放位置10b,10cまで移動することにより,加熱処理される圧延用複合ロール5を第2加熱炉に対して搬入および搬出することができる。なお,圧延用複合ロール5の加熱処理は,炉殻10が閉じられた状態(炉殻10が閉塞位置10aに位置している状態)で行われる。   As shown in FIGS. 2 and 3, the main body of the second heating furnace is composed of two furnace shells 10 having a substantially semi-cylindrical shape made of a refractory material. The furnace shell 10 is configured to be openable and closable. As shown in FIG. 3, the two furnace shells 10 that are in contact with each other at the closing position 10a are respectively opposite in the horizontal direction (the direction of the arrow in the figure). By moving to the open positions 10b and 10c, the rolling composite roll 5 to be heat-treated can be carried into and out of the second heating furnace. Note that the heat treatment of the rolling composite roll 5 is performed in a state where the furnace shell 10 is closed (a state where the furnace shell 10 is located at the closing position 10a).

また,第2加熱炉は,略平坦な床面FLに形成された凹部であるピット20に炉殻10の少なくとも一部が収納され,床面FLのピット20の外側に設けられた第2ロール支持部30により,ロール軸部52の両端が支持されている。この第2ロール支持部30は,略円柱状に形成されており,本実施形態においては,ロール軸部52の両端が,それぞれ,2つずつの第2ロール支持部30により支持されている。ただし,この第2ロール支持部の形状や個数は上記の例に限られず,圧延用複合ロール5を支持できるものであれば,任意の形状や個数のものを使用することができる。   In the second heating furnace, at least a part of the furnace shell 10 is accommodated in a pit 20 which is a recess formed in a substantially flat floor surface FL, and a second roll provided outside the pit 20 on the floor surface FL. Both ends of the roll shaft portion 52 are supported by the support portion 30. The second roll support portion 30 is formed in a substantially cylindrical shape, and in this embodiment, both ends of the roll shaft portion 52 are supported by two second roll support portions 30 respectively. However, the shape and number of the second roll support portions are not limited to the above example, and any shape and number can be used as long as they can support the rolling composite roll 5.

また,ロール軸部52の第2加熱炉の内部にある部分とロール胴部54の両端面部とには,上述したとおり,工程1において,予めセラミックファイバー56で50mm以上の厚みの断熱施工がなされている。一方,ロール軸部52のうち,圧延用複合ロール5の両端部にある断熱していない部分は,炉殻および外気と接触している。よって,この状態で,加熱手段として,例えば,ヒータ40により,第2加熱炉の内部を急激に加熱しても,圧延用複合ロール5のロール胴部54,すなわち外層部のみの温度が上昇し,内層の温度の上昇を防止することができる。   In addition, as described above, heat insulation of 50 mm or more in thickness is performed in advance on the portion inside the second heating furnace of the roll shaft portion 52 and the both end surface portions of the roll body portion 54 with the ceramic fiber 56 in step 1. ing. On the other hand, portions of the roll shaft 52 that are not insulated at both ends of the rolling composite roll 5 are in contact with the furnace shell and the outside air. Therefore, in this state, even if the inside of the second heating furnace is rapidly heated by, for example, the heater 40 as a heating means, the temperature of only the roll body portion 54 of the rolling composite roll 5, that is, the outer layer portion, increases. , The temperature rise of the inner layer can be prevented.

なお,加熱処理される圧延用複合ロール5の製品長さが短く,上記工程2で使用する第2加熱炉の第2ロール支持部30により支持することができない場合には,例えば,第2ロール支持部30により支持可能な圧延用複合ロールの長さに製作し,熱処理後,所定の圧延用複合ロールの長さに切断すればよい。また,別の方法としては,例えば,第2ロール支持部10を圧延用複合ロールの軸方向に移動・設置が可能な構成としてもよい。   When the product length of the rolling composite roll 5 to be heat-treated is short and cannot be supported by the second roll support portion 30 of the second heating furnace used in the above step 2, for example, the second roll What is necessary is just to manufacture to the length of the composite roll for rolling which can be supported by the support part 30, and cut | disconnect to the length of the predetermined composite roll for rolling after heat processing. As another method, for example, the second roll support portion 10 may be configured to be movable / installable in the axial direction of the rolling composite roll.

