JP2003113011A - Method for controlling bacterial disease of rice seedling - Google Patents

Method for controlling bacterial disease of rice seedling

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Publication number
JP2003113011A
JP2003113011A JP2001276180A JP2001276180A JP2003113011A JP 2003113011 A JP2003113011 A JP 2003113011A JP 2001276180 A JP2001276180 A JP 2001276180A JP 2001276180 A JP2001276180 A JP 2001276180A JP 2003113011 A JP2003113011 A JP 2003113011A
Authority
JP
Japan
Prior art keywords
rice
ethyl
seedlings
chlorophenyl
bacterial
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP2001276180A
Other languages
Japanese (ja)
Inventor
Yukio Oguri
幸男 小栗
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sumitomo Chemical Co Ltd
Original Assignee
Sumitomo Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sumitomo Chemical Co Ltd filed Critical Sumitomo Chemical Co Ltd
Priority to JP2001276180A priority Critical patent/JP2003113011A/en
Publication of JP2003113011A publication Critical patent/JP2003113011A/en
Pending legal-status Critical Current

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Abstract

PROBLEM TO BE SOLVED: To provide a method for controlling bacterial diseases of rice seedlings (specifically, Acidovorax avenae, Burkholderia plantarii and Burkholderia glumae due to Pseudomonas glumae Kurita et Tabei of rice plants) that are important disease injuries in the period of raising seedlings in cultivation of paddy rice by which stable effects of a fungicide comprising a copper salt as an active ingredient are obtained even under frequently occurring conditions. SOLUTION: This method for controlling comprises treating rice seeds with the fungicide comprising the copper salt as an active ingredient and treating a nursery bed for raising the seedlings with (1RS,3SR)-2,2-dichloro-N-[1-(4- chlorophenyl-)ethyl]-1-ethyl-3-methylcyclopropanecarboxylamide (compound B).

Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【発明の属する技術分野】本発明は、水稲の苗栽培にお
ける重要病害であるイネ苗細菌病の防除方法に関する。
TECHNICAL FIELD The present invention relates to a method for controlling bacterial disease of rice seedling, which is an important disease in rice seedling cultivation.

【0002】[0002]

【従来の技術および発明が解決しようとする課題】水稲
の栽培において、育苗期に発生する苗細菌病を防除する
ことは非常に重要である。褐条病、もみ枯細菌病による
苗腐敗症、苗立枯細菌病等のイネ苗に対して、銅塩を有
効成分とする殺菌剤が広く利用されている。しかしなが
ら、銅塩を有効成分とする殺菌剤の効力は、イネ苗の栽
培環境によっては大きく変動し、場合によりその効果が
十分でないことが知られている(関東東山病害虫研究年
報第45集−1998 19〜21項)。一方、(1R
S,3SR)−2,2―ジクロロ−N−[1−(4−ク
ロロフェニル−)エチル]−1−エチル−3−メチルシ
クロプルパンカルボキサミドは、一般名カルプロパミド
(Carpropamid)として知られる殺菌性化合
物であるが、イネ苗育苗期のイネ苗細菌病については防
除効果は認められなかった。
2. Description of the Related Art In the cultivation of paddy rice, it is very important to control bacterial diseases of seedlings that occur during the seedling raising period. A fungicide containing copper salt as an active ingredient is widely used for rice seedlings such as brown streak, seedling rot caused by bacterial wilt disease, and bacterial wilt disease. However, the efficacy of a fungicide containing a copper salt as an active ingredient varies greatly depending on the cultivation environment of rice seedlings, and it is known that the effect is not sufficient in some cases (Kanto Higashiyama Disease and Pest Annual Report 45-1998). 19-21). On the other hand, (1R
S, 3SR) -2,2-Dichloro-N- [1- (4-chlorophenyl-) ethyl] -1-ethyl-3-methylcyclopulpancarboxamide is a bactericidal compound known by the generic name Carpropamide. However, no control effect was observed for bacterial disease of rice seedlings during the rice seedling raising period.

