JP2005219084A - Method for manufacturing hot-extruded seamless steel tube having excellent inner surface quality - Google Patents

Method for manufacturing hot-extruded seamless steel tube having excellent inner surface quality Download PDF

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JP2005219084A
JP2005219084A JP2004028924A JP2004028924A JP2005219084A JP 2005219084 A JP2005219084 A JP 2005219084A JP 2004028924 A JP2004028924 A JP 2004028924A JP 2004028924 A JP2004028924 A JP 2004028924A JP 2005219084 A JP2005219084 A JP 2005219084A
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hot
die
seamless steel
steel tube
steel pipe
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Atsushi Sho
篤史 庄
Toshiyuki Hamano
利幸 浜野
Morihito Takatani
守人 高谷
Kimisuke Nishikawa
公介 西川
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Sanyo Special Steel Co Ltd
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Abstract

<P>PROBLEM TO BE SOLVED: To provide a method for manufacturing a hot-extruded seamless steel tube having excellent inner surface quality. <P>SOLUTION: In the method for manufacturing the hot-extruded seamless stainless steel tube having excellent inner surface quality, hot-extrusion is performed by setting the angle θ of inclination of a die to be 10-50° from the perpendicular in the extruding rear end direction. In the method for manufacturing the hot-extruded seamless steel tube having excellent inner surface quality, the angle θ of inclination is set to 20-50°. Unevenness of an inner surface of the steel tube is eliminated, and the quality can be improved. <P>COPYRIGHT: (C)2005,JPO&NCIPI

Description

本発明は、ステンレス鋼の熱間押出継目無鋼管の製造方法に関するものである。   The present invention relates to a method for producing a stainless steel hot-extruded seamless steel pipe.

主に配管用継目無ステンレス鋼管の内面は多くの場合腐食性流体が通るために内面性状の良いものが特に要求される。多くの場合、このような鋼管はマンドレルバーを用いるユージン・セジュルネ方式の押出装置によって製造されている。その場合に、一般に良好な内表面性状を得るためには、例えば特開2002−338984号公報(特許文献1)に開示されているように、熱間加工において使用する潤滑剤組成物であって、硼酸ナトリウムの5水塩を40〜90質量%、炭酸ナトリウムを6〜30質量%、脂肪酸のNa又はCa塩の1種以上を5〜30質量%混合してなる熱間粉体潤滑剤組成物が提案されている。   The inner surface of a seamless stainless steel pipe mainly for piping is particularly required to have a good inner surface property because corrosive fluid passes in many cases. In many cases, such a steel pipe is manufactured by an Eugene Sejurune type extrusion apparatus using a mandrel bar. In that case, in order to obtain a generally good inner surface property, for example, as disclosed in JP-A-2002-338984 (Patent Document 1), it is a lubricant composition used in hot working. A hot powder lubricant composition comprising 40-90% by mass of sodium borate pentahydrate, 6-30% by mass of sodium carbonate, and 5-30% by mass of one or more of Na or Ca salt of fatty acid. Things have been proposed.

また、特開平8−164405号公報(特許文献2)に開示されているように、圧延される際に継目無鋼管と接触する部分の外径が、先端側から後端側に向かって漸増している熱間継目無管圧延用マンドレルバーを用いるものや、特開平8−71618号公報(特許文献3)に開示されているように、表面に、軸方向の中心線平均粗さ(Ra)が1.0〜4.0μmであるCrメッキ被膜を有する熱間継目無管圧延用マンドレルバーを用いるものが提案されている。さらに、特開平9−192724号公報(特許文献4)に開示されているように、押出し素材として表面粗さがRmaxで30〜100μmの中空ビレットを用いた継目無鋼管の熱間押出し製管方法がそれぞれ提案されている。   Further, as disclosed in Japanese Patent Application Laid-Open No. 8-164405 (Patent Document 2), the outer diameter of the portion that contacts the seamless steel pipe when rolled is gradually increased from the front end side toward the rear end side. As described in Japanese Patent Application Laid-Open No. 8-71618 (Patent Document 3), a surface using an axial centerline average roughness (Ra) is used. Has been proposed that uses a mandrel bar for hot seamless pipe rolling having a Cr plating film having a thickness of 1.0 to 4.0 μm. Furthermore, as disclosed in Japanese Patent Application Laid-Open No. 9-192724 (Patent Document 4), a method of hot extruding a seamless steel pipe using a hollow billet having a surface roughness Rmax of 30 to 100 μm as an extrusion material. Each has been proposed.

