JP2005304359A - Heat sterilized liquid whole egg and method for producing the same - Google Patents

Heat sterilized liquid whole egg and method for producing the same Download PDF

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JP2005304359A
JP2005304359A JP2004124362A JP2004124362A JP2005304359A JP 2005304359 A JP2005304359 A JP 2005304359A JP 2004124362 A JP2004124362 A JP 2004124362A JP 2004124362 A JP2004124362 A JP 2004124362A JP 2005304359 A JP2005304359 A JP 2005304359A
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egg
sterilization
liquid
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whole egg
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JP4152343B2 (en
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Shuntaro Ise
俊太郎 伊勢
Masahiko Noguchi
雅彦 野口
Kazufumi Ito
和史 伊藤
Akira Fukai
晃 深井
Nao Horiuchi
菜穂 堀内
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Ise Delica Co ltd
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Abstract

<P>PROBLEM TO BE SOLVED: To provide bag-packed heat sterilized liquid whole egg keeping physical properties similar to those of fresh egg, requiring not so strict asepsis in a process up to packaging, and subjecting a packaged article to heat sterilization. <P>SOLUTION: A method for producing heat sterilized liquid whole egg comprises a process of hermetically packaging thick membrane-containing liquid egg, and a process of sterilization comprising soaking entirely the bag-packed liquid whole egg in hot water having sterilization temperature of 57-61°C, and subjecting the bag-packed liquid whole egg to hot-water spray or steam spray. <P>COPYRIGHT: (C)2006,JPO&NCIPI

Description

本発明は、割卵直後の全卵の物理的性状をできるだけ保持しつつ、殺菌により保存性を向上せしめた加熱殺菌液全卵及びその製造方法に関する。   The present invention relates to a heat-sterilized whole egg whose storability has been improved by sterilization while maintaining the physical properties of the whole egg immediately after breaking as much as possible, and a method for producing the same.

従来、卵殻を除去した液全卵の殺菌工程は、包装容器への充填工程の前に行うのが一般的であった。具体的には、プレートヒーターとホールディングチューブを利用し、所定温度で所定時間加熱するいわゆる連続式殺菌法、及び、撹拌装置を備えたタンク内で所定温度で所定時間加熱するいわゆるバッチ殺菌法がある。いずれの方法も、殺菌工程の後に、液卵が包装容器に充填されることとなっている。これに対し、下記特許文献1で開示されている発明では、濾過工程を経て均質化した液全卵を包装容器へ充填した後に包装容器ごと殺菌工程に供する技術が提案されている。
一方、上記の従来の連続式殺菌法及びバッチ殺菌法のいずれにおいても、液卵をあらかじめ濾過又は撹拌して卵白と卵黄とを均質化しておくのが一般的である。これに対し、下記特許文献2で開示されている発明では、液卵にする前の殻付卵の状態で殺菌工程に供する技術が提案されている。
特開2003−274904号公報(段落番号0018から0036まで及び図1) 特開2002−262832号公報(段落番号0010、0013及び0015)
Conventionally, the sterilization process of the liquid whole egg from which the eggshell has been removed is generally performed before the filling process into the packaging container. Specifically, there are a so-called continuous sterilization method in which a plate heater and a holding tube are used for heating for a predetermined time at a predetermined temperature, and a so-called batch sterilization method in which heating is performed for a predetermined time at a predetermined temperature in a tank equipped with a stirring device. . In any method, the liquid egg is filled in the packaging container after the sterilization step. On the other hand, in the invention disclosed in Patent Document 1 below, a technique is proposed in which the whole packaged egg is filled in the packaging container after being homogenized through the filtration process and then used for the sterilization process.
On the other hand, in any of the conventional continuous sterilization methods and batch sterilization methods described above, it is common to homogenize egg white and egg yolk by filtering or stirring the liquid egg in advance. On the other hand, in the invention disclosed in Patent Document 2 below, a technique for subjecting to a sterilization process in a state of a shelled egg before forming a liquid egg is proposed.
JP 2003-274904 A (paragraph numbers 0018 to 0036 and FIG. 1) JP 2002-262832 A (paragraph numbers 0010, 0013 and 0015)

前記の連続式殺菌法においては、プレートヒーター及びホールディングチューブへ液卵を流動させる必要があることから、通常10〜40メッシュのストレーナーを通す濾過工程がある。また、液全卵のポンプ移送の工程も多いため、卵白の粘度減少を主とする液全卵の物理的損傷が多い。これにより、生卵の有する物理的性状が損なわれることとなる。
また、前記のバッチ殺菌法においても、タンク内の熱交換効率を高めるため撹拌することからやはり液全卵に対する物理的損傷が生じ、生卵の有する物理的性状が損なわれることとなる。
これらの問題点は、包装容器への充填に先立って液全卵を濾過工程を経て均質化するという前記特許文献1記載の発明においても同様に該当するものである。
In the above-mentioned continuous sterilization method, since it is necessary to flow the liquid egg to the plate heater and the holding tube, there is usually a filtration step through a strainer of 10 to 40 mesh. In addition, since there are many pumping steps for the whole liquid egg, there is much physical damage to the whole liquid egg mainly due to a decrease in the viscosity of the egg white. Thereby, the physical property which a raw egg has will be impaired.
In the batch sterilization method as well, since the agitation is performed to increase the heat exchange efficiency in the tank, physical damage to the whole liquid egg also occurs, and the physical properties of the raw egg are impaired.
These problems also apply to the invention described in Patent Document 1 in which the whole liquid egg is homogenized through a filtration step prior to filling the packaging container.

