JP2006084263A - Gas leak inspection device - Google Patents

Gas leak inspection device Download PDF

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JP2006084263A
JP2006084263A JP2004267997A JP2004267997A JP2006084263A JP 2006084263 A JP2006084263 A JP 2006084263A JP 2004267997 A JP2004267997 A JP 2004267997A JP 2004267997 A JP2004267997 A JP 2004267997A JP 2006084263 A JP2006084263 A JP 2006084263A
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gas
inspection
leak
flow meter
flow rate
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JP4281001B2 (en
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Yasuo Kaga
保男 加賀
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National Institute of Advanced Industrial Science and Technology AIST
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Abstract

<P>PROBLEM TO BE SOLVED: To provide a gas leak inspection device for finding a gas leak in an object under inspection by a simple means during gas tightness inspection. <P>SOLUTION: This gas leak inspection device comprises the object under inspection made up of piping, a gas tight container, etc., a gas quantitative feeder 50 for feeding a definite amount of gas to the object, a gas pressure controller 7 for controlling gas pressure in the object, and a flow meter 8 for measuring the amount of gas discharged from the object. The amount of gas flowing through the flow meter 8 is measured with respect to a certain gas pressure in the object while measuring the amount of gas flowing through the flow meter with respect to another gas pressure in the object. This device is characterized in that the amount of gas leak in the object during gas tightness inspection is found from the ratio of a difference in the measured gas pressures to a difference in the gas flow meter. <P>COPYRIGHT: (C)2006,JPO&NCIPI

Description

本発明は、配管工事等の完成検査時に、完成した配管(付属部品一式すべて含めて)や気密容器に漏れが有るか無いかを、定量的に検査するリーク検査装置に関する。   The present invention relates to a leak inspection apparatus for quantitatively inspecting whether or not there is a leak in a completed pipe (including all accessories) and an airtight container at the time of completion inspection such as piping work.

通常ガス配管を行った場合、完成時の引き渡し時に、配管の気密検査が行われる。配管全体で漏れがないことを確認したのち、気密検査成績書等を提出する。しかし、この検査成績書も指定検査圧力で漏れはありませんといった程度のものであり、指定検査圧力で何cc/min(またはg/sec等)以下の気密性能を有する等と定量的に行われるものではない。   When performing normal gas piping, airtight inspection of the piping is performed at the time of delivery at the time of completion. After confirming that there are no leaks in the entire pipe, submit an airtight inspection report. However, this inspection report is of such a level that there is no leakage at the specified inspection pressure, and it is quantitatively performed as having a hermetic performance of several cc / min (or g / sec, etc.) at the specified inspection pressure. is not.

通常簡単に気密検査をする場合、石鹸水等をかけて泡がでないことを確認し漏れがないことを確認している。また、指定検査圧力で配管にガスを封入し、封止してある程度の時間(数時間から十数時間程度かかる)をおいて、圧力の低下しないことを確認して検査している。しかし、前者の場合は配管が長距離の場合は、非常に大変な作業となり、検査漏れになる場合がある。また、後者の場合圧力をかけて封止しても、一日のうちでは朝夕と日中での気温差や、短時間での気温の変動等があると、温度によるガスの体積変化は非常に大きくなるため、圧力が封止時の初期値と同一になるとは限らず、場合によっては高くなる場合もある。   Usually, when performing an air tightness check, it is confirmed that there are no bubbles by applying soapy water, etc., and there is no leakage. In addition, gas is sealed in piping at a specified inspection pressure, and after a certain amount of time (several hours to several tens of hours) is sealed, it is inspected after confirming that the pressure does not drop. However, in the former case, if the piping is long distance, it is a very difficult work, which may result in an inspection failure. In the latter case, even if pressure is applied and sealed, if there is a difference in temperature between morning and evening in the day, or a change in temperature in a short time, the volume change of the gas due to temperature will be extremely high. Therefore, the pressure is not always the same as the initial value at the time of sealing, and may be increased in some cases.