【0003】[0003]

【課題を解決するための手段】本発明者は、かかる状況
下、重要病害であるイネ苗細菌病を防除する方法につい
て鋭意検討した結果、銅塩を有効成分とする殺菌剤によ
りイネ種子(籾)を処理し、(1RS,3SR)−2,
2―ジクロロ−N−[1−(4−クロロフェニル−)エ
チル]−1−エチル−3−メチルシクロプルパンカルボ
キサミドにより育苗する苗床を処理することにより、イ
ネ苗細菌病を安定的に防除することが可能であることを
見出し、本発明に至った。
Means for Solving the Problems Under the circumstances, the present inventor diligently studied a method for controlling a bacterial disease of rice seedlings, which is an important disease. ) Is processed and (1RS, 3SR) -2,
Stable control of rice seedling bacterial disease by treating seedlings grown with 2-dichloro-N- [1- (4-chlorophenyl-) ethyl] -1-ethyl-3-methylcyclopulpancarboxamide It has been found that the above is possible, and the present invention has been completed.

【0004】[0004]

【発明の実施の形態】本発明において、イネ苗細菌病と
はイネ種子伝染性の細菌病害であり、イネの褐条病(Ac
idovorax avenae)、苗立枯細菌病(Burkholderia plan
tarii)、もみ枯細菌病菌による苗腐敗症(Burkholderi
a glumae)が挙げられる。本発明の方法は、苗立枯細菌
病またはもみ枯細菌病に対して効果が優れ、特に苗立枯
細菌病において効果が優れる。
BEST MODE FOR CARRYING OUT THE INVENTION In the present invention, the bacterial disease of rice seedlings is a bacterial disease of rice seed infectious disease, and the bacterial stripe disease (Ac
idovorax avenae), bacterial wilt disease (Burkholderia plan)
tarii), seedling rot (Burkholderi)
a glumae). INDUSTRIAL APPLICABILITY The method of the present invention is highly effective against bacterial wilt disease or bacterial wilt disease, and particularly effective in bacterial wilt disease.