次に,上述した第1加熱炉および第2加熱炉中で行われる工程1および工程2について詳細に説明する。   Next, the process 1 and the process 2 performed in the 1st heating furnace and the 2nd heating furnace mentioned above are demonstrated in detail.

まず,工程1は,熱処理される圧延用複合ロール5のうち,内層(ロール軸部52)の第2加熱炉に収容される部分と外層(ロール胴部54)の両端面部とを断熱した後,第1加熱炉内にて圧延用複合ロール5全体を常温から600〜700℃まで,10〜30℃/Hrの昇温速度で加熱する工程である。   First, after heat-insulating the part accommodated in the 2nd heating furnace of the inner layer (roll shaft part 52) and the both-ends surface part of an outer layer (roll body part 54) among the composite rolls 5 for heat processing to heat-process, In the first heating furnace, the entire composite roll for rolling 5 is heated from room temperature to 600 to 700 ° C. at a heating rate of 10 to 30 ° C./Hr.

ここで,まず,上記外層としてのロール胴部54や内層としてのロール軸部52を断熱する断熱手段としては,その施工厚みが50mm以上となるように,例えばセラミックファイバーなどの断熱材を使用することが好ましい。断熱材の厚みが50mm未満であると,ロール軸部52およびロール胴部54の両端面への断熱効果が乏しく,断熱手段として好適でない。   Here, first, as a heat insulating means for insulating the roll body portion 54 as the outer layer and the roll shaft portion 52 as the inner layer, for example, a heat insulating material such as ceramic fiber is used so that the construction thickness becomes 50 mm or more. It is preferable. If the thickness of the heat insulating material is less than 50 mm, the heat insulating effect on both end faces of the roll shaft portion 52 and the roll body portion 54 is poor, and it is not suitable as a heat insulating means.

また,上述したように,工程1では,上記圧延用複合ロール5の外層(ロール胴部54)および内層(ロール軸部52)を常温から600〜700℃までを10〜30℃/Hrの昇温速度にて加熱することとしている。   As described above, in step 1, the outer layer (roll body portion 54) and the inner layer (roll shaft portion 52) of the composite roll 5 for rolling are raised from room temperature to 600 to 700 ° C. at a rate of 10 to 30 ° C./Hr. Heating is performed at a temperature rate.

これは,加熱温度が600℃未満であると,工程1に続く工程2の実施内容である第2加熱炉内に圧延用複合ロール5を移動させた後に,ロール5の外層表面を1050〜1150℃の間に加熱するのに要する時間が長くなるため,好ましくない。一方,700℃を超えると,第2加熱炉に圧延用複合ロール5を移動後短時間で昇温可能であるが,内層の昇温も速くなり,オーステナイト化温度へ到達するため好ましくない。以上のように,加熱温度の適正温度としては,600℃以上700℃以下が好適である。   This is because when the heating temperature is less than 600 ° C., the outer roll surface of the roll 5 is moved to 1050 to 1150 after the rolling composite roll 5 is moved into the second heating furnace, which is the content of step 2 following step 1. Since it takes a long time to heat during the temperature, it is not preferable. On the other hand, if the temperature exceeds 700 ° C., the temperature can be raised in a short time after the rolling composite roll 5 is moved to the second heating furnace, but the temperature rise of the inner layer is also accelerated and reaches the austenitizing temperature, which is not preferable. As described above, the appropriate heating temperature is preferably 600 ° C. or higher and 700 ° C. or lower.

また,上記工程1においては,上述した好適な加熱温度の範囲内における昇温速度を10〜30℃/Hrとしている。これは,昇温速度が10℃/Hr未満では,加熱に長時間必要とし,非効率的,非経済的となるため好ましくない。一方,昇温速度が30℃/Hrを超えると,外層表面と中心との温度差が大きくなり,低温域では塑性変形も無いことから,ロールが割損する危険があるため好ましくない。以上のように,適切な昇温速度としては,10℃/Hr以上30℃/Hr以下が好ましい。   Moreover, in the said process 1, the temperature increase rate in the range of the suitable heating temperature mentioned above is 10-30 degreeC / Hr. This is not preferable if the rate of temperature increase is less than 10 ° C./Hr, because it takes a long time for heating and becomes inefficient and uneconomical. On the other hand, if the rate of temperature rise exceeds 30 ° C./Hr, the temperature difference between the outer layer surface and the center increases, and there is no plastic deformation in the low temperature range, which is not preferable because there is a risk of the roll breaking. As described above, an appropriate temperature increase rate is preferably 10 ° C./Hr or more and 30 ° C./Hr or less.

