JP2006020521A5 - - Google Patents

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JP2006020521A5
JP2006020521A5 JP2004199027A JP2004199027A JP2006020521A5 JP 2006020521 A5 JP2006020521 A5 JP 2006020521A5 JP 2004199027 A JP2004199027 A JP 2004199027A JP 2004199027 A JP2004199027 A JP 2004199027A JP 2006020521 A5 JP2006020521 A5 JP 2006020521A5
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含蜜糖の製造方法及び製造装置Method and apparatus for producing honey-containing sugar

本発明は、さとうきびを原料とする粉状または液状の含蜜糖の製造方法及び製造装置に関する。   The present invention relates to a method and an apparatus for producing powdered or liquid honey-containing sugar made from sugarcane.

近代的な大規模工場において、工業的に生産され広く普及している一般的な上白糖やグラニュー糖にはない独特の風味を備える伝統的含蜜糖として、主に沖縄で生産される黒糖、主に四国で生産される和三盆糖などが知られている。   Brown sugar produced mainly in Okinawa as a traditional honey-containing sugar that has a unique flavor not found in general white sugar and granulated sugar, which is industrially produced and widely used in modern large-scale factories, Wasanbon sugar produced mainly in Shikoku is known.

黒糖は、さとうきびを絞って得た圧搾汁を加熱し、石灰を加えて灰汁等を取り除いて得た清澄汁を煮詰めて濃縮糖汁とし、冷却して固形化する方法により製造され、無機質栄養素を多く含み独特のコクのある風味を有し主にそのまま食する甘味嗜好品として親しまれている。   Brown sugar is produced by heating the compressed juice obtained by squeezing sugar cane, adding lime and removing ash juice, etc., boiling the clear juice into concentrated sugar juice, cooling and solidifying it. It has a rich and unique flavor and is popular as a sweet taste product that is mainly eaten as it is.

一方、和三盆糖は、特に竹糖といわれる細茎のさとうきびを絞って得た圧搾汁を加熱し、石灰を加えて灰汁を取り除いて得られた清澄汁を煮詰めて濃縮糖汁とし、冷却して得られる結晶糖を砕いて白下糖を得る。この白下糖に水を加えた後、こねて水を馴染ませた(研ぎ)後、濾過袋に入れて加圧して不純物を含む糖蜜を絞りだす分蜜処理を手作業で繰り返し行って製造される淡黄白色の含蜜糖であり、独特の上品な風味があり、銘菓、上菓子の原料として珍重されている。
特開平2001−245700 特開平10−94387 特開昭52−120137
On the other hand, in the case of Wasanbon sugar, the juice obtained by squeezing sugarcane on the stems called bamboo sugar is heated, and the clarified juice obtained by adding lime and removing the ash is boiled to obtain concentrated sugar juice, which is then cooled. The crystal sugar obtained is crushed to obtain white sugar. After adding water to this white sugar, knead it to make it familiar (sharpening), and then manually repeat the honey treatment to put out the molasses containing impurities by putting it in a filter bag and pressurizing it. It is a pale yellowish white honey-containing sugar, has a unique and elegant flavor, and is prized as a raw material for famous confectionery and confectionery.
JP 2001-245700 A JP-A-10-94387 JP-A 52-120137

これら伝統的含蜜糖の独特の風味を種々の食品等に利用したいという食品生産者の需要は高いが、手工業的方法により製造されるがゆえ、生産性、衛生面の点に問題があり需要を満たすに至っていない。   There is a high demand for food producers who want to use the unique flavors of these traditional honey-containing sugars in various foods, etc., but they are manufactured by handicraft methods, so there are problems in terms of productivity and hygiene. Not yet satisfied.

黒糖に関していえば、石灰添加と重力沈降による沈殿操作という非効率な清浄処理で製造されるため、異物や菌等の不純物を多く含み純度も低い。従って、製品間の品質調整を厳密に行なわなければならない大量生産食品の原料として使用するには衛生面および品質安定性の面で問題がある。さらに、黒糖は製造工程に起因してブロック状もしくは粗粒状形態の製品とならざるを得ない。このため液状の含蜜糖の使用が好適な食品原料用途にはそのまま使用することができず不向きといった問題もある。 As for brown sugar, because it is produced by inefficient cleaning process called precipitation operation by lime and gravitational settling, purity is low contains a large amount of impurities such as foreign matter and bacteria. Accordingly, there is a problem in terms of hygiene and quality stability when used as a raw material for mass-produced foods where quality adjustment between products must be strictly performed. Furthermore, brown sugar must be a block or coarse grain product due to the manufacturing process. For this reason, there is also a problem that it cannot be used as it is for food raw material applications where the use of liquid saccharide-containing sugar is suitable.

和三盆糖に関していえば、「研ぎと押し工程」を人の手作業により繰り返し行なう必要があるため、完成までに概ね2週間という多くの日数を要するため大量に生産することができず、また、それゆえに価格も極めて高価であり、大量生産品への利用を困難とならしめている。また、黒糖と同様に和三盆糖も粉状であるから、液状の含蜜糖の使用が好適な食品原料用途にはそのまま使用することができず不向きといった問題がある。   With regard to Wasan Bon Sugar, it is necessary to repeat the “sharpening and pressing process” manually by hand, so it can take many days to complete, so it cannot be produced in large quantities. Therefore, the price is extremely expensive, making it difficult to use for mass-produced products. In addition, since Wasanbon sugar is in the form of powder as well as brown sugar, there is a problem that it cannot be used as it is for food raw materials for which liquid honey-containing sugar is suitable.

そこで、本発明の主たる課題は、さとうきび由来の独特な風味や無機質栄養素を残した高品質な粉状の含蜜糖および液状の含蜜糖を衛生的(異物、菌混入なし)に、かつ工業的に大量生産可能であり、また、エンドユーザーの要望に合わせて黒糖から和三盆的高品質粉状含蜜糖まで広範囲の品質の調整が可能であり、さらに、液状または粉状など各種態様の含蜜糖を得ることが可能である、含蜜糖の製造方法および含蜜糖の製造装置を提供することにある。   Therefore, the main problem of the present invention is that the high-quality powdered and sugar-containing saccharides that leave the unique flavor and mineral nutrients derived from sugar cane are hygienically (no foreign substances and bacteria mixed) and industrial It can be mass-produced and can be adjusted in a wide range of quality from brown sugar to high quality powdered honey containing sugar according to the needs of end users. An object of the present invention is to provide a method for producing honey-containing sugar and an apparatus for producing honey-containing sugar, which are capable of obtaining honey-containing sugar.