一方、たとえばカツ丼、親子丼などのように、白身と黄身とが完全に混合しない状態の方が外観上及び食感上好ましい用途の場合には、全卵又はこれに近い状態の液卵を加熱殺菌せずにパック詰めしてこれをできるだけ低温で保管したものが提供されていた。しかし、衛生上及び保存上の問題から、全卵又はこれに近い状態の液卵であって、加熱殺菌されたパック詰め製品が待望されていた。
ここで、前記特許文献2記載の先行技術においては、殻付卵の状態で加熱することで全卵の状態で加熱殺菌することでこの問題点を解決しようとしている。しかし、加熱殺菌後に包装容器への充填の際に割卵工程が必要となり、この工程を厳密に無菌的に行うことが必要となり、このための管理コストが新たな問題となる。
On the other hand, in the case where it is preferable in terms of appearance and texture that white and yolks are not completely mixed, such as cutlet bowl and parent-child bowl, whole eggs or liquid eggs in a state close to this are used. What was packed without heat sterilization and stored at as low a temperature as possible was provided. However, from the viewpoint of hygiene and storage, a packed product that is a whole egg or a liquid egg in a state close to this and sterilized by heating has been awaited.
Here, in the prior art of the said patent document 2, it is going to solve this problem by heat-sterilizing in the state of a whole egg by heating in the state of a shelled egg. However, an egg breaking step is required when filling the packaging container after heat sterilization, and this step needs to be performed strictly aseptically, and the management cost for this becomes a new problem.

上記の各問題点に鑑み、本発明は、生卵に近い物理的性状をできるだけ保ちつつ、かつ、包装までの工程はさほど厳密な無菌性は要さず、さらに包装品は加熱殺菌が施されている袋詰め液全卵を提供することを課題とする。   In view of the above problems, the present invention maintains physical properties close to that of raw eggs as much as possible, and the process up to packaging does not require strict sterility, and the packaged product is subjected to heat sterilization. It is an object to provide a whole egg-packed liquid egg.

前記の課題に鑑み、本発明に係る加熱殺菌液全卵は、濃厚卵白を含む液全卵を密封包装し、その包装ごと殺菌温度57℃以上61℃以下の温水浸漬、温水スプレー又は蒸気噴霧にて殺菌処理をしたことを特徴とする。
「濃厚卵白」とは、卵黄成分と混じることなく、卵白として分離可能な状態のものをいう。そして、「濃厚卵白を含む液全卵」とは、割卵したままの状態の全く撹拌されていない液全卵、又は、濃厚卵白を認め得る程度の軽度の撹拌がなされた液全卵をいう。
「密封包装」については、内容物を外気から完全に遮断できるものであれば、その材質及び形状は問わない。ただし、温水浸漬、温水スプレー又は蒸気噴霧による殺菌処理が施されるため、耐熱性及び耐水性を備えた材質が要求される。また、殺菌処理の際に、包装内部の温度分布ができるだけ均一となるように、液状の内容物を収容した際に、できるだけ平らな状態を保てるような形状のものが望ましい。具体的には、ナイロン、ポリエチレン、ポリプロピレン製の袋が望ましい。このような袋であれば、内容物を容れた後、口を熱圧着することで容易に密封が可能である。
In view of the above problems, the heat-sterilized liquid whole egg according to the present invention seals and wraps the liquid whole egg containing concentrated egg white, and the whole sterilization temperature is 57 ° C. to 61 ° C. for hot water immersion, hot water spray, or steam spray. It is characterized by having been sterilized.
“Dense egg white” refers to a substance that is separable as egg white without being mixed with egg yolk components. The “liquid whole egg containing a thick egg white” means a liquid whole egg that has not been stirred at all, or a liquid whole egg that has been lightly stirred to such an extent that a thick egg white can be recognized. .
The material and shape of the “sealed packaging” are not limited as long as the contents can be completely shielded from the outside air. However, since sterilization is performed by hot water immersion, hot water spray or steam spray, a material having heat resistance and water resistance is required. In addition, it is desirable that the liquid content be kept as flat as possible when the liquid contents are accommodated so that the temperature distribution inside the package is as uniform as possible during sterilization. Specifically, nylon, polyethylene, and polypropylene bags are desirable. With such a bag, after the contents are filled, the mouth can be easily sealed by thermocompression bonding.

「殺菌温度」とは、撹拌装置を備えたタンクで58℃10分保持するバッチ式殺菌方法と同程度の殺菌効果を得るに必要かつ十分な時間だけ、袋詰め全卵が加熱される温度をいう。この加熱に要する時間は、温度が低いほど長く、また高いほど短くなる。ただし、温度が低すぎる場合には、いくら長時間処理したとしても殺菌は不十分又は不可能である。また、温度が高すぎる場合には、殺菌は十分ではあるが蛋白変性により液卵として使用不可となる。これらの事情を考慮して、本件発明において適切な殺菌温度は、上記の通り、57℃以上かつ61℃以下、さらに望ましくは58℃以上かつ60℃以下となる。
本件発明に係る加熱殺菌液全卵は、濃厚卵白を含む液全卵を密封包装する工程と、前記袋詰めした液全卵をその包装ごと殺菌温度57℃以上かつ61℃以下の温水浸漬、温水スプレー又は蒸気噴霧にて殺菌処理する殺菌工程とを含んでなる製造方法にて製造することができる。
“Sterilization temperature” refers to the temperature at which the whole eggs in a bag are heated for the time necessary and sufficient to obtain the same level of sterilization effect as a batch-type sterilization method in which a tank equipped with a stirring device is maintained at 58 ° C. for 10 minutes. Say. The time required for this heating is longer as the temperature is lower and shorter as it is higher. However, if the temperature is too low, sterilization is insufficient or impossible no matter how long it is treated. If the temperature is too high, sterilization is sufficient, but it cannot be used as a liquid egg due to protein denaturation. Considering these circumstances, the appropriate sterilization temperature in the present invention is 57 ° C. or more and 61 ° C. or less, more preferably 58 ° C. or more and 60 ° C. or less as described above.
The whole heat-sterilized liquid egg according to the present invention includes a step of hermetically packaging a liquid whole egg containing a thick egg white, and the packaged whole liquid egg is immersed in warm water at a sterilization temperature of 57 ° C. or higher and 61 ° C. or lower, It can manufacture with the manufacturing method which comprises the sterilization process of sterilizing by spray or vapor | steam spraying.