また,工程2は,第2加熱炉に圧延用複合ロール5を移動させた後,外層を600〜700℃から1050〜1150℃まで,300〜600℃/Hrの昇温速度で急速加熱する工程である。   Step 2 is a step of rapidly heating the outer layer from 600 to 700 ° C. to 1050 to 1150 ° C. at a heating rate of 300 to 600 ° C./Hr after moving the rolling composite roll 5 to the second heating furnace. It is.

このように,工程2における圧延用複合ロール5の外層の加熱温度としては,1050〜1150℃の間に加熱することが好ましい。加熱温度が1050℃未満であると,拡散温度が低く,炭化物を基地中に十分固溶させることができないため好ましくない。一方,1150℃を超えると,内層への熱の影響が大きくなり,内層の脆化や結晶粒の粗大化を引き起こすため好ましくない。以上のように,加熱温度の適正温度としては,1050℃以上1150℃以下が好適である。   Thus, as the heating temperature of the outer layer of the composite roll 5 for rolling in the process 2, it is preferable to heat between 1050-1150 degreeC. When the heating temperature is less than 1050 ° C., the diffusion temperature is low, and the carbide cannot be sufficiently dissolved in the matrix, which is not preferable. On the other hand, if the temperature exceeds 1150 ° C., the influence of heat on the inner layer is increased, which leads to embrittlement of the inner layer and coarsening of crystal grains. As described above, the appropriate heating temperature is preferably 1050 ° C. or higher and 1150 ° C. or lower.

また,上記工程2において,上述した好適な加熱温度の範囲内における昇温速度を300〜600℃/Hrとしている。これは,昇温温度が300℃/Hr未満では,加熱に長時間必要であるため内層がオーステナイト化し,内層の脆化や結晶粒の粗大化を引き起こすため好ましくない。一方,昇温速度が600℃/Hrを超えると,外層表面の均一な温度分布を確保することが困難となり,外層軸方向で硬度がばらつくことが懸念されるため好ましくない。以上のように,適切な昇温速度としては,300℃/Hr以上600℃/Hr以下であることが好ましい。   Moreover, in the said process 2, the temperature increase rate in the range of the suitable heating temperature mentioned above is 300-600 degreeC / Hr. This is not preferable when the temperature rising temperature is less than 300 ° C./Hr, because heating requires a long time, so that the inner layer becomes austenite, causing embrittlement of the inner layer and coarsening of crystal grains. On the other hand, if the rate of temperature rise exceeds 600 ° C./Hr, it is difficult to ensure a uniform temperature distribution on the outer layer surface, and there is a concern that the hardness may vary in the outer layer axial direction, which is not preferable. As described above, an appropriate temperature increase rate is preferably 300 ° C./Hr or more and 600 ° C./Hr or less.

なお,上述したような工程1および工程2を含む焼入れの後に実施する焼戻しとしては,公知の方法を使用することができるが,本実施形態における実施の目的は,焼入れ時の残留γ(オーステナイト)のマルテンサイトまたはベイナイト変態促進および2次炭化物を析出させ,組織を安定化し,硬度および靭性を向上させることである。したがって,本実施形態における焼戻しの方法としては,例えば,焼入れ後の圧延用複合ロール5を加熱炉に入れ,500〜550℃の範囲で1〜2回焼戻しするとよい。   In addition, as the tempering performed after the quenching including the steps 1 and 2 as described above, a known method can be used, but the purpose of the embodiment in this embodiment is to retain residual γ (austenite) at the time of quenching. Is to promote the transformation of martensite or bainite and to precipitate secondary carbide, stabilize the structure, and improve the hardness and toughness. Therefore, as a method of tempering in the present embodiment, for example, the rolled composite roll 5 after quenching is put in a heating furnace and tempered in the range of 500 to 550 ° C. once or twice.

以下,実施例により本発明をさらに具体的に説明するが,本発明は,下記実施例にのみ限定されるものではない。   Hereinafter, the present invention will be described more specifically with reference to examples. However, the present invention is not limited to the following examples.