上記課題を解決した本発明は次記のとおりである。
<請求項1記載の発明>
以下(1)〜(8)の処理工程を含むことを特徴とする含蜜糖の製造方法。
(1)さとうきびの圧搾により得た圧搾汁、さとうきびの抽出により得た抽出汁、または圧搾汁と抽出汁とを混合した混合汁からなる粗汁を得る粗汁生成工程。
(2)前記粗汁をスクリーン処理して不溶物質の除去を行なう予備濾過工程。
(3)不溶物質が除去された粗汁を膜濾過して不純物および菌類を分離除去するとともに清澄汁を得る膜濾過処理工程。
(4)前記清澄汁を濃縮処理して粗濃縮汁を得る予備濃縮処理工程。
(5)前記粗濃縮汁の一部を晶析して結晶糖を得る晶析処理工程。
(6)晶析処理工程で得られた結晶糖を溶解して溶解糖液を得る溶解工程。
(7)前記溶解糖液と晶析及び溶解処理を行わない前記粗濃縮汁とを混合した混合糖汁を冷却晶析可能な濃度まで濃縮する仕上げ濃縮工程。
(8)仕上げ濃縮により得られた濃縮糖汁を冷却して固形化・粉化して粉状の含蜜糖を得る粉糖化処理工程。
The present invention that has solved the above problems is as follows.
<Invention of Claim 1>
The manufacturing method of a sugar containing sugar characterized by including the process of following (1)-(8).
(1) A crude juice production step for obtaining a crude juice comprising a pressed juice obtained by pressing sugar cane, an extracted juice obtained by extracting sugar cane, or a mixed juice obtained by mixing pressed juice and extracted juice.
(2) A preliminary filtration step in which the crude juice is screened to remove insoluble substances.
(3) A membrane filtration treatment step for separating and removing impurities and fungi by membrane filtration of the crude juice from which insoluble substances have been removed, and obtaining a clarified juice.
(4) A pre-concentration treatment step for obtaining a crude concentrate by concentrating the clear juice.
(5) A crystallization treatment step in which a part of the crude concentrated juice is crystallized to obtain crystalline sugar.
(6) A dissolution step in which the crystal sugar obtained in the crystallization treatment step is dissolved to obtain a dissolved sugar solution.
(7) A finishing concentration step of concentrating the mixed sugar juice obtained by mixing the dissolved sugar liquid and the crude concentrated juice not subjected to crystallization and dissolution treatment to a concentration capable of cooling and crystallization.
(8) A saccharification treatment step in which the concentrated sugar juice obtained by finish concentration is cooled, solidified and pulverized to obtain powdered honey-containing sugar.

<請求項2記載の発明>
粗濃縮汁を液状の含蜜糖として採取する液状含蜜糖採取工程を有する請求項1記載の含蜜糖の製造方法。
<Invention of Claim 2>
Method for producing a molasses sugar according to claim 1, further comprising a liquid mixture solid sugar collecting step of collecting the crude concentrated juice as molasses sugar liquid.

<請求項3記載の発明>
晶析処理工程における晶析処理過程で分離される糖蜜を、粗濃縮汁と混合して、これを液状の含蜜糖として得る液状含蜜糖採取工程を有する請求項1または2記載の含蜜糖の製造方法。
<Invention of Claim 3>
The molasses according to claim 1 or 2, further comprising a liquid molasses collecting step in which the molasses separated in the crystallization treatment step in the crystallization treatment step is mixed with the crude concentrated juice to obtain liquid molasses. A method for producing sugar.

<請求項4記載の発明>
膜処理工程に先立って粗汁のpHを6〜7.5に調整する請求項1〜3の何れか1項に記載の含蜜糖の製造方法。
<Invention of Claim 4>
The manufacturing method of the sugar containing sugar of any one of Claims 1-3 which adjusts the pH of coarse juice to 6-7.5 prior to a membrane treatment process.

<請求項5記載の発明>
予備濃縮処理をプレート型熱交換器または流下液薄膜式熱交換器を備えた濃縮設備により行う請求項1〜4のいずれか1項に記載の含蜜糖の製造方法。
<Invention of Claim 5>
The manufacturing method of the sugar-containing sugar of any one of Claims 1-4 which perform a preconcentration process with the concentration equipment provided with the plate-type heat exchanger or the falling liquid film type heat exchanger.

<請求項6記載の発明>
以下(1)〜(8)の手段を含むことを特徴とする含蜜糖の製造装置。
(1)さとうきびの圧搾により得た圧搾汁、さとうきびの抽出により得た抽出汁、または圧搾汁と抽出汁とを混合した混合汁からなる粗汁を得る粗汁生成手段。
(2)前記粗汁をスクリーン処理して不溶物質の除去を行なう予備濾過手段。
(3)不溶物質が除去された粗汁を膜濾過して不純物および菌類を分離除去するとともに清澄汁を得る膜濾過処理手段。
(4)前記清澄汁を濃縮処理して粗濃縮汁を得る予備濃縮処理手段。
(5)前記粗濃縮汁の一部を晶析して結晶糖を得る晶析処理手段。
(6)晶析処理手段で得られた結晶糖を溶解して溶解糖液を得る結晶糖溶解手段。
(7)前記溶解糖液と晶析及び溶解処理を行わない前記粗濃縮汁とを混合した混合糖汁を冷却晶析可能な濃度まで濃縮する仕上げ濃縮手段。
(8)仕上げ濃縮により得られた濃縮糖汁を冷却して固形化・粉化して粉状の含蜜糖を得る粉糖化処理手段。
<Invention of Claim 6>
An apparatus for producing honey-containing sugar, comprising the following means (1) to (8).
(1) Crude juice producing means for obtaining a crude juice comprising a pressed juice obtained by pressing sugar cane, an extracted juice obtained by extracting sugar cane, or a mixed juice obtained by mixing pressed juice and extracted juice.
(2) Preliminary filtration means for removing insoluble substances by screening the crude juice.
(3) Membrane filtration means for filtering the crude juice from which insoluble substances have been removed to separate and remove impurities and fungi and to obtain a clear juice.
(4) Preconcentration processing means for concentrating the clarified juice to obtain a crude concentrated juice.
(5) A crystallization treatment means for crystallization of a part of the crude concentrated juice to obtain a crystalline sugar.
(6) Crystal sugar dissolving means for dissolving the crystal sugar obtained by the crystallization treatment means to obtain a dissolved sugar solution.
(7) A finishing concentration means for concentrating the mixed sugar juice obtained by mixing the dissolved sugar liquid and the crude concentrated juice not subjected to crystallization and dissolution treatment to a concentration capable of cooling and crystallization.
(8) Powdered saccharification processing means for cooling and concentrating and pulverizing the concentrated sugar juice obtained by finish concentration to obtain powdered honey-containing sugar.

<請求項7記載の発明>
粗濃縮汁を液状の含蜜糖として採取する液状含蜜糖採取手段を備える請求項6記載の含蜜糖の製造装置。
<Invention of Claim 7>
The apparatus for producing honey-containing sugar according to claim 6, further comprising a liquid honey-containing sugar collecting means for collecting the crude concentrated juice as liquid honey-containing sugar.