さらに具体的には、まず、殻付生卵を所定の手順にて洗浄及び殺菌する。次に、この殻付生卵を割卵し、液全卵を得る。この段階で次の包装工程に供してもよい。ただ、卵殻等の夾雑物を除くため、シェルトラップを介してもよい。また、次工程へはポンプによる移送を行うこととしてもよいが、濃厚卵白が残らないような撹拌が実質的に生じないように留意する必要がある。
そして、上記の液全卵は、包装工程に供されることとなる。すなわち、液全卵が、濃厚卵白を含んだ状態で、かつ、殺菌がなされていない状態で前記の包装容器内に密封されることとなる。なお、ここまでの工程における清浄度は、通常の食品加工に要求される程度のもので足り、厳密な無菌性までは要求されない。
More specifically, first, the raw eggs with shells are washed and sterilized by a predetermined procedure. Next, this shelled raw egg is split to obtain a liquid whole egg. At this stage, you may use for the following packaging process. However, a shell trap may be used to remove impurities such as eggshells. Moreover, although it is good also as performing transfer with a pump to the next process, it needs to be careful so that the stirring which does not leave thick egg white does not arise substantially.
And said liquid whole egg will be used for a packaging process. That is, the liquid whole egg is sealed in the packaging container in a state containing a thick egg white and not being sterilized. It should be noted that the cleanliness in the steps so far is sufficient for normal food processing, and strict sterility is not required.

この後、液全卵は、密封包装された状態で、温水浸漬、温水スプレー又は蒸気噴霧にて殺菌処理する殺菌工程に供される。このときの殺菌温度は、前記のとおり、57℃以上かつ61℃以下であれば、十分な殺菌効果が得られつつ、割卵直後の生卵とほぼ同等の物理的性状が保たれることとなる。なお、殺菌温度が58℃以上かつ60℃以下であれば殺菌後の液全卵の物理的性状は、割卵直後の生卵により近いものとなる。
殺菌工程が済むと、包装された加熱殺菌液全卵は、冷却工程を経て、貯蔵、輸送に供されることとなる。
Thereafter, the whole liquid egg is subjected to a sterilization process in which it is sterilized by hot water immersion, hot water spray, or steam spraying in a hermetically packaged state. If the sterilization temperature at this time is 57 ° C. or more and 61 ° C. or less as described above, a sufficient sterilization effect can be obtained, and physical properties almost the same as those of raw eggs immediately after breaking can be maintained. Become. If the sterilization temperature is 58 ° C. or more and 60 ° C. or less, the physical properties of the liquid whole egg after sterilization are closer to the raw egg immediately after the cleavage.
When the sterilization process is completed, the packaged heat-sterilized liquid whole egg is subjected to storage and transportation through a cooling process.

上記の本件発明の構成により、生卵に近い物理的性状をできるだけ保ちつつ、かつ、包装までの工程はさほど厳密な無菌性は要さず、さらに包装品は加熱殺菌が施されている袋詰め液全卵を提供することが可能となる。   According to the configuration of the present invention described above, the physical property close to that of a raw egg is kept as much as possible, and the process up to packaging does not require strict sterility, and the packaged product is packaged by heat sterilization. Liquid whole eggs can be provided.

以下、本発明の実施例を説明する。
(1)サンプル作製
Mサイズの鶏卵の卵殻表面を洗浄し、次いで150ppmの次亜塩素酸ナトリウム溶液中に30秒間浸漬して卵殻表面を殺菌した。そして割卵し、包装工程に供した。
包装工程においては、ポンプで輸送した液全卵を清浄なナイロンポリ袋に1kg充填したのち、口を熱圧着にて閉じて包装した。この充填及び包装の段階では、濃厚卵白は明瞭に残存していた。この液全卵を包装ごと、殺菌工程に供した。
比較例1の殺菌工程においては、56℃の湯槽に75分浸漬して加熱殺菌を施した。これにより、包装内部の液全卵の中心部は28分間56℃に保たれた。
Examples of the present invention will be described below.
(1) Sample preparation The eggshell surface of M-sized eggs was washed, and then immersed in a 150 ppm sodium hypochlorite solution for 30 seconds to sterilize the eggshell surface. The eggs were then split and used for the packaging process.
In the packaging process, 1 kg of liquid whole egg transported by a pump was filled in a clean nylon plastic bag, and then the mouth was closed by thermocompression packaging. At this filling and packaging stage, the thick egg white remained clearly. The whole liquid egg was subjected to a sterilization process for each package.
In the sterilization process of Comparative Example 1, heat sterilization was performed by immersing in a hot bath at 56 ° C. for 75 minutes. Thereby, the center part of the liquid whole egg inside a package was kept at 56 degreeC for 28 minutes.

実施例1の殺菌工程においては、57℃の湯槽に60分浸漬して加熱殺菌を施した。これにより、包装内部の液全卵の中心部は17分間57℃に保たれた。
実施例2の殺菌工程においては、58℃の湯槽に50分浸漬して加熱殺菌を施した。これにより、包装内部の液全卵の中心部は10分間58℃に保たれた。
実施例3の殺菌工程においては、60℃の湯槽に40分浸漬して加熱殺菌を施した。これにより、包装内部の液全卵の中心部は3.5分間60℃に保たれた。
実施例4の殺菌工程においては、61℃の湯槽に37分浸漬して加熱殺菌を施した。これにより、包装内部の液全卵の中心部は2.5分間61℃に保たれた。
In the sterilization process of Example 1, heat sterilization was performed by immersing in a 57 ° C. hot water bath for 60 minutes. Thereby, the center part of the liquid whole egg inside a package was maintained at 57 degreeC for 17 minutes.
In the sterilization process of Example 2, heat sterilization was performed by immersing in a hot water bath at 58 ° C. for 50 minutes. Thereby, the center part of the liquid whole egg inside a package was kept at 58 degreeC for 10 minutes.
In the sterilization process of Example 3, it was immersed in a 60 ° C. hot water bath for 40 minutes for heat sterilization. Thereby, the center part of the liquid whole egg inside a package was kept at 60 degreeC for 3.5 minutes.
In the sterilization process of Example 4, it was immersed in a 61 ° C. hot water bath for 37 minutes for heat sterilization. As a result, the central part of the liquid whole egg inside the package was kept at 61 ° C. for 2.5 minutes.