従来のように、石鹸水をかけて試験したりする場合に、配管が必ずしもいつも検査しやすい位置にあるとは限らず、狭い場所や、手の届かない所、曲がりくねった場所、または配管の裏表で全周に亘って試験しなければならず、実施しにくい場合もある。そして、それを全長に亘って試験しなければならない場合は、非常に大変な作業となる。
特に、リークが危険を招く場合は、より高感度なリーク試験装置として、ヘリウムガスを使用した、ヘリウムリークディテクタ等の高価な装置も市販されている。これは大気中に無いヘリウムガスを使用して、加圧してリーク試験を行い、リークがあればその部分に漏れたヘリウムが存在するため、検出器が反応する様になっているものである。これも石鹸水の泡を目で見る代わりに、ヘリウムガスをディテクタで検出するものである。つまり漏れている部分からでてくるガスが有るか無いかを調べる方法であり、原理的には石鹸水と同じ方法となる。従って、前記と同様に、検査部全体をくまなく検査しなければならず、検査に大変な作業を要する。
When testing with soapy water as in the past, piping is not always in a position that is easy to inspect. In this case, the test must be performed over the entire circumference, which may be difficult to implement. And if it has to be tested over its entire length, it is a very difficult task.
In particular, when a leak causes danger, an expensive apparatus such as a helium leak detector using helium gas is also commercially available as a more sensitive leak test apparatus. In this case, a helium gas not in the atmosphere is used for pressurization and a leak test is performed. If there is a leak, the leaked helium is present in that portion, so that the detector reacts. This also detects helium gas with a detector instead of seeing soapy water bubbles. In other words, it is a method for examining whether or not there is gas coming out from the leaking portion, and in principle it is the same method as soapy water. Therefore, as described above, the entire inspection section must be inspected thoroughly, and inspection requires a great deal of work.

本発明の目的は、上記の問題点に鑑み、気密検査時における被検査対象物のガスリークを簡便な手段で求めることを可能にしたガスリーク検査装置を提供することにある。   In view of the above-described problems, an object of the present invention is to provide a gas leak inspection apparatus capable of obtaining a gas leak of an object to be inspected at an airtight inspection by a simple means.

本発明は、上記の問題を解決するために、下記の手段を採用した。
第1の手段は、配管や気密容器等からなる被検査対象物と、該被検査対象物に一定量のガスを供給するガス定量供給装置と、前記被検査対象物内のガス圧力を制御するガス圧力制御装置と、前記被検査対象物から排出されるガス量を計測する流量計とから構成され、前記被検査対象物におけるあるガス圧力に対する前記流量計におけるガス流量を計測するとともに、前記被検査対象物における他のあるガス圧力に対する前記流量計におけるガス流量とを計測し、前記計測されたガス圧力の差に対する前記ガス流量計の差との比から、気密検査時における被検査対象物のガスリーク量を求めることを特徴とするガスリーク検査装置である。
The present invention employs the following means in order to solve the above problems.
The first means controls an object to be inspected consisting of a pipe, an airtight container, etc., a gas fixed amount supply device for supplying a certain amount of gas to the object to be inspected, and a gas pressure in the object to be inspected. A gas pressure control device; and a flow meter that measures the amount of gas discharged from the object to be inspected, and measures the gas flow rate in the flow meter with respect to a certain gas pressure in the object to be inspected. The gas flow rate in the flow meter with respect to some other gas pressure in the inspection object is measured, and from the ratio of the difference in the gas flow meter with respect to the difference in the measured gas pressure, the inspection object at the time of the airtight inspection A gas leak inspection apparatus characterized by obtaining a gas leak amount.

請求項1に記載の発明によれば、一カ所から一度に被検査対象物である全ラインが測定できる利点が有り、その測定デ−タも流量値(質量流量換算)であるため定量的な表現となる。
また、測定が簡単で全体を一度に検査できるので、被検査対象物としてラインの定期的な保守等にも使用でき、異常が早期に発見でき、ラインを予め何カ所かに分けられるようにバルブを付けて配管を区切るようにすれば、部分毎にチェックができ、異常箇所も迅速に発見できる。
According to the first aspect of the present invention, there is an advantage that all lines that are the objects to be inspected can be measured from one place at a time, and since the measurement data is also a flow rate value (mass flow rate conversion), it is quantitative. It becomes an expression.
In addition, since the measurement is simple and the whole can be inspected at once, it can also be used for periodic maintenance of the line as the object to be inspected, so that abnormalities can be detected early, and the line can be divided into several places in advance. If the pipes are separated by attaching, the check can be made for each part, and the abnormal part can be found quickly.