特開2002−338984号公報JP 2002-338984 A 特開平8−164405号公報JP-A-8-164405 特開平8−71618号公報JP-A-8-71618 特開平9−192724号公報Japanese Patent Laid-Open No. 9-192724

上述した特許文献1の場合のように、ビレット−マンドレル間の潤滑剤を変えたり、特許文献2のように、マンドレルバーの形状、特許文献3のように、マンドレルバーの表面粗さを変えたり、特許文献4のように、押出に用いる中空ビレット内表面の表面粗さを研磨によってRmaxを30〜100μmとする等の提案がされているが、全て内面の潤滑や粗度という観点だけで検討され、内面凹凸の発生機構からの対策を検討したものではなかった。   As in the case of Patent Document 1 described above, the lubricant between the billet and the mandrel is changed, the shape of the mandrel bar is changed as in Patent Document 2, and the surface roughness of the mandrel bar is changed as in Patent Document 3. As proposed in Patent Document 4, the surface roughness of the inner surface of the hollow billet used for extrusion has been proposed to be Rmax of 30 to 100 μm by polishing. However, all studies were made only from the viewpoint of lubrication and roughness of the inner surface. However, the countermeasures from the generation mechanism of the inner surface unevenness were not examined.

一般的にユージン・セジュルネ方式の押出では、押出比が15を超えるようになると、ビレットの表面粗さを小さくしても、チューブの内表面にビレットの凹凸以上の凹凸が発生する。この凹凸が大きい場合、外観を損ねることは勿論のこと、腐食性流体の配管として使用した際に局部腐食の起点となり、チューブが早期寿命を迎える場合がある。また、ビレット−マンドレル間の潤滑剤やマンドレルバーの形状等の変更は、内面の焼付きには効果があるが、凹凸の発生には効果が見られない。このように、内表面の凹凸発生に対してダイスからの検討がされていなかった。   In general, when the extrusion ratio exceeds 15 in the Eugene Sejurune extrusion, irregularities more than the irregularities of the billet are generated on the inner surface of the tube even if the surface roughness of the billet is reduced. When this unevenness is large, not only the appearance is impaired, but also when used as a piping for corrosive fluid, it becomes a starting point for local corrosion, and the tube may reach an early life. Moreover, the change of the lubricant between the billet and the mandrel, the shape of the mandrel bar and the like are effective for seizing the inner surface, but are not effective for the generation of unevenness. As described above, the dice have not been studied for the occurrence of irregularities on the inner surface.

上述のような問題を解消するために、発明者らは鋭意検討を重ねた結果、先ず、この凹凸は、ビレットにかかるコンテナ−マンドレル間の鉛直方向の応力が影響し、大きくなるほど凹凸の大きさも大きくなることが分かった。次に、この凹凸は、コンテナ−マンドレル間の応力による変形で生じた、ビレット内表面の微小な凹凸部が起点となるもので、ダイスに近づくに従い、凸部から凹部へ溶融ガラスが流入することで増長される機構で生じるものであることが分かった。   In order to solve the above-mentioned problems, the inventors have intensively studied, and as a result, the unevenness is affected by the vertical stress between the container and the mandrel applied to the billet. It turns out that it grows. Next, these irregularities start from the minute irregularities on the inner surface of the billet that are generated by deformation due to the stress between the container and the mandrel. As the die approaches, the molten glass flows from the convex part to the concave part. It was found to be caused by a mechanism that is increased by