比較例2の殺菌工程においては、62℃の湯槽に35分浸漬して加熱殺菌を施した。これにより、包装内部の液全卵の中心部は1.5分間62℃に保たれた。
殺菌工程後は、20℃の井水を10分間スプレーして冷却し、さらに5℃の冷水を20分間スプレーして冷却した。冷却後、8℃にて冷蔵保存した。
(2)殺菌試験
包装前の液全卵に、サルモネラ菌(Salmonella sp.)を播種した上で上記(1)のとおり各実施例及び比較例のサンプルを作製した。なお、殺菌工程前のサルモネラ菌数は、液全卵1g当たり2×103cfuであった。
In the sterilization process of Comparative Example 2, heat sterilization was performed by immersing in a 62 ° C. hot water bath for 35 minutes. As a result, the center of the liquid whole egg inside the package was kept at 62 ° C. for 1.5 minutes.
After the sterilization step, 20 ° C. well water was sprayed for 10 minutes to cool, and then 5 ° C. cold water was sprayed for 20 minutes to cool. After cooling, it was refrigerated at 8 ° C.
(2) Bactericidal test After inoculating Salmonella sp. On the liquid whole eggs before packaging, samples of each example and comparative example were prepared as described in (1) above. In addition, the Salmonella count before the sterilization process was 2 × 10 3 cfu per 1 g of the whole liquid egg.

上記液全卵の殺菌工程後、1日目から8日目までの各日、各サンプルを寒天培養し、液全卵1g当たりの一般生菌、大腸菌群及びサルモネラ菌のコロニー数(cfu)を算定した。
その結果、各実施例及び比較例のいずれにおいても、1日目から8日目までの各日とも、一般生菌、大腸菌群及びサルモネラ菌は検出されなかった。したがって、殺菌温度が56℃、57℃、58℃、60℃、61℃及び62℃の場合いずれも、十分な殺菌効果が認められた。なお、殺菌温度が55℃以下の場合についてもこの試験を試みたが、十分な殺菌効果を得るための湯槽浸漬時間が90分を超えてしまうため、商業的な製造条件を満たさないと判断した。
Each sample from day 1 to day 8 after the sterilization process of the liquid whole egg, each sample is agar-cultured, and the number of colonies (cfu) of general viable bacteria, coliforms and Salmonella per gram of liquid whole egg is calculated. did.
As a result, in each of the Examples and Comparative Examples, no viable bacteria, coliforms and Salmonella were detected on each day from the first day to the eighth day. Therefore, a sufficient sterilizing effect was recognized in all cases where the sterilization temperature was 56 ° C, 57 ° C, 58 ° C, 60 ° C, 61 ° C and 62 ° C. In addition, although this test was tried also about the case where sterilization temperature is 55 degrees C or less, since the bath immersion time for obtaining sufficient sterilization effect would exceed 90 minutes, it judged that it did not satisfy commercial manufacturing conditions. .

(3)物性試験
以下の各物性試験においては、(1)で得られた各実施例及び比較例の液全卵を袋から取り出し、ホモミキサーで2,000rpmにて2分間均質化したものをサンプルとして用いた。
また、陽性対象として、(1)の各実施例及び比較例と同じ大きさで同じ産卵日の鶏卵を用いて、(1)と同様に包装工程までは行い、殺菌工程は行わない液全卵を準備した。
一方、陰性対象として、(1)の各実施例及び比較例と同じ大きさで同じ産卵日の鶏卵を用いて、(1)と同様の卵殻表面洗卵及び殺菌を施して割卵した液全卵を、その卵白と卵黄とが均一になるまで撹拌混合した後、20メッシュのストレーナーを通し、60℃で3.5分間プレート殺菌を行い、清潔な充填機を用いて(1)と同様の包装工程に供したものを準備した。
(3) Physical property test In each of the following physical property tests, the liquid whole eggs of each Example and Comparative Example obtained in (1) were taken out of the bag, and homogenized at 2,000 rpm for 2 minutes. Used as a sample.
In addition, as a positive target, using the same size eggs as the examples and comparative examples of (1) and the same egg-laying date, the whole egg is processed until the packaging process as in (1) and without the sterilization process. Prepared.
On the other hand, as a negative target, using all the eggs of the same spawning day with the same size as each Example and Comparative Example of (1), the whole liquid that was divided by egg washing and sterilization in the same manner as in (1) The egg is stirred and mixed until the egg white and egg yolk are uniform, then passed through a 20 mesh strainer, sterilized at 60 ° C. for 3.5 minutes, and the same as in (1) using a clean filling machine. What was used for the packaging process was prepared.