<請求項8記載の発明>
晶析処理手段における晶析処理にて分離された糖蜜を、粗濃縮汁と混合し、これを液状の含蜜糖として採取する液状含蜜糖採取手段を備える請求項6または7記載の含蜜糖の製造装置。
<Invention of Claim 8>
The molasses according to claim 6 or 7, further comprising liquid molasses collecting means for mixing the molasses separated by the crystallization treatment in the crystallization treatment means with the crude concentrated juice and collecting the molasses as liquid molasses. Sugar production equipment.

本発明によれば、従来行われている石灰による糖汁清浄方法に代えて限外濾過膜などによる膜濾過処理を採用し、異物や菌を含まない清澄汁を得ることができ、これから衛生的で高品質な液状または粉状の含蜜糖が製造可能となる。   According to the present invention, it is possible to obtain a clarified juice that does not contain foreign substances or bacteria by adopting a membrane filtration process using an ultrafiltration membrane or the like instead of the conventional lime-based method for cleaning juice using lime. High-quality liquid or powdered honey sugar can be produced.

また、溶解糖液と晶析及び溶解処理を行わない前記粗濃縮汁とを混合した混合糖汁を得る。そして、この混合糖汁を冷却晶析可能な濃度まで濃縮する仕上げ濃縮を行い、この仕上げ濃縮により得られた濃縮糖汁を冷却して固形化して粉状の含蜜糖を得るものである。したがって、結晶糖の純度(晶析具合)を調整することにより、あるいは溶解糖液と粗濃縮汁との混合割合を適宜変更することにより、黒糖的品質から和三盆糖的品質あるいはそれ以上の品質の粉状の含蜜糖を生産設備を変更することなく容易に製造できる。   Further, a mixed sugar juice obtained by mixing the dissolved sugar solution and the crude concentrated juice not subjected to crystallization and dissolution treatment is obtained. Then, final concentration for concentrating the mixed sugar juice to a concentration capable of cooling and crystallization is performed, and the concentrated sugar juice obtained by the finish concentration is cooled and solidified to obtain powdered honey-containing sugar. Therefore, by adjusting the purity (crystallizing condition) of crystal sugar, or by appropriately changing the mixing ratio of dissolved sugar liquid and crude concentrated juice, quality from brown sugar quality to Wanbon sugar quality or higher Can be easily produced without changing the production equipment.

また、粗濃縮汁をそのまま採取するか、あるいは、晶析処理工程に供した粗濃縮汁の晶析過程で結晶糖と分離された糖蜜と粗濃縮汁とを混合したものを採取して、液状の含蜜糖を得ることができる。この液状含蜜糖についても前記混合割合を調整するなどにより従来にない品質のものを得ることができる。   Alternatively, the crude concentrated juice may be collected as it is, or a mixture of crystal sugar, molasses separated in the crystallization process of the crude concentrated juice used in the crystallization treatment step and the crude concentrated juice may be collected to obtain a liquid Can be obtained. As for this liquid sugar-containing sugar, it is possible to obtain an unprecedented quality by adjusting the mixing ratio.

そして、本発明では人手による手作業を必要とせず完全自動化された工業的生産が可能であり、高品質な粉状または液状の含蜜糖を低コストに大量生産が可能である。   In the present invention, it is possible to perform industrial production that is completely automated without requiring manual work by hand, and mass production of high-quality powdery or liquid honey cane sugar is possible at low cost.

次いで、本発明の実施の形態を図面を参照しながら以下に詳述する。図1は、本発明にかかる粉状の含蜜糖および液状の含蜜糖の製造プロセスのフロー図である。   Next, embodiments of the present invention will be described in detail below with reference to the drawings. FIG. 1 is a flow diagram of a process for producing powdered honey sugar and liquid honey sugar according to the present invention.

さとうきびをカッターで裁断し、シュレッダーでさらに細裂したのち、搬送用コンベア等により後続の粗汁生成工程へ供給する。粗汁生成工程では、公知の圧搾方法により圧搾処理して粗汁を得る。粗汁は公知の抽出方法により得てもよく、圧搾により得られる圧搾汁と抽出により得られる抽出汁とを混合したものを粗汁としてもよい。圧搾処理するにあたっては糖分抽出率よりも抽出糖液純度に重点を置いた処理を行なうのが望ましく搾出率としては80〜90%を確保するのが適当である。したがって、通常の原糖工場における4重〜6重ミルではなく3重ミルにて圧搾を行なうのが適当である。多重ミルでは後続のミルほど得られる糖液の純糖度が下がるため、初号ミルから得られる糖液の比率を高めて高品質糖汁を得るようにする。圧搾残滓として発生するバガス等は、これらは家畜飼料・敷藁として農家に還元して有効活用するのが望ましい。 The sugar cane is cut with a cutter and further shredded with a shredder, and then supplied to the subsequent coarse juice production process by a conveyor for transportation. In the coarse juice production step, the crude juice is obtained by squeezing by a known squeezing method. The crude juice may be obtained by a known extraction method, or a mixture of a pressed juice obtained by pressing and an extracted juice obtained by extraction may be used. In the squeezing treatment, it is desirable to perform the treatment with an emphasis on the purity of the extracted sugar solution rather than the sugar extraction rate, and it is appropriate to secure 80 to 90% as the squeezing rate. Therefore, it is appropriate to squeeze in a triple mill instead of a quadruple to 6-fold mill in a normal raw sugar factory. Since pure sugar content of sugar solution obtained as subsequent mill decreases in multiple mill, so as to obtain a high quality sugar juice to increase the ratio of the obtained that molasses from first issue mill. It is desirable that bagasse, etc. generated as squeezed residue is returned to farmers as animal feed and bedding for effective use.

通常、得られる粗汁のpHは、5〜6付近であり、この状況下においては、粗汁中の蔗糖分が加水分解し還元糖に変化するため、製品の品質向上の点から後段の限外濾過処理工程前に粗汁に対して石灰、苛性ソーダ、炭酸ソーダ等を適宜添加して粗汁のpHを6〜7.5に調整し還元糖生成を抑制するのが望ましい。   Usually, the pH of the obtained crude juice is around 5-6, and under this situation, the sucrose content in the crude juice is hydrolyzed and converted into reducing sugar, so that it is limited in the latter stage from the viewpoint of improving the quality of the product. Before the outer filtration treatment step, it is desirable that lime, caustic soda, sodium carbonate or the like is appropriately added to the crude juice to adjust the pH of the crude juice to 6 to 7.5 to suppress reducing sugar production.

他方、粗汁中には、さとうきび由来の繊維状物質(「ピスとも呼ばれる」)や砂土砂その他異物(以下「不溶性夾雑物」とも言う。)が混入しているので、後段の膜濾過処理に備えて、これらの不溶性夾雑物を除去する予備濾過処理を施す。予備濾過処理は、スクリーン処理が好適である。   On the other hand, in the coarse juice, sugarcane-derived fibrous substances (also referred to as “pis”), sand, sand and other foreign matters (hereinafter also referred to as “insoluble impurities”) are mixed. In addition, a prefiltration treatment for removing these insoluble impurities is performed. A screen treatment is suitable for the prefiltration treatment.