本発明の実施形態を図1乃至図6を用いて説明する。
図1は、本実施形態の発明に係るガスリーク検査装置の構成を示す図。図2はガスリーク検査装置に適用される被検査対象物の構成の一例を示す図ある。
これらの図において、入口ガス定量供給装置50は、ガスボンベ1、減圧弁2、質量流量型流量制御装置3、圧力計5、ガス供給口11によって構成され、出口ガス流量計測装置51はガス導入口12、圧力計6、加圧制御装置7、質量流量型流量計8、排気ライン10によって構成される。また、被検査対象物54は被検査対象物本体、バルブ61、圧力計62等で構成される。
これらの図に示すように、図1に示すガスリーク検査装置の入口ガス定量供給装置50のガス供給接続口11は、図2に示す被検査対象物54である被測定対象ラインガス入口25に接続されてガスが供給され、被検査対象物54の被測定対象ラインガス出口26は、図1に示す流量測定装置接続口12に接続され、出口ガス流量計測装置51の質量流量型流量計8を通過したガス量を測定することによってガスリークが測定される。
ここで、 入口ガス定量供給装置50は、図2に示す被検査対象物54に測定中常に一定値のガスを安定供給するのみであり、出口ガス流量計測装置51に設けた加圧装置7を使用して、被検査対象物54である被検査対象ライン(被検査配管)の内圧を変え、印加圧力値(圧力計6)に対するそのときの質量流量型流量計8のガス流量を測定する。
An embodiment of the present invention will be described with reference to FIGS.
FIG. 1 is a diagram showing a configuration of a gas leak inspection apparatus according to the invention of this embodiment. FIG. 2 is a diagram illustrating an example of a configuration of an inspection target applied to the gas leak inspection apparatus.
In these drawings, an inlet gas fixed amount supply device 50 includes a gas cylinder 1, a pressure reducing valve 2, a mass flow rate type flow rate control device 3, a pressure gauge 5, and a gas supply port 11. An outlet gas flow rate measuring device 51 is a gas introduction port. 12, a pressure gauge 6, a pressurization control device 7, a mass flow type flow meter 8, and an exhaust line 10. Further, the inspection object 54 includes an inspection object main body, a valve 61, a pressure gauge 62, and the like.
As shown in these drawings, the gas supply connection port 11 of the inlet gas quantitative supply device 50 of the gas leak inspection apparatus shown in FIG. 1 is connected to the measurement target line gas inlet 25 which is the inspection target 54 shown in FIG. Then, the gas to be measured is supplied, and the line gas outlet 26 of the object 54 to be inspected is connected to the flow measuring device connection port 12 shown in FIG. 1, and the mass flow type flow meter 8 of the outlet gas flow measuring device 51 is connected. Gas leak is measured by measuring the amount of gas passed.
Here, the inlet gas fixed amount supply device 50 only stably supplies a constant value of gas during measurement to the inspection object 54 shown in FIG. 2, and the pressurization device 7 provided in the outlet gas flow rate measuring device 51 is provided. In use, the internal pressure of the inspection target line (inspected piping) that is the inspection target 54 is changed, and the gas flow rate of the mass flow rate flow meter 8 at that time with respect to the applied pressure value (pressure gauge 6) is measured.

このように、本実施形態のガスリーク検査装置においては、被検査対象物54からのガスリーク量が印加ガス圧力に比例して大きくなる現象に着目したものであり、出口ガス流量計測装置51側に加圧用の加圧制御装置7を設け、これによって圧力を2点以上変化させる。ガスリークが有る場合はその出口側の質量流量型流量計8のガス流量値に変化を生ずる。このように、入口側の流量は一定を保つているだけで出口側の流量の変化のみを測定してガスリークを検査することが可能となる。この原理を応用し出口側の一台の質量流量型流量計のみで、圧力に対する流量値の変化を測定し、その変化の傾きから安定して、高い精度でリークするガスを定量的に求めることができる。
この場合、質量流量型流量計8のカタログ値の精度としての相対精度(±0.2%)の範囲で測定できるので非常に高精度な測定を可能とする。絶対精度(±2%)を利用して測定する場合の10倍の精度を達成できる。
As described above, in the gas leak inspection apparatus according to the present embodiment, attention is paid to the phenomenon that the amount of gas leak from the inspection object 54 increases in proportion to the applied gas pressure, and is added to the outlet gas flow rate measurement apparatus 51 side. A pressure control device 7 for pressure is provided, and thereby the pressure is changed by two or more points. When there is a gas leak, a change occurs in the gas flow rate value of the mass flow type flow meter 8 on the outlet side. In this way, it is possible to inspect the gas leak by measuring only the change in the flow rate on the outlet side while keeping the flow rate on the inlet side constant. Apply this principle to measure the change in flow rate value with respect to pressure with only one mass flow meter on the outlet side, and quantitatively determine the gas that leaks stably and with high accuracy from the slope of the change. Can do.
In this case, since the measurement can be performed within the range of the relative accuracy (± 0.2%) as the accuracy of the catalog value of the mass flow type flow meter 8, a very high accuracy measurement is possible. It is possible to achieve 10 times the accuracy when measuring using absolute accuracy (± 2%).