【0005】本発明における銅塩を有効成分とする殺菌
剤(以下、本種子処理剤と記す)において、銅塩として
は水酸化第2銅、塩基性塩化銅が挙げられ、水酸化第2
銅が好ましい。本種子処理剤としては、市販されている
ようなイプコナゾール・銅水和剤やノニルフェノールス
ルホン酸銅などを用いることができるが、有効成分とし
て銅塩が含まれていればよく、他の殺菌性有効成分、担
体、製剤用補助剤等がその他の成分として含まれていて
もよい。本種子処理剤としては、乳剤、水和剤、粉剤、
粒剤等の種々の製剤形態を取り得るが、製剤中における
銅塩は重量%で通常0.1〜50%である。かかる製剤
化の際に用いられる担体としては、カオリンクレー、ア
ッタパルジャイトクレー、ベントナイト、モンモリロナ
イト、酸性白土、パイロフィライト、タルク、珪藻土、
方解石等の鉱物、トウモロコシ穂軸粉、クルミ殻粉等の
天然有機物、尿素等の合成有機物、炭酸カルシウム、硫
酸アンモニウム等の塩類、合成含水酸化珪素等の合成無
機物等からなる微粉末あるいは粒状物等の固体担体、キ
シレン、アルキルベンゼン、メチルナフタレン等の芳香
族炭化水素類、イソプロパノール、エチレングリコー
ル、プロピレングリコール、セロソルブ等のアルコ−ル
類、アセトン、シクロヘキサノン、イソホロン等のケト
ン類、ダイズ油、綿実油等の植物油、石油系脂肪族炭化
水素類、エステル類、ジメチルスルホキシド、アセトニ
トリル等の液体担体が挙げられる。本種子処理剤による
イネ種子(籾)の処理方法としては、粉剤である本種子
処理剤にてイネ種子を粉衣する方法;乳剤、水和剤また
は水懸濁剤である本種子処理剤を水で希釈し、得られる
希釈液を種子に散布する方法;あるいは本種子処理剤ま
たはその希釈液にイネ種子を浸漬する方法があげられ
る。本種子処理剤の使用量は、処理の方法により変わり
得るが、種子への粉衣処理または散布処理の場合は、本
種子処理剤は、イネ種子1kgあたりの銅として換算量
として、通常0.02〜1g、好ましくは0.05〜
0.5gである。浸漬処理の場合は、浸漬する液は銅と
しての換算濃度として、通常0.002〜0.2重量
%、好ましくは0.005〜0.05重量%である。該
浸漬処理における浸漬時間は、浸漬液中の銅の濃度によ
り変化するが、通常は10分間〜24時間の範囲であ
る。
In the bactericide containing a copper salt as an active ingredient in the present invention (hereinafter referred to as the present seed treatment agent), examples of the copper salt include cupric hydroxide and basic copper chloride.
Copper is preferred. As the seed treatment agent, it is possible to use ipconazole / copper wettable powder such as commercially available and copper nonylphenol sulfonate, etc., as long as it contains a copper salt as an active ingredient, other bactericidal effect Ingredients, carriers, auxiliaries for preparations, etc. may be contained as other ingredients. The seed treatment agent, emulsion, wettable powder, powder,
Various formulation forms such as granules can be adopted, but the copper salt in the formulation is usually 0.1 to 50% by weight. As the carrier used in such formulation, kaolin clay, attapulgite clay, bentonite, montmorillonite, acid clay, pyrophyllite, talc, diatomaceous earth,
Fine powder or granules of minerals such as calcite, natural organic substances such as corn cob powder, walnut shell powder, synthetic organic substances such as urea, salts such as calcium carbonate and ammonium sulfate, synthetic inorganic substances such as synthetic hydrous silicon oxide, etc. Solid carriers, aromatic hydrocarbons such as xylene, alkylbenzene and methylnaphthalene, alcohols such as isopropanol, ethylene glycol, propylene glycol and cellosolve, ketones such as acetone, cyclohexanone and isophorone, vegetable oils such as soybean oil and cottonseed oil. , Liquid carriers such as petroleum-based aliphatic hydrocarbons, esters, dimethylsulfoxide, and acetonitrile. As a method for treating rice seed (hull) with the present seed treating agent, a method of dressing rice seed with the present seed treating agent which is a powder; the present seed treating agent which is an emulsion, a wettable powder or a water suspension agent Examples thereof include a method of diluting with water and spraying the resulting diluted solution onto seeds; or a method of immersing rice seeds in the present seed treatment agent or a diluted solution thereof. The use amount of the present seed treatment agent may vary depending on the method of treatment, but in the case of dressing treatment or spraying treatment on seeds, the present seed treatment agent is usually 0. 02 to 1 g, preferably 0.05 to
It is 0.5 g. In the case of the dipping treatment, the dipping liquid has a converted concentration as copper of usually 0.002 to 0.2% by weight, preferably 0.005 to 0.05% by weight. The immersion time in the immersion treatment varies depending on the concentration of copper in the immersion liquid, but is usually in the range of 10 minutes to 24 hours.