スクリーンとしては、連続排出が可能であり可動部がなく操作が容易であることから、固定型の傾斜型ウェッジワイヤースクリーンが適する。スクリーンの性能については、粗汁中の組成を考慮して適宜定めればよい。後段の濾過膜がスパイラル構造の場合にはスリット間への閉塞を考慮する必要があるので、50μm以上の不溶性物質を除去することが可能な性能のスクリーンが適当である。後段の限外濾過膜がチューブラータイプのものであれば、液流路の閉塞はあまり考えられないため、濃縮倍率、ピスの除去率を考慮して適宜スクリーンを選択する。なお、スクリーンは、2段配置してもよく、例えば1段目では100〜300μmカット、2段目にて50μmカットするようにしてもよい。この場合、後工程の膜処理負荷がより下がる。また、予備濾過処理の最終段にチェック濾過を加えてもよい。 As the screen, a fixed inclined wedge wire screen is suitable because it can be continuously discharged and has no moving parts and is easy to operate. The performance of the screen may be appropriately determined in consideration of the composition in the crude juice. When the subsequent filtration membrane has a spiral structure, it is necessary to consider the clogging between the slits. Therefore, a screen having a performance capable of removing insoluble substances of 50 μm or more is suitable. If the subsequent ultrafiltration membrane is a tubular type, it is unlikely that the liquid flow path is clogged. Therefore, the screen is appropriately selected in consideration of the concentration ratio and the removal rate of piss. The screen may be arranged in two stages, for example, the first stage may be cut by 100 to 300 μm, and the second stage may be cut by 50 μm. In this case, the film processing load in the subsequent process is further reduced. Further, check filtration may be added to the final stage of the preliminary filtration treatment.

予備濾過処理した粗汁は、後段の膜濾過処理における膜透過性の向上(糖液粘度の低下)と濃縮効率向上のため加熱するのが望ましい。粗汁をどの程度まで加熱するかは、後段の濾過膜の温度仕様を考慮して適宜定めればよいが、50〜80℃程度とするのが好適である。加熱源は低圧蒸気(0.1〜0.2MPaG)を用い、製品の風味の保持と効率向上のためプレート式の熱交換器を用いるのが好適である。   The pre-filtered crude juice is preferably heated to improve membrane permeability (decrease in sugar solution viscosity) and improve concentration efficiency in the subsequent membrane filtration treatment. The extent to which the crude juice is heated may be appropriately determined in consideration of the temperature specification of the subsequent filtration membrane, but is preferably about 50 to 80 ° C. It is preferable to use low-pressure steam (0.1 to 0.2 MPaG) as a heating source and a plate-type heat exchanger for maintaining the flavor of the product and improving efficiency.

粗汁を加熱したならば、粗汁中の微細懸濁固形分・高分子不純物を分離除去すべく濾過膜を用いて膜濾過処理する。膜濾過処理では沈殿成分を含め製品品質の低下に繋がる一般細菌類も除去される。膜濾過処理では後段に供給する清澄汁とともに不純物を多く含む濃縮廃液が得られるが、この濃縮廃液は前記予備濾過処理の残滓とともに肥料などとしてリサイクルするのが望ましい。   When the crude juice is heated, it is subjected to membrane filtration using a filtration membrane to separate and remove fine suspended solids and polymer impurities in the crude juice. The membrane filtration treatment also removes general bacteria that lead to a decrease in product quality, including precipitated components. In the membrane filtration treatment, a concentrated waste liquid containing a large amount of impurities is obtained together with the clarified juice supplied to the subsequent stage, and it is desirable to recycle this concentrated waste liquid as a fertilizer together with the residue of the preliminary filtration treatment.

膜濾過処理は、クロスフロータイプの連続膜濾過処理とするのが適当である。濃縮倍率を順次高める複数段の膜処理に分割して処理してもよい。数段に分割して濃縮を行った方が膜面積を少なくすることができる。膜処理を数段に分ける決定因子としては、各濃縮倍率での膜処理能力によって決定する。また、注水することにより、透析濾過の効果がえられ、不溶性懸濁物質濃度を低下させることになるので、糖液の回収率を高めることができる。   The membrane filtration treatment is suitably a cross flow type continuous membrane filtration treatment. You may divide | segment and process into the multistage film | membrane process which raises a concentration ratio sequentially. The membrane area can be reduced by concentration in several stages. The determinant for dividing the membrane treatment into several stages is determined by the membrane treatment ability at each concentration ratio. In addition, by irrigating water, the effect of diafiltration is obtained and the concentration of insoluble suspended solids is reduced, so that the recovery rate of sugar solution can be increased.

膜濾過処理に用いる膜としては、限外濾過膜、精密濾過膜等の公知分離膜のなかから適宜選択することができる。濾過膜の耐温度に関する仕様は、粗汁の温度を考慮して適宜選択すればよく、具体的には50℃以上、好適には80℃以上で使用できるものが望ましい。膜構造や膜材質については特に限定されない。本発明の目的である粗汁中の菌類除去および生産性の向上を考慮すると、分画分子量30000〜100000程度であり、運転圧力が3〜5kgf/cm2G程度の限外濾過膜が特に好適である。 The membrane used for the membrane filtration treatment can be appropriately selected from known separation membranes such as an ultrafiltration membrane and a microfiltration membrane. The specification relating to the temperature resistance of the filtration membrane may be appropriately selected in consideration of the temperature of the crude juice, and specifically, it is desirable that it can be used at 50 ° C. or higher, preferably 80 ° C. or higher. The film structure and film material are not particularly limited. In view of the removal of fungi in the crude juice and the improvement of productivity, which are the objects of the present invention, an ultrafiltration membrane having a fractional molecular weight of about 30,000 to 100,000 and an operating pressure of about 3 to 5 kgf / cm 2 G is particularly suitable. It is.

膜濾過処理して得られた清澄汁は、目的の濃度(Brix:以下Bxと略す)まで予備濃縮処理して粗濃縮汁を得る。予備濃縮処理工程では、熱効率のよい多重効用缶が有利である。濃縮装置としては、カランドリアタイプのものを用いることができ、膜濾過処理により増粘性の物質の除去を行っているので、熱交換効率の高いプレート型熱交換器、流下液薄膜式熱交換器を使用することができる。   The clarified juice obtained by the membrane filtration treatment is pre-concentrated to a target concentration (Brix: hereinafter abbreviated as Bx) to obtain a crude concentrated juice. In the preconcentration process, a multi-effect can with high thermal efficiency is advantageous. As the concentrator, a Calandria type can be used, and the thickening material is removed by membrane filtration treatment. Therefore, a plate type heat exchanger with high heat exchange efficiency, a falling liquid film type heat exchanger Can be used.