(実施例1〜6に係る圧延用複合ロールの製造)
外層材として,C:1.9〜2.1%,Si:0.7〜1.0%,Mn:0.6〜1.0%,Cr:4.5〜7.5%,Mo:5.0〜8.0%,V:4.0〜5.5%,残部がFeおよび不可避的元素からなるハイス系化学成分で構成される溶湯を用いて,遠心鋳造法により外層を形成した。次いで,この外層の内部にダクタイル鋳鉄からなる内層材を静置鋳造して,胴寸法の直径が809mm,長さが2210mm,外層の厚みが80mmの圧延用複合ロールを製造した。
(Manufacture of the composite roll for rolling which concerns on Examples 1-6)
As an outer layer material, C: 1.9 to 2.1%, Si: 0.7 to 1.0%, Mn: 0.6 to 1.0%, Cr: 4.5 to 7.5%, Mo: 5.0 to 8.0%, V: 4.0 to 5.5%, the outer layer was formed by centrifugal casting using a molten metal composed of a high-speed chemical component consisting of Fe and inevitable elements as the balance. . Next, an inner layer material made of ductile cast iron was statically cast inside the outer layer to produce a composite roll for rolling having a body size diameter of 809 mm, a length of 2210 mm, and an outer layer thickness of 80 mm.

その後,下記に示す熱処理を実施した。上記図1〜図3およびその説明に示すように,加熱処理される圧延用複合ロールのロール軸部のうち第2加熱炉内に収容される部分とロール胴部の両端面部とを55mmの厚みのセラミックファイバーで覆うことにより断熱し,さらに,この圧延用複合ロールを,第1加熱炉内で下記表1(実施例1〜6)の工程1の欄に記載された各々の加熱温度,昇温速度にて加熱した。   Thereafter, the following heat treatment was performed. As shown in FIGS. 1 to 3 and the description thereof, a portion of the roll shaft portion of the rolling composite roll to be heat-treated and a portion accommodated in the second heating furnace and both end surface portions of the roll body portion are 55 mm thick. The composite roll for rolling is further insulated by covering with a ceramic fiber, and the heating temperature and the temperature are increased in the first heating furnace described in the column of step 1 in Table 1 (Examples 1 to 6) below. Heated at a warm rate.

続いて,この圧延用複合ロールを上記第2加熱炉に移動させ,その後,当該圧延用複合ロールを表1(実施例1〜6)の工程2の欄に記載された加熱温度,昇温速度で各々加熱した。さらに,衝風冷却により急冷して焼入れし,その後約550℃で約15時間保持する焼戻しを2回実施して,実施例1〜6に係る熱処理後の圧延用複合ロールを製造した。   Subsequently, the rolling composite roll is moved to the second heating furnace, and then the rolling composite roll is heated at the heating temperature and rate of temperature described in Step 2 of Table 1 (Examples 1 to 6). Each was heated. Further, quenching was performed by quenching by blast cooling, followed by tempering that was held at about 550 ° C. for about 15 hours twice, to produce a heat-treated composite roll according to Examples 1 to 6.

(比較例1〜8に係る圧延用複合ロールの製造)
外層材として,上記実施例1〜6と同じハイス系化学成分からなる溶湯を用いて遠心鋳造法により外層を形成した後,この外層の内部にダクタイル鋳鉄からなる内層材を静置鋳造して,胴寸法の直径が809mm,長さが2210mm,外層の厚みが80mmの圧延用複合ロールを製造した。
(Manufacture of the composite roll for rolling which concerns on Comparative Examples 1-8)
As an outer layer material, after forming the outer layer by centrifugal casting using the same high-speed chemical component as in Examples 1 to 6, the inner layer material made of ductile cast iron is statically cast inside the outer layer, A composite roll for rolling with a body size diameter of 809 mm, a length of 2210 mm, and an outer layer thickness of 80 mm was produced.