また、コンテナーマンドレル間の応力の低減には、プレッシングディスクーダイス間の応力を低減させることが有効で、手段として鋼管の内面が良好となる基準(表面粗さRy≦13)以下とするには、パッドガラスが当たるダイスの接触面を押出し後方側に10〜50度傾斜させることが有効であることが分かった。さらに、ダイス角を20度以上とすると非常に良好なRy≦10μmを達成できることが分かった。ただ、傾斜角が50度を超えるようになると、外面のガラス膜が厚くなり、外径精度が悪くなったり、パットガラスの原単位が上昇しコスト高になることが分かった。これらの知見の基づいて、本発明は完成されたものである。   In order to reduce the stress between the container mandrels, it is effective to reduce the stress between the pressing disc and the die, and as a means to make the inner surface of the steel pipe good, the standard (surface roughness Ry ≦ 13) or less. It was found that it is effective to extrude the contact surface of the die against which the pad glass hits and incline 10 to 50 degrees toward the rear side. Furthermore, it was found that when the dice angle is 20 degrees or more, very good Ry ≦ 10 μm can be achieved. However, it has been found that when the inclination angle exceeds 50 degrees, the glass film on the outer surface becomes thick, the outer diameter accuracy deteriorates, the basic unit of the pad glass increases, and the cost increases. Based on these findings, the present invention has been completed.

その発明の要旨とするところは、
(1)ステンレス鋼の熱間押出継目無鋼管の製造方法において、鉛直線上から押出後端方向にダイス傾斜角θを10〜50度傾斜させて熱間押出することを特徴とする内面品質が良好な熱間押出継目無鋼管の製造方法。
(2)前記(1)に記載の傾斜角度θを20〜50度としたことを特徴とする内面品質が良好な熱間押出継目無鋼管の製造方法にある。
The gist of the invention is that
(1) In the method of manufacturing a stainless steel hot-extruded seamless steel pipe, the inner surface quality is good, characterized in that the die inclination angle θ is inclined 10 to 50 degrees from the vertical line toward the rear end of the extrusion, and hot extrusion is performed. Method for producing a seamless hot-extruded seamless steel pipe.
(2) The method for producing a hot extruded seamless steel pipe having good inner surface quality, characterized in that the inclination angle θ described in (1) is 20 to 50 degrees.

以上述べたように、本発明による鉛直線上から押出後端方向にダイス傾斜角θを10〜50度傾斜させて熱間押出することにより、鋼管の内表面の凹凸がなくなり品質の向上を図ることが出来る極めて優れた効果を奏するものである。   As described above, the unevenness of the inner surface of the steel pipe is eliminated and the quality is improved by hot extruding by tilting the die inclination angle θ by 10 to 50 degrees in the direction of the rear end of extrusion from the vertical line according to the present invention. It has an extremely excellent effect.

以下、本発明について図面に従って詳細に説明する。
図1は、本発明に係る継目無鋼管の熱間押出装置の全体概念図である。この図1(a)に示すように、所定温度に加熱されたビレット1は、プレッシングディスク2を介してステム3によりコンテナ4内に装入される。その時、マンドレル5も図のような状態にあり、ステム3と同時に前進する。この時、ステム3後部のシリンダー(図示せず)は低圧の状態にある。その後、ビレット1の先端がダイホルダー6に接触し、ビレット1が低圧で加圧される。その後、シリンダーは高圧に掛りビレット1はダイホルダー6内ダイス7の内径寸法に押出されるような構成からなる。符号8はライナーであり、9はチューブであり、10はパッキングリングであり、11はパッドガラスである。
Hereinafter, the present invention will be described in detail with reference to the drawings.
FIG. 1 is an overall conceptual diagram of a seamless steel pipe hot extrusion apparatus according to the present invention. As shown in FIG. 1A, the billet 1 heated to a predetermined temperature is loaded into the container 4 by the stem 3 via the pressing disk 2. At that time, the mandrel 5 is also in the state shown in the figure, and advances simultaneously with the stem 3. At this time, the cylinder (not shown) at the rear of the stem 3 is in a low pressure state. Thereafter, the tip of the billet 1 comes into contact with the die holder 6 and the billet 1 is pressurized at a low pressure. Thereafter, the cylinder is subjected to high pressure, and the billet 1 is pushed to the inner diameter of the die 7 in the die holder 6. Reference numeral 8 is a liner, 9 is a tube, 10 is a packing ring, and 11 is a pad glass.