粗濃縮汁の一部は、晶析処理して結晶糖を得るのに用いる。晶析処理は、粗濃縮汁を真空下で炊きあげて粗汁中の糖を晶析させ、その後に遠心分離機等で固液分離するとともに洗浄処理等して結晶糖を得る公知の晶析処理とすることができる。このような晶析処理は通常の原料糖や精製糖の晶析処理に使用されている公知の晶析設備を利用することができる。晶析処理では、分離操作等の適宜の操作により98%以上の純度の結晶糖を得るのが好適である。   A part of the crude juice is used for crystallization to obtain crystal sugar. Crystallization treatment is a known crystallization method in which crude concentrated juice is cooked under vacuum to crystallize the sugar in the crude juice, and then subjected to solid-liquid separation with a centrifugal separator or the like and washing treatment to obtain crystal sugar. It can be a process. For such crystallization treatment, a known crystallization equipment used for crystallization treatment of ordinary raw sugar or purified sugar can be used. In the crystallization treatment, it is preferable to obtain crystal sugar having a purity of 98% or more by an appropriate operation such as a separation operation.

得られた結晶糖は再溶解し、前記粗濃縮糖汁に任意の割合で混合して、任意の純度の混合糖汁を得る。製品を得るにあたっては好適には混合糖汁は純度92%以上とするのが好適である。   The obtained crystalline sugar is redissolved and mixed with the crude concentrated sugar juice at an arbitrary ratio to obtain a mixed sugar juice of arbitrary purity. In obtaining a product, it is preferable that the mixed sugar juice has a purity of 92% or more.

得られた混合糖汁は、仕上げ濃縮処理して濃縮糖汁とする。仕上げ濃縮は、冷却晶析が可能な濃度領域、具体的にはBx95以上となるまで煮詰めて濃縮する。操作は風味の減少や変質、分解を防ぐため連続式の薄膜濃縮装置が好適であるが、バッチ式の濃縮装置(釜)でも良い。   The obtained mixed sugar juice is finished and concentrated to obtain concentrated sugar juice. The final concentration is concentrated by boiling until it reaches a concentration range where cooling crystallization is possible, specifically, Bx95 or more. The operation is preferably a continuous thin-film concentrator in order to prevent a decrease in flavor, alteration or decomposition, but a batch-type concentrator (pot) may also be used.

仕上げ濃縮により得られた濃縮糖汁は固形化・粉化処理して粉状の含蜜糖とする。濃縮糖汁は過飽和状態にあるため、攪拌、冷却することにより一部乾燥させて、固形化されて粉状となる。なお、この際に発生するダマを篩により除去もしくは粉砕すれば均質な粉体を得ることができる。冷却および乾燥は、リボン羽根またはパドル羽根を有する混合・冷却機を3段連続して配置した多段式の攪拌装置により行なうのが好適である。粉状の含蜜糖はカビの発生を防止するため、乾燥機で所望する水分まで乾燥し水分を調節するのが望ましい。水分含有率は、必要となる糖製品に応じて適宜乾燥具合を定めればよい。水分含有量は低い方が望ましいが、4.0重量%をうわまわらなければよい。なお、得られた粉状の含蜜糖は製品化するにあたってダマが混入しないように篩によりダマを除去もしくは粉砕機や解砕機等により適当に粉砕/解砕処理してより品質的に優れた粉状の含蜜糖を得ることができる。   The concentrated sugar juice obtained by finishing concentration is solidified and powdered to form powdered honey sugar. Since the concentrated sugar juice is in a supersaturated state, it is partially dried by stirring and cooling and solidified into a powder. It is to be noted that a homogeneous powder can be obtained by removing or crushing lumps generated at this time with a sieve. Cooling and drying are preferably performed by a multistage stirring device in which three stages of mixing / cooling machines having ribbon blades or paddle blades are arranged in succession. In order to prevent the occurrence of mold from powdered saccharide-containing sugar, it is desirable to adjust the moisture by drying to the desired moisture in a dryer. The moisture content may be determined appropriately depending on the required sugar product. It is desirable that the water content is low, but 4.0% by weight is not required. In addition, the powdered honey-containing sugar obtained is superior in quality by removing lumps with a sieve or by appropriately pulverizing / disintegrating with a pulverizer or a pulverizer so that lumps are not mixed when commercialized. Powdered honey sugar can be obtained.

他方、本発明においては、粗濃縮汁を採取してそのまま液状の含蜜糖とすることができる。また、晶析処理工程に供した粗濃縮汁の晶析過程で結晶糖と分離された糖蜜を、晶析処理工程に供しない粗濃縮汁と混合して、採取して液状の含蜜糖とすることもできる。これらの液状の含蜜糖は、膜濾過処理を行い菌類の分離除去が行われている粗濃縮汁から得るものであるために、各種食品等に利用可能な衛生的な液状の含蜜糖である。   On the other hand, in the present invention, the crude concentrated juice can be collected and used as it is as liquid saccharide-containing sugar. In addition, the molasses separated from the crystalline sugar in the crystallization process of the crude concentrated juice subjected to the crystallization treatment process is mixed with the crude concentrated juice not subjected to the crystallization treatment process, and collected to obtain a liquid molasses sugar. You can also These liquid saccharides are obtained from crude concentrated juices that have been subjected to membrane filtration treatment and fungi are separated and removed. Therefore, these liquid saccharides are sanitary liquid saccharides that can be used for various foods. is there.

なお、本発明では上述のとおり菌類の除去処理が行なわれているものの、液状の含蜜糖は乾燥状態の粉状の含蜜糖と比較して、外部からの菌類などの影響を受けやすいためより高度な品質管理が要求される。このため、濃縮、希釈あるいは貯蔵にあたっては、除菌、殺菌灯などの雑菌汚染対策をより徹底するのが好適である。また、コンタミ防止・細菌増殖防止の各種対策を実施するともに、長期保存を可能とするため、温度調整機能を持たせた貯蔵槽に貯蔵し、室内貯蔵とするのが適する。   In the present invention, although the fungus removal treatment is performed as described above, the liquid honey sugar is more susceptible to external fungi and the like than the dry powdery honey sugar. More advanced quality control is required. For this reason, in concentrating, diluting, or storing, it is preferable to take thorough measures against contamination of bacteria such as sterilization and germicidal lamp. In addition, various measures for preventing contamination and preventing bacterial growth are implemented, and in order to enable long-term storage, it is suitable to store in a storage tank with a temperature adjustment function and store it indoors.