これらの陽性対象及び陰性対象のいずれも、以下の各試験に際しては、各実施例及び比較例の液全卵と同様に、ホモミキサーで2,000rpmにて2分間均質化したものをサンプルとして用いた。
(3−1)粘度
各サンプルを10℃に冷却し、B型粘度計(ハーケ社)にて、R3ロータを使用して回転数200rpmにおける粘度を測定した。粘度の評価は、陰性対照の粘度を上回る場合を「優」とし、及び陰性対照の粘度以下の場合を「不可」とした。その結果を、下記の表1に示す。
For each of these positive and negative subjects, the sample homogenized with a homomixer at 2,000 rpm for 2 minutes was used as a sample in the following tests, as in the liquid whole eggs of each Example and Comparative Example. It was.
(3-1) Viscosity Each sample was cooled to 10 ° C., and the viscosity at a rotation speed of 200 rpm was measured with a B-type viscometer (Haake) using an R3 rotor. The evaluation of the viscosity was “excellent” when the viscosity was higher than that of the negative control, and “impossible” when the viscosity was lower than the viscosity of the negative control. The results are shown in Table 1 below.

Figure 2005304359
上記表1に示すとおり、いずれの実施例及び比較例も陽性対象の粘度を上回った。よって、粘度で見る限り、実施例と比較例とは同程度の評価となった。ただし、各実施例の粘度は、比較例の粘度に比べて少なくとも下回ってはいないことから、粘度に関して実施例は比較例に対して少なくとも劣ってはいない、ということはいえる。
(3−2)起泡性試験
起泡性試験として、下記の泡の高さ及び泡密度の測定を通して、加熱殺菌液全卵の泡立ちやすさに対する殺菌温度の影響を評価した。
Figure 2005304359
As shown in Table 1 above, all of the examples and comparative examples exceeded the viscosity of the positive target. Therefore, as far as the viscosity is concerned, the examples and comparative examples were evaluated to the same degree. However, since the viscosity of each example is not at least lower than the viscosity of the comparative example, it can be said that the example is not at least inferior to the comparative example with respect to the viscosity.
(3-2) Foaming property test As the foaming property test, the effect of the sterilization temperature on the easiness of foaming of the whole heat-sterilized liquid egg was evaluated through the measurement of the foam height and the foam density described below.

(3−2−1)泡の高さ
各サンプル300gを25℃に加温した後に270gの上白糖を添加し、これをボールに入れ、縦型ホイップミキサーにて撹拌しつつ、ボール底面からのホイップ液全卵の泡の高さ(cm)を、撹拌時間3分、5分、7分、10分、14分、17分及び20分の時点で測定した。
泡の高さについては、その数値が大きいほど良く空気を含んでおり、起泡性が良好であると評価できる。具体的な評価としては、撹拌時間20分で数値が最大であった場合を「優」とし、並びに撹拌時間20分より前で数値が最大であった場合はその最大数値に対する撹拌時間20分の数値の減少率が5%未満のときを「良」とし、及び5%以上のときを「不可」とした。その結果を、下記の表2に示す。
(3-2-1) Foam height After 300 g of each sample was heated to 25 ° C., 270 g of white sucrose was added, and this was placed in a bowl and stirred with a vertical whip mixer. The foam height (cm) of the whole whipped liquid egg was measured at the time points of stirring time of 3 minutes, 5 minutes, 7 minutes, 10 minutes, 14 minutes, 17 minutes and 20 minutes.
As for the height of the foam, the larger the numerical value, the better the air is contained, and it can be evaluated that the foamability is good. As a specific evaluation, the case where the numerical value was the maximum at 20 minutes of stirring was “excellent”, and when the numerical value was the maximum before the stirring time of 20 minutes, the stirring time was 20 minutes relative to the maximum value. When the numerical reduction rate was less than 5%, it was judged as “good”, and when it was 5% or more, it was judged as “impossible”. The results are shown in Table 2 below.

Figure 2005304359
上記表2に示すとおり、実施例2(58℃)及び実施例3(60℃)においては、撹拌時間が長くなるにつれて起泡性が向上しており、ほぼ生卵と同視できる陽性対照と同様の挙動となった。すなわち、泡の高さでは、実施例2及び3は生卵とほぼ同様と評価することができる。
また、実施例1(57℃)及び実施例4(61℃)は、撹拌時間20分までに数値が最大となるものの、その減少率は5%未満と小さく、実用上は問題ないものと思われる。
一方、比較例1(56℃)及び比較例2(62℃)は、撹拌時間20分までに数値が最大となり、その減少率が5%以上であり、陰性対照と挙動を同じくした。この結果は、撹拌時間が長くなるにつれて、気泡を構成する膜が損傷されやすくなることを推認させる。
Figure 2005304359
As shown in Table 2 above, in Example 2 (58 ° C.) and Example 3 (60 ° C.), the foaming property is improved as the stirring time becomes longer, which is almost the same as the positive control that can be regarded as a raw egg. It became the behavior of. That is, in the height of the bubbles, Examples 2 and 3 can be evaluated as almost the same as the raw eggs.
In Example 1 (57 ° C.) and Example 4 (61 ° C.), the maximum value is reached by 20 minutes of stirring time, but the decrease rate is as small as less than 5%, and there is no problem in practical use. It is.
On the other hand, in Comparative Example 1 (56 ° C.) and Comparative Example 2 (62 ° C.), the value reached the maximum by 20 minutes of stirring time, and the decrease rate was 5% or more, and the behavior was the same as the negative control. This result suggests that the membrane constituting the bubbles is likely to be damaged as the stirring time becomes longer.

(3−2−2)泡密度
上記(3−2−1)と同一のホイップ液全卵について、所定容積の重量を測定して、さらに当該容積で除した数値により泡密度(g/ml)を測定した。
泡密度については、その数値が小さいほど良く空気を含んでおり、起泡性が良好であると評価できる。具体的な評価としては、撹拌時間20分で数値が最小であった場合を「優」とし、並びに撹拌時間20分より前で数値が最小であった場合はその最小数値に対する撹拌時間20分の数値の増加率が2%未満のときを「良」とし、及び2%以上のときを「不可」とした。その結果を、下記の表3に示す。
(3-2-2) Foam density For the whole whipped egg as in (3-2-1) above, the weight of a predetermined volume is measured, and the foam density (g / ml) is further divided by the volume. Was measured.
As for the bubble density, the smaller the numerical value, the better the air is contained, and it can be evaluated that the foamability is good. Specifically, when the numerical value is minimum at 20 minutes of stirring time, “excellent”, and when the numerical value is minimum before 20 minutes of stirring time, the stirring time is 20 minutes relative to the minimum value. When the numerical increase rate was less than 2%, it was judged as “good”, and when it was 2% or more, it was judged as “impossible”. The results are shown in Table 3 below.