図1(b)はパッドガラス部の拡大図であり、この図1(b)に示すように、上述した図1(a)の押出機構での熱間押出でのガラス潤滑剤は、押出直前のパッドガラス11をセットした状態から、ビレット1と接する面のガラスが押出中に溶けてガラスがパイプ9の表面に付着しダイス7との間の潤滑をする。この場合において、上述したように、コンテナ4−マンドレル5間の応力の低減にはプレッシングディスク2−ダイス7間の応力を低減させることが有効で、手段としてパイプ9の内面が良好となる基準(表面粗さRy≦13)以下とするには、パッドガラスが当たるダイス7の接触面を押出し後方側にダイス傾斜角θを10〜50度傾斜させることが有効である。さらに、ダイス傾斜角θを20度以上とすると非常に良好な表面粗さRy≦10μmが達成できる。   FIG. 1B is an enlarged view of the pad glass portion. As shown in FIG. 1B, the glass lubricant in the hot extrusion in the above-described extrusion mechanism of FIG. From the state in which the pad glass 11 is set, the glass on the surface in contact with the billet 1 melts during extrusion, and the glass adheres to the surface of the pipe 9 and lubricates between the dies 7. In this case, as described above, it is effective to reduce the stress between the pressing disk 2 and the die 7 in order to reduce the stress between the container 4 and the mandrel 5. In order to make the surface roughness Ry ≦ 13) or less, it is effective to extrude the contact surface of the die 7 against which the pad glass hits and incline the die inclination angle θ 10 to 50 degrees toward the rear side. Furthermore, when the die inclination angle θ is 20 degrees or more, a very good surface roughness Ry ≦ 10 μm can be achieved.

図2は、ステンレス鋼管内面の凹凸発生状態を示す図である。図2(a)はステンレス鋼管が押出される前の状態を示し、図2(b)は押出後のビレット−チューブ成形遷移域の状態を示している。鋼管内表面の凹凸は、ビレットにかかるコンテナーマンドレル間の鉛直線方向の応力が影響し、大きくなるほど凹凸の大きさも大きくなる。この凹凸はコンテナ−マンドレル間の応力による変形で生じた、ビレット内表面の微小な凹凸部が起点となるものであって、ダイスに近づくに従い、凸部から凹部への溶融ガラスの流入することで増長される機構で生じるものであることがこの図で分かる。   FIG. 2 is a view showing the state of occurrence of irregularities on the inner surface of the stainless steel pipe. FIG. 2A shows a state before the stainless steel pipe is extruded, and FIG. 2B shows a state of the billet-tube forming transition area after the extrusion. The unevenness on the inner surface of the steel pipe is affected by the stress in the vertical direction between the container mandrels applied to the billet, and the larger the unevenness, the larger the size of the unevenness. This unevenness is caused by the deformation of the billet inner surface caused by deformation due to stress between the container and the mandrel, and as the die approaches, the molten glass flows from the protrusion to the recess. It can be seen in this figure that this occurs with the mechanism being increased.