図1に示されるフロー図に基づいて本発明の内容を実証実験した。
(試料1)
テストミルを用いてキビを絞り、濃度(Bx)21、純糖率88.3%の粗汁を152kg得た。搾汁率は、純度を重視して約90%とした。その後、粗汁を300μmのウェッジワイヤースクリーンに通して不溶夾雑物を分離除去した。その後に、15°Beの石灰乳を徐々に添加して、pHを6.5〜7.5の範囲に調整し一定時間放置してSS分を十分に沈降させて上澄み液を回収した。
Based on the flowchart shown in FIG. 1, the content of the present invention was verified.
(Sample 1)
Mill was squeezed using a test mill to obtain 152 kg of crude juice having a concentration (Bx) of 21 and a pure sugar ratio of 88.3%. The squeeze rate was about 90% with emphasis on purity. Thereafter, the coarse juice was passed through a 300 μm wedge wire screen to separate and remove insoluble impurities. Thereafter, lime milk of 15 ° Be was gradually added to adjust the pH to a range of 6.5 to 7.5 and left for a certain period of time to sufficiently settle the SS component, and the supernatant was recovered.

この上澄み液を、温度55〜60℃に保持したのち、濾過面積:0.5m2、分画分子量:50KDの限外濾過膜を備えた限外濾過処理装置により膜濾過処理して清澄汁を得た。限外濾過装置の運転条件は、循環流量:3.6m3/hr、圧力0.3Mpa、透過液流量21〜40L/hr、運転温度:50〜60℃とした。 The supernatant is kept at a temperature of 55 to 60 ° C. and then subjected to membrane filtration with an ultrafiltration apparatus equipped with an ultrafiltration membrane having a filtration area of 0.5 m 2 and a molecular weight cut off of 50 KD. Obtained. The operating conditions of the ultrafiltration device were a circulation flow rate: 3.6 m 3 / hr, a pressure of 0.3 Mpa, a permeate flow rate of 21 to 40 L / hr, and an operating temperature of 50 to 60 ° C.

上記運転条件で、粗汁152kgを限外濾過処理したところ清澄汁132.3kg、清澄汁濃度(Bx)20.5、濃縮廃液18.8kg、濃縮廃液濃度(Bx)22、濃縮倍率8倍の結果が得られた。十分実用性のある結果である。   Under the above operating conditions, 152 kg of crude juice was subjected to ultrafiltration treatment. As a result, 132.3 kg of clarified juice, 20.5 clarified juice concentration (Bx), 18.8 kg of concentrated waste solution, 22 concentration of concentrated waste solution (Bx), and 8 times concentration ratio Results were obtained. This is a sufficiently practical result.

次いで、この膜濾過処理して得られた清澄汁を、濃縮缶サイズ:250mmφ×1330mmH、加熱伝面:0.47m2の濃縮缶に張り込み、真空下で加熱して水分を蒸発させ、濃度(Bx)72まで濃縮して粗濃縮汁を得た。濃縮缶の運転条件は、張り込み液量:28L、運転圧力:約118torr、運転温度:60℃、スチーム圧力:2kg/cm2Gとした。 Next, the clarified juice obtained by the membrane filtration treatment was put into a concentrated can of a concentrated can size: 250 mmφ × 1330 mmH, heating transmission surface: 0.47 m 2 , heated under vacuum to evaporate water, and the concentration ( Bx) to 72 to obtain a crude concentrate. The operation conditions of the concentration can were as follows: the amount of the applied liquid: 28 L, the operating pressure: about 118 torr, the operating temperature: 60 ° C., and the steam pressure: 2 kg / cm 2 G.

上記運転条件で、濃度(Bx)20.5の清澄汁132.3kgを予備濃縮処理したところ粗濃縮汁31.3kg、粗濃縮汁濃度(Bx)72.0、濃縮倍率:4.2倍の結果が得られた。また、この粗濃縮汁の品質を分析したところ、濃度(Bx)74.0、糖度65.34%、純糖率88.29%、転化糖率1.12%、色価(Stammer Color Valueをいい、以下SCVと略す。)194という結果が得られた。十分実用性のある結果である。   Under the above operating conditions, 132.3 kg of clarified juice having a concentration (Bx) of 20.5 was pre-concentrated, and then 31.3 kg of crude concentrated juice, 72.0 of crude concentrated juice (Bx), and concentration ratio: 4.2 times. Results were obtained. Further, when the quality of the crude concentrated juice was analyzed, the concentration (Bx) was 74.0, the sugar content was 65.34%, the pure sugar rate was 88.29%, the invert sugar rate was 1.12%, and the color value (Stamer Color Value) Good, hereinafter abbreviated as SCV.) A result of 194 was obtained. This is a sufficiently practical result.

次いで、得られた粗濃縮汁のうち15.7kgを結晶缶を用いて真空下で晶析処理し、得られたスラリーを遠心分離機を用いて固液分離するととともに、分離機バスケット上に残った結晶ケーキに温水を噴射して結晶表面に付着する蜜分を除去して、高純度の結晶糖5.63kgを得た。この結晶糖の品質を分析したところ、糖度98.88%、純糖率99.6%、転化糖率0.02%、水分0.74重量%、灰分0.041重量%、色価(SCV)3.95という結果が得られた。   Next, 15.7 kg of the obtained crude concentrated juice is crystallized under vacuum using a crystal can, and the resulting slurry is subjected to solid-liquid separation using a centrifuge and remains on the separator basket. Warm water was sprayed onto the crystal cake to remove the honey content adhering to the crystal surface to obtain 5.63 kg of high-purity crystal sugar. When the quality of the crystal sugar was analyzed, the sugar content was 98.88%, the pure sugar ratio was 99.6%, the invert sugar ratio was 0.02%, the water content was 0.74% by weight, the ash content was 0.041% by weight, and the color value (SCV ) A result of 3.95 was obtained.

その後にこの高純度結晶糖を温水にて濃度(Bx)72となるように溶解して溶解糖液を7.8kg得た。この濃度(Bx)72の溶解糖液と前記濃度(Bx)72の粗濃縮汁とを5:2の割合で混合して金属製のボールに分取し、コンロで加熱して仕上げ濃縮処理して、濃度(Bx)96の濃縮糖汁を得た。高濃度(Bx)のため濃縮度合いの管理は温度で行い、その温度は115〜130℃とした。   Thereafter, the high-purity crystalline sugar was dissolved in warm water to a concentration (Bx) of 72 to obtain 7.8 kg of a dissolved sugar solution. This dissolved sugar solution with the concentration (Bx) 72 and the crude concentrated juice with the concentration (Bx) 72 are mixed at a ratio of 5: 2, separated into metal balls, and heated and finished with a stove for concentration. Thus, concentrated sugar juice having a concentration (Bx) of 96 was obtained. Because of the high concentration (Bx), the degree of concentration was controlled by temperature, and the temperature was 115 to 130 ° C.