その後,下記に示す熱処理を行った。上記図1〜図3およびその説明に示すように,加熱処理される圧延用複合ロールのロール軸部のうち第2加熱炉内に収容される部分とロール胴部の両端面部とを,55mmの厚みのセラミックファイバーで覆うことにより断熱し,さらに,この圧延用複合ロールを,第1加熱炉内で下記表1(比較例1〜8)の工程1の欄に記載されたそれぞれの加熱温度,昇温速度で加熱した。   Thereafter, the following heat treatment was performed. As shown in FIGS. 1 to 3 and the description thereof, a portion of the roll shaft portion of the rolling composite roll to be heat-treated and a portion accommodated in the second heating furnace and both end surface portions of the roll body portion are 55 mm in length. Each of the heating rolls described in the column of step 1 of the following Table 1 (Comparative Examples 1 to 8) in the first heating furnace is further insulated by covering with a ceramic fiber having a thickness. It heated at the temperature increase rate.

続いて,この圧延用複合ロールを上記第2加熱炉に移動させ,その後,当該圧延用複合ロールを表1(比較例1〜8)の工程2の欄に記載された加熱温度,昇温速度にて各々加熱した。さらに,衝風冷却により急冷して焼入れし,その後約550℃で約15時間保持する焼戻しを2回実施して,比較例1〜8に係る熱処理後の圧延用複合ロールを製造した。   Subsequently, this rolling composite roll is moved to the second heating furnace, and then the rolling composite roll is heated at the heating temperature and rate of temperature described in Step 2 of Table 1 (Comparative Examples 1 to 8). Each was heated. Further, quenching was performed by quenching by blast cooling, followed by tempering that was held at about 550 ° C. for about 15 hours twice, to produce a heat-treated composite roll according to Comparative Examples 1-8.

上述したようにして製造された,実施例1〜6および比較例1〜8に係る圧延用複合ロールについて,以下のようにして,引張試験および硬度の測定を行った。   About the composite roll for rolling which concerns on Examples 1-6 and Comparative Examples 1-8 manufactured as mentioned above, the tension test and the measurement of hardness were performed as follows.

(引張試験)
上記実施例1〜6および比較例1〜8の圧延用複合ロールについて,各々のロールの内層部よりJIS4号の引張り試験片を採取し,引張り試験を実施した(JIS Z2201)。その結果を下記表1に併せて示す。
(Tensile test)
About the composite roll for rolling of the said Examples 1-6 and Comparative Examples 1-8, the tension test piece of JIS4 was extract | collected from the inner-layer part of each roll, and the tension test was implemented (JISZ2201). The results are also shown in Table 1 below.

(硬度の測定)
上記実施例1〜6および比較例1〜8の圧延用複合ロールについて,各々のロールの外層の酸化皮膜を取り除くために,機械加工により,外周面から径方向に片肉で15mm削り取った。削り取った後の面が,圧延用複合ロールの初径面として供される。この初径面の硬度をショア硬度計により測定した。その結果を下記表1に併せて示す。
(Measurement of hardness)
About the composite roll for rolling of the said Examples 1-6 and Comparative Examples 1-8, in order to remove the oxide film of the outer layer of each roll, 15 mm was shaved off from the outer peripheral surface by the single-piece | unit thickness to the radial direction. The surface after scraping is used as the initial diameter surface of the composite roll for rolling. The hardness of this initial diameter surface was measured with a Shore hardness meter. The results are also shown in Table 1 below.

Figure 2006299360
Figure 2006299360

(結果の評価)
表1に示したように,実施例1〜6に係る圧延用複合ロールにおいては,比較例3,5,6および8に係るロールと比べ,いずれもその引張り強度は400MPa以上と高く,上述したように,内層材として鋳鉄剤を用いた場合に発生していた内層の偏析部が溶融することによる強靭性の低下が発生していないものと判断される。さらに,硬度についても,実施例1〜6に係る圧延用複合ロールは,比較例1〜8に係るロールと同様に高い値を有しており,健全な熱処理が実施されていることが明確であるといえる。
(Evaluation of results)
As shown in Table 1, in the rolling composite rolls according to Examples 1 to 6, all the tensile strengths were higher than 400 MPa as compared with the rolls according to Comparative Examples 3, 5, 6 and 8, which were described above. Thus, it is judged that the deterioration of toughness due to melting of the segregated portion of the inner layer that occurred when the cast iron agent was used as the inner layer material did not occur. Furthermore, also about hardness, the composite roll for rolling which concerns on Examples 1-6 has a high value similarly to the roll which concerns on Comparative Examples 1-8, and it is clear that the sound heat processing is implemented. It can be said that there is.