Figure 2005304359
上記表3に示すとおり、実施例2(58℃)及び実施例3(60℃)においては、撹拌時間が長くなるにつれて起泡性が向上しており、ほぼ生卵と同視できる陽性対照と同様の挙動となった。すなわち、泡密度では、実施例2及び3は生卵とほぼ同様と評価することができる。
また、実施例1(57℃)及び実施例4(61℃)は、撹拌時間20分までに数値が最小となるものの、その増加率は2%未満と小さく、実用上は問題ないものと思われる。
一方、比較例1(56℃)及び比較例2(62℃)は、撹拌時間20分までに数値が最小となり、その増加率が2%以上であり、陰性対照と挙動を同じくした。この結果は、泡の高さの場合と同様、撹拌時間が長くなるにつれて、気泡を構成する膜が損傷されやすくなることを推認させる。
Figure 2005304359
As shown in Table 3 above, in Example 2 (58 ° C.) and Example 3 (60 ° C.), the foaming property is improved as the stirring time becomes longer, which is almost the same as the positive control that can be regarded as a raw egg. It became the behavior of. That is, in the foam density, Examples 2 and 3 can be evaluated as almost the same as a raw egg.
In Example 1 (57 ° C.) and Example 4 (61 ° C.), although the numerical value is minimized by 20 minutes of stirring time, the increase rate is as small as less than 2%, and it seems that there is no problem in practical use. It is.
On the other hand, in Comparative Example 1 (56 ° C.) and Comparative Example 2 (62 ° C.), the numerical value reached the minimum by 20 minutes and the increase rate was 2% or more, and the behavior was the same as that of the negative control. This result suggests that the film constituting the bubbles is likely to be damaged as the stirring time becomes longer as in the case of the height of the bubbles.

(3−2−3)起泡性試験のまとめ
以上、泡の高さ及び泡密度の試験結果の評価は、完全に一致していた。したがって、起泡性の観点からは、殺菌温度は57℃以上61℃以下が好適であり、とりわけ、58℃以上60℃以下が望ましいことが判明した。
(3−3)起泡安定性試験
起泡安定性試験により、泡立てた加熱殺菌液全卵の経時的安定性に対する殺菌温度の影響を評価した。
各サンプル300gを25℃に加温した後に270gの上白糖を添加し、これをボールに入れ、縦型ホイップミキサーにて10分間撹拌した。このホイップ液全卵を容量280mlの容器に入れ5時間室温放置し、再び液化した部分の容積を測定した。
(3-2-3) Summary of foamability test As described above, the evaluation of the test results of the foam height and the foam density was completely consistent. Therefore, from the viewpoint of foamability, it has been found that the sterilization temperature is preferably 57 ° C. or more and 61 ° C. or less, and particularly preferably 58 ° C. or more and 60 ° C. or less.
(3-3) Foaming stability test By the foaming stability test, the influence of the sterilization temperature on the temporal stability of the foamed heat-sterilized liquid whole egg was evaluated.
After heating 300 g of each sample to 25 ° C., 270 g of white sucrose was added, and this was placed in a bowl and stirred for 10 minutes with a vertical whip mixer. This whole whipped solution egg was placed in a container having a capacity of 280 ml and allowed to stand at room temperature for 5 hours, and the volume of the liquefied portion was measured again.

起泡安定性については、その数値が小さいほどホイップした状態がより長時間にわたって保持されると評価できる。具体的な評価としては、再び液化した部分が35ml未満であった場合は「優」とし、35ml以上40ml未満であった場合は「良」とし、及び40ml以上であった場合は「不可」とした。その結果を、下記の表4に示す。   About foaming stability, it can be evaluated that the whipped state is hold | maintained over a long time, so that the numerical value is small. As a specific evaluation, when the liquefied portion was less than 35 ml, it was “excellent”, when it was 35 ml or more but less than 40 ml, “good”, and when it was 40 ml or more, “impossible”. did. The results are shown in Table 4 below.

Figure 2005304359
上記表4に示すとおり、実施例1(57℃)、実施例2(58℃)及び実施例3(60℃)は良好な結果であり、また、実施例4(61℃)及び比較例2(62℃)も比較的良好であった。一方、比較例1(56℃)は再び液化した部分が多く、悪い評価となった。
この起泡安定性試験により、殺菌温度が57℃以上であれば気泡安定性は良好であることが判明した。とりわけ、57℃以上60℃以下が望ましいことが判明した。
(3−4)乳化安定性試験
乳化安定性試験により、加熱殺菌液全卵の乳化力に対する殺菌温度の影響を評価した。
Figure 2005304359
As shown in Table 4 above, Example 1 (57 ° C.), Example 2 (58 ° C.) and Example 3 (60 ° C.) are good results, and Example 4 (61 ° C.) and Comparative Example 2 (62 ° C.) was also relatively good. On the other hand, Comparative Example 1 (56 ° C.) had many portions that were liquefied again, which was a bad evaluation.
The foam stability test revealed that the bubble stability was good when the sterilization temperature was 57 ° C. or higher. In particular, it has been found that 57 ° C. or higher and 60 ° C. or lower is desirable.
(3-4) Emulsification stability test The effect of the sterilization temperature on the emulsification power of the whole heat-sterilized liquid egg was evaluated by an emulsion stability test.