図3は、ダイス角度θとRyとの関係を示す図である。この図に示すように、ダイス角度θを10度以上とするRy値の低下することが分かる。特にRy≦10μmとするには、パットガラスが当たるダイスの接触面を押出し後方に20度傾斜にする必要がある。すなわち、本発明に係るダイス傾斜角θを10〜50度傾斜させて熱間押出する理由は、10度未満では、内面肌が良好となる効果が十分でなく、また、50度を超えると外面のガラス膜が厚くなって外径精度が悪くなり、ガラスの消費量が多くなりコストアップとなる。従って、その範囲を10〜50度とした。好ましくは20〜50度とする。   FIG. 3 is a diagram showing the relationship between the die angle θ and Ry. As shown in this figure, it can be seen that the Ry value when the die angle θ is 10 degrees or more is lowered. In particular, in order to satisfy Ry ≦ 10 μm, it is necessary to extrude the contact surface of the die hit by the pad glass and incline 20 degrees backward. That is, the reason why the die inclination angle θ according to the present invention is hot-extruded by inclining by 10 to 50 degrees is that the effect of improving the inner skin is not sufficient if it is less than 10 degrees, and the outer surface is more than 50 degrees. As the glass film becomes thicker, the accuracy of the outer diameter deteriorates, and the amount of glass consumed increases and the cost increases. Therefore, the range was set to 10 to 50 degrees. Preferably, the angle is 20 to 50 degrees.

以下、本発明について実施例によって具体的に説明する。
SUS304なる鋼種を用いて、押出温度1210〜1240℃、ビレット内面Ry:7.5μmなるものを、表1に示すようなビレット径、チューブ径、押出比、およびダイス角度にて行なった。その結果を表1に示す。
Hereinafter, the present invention will be specifically described with reference to examples.
Using a steel type of SUS304, an extrusion temperature of 1210 to 1240 ° C. and a billet inner surface Ry of 7.5 μm were performed at the billet diameter, tube diameter, extrusion ratio, and die angle as shown in Table 1. The results are shown in Table 1.

Figure 2005219084
Figure 2005219084

表1に示すように、No.1〜2、4〜6、9〜11は本発明例であり、No.3、7〜8、12〜13は比較例である。比較例No.3はダイス角度が小さいためにチューブ内面Ryが高い。比較例No.7はダイス角度が大きいために外径精度が悪い。比較例No.8はダイス角度が小さいためにチューブ内面Ryが高い。比較例No.12はダイス角度が大きいために外径精度が悪い。比較例No.8はダイス角度が0のためにチューブ内面Ryが高いことが分かる。これに対し、本発明例であるNo.1〜2、4〜6、9〜11はいずれもチューブ内面Ryが低く、鋼管の内表面の凹凸がなくなり外径精度の優れた鋼管を得ることが可能となり、品質の向上を図ることが出来た。   As shown in Table 1, no. 1-2, 4-6, 9-11 are examples of the present invention. 3, 7-8, 12-13 are comparative examples. Comparative Example No. No. 3 has a high tube inner surface Ry because the die angle is small. Comparative Example No. 7 has a poor outer diameter accuracy due to a large die angle. Comparative Example No. Since No. 8 has a small die angle, the tube inner surface Ry is high. Comparative Example No. No. 12 has a poor outer diameter accuracy due to a large die angle. Comparative Example No. It can be seen that No. 8 has a high tube inner surface Ry because the die angle is zero. On the other hand, No. which is an example of the present invention. 1 to 2, 4 to 6, and 9 to 11 all have a low tube inner surface Ry, it is possible to obtain a steel pipe with excellent outer diameter accuracy by eliminating irregularities on the inner surface of the steel pipe, and improving quality. It was.

本発明に係る継目無鋼管の熱間押出装置の全体概念図である。1 is an overall conceptual diagram of a seamless steel pipe hot extrusion apparatus according to the present invention. ステンレス鋼管内面の凹凸発生状態を示す図である。It is a figure which shows the unevenness | corrugation generation | occurrence | production state of a stainless steel pipe inner surface. ダイス角度θと製品チューブ内面のRyとの関係を示す図である。It is a figure which shows the relationship between die angle (theta) and Ry of a product tube inner surface.