【0006】本種子消毒剤にて処理されたイネ種子は、
通常、常法に従い浸種・催芽処理が行われる。その後、
該イネ種子は、苗床に播種され、育苗される。苗床は通
常、育苗箱内に床土を敷き詰めたものが用いられる。こ
こで、床土とは、イネの育苗期に用いられる土壌または
土壌代用の培地を意味する。具体的には、土壌としては
市販のイネ育苗用粒状培土、農家が自宅で利用する畑
土、水田土、山土があげられ、土壌代用の培地としては
育苗用マット、ロックウール培地があげられる。該苗床
に対して、(1RS,3SR)−2,2―ジクロロ−N
−[1−(4−クロロフェニル−)エチル]−1−エチ
ル−3−メチルシクロプルパンカルボキサミド(以下、
化合物Bと記す。)が処理される。処理時期としては、
イネ種子の播種の前後が好ましい。処理方法としては、
具体的には下記の方法により行われる。 1)床土を育苗箱に詰める前に、化合物Bの粉剤;粒剤
を床土に予め混和処理する。 2)床土を育苗箱に詰めた後、イネ種子の播種前または
播種後の覆土前後に、化合物Bの粒剤を床土表面に散粒
処理する。 3)床土を育苗箱に詰めた後、イネ種子の播種前または
播種後の覆土前後に、化合物Bの水和剤、顆粒水和剤ま
たは水懸濁剤を、所定濃度に水で希釈した希釈液を床土
表面に散布処理または潅注処理する。
Rice seeds treated with this seed disinfectant are
Usually, soaking and germination treatment are carried out according to a conventional method. afterwards,
The rice seeds are sown on a nursery and raised. The nursery is usually a nursery box with bed soil laid. Here, the bed soil means a soil or a soil substitute medium used in the rice seedling raising period. Specifically, the soil includes commercially available granular soil for raising rice seedlings, upland soil used by farmers at home, paddy soil, and mountain soil, and the soil substitute medium includes mats for raising seedlings and rock wool medium. . For the nursery, (1RS, 3SR) -2,2-dichloro-N
-[1- (4-chlorophenyl-) ethyl] -1-ethyl-3-methylcyclopulpancarboxamide (hereinafter,
It is referred to as Compound B. ) Is processed. As the processing time,
Before and after sowing of rice seeds is preferable. As a processing method,
Specifically, it is performed by the following method. 1) Before packing the bed soil in a nursery box, a powder of Compound B; granules are mixed in advance with the bed soil. 2) After the bed soil is packed in a nursery box, the granules of the compound B are dispersed on the surface of the bed soil before seeding of rice seeds or before and after covering with soil. 3) After the bed soil was packed in a nursery box, a wettable powder of Compound B, a wettable granule or a water suspension was diluted with water to a predetermined concentration before or after sowing of rice seeds or before and after covering with soil. The diluted solution is sprayed or irrigated on the soil surface.

【0007】化合物Bは、他の何らの成分も加えずその
まま用いてもよいが、通常は上記のような粉剤、粒剤、
水和剤、顆粒水和剤、水懸濁剤等の製剤形態にて用いら
れる。該製剤における化合物Bは重量%で通常0.1〜
50%である。本発明の方法においては、化合物Bは粒
剤として苗床に散粒処理されることが好ましい。化合物
Bの処理量は、面積が1,800cm2の育苗箱の場
合、1箱あたり通常0.2〜10g、好ましくは0.5
〜4g使用される。
The compound B may be used as it is without adding any other components, but usually, the above-mentioned powders, granules,
It is used in the form of preparations such as wettable powders, wettable powders, and water suspensions. The compound B in the formulation is usually 0.1% by weight.
50%. In the method of the present invention, compound B is preferably granulated as a granule on the seedbed. In the case of a nursery box having an area of 1,800 cm 2 , the treatment amount of the compound B is usually 0.2 to 10 g per box, preferably 0.5.
~ 4g is used.

【0008】化合物Bにて処理された苗床は、通常、出
芽器内またはビニールハウス内に移されて、イネ種子の
芽出しを行わせた後、田植え時まで常法に従い育苗され
る。
The seedbed treated with the compound B is usually transferred to a germinator or a greenhouse to germinate rice seeds, and then seedlings are grown according to a conventional method until the time of rice planting.

【0009】[0009]

【実施例】以下、製剤例および試験例にて本発明をさら
に詳しく説明するが、本発明は以下の例のみに限定され
るものではない。尚、部は重量部を表す。 製剤例1(本種子処理剤) 水酸化第2銅4.6部、イプコナゾール5部、リグニン
スルホン酸カルシウム3部、ラウリル硫酸ナトリウム2
部及び合成含水酸化珪素85.4部をよく粉砕混合し
て、銅塩を有効成分とする水和剤を得る。
EXAMPLES The present invention will be described in more detail below with reference to formulation examples and test examples, but the present invention is not limited to the following examples. In addition, a part represents a weight part. Formulation Example 1 (the present seed treatment agent) 4.6 parts of cupric hydroxide, 5 parts of ipconazole, 3 parts of calcium lignin sulfonate, sodium lauryl sulfate 2
Parts and 85.4 parts of synthetic hydrous silicon oxide are well pulverized and mixed to obtain a wettable powder containing a copper salt as an active ingredient.