図3は、被検査対象物54にリークのない場合の測定例を示す図であり、横軸は図1に示す出口ガス流量計測装置51の圧力計6によって計測された圧力値、縦軸は図1に示す出口ガス流量計測装置51の質量流量型流量計8によって計測されたガス流量値である。
同図に示すように、被検査対象物54にリークのない場合は、加圧制御装置7を使用して加圧した状態でも、質量流量型流量計8に減少を生じないのでガス圧力に対して流量の測定値が一定値であることを示す。
FIG. 3 is a diagram showing a measurement example in the case where there is no leak in the inspection object 54. The horizontal axis is the pressure value measured by the pressure gauge 6 of the outlet gas flow rate measuring device 51 shown in FIG. It is the gas flow rate value measured by the mass flow type flow meter 8 of the outlet gas flow rate measuring device 51 shown in FIG.
As shown in the figure, when there is no leak in the inspected object 54, the mass flow type flow meter 8 does not decrease even when pressurized using the pressurization control device 7, so that the gas pressure is not affected. Indicates that the measured value of the flow rate is constant.

図4は被検査対象物54に多少リークのある場合の測定例を示す図であり、出口ガス流量計測装置51の加圧制御装置7の圧力を上昇していくと、質量流量型流量計8の流量の測定値が減少してゆく。この例から解るように圧力を上昇させて流量値が減少するか否かを検出することにより、リークが有るか無いか検出できる。より高気密の検査をする場合は流量計のレンジが小さいものを使用すればその機器の検出限界(再現性の範囲)まで使用できる。   FIG. 4 is a diagram showing a measurement example in the case where there is a slight leak in the inspection object 54. When the pressure of the pressurization control device 7 of the outlet gas flow rate measuring device 51 is increased, the mass flow rate flow meter 8 is shown. The measured value of the flow rate decreases. As can be seen from this example, whether or not there is a leak can be detected by detecting whether or not the flow rate value is decreased by increasing the pressure. When performing a higher airtightness inspection, if the flowmeter has a smaller range, it can be used up to the detection limit (reproducibility range) of the device.

このように、本発明のガスリーク検査装置は、ガス被検査対象物54における圧力計6において計測されたあるガス圧力に対する質量流量型流量計8において計測されたガス流量と、被検査対象物54における圧力計6において計測された他のあるガス圧力に対する質量流量型流量計8において計測されたガス流量とを求め、前記検出された両ガス圧力の差に対する両ガス流量との差との比(勾配)を求め、この比(勾配)から被検査対象物のガスリーク量を定量的に求めるものである。   As described above, the gas leak inspection apparatus of the present invention is configured so that the gas flow rate measured by the mass flow type flow meter 8 with respect to a certain gas pressure measured by the pressure gauge 6 of the gas inspection target 54 and the inspection target 54 The gas flow rate measured by the mass flow type flow meter 8 with respect to some other gas pressure measured by the pressure gauge 6 is obtained, and the ratio (gradient) of the difference between the two gas flow rates with respect to the detected difference between the two gas pressures. ) And the amount of gas leakage of the object to be inspected is quantitatively determined from this ratio (gradient).