符号の説明Explanation of symbols

1 ビレット
2 プレッシングディスク
3 ステム
4 コンテナ
5 マンドレル
6 ダイホルダー
7 ダイス
8 ライナー
9 チューブ
10 パッキングリング
11 パッドガラス
θ ダイス傾斜角


特許出願人 山陽特殊製鋼株式会社
代理人 弁理士 椎 名 彊


1 Billet 2 Pressing Disc 3 Stem 4 Container 5 Mandrel 6 Die Holder 7 Die 8 Liner 9 Tube 10 Packing Ring 11 Pad Glass θ Dice Tilt Angle


Patent Applicant Sanyo Special Steel Co., Ltd.
Attorney: Attorney Shiina


Claims (2)

ステンレス鋼の熱間押出継目無鋼管の製造方法において、鉛直線上から押出後端方向にダイス傾斜角θを10〜50度傾斜させて熱間押出することを特徴とする内面品質が良好な熱間押出継目無鋼管の製造方法。 In a method for producing a hot-extruded seamless steel pipe made of stainless steel, hot extrusion with good inner surface quality is characterized in that the die inclination angle θ is inclined by 10 to 50 degrees from the vertical line toward the rear end of the extrusion, and hot extrusion is performed. Manufacturing method of extruded seamless steel pipe. 請求項1に記載の傾斜角度θを20〜50度としたことを特徴とする内面品質が良好な熱間押出継目無鋼管の製造方法。 A method for producing a hot-extruded seamless steel pipe with good inner surface quality, wherein the inclination angle θ according to claim 1 is 20 to 50 degrees.
JP2004028924A 2004-02-05 2004-02-05 Method for manufacturing hot-extruded seamless steel tube having excellent inner surface quality Withdrawn JP2005219084A (en)

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CN101758102A (en) * 2010-03-15 2010-06-30 北京机电研究所 Mold for extruding and forming thick-walled seamless steel pipes
CN101920277A (en) * 2010-08-11 2010-12-22 上海交通大学 Extrusion mould for magnesium alloy seamless pipe
WO2013187716A1 (en) * 2012-06-13 2013-12-19 한국생산기술연구원 Extrusion die using shock-absorbing pad and method for manufacturing extrusion
CN104117546A (en) * 2013-04-28 2014-10-29 广东兴发铝业有限公司 Metal seamless tube production equipment and seamless tube production method
US10916967B2 (en) 2014-10-23 2021-02-09 Vikram Kumar Audit method and system and supply method and system for PV power injection and consumption in a power grid system
CN113182373A (en) * 2021-05-18 2021-07-30 山西太钢不锈钢股份有限公司 Extrusion method of nickel-based alloy seamless steel pipe

Cited By (8)

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JP2008207191A (en) * 2007-02-23 2008-09-11 Sumitomo Metal Ind Ltd Die for hot extrusion, and method for manufacturing hot extruded material
JP4677998B2 (en) * 2007-02-23 2011-04-27 住友金属工業株式会社 DIE FOR HOT EXTRUSION PROCESS AND METHOD FOR PRODUCING HOT EXTRUSION MATERIAL
CN101758102A (en) * 2010-03-15 2010-06-30 北京机电研究所 Mold for extruding and forming thick-walled seamless steel pipes
CN101920277A (en) * 2010-08-11 2010-12-22 上海交通大学 Extrusion mould for magnesium alloy seamless pipe
WO2013187716A1 (en) * 2012-06-13 2013-12-19 한국생산기술연구원 Extrusion die using shock-absorbing pad and method for manufacturing extrusion
CN104117546A (en) * 2013-04-28 2014-10-29 广东兴发铝业有限公司 Metal seamless tube production equipment and seamless tube production method
US10916967B2 (en) 2014-10-23 2021-02-09 Vikram Kumar Audit method and system and supply method and system for PV power injection and consumption in a power grid system
CN113182373A (en) * 2021-05-18 2021-07-30 山西太钢不锈钢股份有限公司 Extrusion method of nickel-based alloy seamless steel pipe

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