【0010】製剤例2(化合物Bを含有する粒剤) (1RS,3SR)−2,2―ジクロロ−N−[1−
(4−クロロフェニル−)エチル]−1−エチル−3−
メチルシクロプルパンカルボキサミド4部、ジオクチル
スルホサクシネートナトリウム塩2部、合成含水酸化珪
素1部、ベントナイト30部、カオリンクレー63部を
粉砕混合し、水を加えてよく練り合わせた後、造粒乾燥
して、化合物Bの4%粒剤を得る。
Formulation Example 2 (Granule containing Compound B) (1RS, 3SR) -2,2-dichloro-N- [1-
(4-Chlorophenyl-) ethyl] -1-ethyl-3-
Methylcyclopurpancarboxamide (4 parts), dioctylsulfosuccinate sodium salt (2 parts), synthetic hydrous silicon oxide (1 part), bentonite (30 parts), and kaolin clay (63 parts) were pulverized and mixed, and water was added to the mixture, followed by granulation and drying. To obtain 4% granules of compound B.

【0011】試験例1 イネの苗立枯細菌病菌を人工的に感染させたイネ種子
(以下、汚染籾と記す。)を調製した。市販のテクリー
ドCフロアブル(クミアイ化学製;種類名「イプコナゾ
ール・銅水和剤」;イプコナゾール5%と水酸化第2銅
4.6%を含有するフロアブル剤)を水で希釈し、所定
濃度の希釈液を調製した。10gの上記の汚染籾を、2
0mlの該希釈液に、室温にて24時間浸種処理した。
その後、1日間風乾した後、該籾を通常のイネの栽培方
法に従い、浸種(18℃3日間)、催芽(30℃1日
間)を行った。市販のイネ育苗用粒状培土を直径10c
mのプラスチックポットに充填した。種子処理を行った
上記の催芽籾を該培土上に播種し、覆土前に培土および
種子の上から市販のウィン箱粒剤(日本バイエルアグロ
ケム製:種類名「カルプロパミド粒剤」;化合物B4%
を含有する粒剤)の所定量を均一に散粒処理した。その
後、上記のイネ育苗用粒状培土にて覆土し、充分量の潅
水を行った。この時のイネ播種量は、標準的な育苗箱
(30×60×3cm)あたり150g相当であり、粒
剤処理量は、標準的な育苗箱あたり50g相当である。
播種後、出芽器内で出芽処理(30℃3日間)を行った
後、温室内にて14日間栽培した。その後、苗立枯細菌
病について、非発病苗率{非発病苗率(%)=健全苗数
/(発病苗数+健全苗数)×100}を調査した。尚、
各処理区は3反復で実施し、結果は3反復の平均値を用
いた。結果を表1に示す。
Test Example 1 Rice seeds (hereinafter, referred to as contaminated paddy) artificially infected with rice seedling wilting bacteria were prepared. Commercially available Techreed C Flowable (made by Kumiai Chemical; type name "Ipconazole / copper wettable powder; flowable agent containing 5% ipconazole and 4.6% cupric hydroxide") is diluted with water to a predetermined concentration. A liquid was prepared. 2 g of 10 g of the above contaminated paddy
0 ml of the diluted solution was soaked at room temperature for 24 hours.
Then, after air-drying for 1 day, the paddy was soaked (18 ° C. for 3 days) and germinated (30 ° C. for 1 day) according to a usual rice cultivation method. Diameter 10c of commercially available granular soil for rice seedling raising
m plastic pot. The above-mentioned germinated paddy that has been subjected to seed treatment is sown on the soil, and a commercially available Win box granule (manufactured by Japan Bayer Agrochem: type name "carpropamide granule"; compound B4%) is applied to the soil and seeds before covering with soil.
Granules containing a certain amount of) were uniformly dispersed. Then, the soil was covered with the above-mentioned granular soil for raising rice seedlings, and a sufficient amount of water was applied. The rice seeding amount at this time is equivalent to 150 g per standard seedling raising box (30 × 60 × 3 cm), and the granule treatment amount is equivalent to 50 g per standard seedling raising box.
After sowing, a germination treatment (30 ° C. for 3 days) was performed in a germination device, and then cultivation was performed in a greenhouse for 14 days. After that, regarding the seedling wilt disease, the rate of non-diseased seedlings {non-diseased seedling rate (%) = number of healthy seedlings / (number of diseased seedlings + number of healthy seedlings) × 100} was investigated. still,
Each treatment was carried out in 3 replicates, and the result was the average of 3 replicates. The results are shown in Table 1.