仕上げ濃縮処理により得られた濃縮糖汁を金属製のボールごとコンロから降ろし、自然放冷しながら木べらで攪拌混合して結晶化させて粗粉状の含蜜糖を得た。さらに、この粗粉状含蜜糖を70℃に保ったエアーバスで1時間乾燥したのち乳鉢で更にダマを粉砕して均質な粉状含蜜糖を得た。この粉状含蜜糖は淡黄白色を示すものであった。なお、混合濃縮糖汁8kgに対して粉状含蜜糖5kgを得ることができた。十分高効率な生産性である。この粉状含蜜糖の品質を分析したところ、純糖度96.3%、転化糖率0.44%、水分2.2重量%、灰分1.19重量%、色価(SCV)44であった。十分な品質である。   The concentrated sugar juice obtained by the finish concentration treatment was dropped from the stove together with a metal bowl, stirred and mixed with a wooden spatula while allowed to cool naturally, and crystallized to obtain coarse powdered honey-containing sugar. Further, the coarsely powdered honey sugar was dried for 1 hour in an air bath maintained at 70 ° C., and further pulverized in a mortar to obtain a homogeneous pulverized honey sugar. This powdery honey-containing sugar had a pale yellowish white color. In addition, 5 kg of powdered honey sugar was able to be obtained with respect to 8 kg of mixed concentrated sugar juice. Highly efficient productivity. Analysis of the quality of the powdered honey sugar revealed a purity of 96.3%, an invert sugar rate of 0.44%, a moisture content of 2.2% by weight, an ash content of 1.19% by weight, and a color value (SCV) of 44. It was. Sufficient quality.

この粉状含蜜糖および前記粗濃縮汁(液状含蜜糖)の組成を分析し他の甘味製品の組成と比較したところ表1に示す結果が得られた。   The composition of the powdered honey sugar and the crude concentrated juice (liquid honey sugar) was analyzed and compared with the composition of other sweet products. The results shown in Table 1 were obtained.

Figure 2006020521
Figure 2006020521

本発明の製造方法に従って製造された上記粉状または液状含蜜糖は、広く一般に工業的に生産品として知られ、市販されている上白糖、グラニュー糖と比較すると、伝統的製法により得られる黒糖のように風味に影響を与える無機質栄養素を多く含んでいることが示されている。   The above powdered or liquid honey containing sugar produced according to the production method of the present invention is widely known as a product in general and industrially. Compared to commercially available white sugar and granulated sugar, brown sugar obtained by a traditional production method It is shown that it contains a lot of mineral nutrients that affect the flavor.

また、前記濃度(Bx)72の溶解糖液と前記濃度(Bx)72の粗濃縮汁とを5:4の割合で混合した混合汁からも同様にして粉状含蜜糖(試料2)を得た。試料2にかかる粉状含蜜糖の品質は、純糖度94.6%、転化糖率0.74%、水分2.4重量%、灰分1.83重量%、色価(SCV)68であった。十分な品質である。試料2にかかる粉状含蜜糖も淡黄白色を示すものであった。   Similarly, powdered honey sugar (sample 2) is also obtained from a mixed juice obtained by mixing the dissolved sugar solution having the concentration (Bx) 72 and the crude concentrated juice having the concentration (Bx) 72 at a ratio of 5: 4. Obtained. The quality of the powdered sucrose containing sample 2 is 94.6% pure sugar, 0.74% invert sugar, 2.4% by weight moisture, 1.83% by weight ash, and color value (SCV) 68. It was. Sufficient quality. The powdered sucrose containing sample 2 also showed a pale yellowish white color.

この試料2にかかる粉状含蜜糖と前記実施例1で作成した試料1にかかる粉状含蜜糖と黒糖とが備える風味について試験を行った。結果、黒糖は、独特のコクがあり、えぐみのある風味であった。試料1にかかる粉状含蜜糖および試料2にかかる粉状含蜜糖は黒糖のようなえぐみはなく和三盆的な上品な甘味と香りを有するものであった。また、試料1にかかる粉状含蜜糖よりも、試料2にかかる粉状含蜜糖のほうが、さとうきび由来の風味が強く感じられるものであった。粗濃縮汁と溶解糖液の割合により風味の変化がもたらされることも示された。   The taste of the powdered honey sugar according to Sample 2 and the powdery honey sugar and brown sugar according to Sample 1 prepared in Example 1 were tested. As a result, brown sugar had a unique and rich flavor. The powdered honey sugar according to Sample 1 and the powdered honey sugar according to Sample 2 had no sweetness like brown sugar and had a refined sweetness and fragrance like Japanese sanbon. In addition, the powdered honey sugar according to sample 2 was more strongly perceived as sugarcane-derived flavor than the powdered honey sugar according to sample 1. It was also shown that the ratio of the crude concentrate to the dissolved sugar solution caused a change in flavor.

また、試料2にかかる粉状含蜜糖、試料1にかかる粉状含蜜糖、これらの原料の粗濃縮汁および黒糖中の一般性菌およびカビ・酵母の有無を調べた。結果、黒糖については一般性菌が400個/g、カビ・酵母が10個/g検出されたのに対して、粗濃縮汁については一般性菌およびカビ・酵母ともに0個/2.5g、試料1および2にかかる粉状含蜜糖については一般性菌、カビ・酵母とも0個/0.5gという結果であった。本発明の製品が、黒糖と比較して一般性菌、カビ・酵母の含有量が格段に少ない(ない)ものであることが示された。   In addition, the presence of powdered honey sugar according to Sample 2, the powdered honey sugar according to Sample 1, the crude concentrated juice and brown sugar of these raw materials, and the presence of common bacteria and mold / yeast were examined. As a result, 400 bacterium / g of general bacteria were detected for brown sugar and 10 bacterium / g for mold / yeast, whereas 0 / 2.5 g for general bacteria and mold / yeast were used for crude concentrate. As for the powdered honey-containing sugars on Samples 1 and 2, the results were 0 / 0.5 g for both general bacteria, molds and yeasts. It was shown that the product of the present invention has significantly less (not) the content of common bacteria, molds and yeasts compared to brown sugar.

以上実施例1および2より、本発明の製造方法によれば、原料由来の風味を残した含蜜糖を、衛生的かつ工業的大量に生産することが可能であることが示された。   As described above, Examples 1 and 2 indicate that according to the production method of the present invention, it is possible to produce a large amount of sanitary and industrially large amounts of honey-containing sugar that leaves a flavor derived from the raw material.

本発明は、各種天然素材由来の風味を残した粉状または液状の含蜜糖を衛生的かつ工業的大量に生産する分野のほか、各種天然素材由来の風味を残した含蜜糖を原料として他の製品を生産する分野においても利用することができる。   In addition to the field of producing hygienic and industrial mass production of powdered or liquid honey-containing sugar that leaves flavors derived from various natural materials, the present invention uses honey-containing sugar that leaves flavors derived from various natural materials as raw materials. It can also be used in the field of producing other products.

本発明にかかる方法のフロー図である。FIG. 3 is a flow diagram of a method according to the present invention.