これに対し,比較例1に係るロールは,工程1における昇温速度が,本発明に係る熱処理方法における下限値である10℃/Hrより低い9℃/Hrで実施しているため,引張り強度は,実施例1〜6と同様に高い値を有しており,内層の内部には偏析が生じていないと判断されるが,上述のように,処理時間を多く必要とするため,生産性の点から好ましくない。   On the other hand, since the roll according to Comparative Example 1 is carried out at 9 ° C./Hr, the temperature increase rate in Step 1 is lower than 10 ° C./Hr, which is the lower limit value in the heat treatment method according to the present invention. Has a high value as in Examples 1 to 6, and it is judged that segregation does not occur in the inner layer. However, as described above, a long processing time is required. From the point of view, it is not preferable.

また,比較例2に係るロールは,工程1における昇温速度が,本発明に係る熱処理方法における上限値である30℃/Hrより高い34℃/Hrで実施しているため,本工程1の加熱処理中にロールが割損した。なお,工程1中ロールが割損したため,比較例2については,工程2は実施していない。   Moreover, since the roll according to Comparative Example 2 is performed at 34 ° C./Hr, which is higher than the upper limit of 30 ° C./Hr, which is the upper limit value in the heat treatment method according to the present invention, in the step 1, The roll broke during the heat treatment. In addition, since the roll was broken during the process 1, the process 2 was not performed for the comparative example 2.

また,比較例3に係るロールは,工程2における昇温速度が,本発明に係る熱処理方法における下限値である300℃/Hrより低い290℃/Hrで実施しているため,引張り強度は,実施例1〜6と比べて,極端に低い値となった。このことから,比較例3に係るロールにおいては,上述のとおり,加熱時間を多く必要とするため,内層がオーステナイト化し,内層が脆化または結晶粒が粗大化しているものと判断される。   Moreover, since the roll according to Comparative Example 3 is carried out at 290 ° C./Hr where the rate of temperature increase in Step 2 is lower than 300 ° C./Hr, which is the lower limit in the heat treatment method according to the present invention, the tensile strength is Compared to Examples 1 to 6, the value was extremely low. From this, in the roll which concerns on the comparative example 3, since many heating time is required as above-mentioned, it is judged that the inner layer is austenite and the inner layer becomes embrittled or the crystal grain is coarsened.

また,比較例4に係るロールは,工程2における昇温速度が,本発明に係る熱処理方法における上限値である600℃/Hrより高い615℃/Hrで実施しているため,引張り強度は,実施例1〜6に比べ遜色ない試験結果が得られたものの,外層表面の均一な温度分布の確保が困難となり,表層軸方向で硬度にばらつきが発生した。具体的には,ロールの軸方向両端部で硬度Hsが78,78,軸方向中央部で硬度Hsが82となった。   Moreover, since the roll according to Comparative Example 4 is performed at 615 ° C./Hr, which is higher than the upper limit of 600 ° C./Hr in the heat treatment method according to the present invention, the tensile strength in Step 2 is Although test results comparable to those of Examples 1 to 6 were obtained, it was difficult to ensure a uniform temperature distribution on the outer layer surface, and the hardness varied in the surface layer axis direction. Specifically, the hardness Hs was 78, 78 at both axial end portions of the roll, and the hardness Hs was 82 at the axial central portion.

また,比較例5に係るロールは,工程1における加熱温度が,本発明に係る熱処理方法における下限値である600℃より低い580℃で実施しているため,引張り強度は実施例1〜6に比べ低い値となった。このことから,上述のとおり,比較例5に係るロールにおいては,加熱時間を多く必要とするため,内層がオーステナイト化し,内層が脆化または結晶粒が粗大化していると判断される。   Moreover, since the roll which concerns on the comparative example 5 is implemented at 580 degreeC in which the heating temperature in the process 1 is lower than 600 degreeC which is the minimum value in the heat processing method which concerns on this invention, tensile strength is in Examples 1-6. Compared to the lower value. Therefore, as described above, the roll according to Comparative Example 5 requires a lot of heating time, and therefore, it is determined that the inner layer is austenitic and the inner layer is brittle or the crystal grains are coarsened.