【0012】[0012]

【表1】 [Table 1]

【0013】[0013]

【発明の効果】銅塩を有効成分とする殺菌剤にてイネ種
子(籾)を処理し、(1RS,3SR)−2,2―ジク
ロロ−N−[1−(4−クロロフェニル−)エチル]−
1−エチル−3−メチルシクロプルパンカルボキサミド
にて苗床を処理することにより、イネ苗細菌病に対する
銅塩の効果が増強される。
EFFECTS OF THE INVENTION Rice seeds (rice) are treated with a fungicide containing a copper salt as an active ingredient, and (1RS, 3SR) -2,2-dichloro-N- [1- (4-chlorophenyl-) ethyl]. −
Treatment of seedbeds with 1-ethyl-3-methylcyclopulpancarboxamide enhances the effect of copper salts on rice seedling bacterial disease.

Claims (4)

【特許請求の範囲】[Claims] 【請求項1】イネ苗細菌病を防除する方法であって、銅
塩を有効成分とする殺菌剤によりイネ種子を処理し、
(1RS,3SR)−2,2―ジクロロ−N−[1−
(4−クロロフェニル−)エチル]−1−エチル−3−
メチルシクロプルパンカルボキサミドにより苗床を処理
することを特徴とする防除方法。
1. A method for controlling bacterial diseases of rice seedlings, which comprises treating rice seeds with a fungicide containing a copper salt as an active ingredient,
(1RS, 3SR) -2,2-dichloro-N- [1-
(4-Chlorophenyl-) ethyl] -1-ethyl-3-
A method for controlling pests, which comprises treating a nursery bed with methylcyclopulpancarboxamide.
【請求項2】イネ苗細菌病が、もみ枯細菌病または苗立
枯細菌病である請求項1に記載の防除方法。
2. The control method according to claim 1, wherein the bacterial disease of rice seedlings is bacterial blight of bacterial blight or bacterial disease of bacterial blight of seedlings.
【請求項3】銅塩を有効成分とする殺菌剤が、2−
〔(4−クロロフェニル)メチル〕−5−(1−メチル
エチル)−1−(1H−1,2,4−トリアゾール−1
−イルメチル)シクロペンタノールをも含有している請
求項1または2に記載の防除方法。
3. A bactericide containing a copper salt as an active ingredient is 2-
[(4-Chlorophenyl) methyl] -5- (1-methylethyl) -1- (1H-1,2,4-triazole-1
The control method according to claim 1 or 2, further comprising -ylmethyl) cyclopentanol.
【請求項4】(1RS,3SR)−2,2―ジクロロ−
N−[1−(4−クロロフェニル−)エチル]−1−エ
チル−3−メチルシクロプルパンカルボキサミドによる
苗床の処理が、(1RS,3SR)−2,2―ジクロロ
−N−[1−(4−クロロフェニル−)エチル]−1−
エチル−3−メチルシクロプルパンカルボキサミドを含
有する粒剤をイネ種子播種後覆土前の苗床へ散粒処理で
ある請求項1〜3に記載の防除方法。
4. (1RS, 3SR) -2,2-dichloro-
Treatment of the nursery with N- [1- (4-chlorophenyl-) ethyl] -1-ethyl-3-methylcyclopulpancarboxamide resulted in (1RS, 3SR) -2,2-dichloro-N- [1- (4 -Chlorophenyl-) ethyl] -1-
The control method according to any one of claims 1 to 3, wherein the granules containing ethyl-3-methylcyclopulpancarboxamide are granulated to a seedbed after seeding with rice and before covering with soil.
JP2001276180A 2001-07-31 2001-09-12 Method for controlling bacterial disease of rice seedling Pending JP2003113011A (en)

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JP2001231219 2001-07-31
JP2001-231219 2001-07-31
JP2001276180A JP2003113011A (en) 2001-07-31 2001-09-12 Method for controlling bacterial disease of rice seedling

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Publication Number Publication Date
JP2003113011A true JP2003113011A (en) 2003-04-18

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Country Link
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