Claims (8)

以下(1)〜(8)の処理工程を含むことを特徴とする含蜜糖の製造方法。
(1)さとうきびの圧搾により得た圧搾汁、さとうきびの抽出により得た抽出汁、または圧搾汁と抽出汁とを混合した混合汁からなる粗汁を得る粗汁生成工程。
(2)前記粗汁をスクリーン処理して不溶物質の除去を行なう予備濾過工程。
(3)不溶物質が除去された粗汁を膜濾過して不純物および菌類を分離除去するとともに清澄汁を得る膜濾過処理工程。
(4)前記清澄汁を濃縮処理して粗濃縮汁を得る予備濃縮処理工程。
(5)前記粗濃縮汁の一部を晶析して結晶糖を得る晶析処理工程。
(6)晶析処理工程で得られた結晶糖を溶解して溶解糖液を得る溶解工程。
(7)前記溶解糖液と晶析及び溶解処理を行わない前記粗濃縮汁とを混合した混合糖汁を冷却晶析可能な濃度まで濃縮する仕上げ濃縮工程。
(8)仕上げ濃縮により得られた濃縮糖汁を冷却して固形化・粉化して粉状の含蜜糖を得る粉糖化処理工程。
The manufacturing method of a sugar containing sugar characterized by including the process of following (1)-(8).
(1) A crude juice production step for obtaining a crude juice comprising a pressed juice obtained by pressing sugar cane, an extracted juice obtained by extracting sugar cane, or a mixed juice obtained by mixing pressed juice and extracted juice.
(2) A preliminary filtration step in which the crude juice is screened to remove insoluble substances.
(3) A membrane filtration treatment step for separating and removing impurities and fungi by membrane filtration of the crude juice from which insoluble substances have been removed, and obtaining a clarified juice.
(4) A pre-concentration treatment step for obtaining a crude concentrate by concentrating the clear juice.
(5) A crystallization treatment step in which a part of the crude concentrated juice is crystallized to obtain crystalline sugar.
(6) A dissolution step in which the crystal sugar obtained in the crystallization treatment step is dissolved to obtain a dissolved sugar solution.
(7) A finishing concentration step of concentrating the mixed sugar juice obtained by mixing the dissolved sugar liquid and the crude concentrated juice not subjected to crystallization and dissolution treatment to a concentration capable of cooling and crystallization.
(8) A saccharification treatment step in which the concentrated sugar juice obtained by finish concentration is cooled, solidified and pulverized to obtain powdered honey-containing sugar.
粗濃縮汁を液状の含蜜糖として採取する液状含蜜糖採取工程を有する請求項1記載の含蜜糖の製造方法。 Method for producing a molasses sugar according to claim 1, further comprising a liquid mixture solid sugar collecting step of collecting the crude concentrated juice as molasses sugar liquid. 晶析処理工程における晶析処理過程で分離される糖蜜を、粗濃縮汁と混合して、これを液状の含蜜糖として得る液状含蜜糖採取工程を有する請求項1または2記載の含蜜糖の製造方法。 The molasses according to claim 1 or 2, further comprising a liquid molasses collecting step in which the molasses separated in the crystallization treatment step in the crystallization treatment step is mixed with the crude concentrated juice to obtain liquid molasses. A method for producing sugar. 膜処理工程に先立って粗汁のpHを6〜7.5に調整する請求項1〜3の何れか1項に記載の含蜜糖の製造方法。   The manufacturing method of the sugar containing sugar of any one of Claims 1-3 which adjusts the pH of coarse juice to 6-7.5 prior to a membrane treatment process. 予備濃縮処理をプレート型熱交換器または流下液薄膜式熱交換器を備えた濃縮設備により行う請求項1〜4のいずれか1項に記載の含蜜糖の製造方法。   The manufacturing method of the sugar-containing sugar of any one of Claims 1-4 which perform a preconcentration process with the concentration equipment provided with the plate type heat exchanger or the falling film thin film type heat exchanger. 以下(1)〜(8)の手段を含むことを特徴とする含蜜糖の製造装置。
(1)さとうきびの圧搾により得た圧搾汁、さとうきびの抽出により得た抽出汁、または圧搾汁と抽出汁とを混合した混合汁からなる粗汁を得る粗汁生成手段。
(2)前記粗汁をスクリーン処理して不溶物質の除去を行なう予備濾過手段。
(3)不溶物質が除去された粗汁を膜濾過して不純物および菌類を分離除去するとともに清澄汁を得る膜濾過処理手段。
(4)前記清澄汁を濃縮処理して粗濃縮汁を得る予備濃縮処理手段。
(5)前記粗濃縮汁の一部を晶析して結晶糖を得る晶析処理手段。
(6)晶析処理手段で得られた結晶糖を溶解して溶解糖液を得る結晶糖溶解手段。
(7)前記溶解糖液と晶析及び溶解処理を行わない前記粗濃縮汁とを混合した混合糖汁を冷却晶析可能な濃度まで濃縮する仕上げ濃縮手段。
(8)仕上げ濃縮により得られた濃縮糖汁を冷却して固形化・粉化して粉状の含蜜糖を得る粉糖化処理手段。
An apparatus for producing honey-containing sugar, comprising the following means (1) to (8).
(1) Crude juice producing means for obtaining a crude juice comprising a pressed juice obtained by pressing sugar cane, an extracted juice obtained by extracting sugar cane, or a mixed juice obtained by mixing pressed juice and extracted juice.
(2) Preliminary filtration means for removing insoluble substances by screening the crude juice.
(3) Membrane filtration means for filtering the crude juice from which insoluble substances have been removed to separate and remove impurities and fungi and to obtain a clear juice.
(4) Preconcentration processing means for concentrating the clarified juice to obtain a crude concentrated juice.
(5) A crystallization treatment means for crystallization of a part of the crude concentrated juice to obtain a crystalline sugar.
(6) Crystal sugar dissolving means for dissolving the crystal sugar obtained by the crystallization treatment means to obtain a dissolved sugar solution.
(7) A finishing concentration means for concentrating the mixed sugar juice obtained by mixing the dissolved sugar liquid and the crude concentrated juice not subjected to crystallization and dissolution treatment to a concentration capable of cooling and crystallization.
(8) Powdered saccharification processing means for cooling and concentrating and pulverizing the concentrated sugar juice obtained by finish concentration to obtain powdered honey-containing sugar.
粗濃縮汁を液状の含蜜糖として採取する液状含蜜糖採取手段を備える請求項6記載の含蜜糖の製造装置。   The apparatus for producing honey-containing sugar according to claim 6, further comprising a liquid honey-containing sugar collecting means for collecting the crude concentrated juice as liquid honey-containing sugar. 晶析処理手段における晶析処理にて分離された糖蜜を、粗濃縮汁と混合し、これを液状の含蜜糖として採取する液状含蜜糖採取手段を備える請求項6または7記載の含蜜糖の製造装置。   The molasses according to claim 6 or 7, further comprising liquid molasses collecting means for mixing the molasses separated by the crystallization treatment in the crystallization treatment means with the crude concentrated juice and collecting the molasses as liquid molasses. Sugar production equipment.
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