サンプル63.4g、水28.2g、醸造酢(酸度5%)16.0g、精製塩2.4g及び大豆サラダ油80.0gの混合物を、ホモミキサー(特殊機化工業)を用いて5,000rpmで7分間乳化させた。この乳化物を容量110mlの容器に入れ5時間室温放置し、分離した液体の容積を測定した。
乳化安定性については、その数値が小さいほど乳化力がより長時間にわたって保持されると評価できる。具体的な評価としては、再び液化した部分が5.5ml未満であった場合は「優」とし、5.5ml以上7.5ml未満であった場合は「良」とし、及び7.5ml以上であった場合は「不可」とした。その結果を、下記の表5に示す。
A mixture of 63.4 g of sample, 28.2 g of water, 16.0 g of brewed vinegar (acidity 5%), 2.4 g of purified salt and 80.0 g of soybean salad oil was mixed at 5,000 rpm using a homomixer (Special Machine Industries). And emulsified for 7 minutes. This emulsion was placed in a 110 ml capacity container and allowed to stand at room temperature for 5 hours, and the volume of the separated liquid was measured.
About emulsification stability, it can be evaluated that the emulsification power is maintained over a longer time as the numerical value is smaller. As a specific evaluation, when the liquefied portion was less than 5.5 ml, it was “excellent”, and when it was 5.5 ml or more and less than 7.5 ml, “good”, and 7.5 ml or more. When there was, it was set as “impossible”. The results are shown in Table 5 below.

Figure 2005304359
上記表5に示すとおり、実施例2(58℃)、実施例3(60℃)、実施例4(61℃)及び比較例2(62℃)は良好な結果であり、また、実施例1(57℃)は比較的良好であった。一方、比較例1(56℃)は分離した液体が多く、悪い評価となった。
この起泡安定性試験により、殺菌温度が57℃以上であれば気泡安定性は良好であることが判明した。とりわけ、58℃以上が望ましいことが判明した。
(3−5)調理性試験
調理性試験として、加熱殺菌液全卵をかき卵及びプリンに調理し、その物性を評価した。
Figure 2005304359
As shown in Table 5 above, Example 2 (58 ° C.), Example 3 (60 ° C.), Example 4 (61 ° C.) and Comparative Example 2 (62 ° C.) are good results. (57 ° C.) was relatively good. On the other hand, Comparative Example 1 (56 ° C.) had a lot of separated liquids, which was a bad evaluation.
The foam stability test revealed that the bubble stability was good when the sterilization temperature was 57 ° C. or higher. In particular, it has been found that 58 ° C. or higher is desirable.
(3-5) Cooking property test As a cooking property test, the whole heat-sterilized liquid egg was cooked into a cooked egg and pudding, and its physical properties were evaluated.

かき卵の調理においては、水400mlを沸騰させ、その中に各サンプル100gを回し入れ、直後に火を止めた。これを5メッシュのふるいにあけ、ふるい上に残った残差の重量(g)を測定した。すなわち、この残査重量が多いほど、かき卵として良好であったと評価できる。具体的な評価は、残査重量が110g以上であれば「優」、90g以上110g未満であれば「良」、及び90g未満であれば「不可」とした。
一方、プリンの調理においては、サンプル78.0g、砂糖32.4g及び牛乳189.6gを均一に混合したものを45g、プリン型に充填し、これをスチームオーブン中で83℃、25分間加熱して、高さ3cmのプリンを得た。このプリンの破断強度(N)を、クリープメーター(ヤマト科学)を用いて測定した。すなわち、この破断強度が高いほど、プリンとしての食感に優れるものと評価できる。具体的な評価は、破断強度が0.16N以上であれば「優」、0.13N以上0.16N未満であれば「良」、及び0.13N未満であれば「不可」とした。
In cooking the shaved egg, 400 ml of water was boiled, and 100 g of each sample was put in it, and the fire was turned off immediately. This was opened in a 5-mesh sieve, and the residual weight (g) remaining on the sieve was measured. In other words, it can be evaluated that the larger the residual weight, the better as a shaved egg. The specific evaluation was “excellent” if the residual weight was 110 g or more, “good” if it was 90 g or more and less than 110 g, and “impossible” if it was less than 90 g.
On the other hand, in the cooking of pudding, 45 g of a uniform mixture of 78.0 g of sample, 32.4 g of sugar and 189.6 g of milk was filled into a pudding mold and heated in a steam oven at 83 ° C. for 25 minutes. Thus, a 3 cm high pudding was obtained. The breaking strength (N) of this pudding was measured using a creep meter (Yamato Scientific). That is, it can be evaluated that the higher the breaking strength, the better the texture as a pudding. The specific evaluation was “excellent” when the breaking strength was 0.16 N or higher, “good” when 0.13 N or higher and lower than 0.16 N, and “impossible” when lower than 0.13 N.

上記の調理性試験の結果を、下記の表6に示す。なお、かき卵調理における評価と、プリン調理における評価は一致した。   The results of the above cooking test are shown in Table 6 below. In addition, the evaluation in the cooked egg cooking coincided with the evaluation in the pudding cooking.

Figure 2005304359
上記表6に示すとおり、実施例1(57℃)、実施例2(58℃)及び実施例3(60℃)は良好な結果であり、また、比較例1(56℃)及び実施例4(62℃)は比較的良好であった。一方、比較例2は陰性対照と同様の結果であり悪い評価となった。
この調理性試験により、かき卵及びプリンの調理には殺菌温度が61℃以下であれば好適であることが判明した。とりわけ、57℃以上60℃以下が望ましいことが判明した。
(4)まとめ
まず、前記(2)の殺菌試験の結果からは、殺菌温度が56℃以上62℃であれば十分な殺菌効果が得られることが判明した。
Figure 2005304359
As shown in Table 6 above, Example 1 (57 ° C.), Example 2 (58 ° C.) and Example 3 (60 ° C.) are good results, and Comparative Example 1 (56 ° C.) and Example 4 (62 ° C.) was relatively good. On the other hand, Comparative Example 2 had the same result as the negative control and was evaluated as bad.
From this cooking test, it has been found that cooking of cooked eggs and pudding is suitable if the sterilization temperature is 61 ° C. or lower. In particular, it has been found that 57 ° C. or higher and 60 ° C. or lower is desirable.
(4) Summary First, from the results of the sterilization test of (2), it was found that if the sterilization temperature is 56 ° C. or higher and 62 ° C., a sufficient sterilization effect can be obtained.