図5は、図1に示したガスリーク検査装置の入口ガス定量供給装置50と異なる入口ガス定量供給装置50の構成を示す図であり、質量流量型流量制御装置3と直列に切換バルブ20を設けるともに、質量流量型流量制御装置3と切換バルブ20との直列体と並列に補助回路用減圧弁21と切換バルブ20との直列体を接続したものであり、補助回路用減圧弁21を用いることによって、測定圧近傍まで、ガスを別回路から供給し、待ち時間を短縮し、能率向上を図ろうとするものである。
このように構成することにより、配管容量の大きい場合に、微少リーク量の範囲で計測したい場合、供給流量を増加し、定常状態に達するまでの時間を短くして、計測時間の短縮化を図ることができる。
FIG. 5 is a diagram showing a configuration of an inlet gas quantitative supply device 50 different from the inlet gas quantitative supply device 50 of the gas leak inspection apparatus shown in FIG. 1, and a switching valve 20 is provided in series with the mass flow rate type flow rate control device 3. In both cases, a series body of the auxiliary circuit pressure reducing valve 21 and the switching valve 20 is connected in parallel with the series body of the mass flow rate type flow rate control device 3 and the switching valve 20, and the auxiliary circuit pressure reducing valve 21 is used. Thus, the gas is supplied from a separate circuit to the vicinity of the measurement pressure, the waiting time is shortened, and the efficiency is improved.
By configuring in this way, when the pipe capacity is large, if you want to measure in the range of minute leak amount, increase the supply flow rate, shorten the time to reach steady state, and shorten the measurement time be able to.

図6は、図1に示したガスリーク検査装置の入口ガス定量供給装置50及び出口ガス流量計測装置51と異なる入口ガス定量供給装置50及び出口ガス流量計測装置51の構成を示す図であり、入口ガス定量供給装置50において、質量流量型流量制御装置3と直列に切換バルブ20を設け、さらに質量流量型流量制御装置3と切換バルブ20との直列体と並列に質量流量型流量制御装置4と切換バルブ20との直列体を接続し、出口ガス流量計測装置51において、切換バルブ20と直列に質量流量型流量計8を設け、さらに切換バルブ20と質量流量型流量計8の直列体と並列に切換バルブ20と質量流量型流量計9との直列体を接続したものである。   FIG. 6 is a diagram showing the configuration of an inlet gas fixed amount supply device 50 and an outlet gas flow rate measuring device 51 different from the inlet gas fixed amount supply device 50 and the outlet gas flow rate measuring device 51 of the gas leak inspection apparatus shown in FIG. In the gas fixed amount supply device 50, a switching valve 20 is provided in series with the mass flow rate type flow rate control device 3, and the mass flow rate type flow rate control device 4 is provided in parallel with the series body of the mass flow rate type flow rate control device 3 and the switching valve 20. A series body of the switching valve 20 is connected, and the outlet gas flow rate measuring device 51 is provided with a mass flow type flow meter 8 in series with the switching valve 20, and further in parallel with the series body of the switching valve 20 and the mass flow type flow meter 8. A series body of the switching valve 20 and the mass flow type flow meter 9 is connected to the above.

このように構成することにより、大〜小流量をより容易に測定することが可能となり、流量計を複数(2台以上)用いて、リーク量が大きい場合から小さい場合まで種々の状況に対応出来る使いやすい構造とすることができる。
最初の段階では大きなリークも予想され、その場合は大きな流量計を使用して測定し、後に小流量レンジに切り換えて、微少量の検査へと段階的に実施できる構造としたものである。異なるレンジのものを揃えて、だんだん小さくしてゆくことによって、一台の装置で広範囲に対応することができると同時に、より容易に使用することができる。
By configuring in this way, it becomes possible to easily measure a large to small flow rate, and a plurality of flow meters (two or more) can be used to cope with various situations from a large leak amount to a small leak amount. Easy to use structure.
In the first stage, a large leak is also expected. In such a case, the measurement is performed using a large flow meter, and the structure is such that a small flow rate range can be measured later and a small amount of inspection can be carried out step by step. By arranging different ranges and making them smaller, it is possible to handle a wide range with a single device, and at the same time, it can be used more easily.