また,比較例6に係るロールは,工程1における加熱温度が,本発明に係る熱処理方法の上限値である700℃より高い715℃で実施しているため,引張り強度が実施例1〜6に比べ低い値となった。このことから,上述のとおり,比較例6に係るロールにおいては,内層が加熱中オーステナイト化したことにより,内層が脆化または結晶粒が粗大化しているものと判断される。   Moreover, since the roll which concerns on the comparative example 6 is implemented at 715 degreeC whose heating temperature in the process 1 is higher than 700 degreeC which is the upper limit of the heat processing method which concerns on this invention, tensile strength is in Examples 1-6. Compared to the lower value. From this, as described above, in the roll according to Comparative Example 6, it is determined that the inner layer is austenitized during heating, so that the inner layer is embrittled or crystal grains are coarsened.

また,比較例7に係るロールは,工程2における加熱温度が,本発明に係る熱処理方法における下限値である1050℃より低い1000℃で実施しているため,硬度が著しく低い。このことから,上述のとおり,比較例7に係るロールにおいては,拡散温度が低く炭化物を基地中に十分固溶させることができないものと判断される。   Further, the roll according to Comparative Example 7 has a remarkably low hardness because the heating temperature in step 2 is 1000 ° C. which is lower than the lower limit of 1050 ° C. in the heat treatment method according to the present invention. From this, as mentioned above, in the roll which concerns on the comparative example 7, it is judged that a diffusion temperature is low and a carbide | carbonized_material cannot fully dissolve in a base.

また,比較例8に係るロールは,工程2における加熱温度が,本発明に係る熱処理方法における上限値である1150℃より高い1160℃で実施しているため,引張り強度が実施例1〜6よりも低い。このことから,上述のとおり,比較例8に係るロールにおいては,内層が加熱中にオーステナイト化したことにより,内層が脆化または結晶粒が粗大化していると判断される。   Moreover, since the roll which concerns on the comparative example 8 is implemented at 1160 degreeC whose heating temperature in process 2 is higher than 1150 degreeC which is the upper limit in the heat processing method which concerns on this invention, tensile strength is from Examples 1-6. Is also low. From this, as described above, in the roll according to Comparative Example 8, it is judged that the inner layer is austenitized during heating, so that the inner layer is embrittled or crystal grains are coarsened.

このように,本実施形態に係る圧延用複合ロールの熱処理方法によれば,内層の昇熱を最小限に抑え,内層の脆化,結晶粒の粗大化を防止するとともに,短時間で外層のみをオーステナイト化でき,外層の炭化物を基地中に十分に固溶させ,ハイスの特性を引き出すことが可能となる。   Thus, according to the heat treatment method for a composite roll for rolling according to the present embodiment, the heating of the inner layer is minimized, the embrittlement of the inner layer and the coarsening of the crystal grains are prevented, and only the outer layer is formed in a short time. The austenite can be converted into austenite, and the carbides of the outer layer can be sufficiently dissolved in the matrix to bring out the characteristics of high speed steel.

以上,添付図面を参照しながら本発明の好適な実施形態について説明したが,本発明はかかる例に限定されないことは言うまでもない。当業者であれば,特許請求の範囲に記載された範疇内において,各種の変更例または修正例に想到し得ることは明らかであり,それらについても当然に本発明の技術的範囲に属するものと了解される。   As mentioned above, although preferred embodiment of this invention was described referring an accompanying drawing, it cannot be overemphasized that this invention is not limited to this example. It will be apparent to those skilled in the art that various changes and modifications can be made within the scope of the claims, and these are of course within the technical scope of the present invention. Understood.

本発明は,外層にハイス材を用いた熱間圧延または冷間圧延用複合ロールの熱処理方法に適用可能である。   The present invention can be applied to a heat treatment method for a hot roll or a cold roll composite roll using a high-speed steel as an outer layer.

本発明の一実施形態に係る工程1に使用する第1加熱炉の構成の概要を示す説明図である。It is explanatory drawing which shows the outline | summary of a structure of the 1st heating furnace used for the process 1 which concerns on one Embodiment of this invention. 本発明の一実施形態に係る工程2に使用する第2加熱炉の構成の概要を示す説明図である。It is explanatory drawing which shows the outline | summary of a structure of the 2nd heating furnace used for the process 2 which concerns on one Embodiment of this invention. 図2のA−A矢視図である。It is an AA arrow line view of FIG.