また、上記各物性試験の結果に対する評価を下記表7に掲げる。   Moreover, evaluation with respect to the result of each said physical property test is hung up in the following Table 7.

Figure 2005304359
すなわち、比較例1の評価より、殺菌温度56℃で処理した加熱殺菌液全卵は、起泡性、起泡安定性及び乳化安定性に難があることが判明した。また、比較例2の殺菌温度62℃で処理した加熱殺菌液全卵は、起泡性及び調理性に難があることが判明した。
一方、実施例1から4までの評価より、殺菌温度57℃以上61℃以下で処理した加熱殺菌液全卵であれば、いずれの試験においてもおおむね良好な結果が得られている。特に、実施例2及び実施例3の評価からは、殺菌温度58℃以上60℃以下で処理した加熱殺菌液全卵は、いずれの試験においても優れた結果が得られている。
Figure 2005304359
That is, from the evaluation of Comparative Example 1, it was found that the whole heat-sterilized egg processed at a sterilization temperature of 56 ° C. has difficulty in foaming property, foaming stability and emulsion stability. Moreover, it turned out that the heat sterilization liquid whole egg processed at the sterilization temperature of 62 degreeC of the comparative example 2 has difficulty in foamability and cooking property.
On the other hand, from the evaluations of Examples 1 to 4, generally good results were obtained in any test as long as the heat sterilized whole eggs were processed at a sterilization temperature of 57 ° C. or more and 61 ° C. or less. In particular, from the evaluation of Example 2 and Example 3, the heat sterilization liquid whole eggs treated at a sterilization temperature of 58 ° C. or more and 60 ° C. or less have excellent results in any test.

以上より、液全卵を包装した後に加熱殺菌する場合の殺菌温度については、57℃以上61℃以下であれば、十分な殺菌性を発揮しつつ、生卵に近い物性を保持することが可能であるといえる。
さらに、生卵に近い物性が保持されるという観点から、58℃以上60℃以下の殺菌温度はより優れている、といえる。
From the above, the pasteurization temperature when packaging and sterilization after packaging the whole liquid egg, if it is 57 ° C or more and 61 ° C or less, can maintain physical properties close to raw eggs while exhibiting sufficient sterilization properties. You can say that.
Furthermore, it can be said that the sterilization temperature of 58 ° C. or more and 60 ° C. or less is more excellent from the viewpoint that physical properties close to that of raw eggs are maintained.

Claims (4)

濃厚卵白を含む液全卵を密封包装し、その包装ごと殺菌温度57℃以上かつ61℃以下の温水浸漬、温水スプレー又は蒸気噴霧にて殺菌処理をしたことを特徴とする加熱殺菌液全卵。   A heat-sterilized liquid whole egg, wherein the whole egg containing liquid egg white is hermetically packaged and sterilized by warm water immersion, warm water spray or steam spraying at a sterilization temperature of 57 ° C. or more and 61 ° C. or less. 前記殺菌温度を、58℃以上かつ60℃以下としたことを特徴とする請求項1記載の加熱殺菌液全卵。   The heat sterilization liquid whole egg according to claim 1, wherein the sterilization temperature is 58 ° C or higher and 60 ° C or lower. 濃厚卵白を含む液全卵を密封包装する工程と、
前記袋詰めした液全卵をその包装ごと殺菌温度57℃以上かつ61℃以下の温水浸漬、温水スプレー又は蒸気噴霧にて殺菌処理する殺菌工程とを含んでなることを特徴とする加熱殺菌液全卵の製造方法。
Sealing and packaging the whole liquid egg containing rich egg white;
A whole pasteurized liquid egg comprising a sterilization step of sterilizing the whole egg in its package by warm water immersion at a sterilization temperature of 57 ° C. or more and 61 ° C. or less, hot water spray or steam spraying. Egg manufacturing method.
前記殺菌温度を、58℃以上かつ60℃以下としたことを特徴とする請求項3記載の加熱殺菌液全卵の製造方法。   The method for producing a heat-sterilized liquid whole egg according to claim 3, wherein the sterilization temperature is 58 ° C or higher and 60 ° C or lower.
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007222099A (en) * 2006-02-24 2007-09-06 Ise Delica Kk Method for producing pasteurized liquid whole egg, and food using liquid whole egg food
JP2013074840A (en) * 2011-09-30 2013-04-25 Q P Corp Bottled sterilized whole egg liquid and production method thereof
JP2015023827A (en) * 2013-07-26 2015-02-05 キユーピー株式会社 Method for preventing the turbidity of egg soup, sterilization working liquid whole egg for egg soup, egg soup using the sterilization working liquid whole egg, and method for producing the egg soup

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007222099A (en) * 2006-02-24 2007-09-06 Ise Delica Kk Method for producing pasteurized liquid whole egg, and food using liquid whole egg food
JP4630834B2 (en) * 2006-02-24 2011-02-09 イセデリカ株式会社 Sterilization liquid whole egg manufacturing method and liquid whole egg food
JP2013074840A (en) * 2011-09-30 2013-04-25 Q P Corp Bottled sterilized whole egg liquid and production method thereof
JP2015023827A (en) * 2013-07-26 2015-02-05 キユーピー株式会社 Method for preventing the turbidity of egg soup, sterilization working liquid whole egg for egg soup, egg soup using the sterilization working liquid whole egg, and method for producing the egg soup

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