本実施形態の発明に係るガスリーク検査装置の構成をに示す図である。It is a figure showing the composition of the gas leak inspection device concerning the invention of this embodiment. ガスリーク検査装置に適用される被検査対象物の構成の一例を示す図ある。It is a figure which shows an example of a structure of the to-be-inspected target applied to a gas leak inspection apparatus. 被検査対象物54にリークのない場合の測定例を示す図である。It is a figure which shows the example of a measurement when the to-be-inspected target object 54 has no leak. 被検査対象物54に多少リークのある場合の測定例を示す図である。It is a figure which shows the example of a measurement in case the to-be-inspected target object 54 has some leaks. 図1に示したガスリーク検査装置の入口ガス定量供給装置50と異なる入口ガス定量供給装置50の構成を示す図である。It is a figure which shows the structure of the inlet gas fixed quantity supply apparatus 50 different from the inlet gas fixed quantity supply apparatus 50 of the gas leak test | inspection apparatus shown in FIG. 図1に示したガスリーク検査装置の入口ガス定量供給装置50及び出口ガス流量計測装置51と異なる入口ガス定量供給装置50及び出口ガス流量計測装置51の構成を示す図である。It is a figure which shows the structure of the inlet gas fixed supply device 50 and the outlet gas flow measuring device 51 which are different from the inlet gas fixed supply device 50 and the outlet gas flow measuring device 51 of the gas leak inspection apparatus shown in FIG.

符号の説明Explanation of symbols

1 ガスボンベ
2 減圧弁
3,4 質量流量型流量制御装置
5,6 圧力計
7 加圧制御装置
8,9 質量流量型流量計
10 排気
11 ガス供給接続口
12 流量測定装置接続口
20 切換バルブ
21 補助回路用減圧弁
25 被測定対象ラインガス入口
26 被測定対象ラインガス出口
50 入口ガス定量供給装置
51 出口ガス流量計測装置
54 被検査対象物(通過型)
61 バルブ
62 圧力計
1 Gas cylinder
2 Reducing valve 3, 4 Mass flow type flow control device
5,6 Pressure gauge
7 Pressure controller
8,9 Mass flow type flow meter
10 exhaust
11 Gas supply connection port
12 Flowmeter connection port
20 Switching valve 21 Auxiliary circuit pressure reducing valve 25 Measurement target line gas inlet 26 Measurement target line gas outlet 50 Inlet gas fixed supply device 51 Outlet gas flow rate measurement device 54 Inspected object (passing type)
61 Valve 62 Pressure gauge

Claims (1)

配管や気密容器等からなる被検査対象物と、該被検査対象物に一定量のガスを供給するガス定量供給装置と、前記被検査対象物内のガス圧力を制御するガス圧力制御装置と、前記被検査対象物から排出されるガス量を計測する流量計とから構成され、前記被検査対象物におけるあるガス圧力に対する前記流量計におけるガス流量を計測するとともに、前記被検査対象物における他のあるガス圧力に対する前記流量計におけるガス流量とを計測し、前記計測されたガス圧力の差に対する前記ガス流量計の差との比から、気密検査時における被検査対象物のガスリーク量を求めることを特徴とするガスリーク検査装置。
An object to be inspected consisting of piping, an airtight container, etc., a gas metering supply device for supplying a certain amount of gas to the object to be inspected, a gas pressure control device for controlling the gas pressure in the object to be inspected, A flow meter for measuring the amount of gas discharged from the object to be inspected, and measuring a gas flow rate in the flow meter for a certain gas pressure in the object to be inspected, and other in the object to be inspected Measuring a gas flow rate in the flow meter for a certain gas pressure, and obtaining a gas leak amount of an object to be inspected during an airtight inspection from a ratio of the difference in the gas flow meter to a difference in the measured gas pressure Characteristic gas leak inspection device.
JP2004267997A 2004-09-15 2004-09-15 Gas leak inspection device Active JP4281001B2 (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102928181A (en) * 2012-10-31 2013-02-13 中国石油化工股份有限公司 Simulation system for inner leak detection of hydrocarbon valve
US10656050B2 (en) 2015-01-09 2020-05-19 Avl Test Systems, Inc. System and method for detecting a leak in an exhaust gas sampling apparatus
US10852211B2 (en) * 2018-04-24 2020-12-01 Korea Institute Of Energy Research Apparatus and method for gas leakage measurement in a high pressure reactor

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102928181A (en) * 2012-10-31 2013-02-13 中国石油化工股份有限公司 Simulation system for inner leak detection of hydrocarbon valve
US10656050B2 (en) 2015-01-09 2020-05-19 Avl Test Systems, Inc. System and method for detecting a leak in an exhaust gas sampling apparatus
US10852211B2 (en) * 2018-04-24 2020-12-01 Korea Institute Of Energy Research Apparatus and method for gas leakage measurement in a high pressure reactor

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