符号の説明Explanation of symbols

1 炉殻
2 炉扉
3 ロール載置台
4 コロ
5 圧延用複合ロール
6 第1ロール支持部材
7 バーナ
10 炉殻
20 ピット
30 第2ロール支持部材
40 ヒータ
52 ロール軸部
54 ロール胴部
56 セラミックファイバー(断熱材)
DESCRIPTION OF SYMBOLS 1 Furnace shell 2 Furnace door 3 Roll mounting stand 4 Roll 5 Composite roll for rolling 6 First roll support member 7 Burner 10 Furnace shell 20 Pit 30 Second roll support member 40 Heater 52 Roll shaft part 54 Roll body part 56 Ceramic fiber ( Insulation)

Claims (1)

遠心力鋳造により形成されるハイス材からなる外層に,強靭性を有する材料からなる内層を冶金的に一体化して製造される圧延用複合ロールに対して,オーステナイト化温度まで加熱後に冷却する焼入れ処理を行った後,焼戻し処理を行う圧延用複合ロールの熱処理方法において:
前記オーステナイト化温度までの加熱は,第1加熱炉中で行う第1工程と,第2加熱炉中で行う第2工程とを含み,
前記第1工程は,前記圧延用複合ロールのうち,前記内層の前記第2加熱炉に収容される部分と前記外層の両端面部とを断熱した後,前記第1加熱炉内にて前記圧延用複合ロール全体を常温から600〜700℃まで,10〜30℃/Hrの昇温速度で加熱する工程であり,
前記第2工程は,前記第2加熱炉に前記圧延用複合ロールを移動させた後,前記外層を600〜700℃から1050〜1150℃まで,300〜600℃/Hrの昇温速度で加熱する工程であることを特徴とする,圧延用複合ロールの熱処理方法。


Quenching treatment that cools after heating to the austenitizing temperature for a composite roll for rolling manufactured by metallurgically integrating an inner layer made of a tough material with an outer layer made of high-speed steel formed by centrifugal casting In the heat treatment method for a composite roll for rolling that is tempered after performing:
The heating to the austenitizing temperature includes a first step performed in a first heating furnace and a second step performed in a second heating furnace,
The first step insulates the portion of the inner roll that is accommodated in the second heating furnace and both end faces of the outer layer, and then rolls the rolling in the first heating furnace. The entire composite roll is heated from room temperature to 600 to 700 ° C. at a heating rate of 10 to 30 ° C./Hr.
In the second step, after the rolling composite roll is moved to the second heating furnace, the outer layer is heated from 600 to 700 ° C. to 1050 to 1150 ° C. at a temperature rising rate of 300 to 600 ° C./Hr. A heat treatment method for a composite roll for rolling, which is a process.


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Publication number Priority date Publication date Assignee Title
WO2008023744A1 (en) 2006-08-22 2008-02-28 Mitsubishi Chemical Corporation Lithium difluorophosphate, electrolytic solution containing lithium difluorophosphate, process for producing lithium difluorophosphate, process for producing nonaqueous electrolytic solution, nonaqueous electrolytic solution, and nonaqueous-electrolytic-solution secondary cell employing the same
JP2009061473A (en) * 2007-09-06 2009-03-26 Sumitomo Metal Ind Ltd Method for manufacturing high-strength component
CN114082922A (en) * 2021-12-31 2022-02-25 甘肃酒钢集团西部重工股份有限公司 Method for manufacturing high-speed steel roller
CN114737139A (en) * 2022-03-09 2022-07-12 华勇略 Grain grinding roller and preparation method thereof

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Publication number Priority date Publication date Assignee Title
WO2008023744A1 (en) 2006-08-22 2008-02-28 Mitsubishi Chemical Corporation Lithium difluorophosphate, electrolytic solution containing lithium difluorophosphate, process for producing lithium difluorophosphate, process for producing nonaqueous electrolytic solution, nonaqueous electrolytic solution, and nonaqueous-electrolytic-solution secondary cell employing the same
JP2009061473A (en) * 2007-09-06 2009-03-26 Sumitomo Metal Ind Ltd Method for manufacturing high-strength component
CN114082922A (en) * 2021-12-31 2022-02-25 甘肃酒钢集团西部重工股份有限公司 Method for manufacturing high-speed steel roller
CN114737139A (en) * 2022-03-09 2022-07-12 华勇略 Grain grinding roller and preparation method thereof

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