JP2001269123A - Ice cream and method for producing the same - Google Patents

Ice cream and method for producing the same

Info

Publication number
JP2001269123A
JP2001269123A JP2000087304A JP2000087304A JP2001269123A JP 2001269123 A JP2001269123 A JP 2001269123A JP 2000087304 A JP2000087304 A JP 2000087304A JP 2000087304 A JP2000087304 A JP 2000087304A JP 2001269123 A JP2001269123 A JP 2001269123A
Authority
JP
Japan
Prior art keywords
ice cream
fat
mix
freezer
milk
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP2000087304A
Other languages
Japanese (ja)
Other versions
JP3999920B2 (en
Inventor
Norio Ikeda
範夫 池田
Makoto Shioda
誠 塩田
Toshimitsu Yoshioka
俊満 吉岡
Yuichi Shimada
勇一 島田
Hiroyuki Hata
博之 秦
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Snow Brand Milk Products Co Ltd
Original Assignee
Snow Brand Milk Products Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Snow Brand Milk Products Co Ltd filed Critical Snow Brand Milk Products Co Ltd
Priority to JP2000087304A priority Critical patent/JP3999920B2/en
Publication of JP2001269123A publication Critical patent/JP2001269123A/en
Application granted granted Critical
Publication of JP3999920B2 publication Critical patent/JP3999920B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Landscapes

  • Confectionery (AREA)

Abstract

PROBLEM TO BE SOLVED: To provide an ice cream whose milk fat is not oxidized by the irradiation of light and whose flavor is good, even when preserved in a showcase or the like for a long time. SOLUTION: This method for producing the ice cream comprises a step of performing the homogenization treatment of an ice cream mix at a homogeneous pressure of 500 to 800 kg/cm2 to obtain an average fat particle diameter of 0.3 to 0.6 μm and a process for extruding the ice cream mix from a freezer at -3.0 to -5.0 deg.C.

Description

【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【0001】[0001]

【発明の属する技術分野】本発明は、平均脂肪粒子径及
び遊離脂肪率を一定範囲に調整したアイスクリーム及び
その製造方法に関する。本発明のアイスクリームは、光
照射による乳脂肪の酸化が抑制され、ショーケース等で
長期間保存しても風味が良好であるという特徴を有す
る。
TECHNICAL FIELD The present invention relates to an ice cream in which the average fat particle size and the free fat percentage are adjusted to a certain range, and a method for producing the same. The ice cream of the present invention is characterized in that the oxidation of milk fat by light irradiation is suppressed, and the flavor is good even when stored for a long time in a showcase or the like.

【0002】[0002]

【従来の技術】アイスクリームについては、「乳及び乳
製品の成分規格等に関する省令(昭和26年12月27
日厚生省令第52号)」に成分規格や製造方法の基準が
定められている。それによれば、アイスクリーム(乳固
形分15.0%以上、乳脂肪分8.0%、大腸菌群:陰
性、一般細菌:1g当り10万以下)、アイスミルク
(乳固形分10.0%以上、乳脂肪分3.0%、大腸菌
群:陰性、一般細菌:1g当り5万以下)、ラクトアイ
ス(乳固形分3.0%以上、大腸菌群:陰性、一般細
菌:溶解水1ml当り1万以下)に分類される。近年、
大手量販店、デパート、スーパーマーケット、コンビニ
エンスストア等では、アイスクリームをショーケースに
陳列し、商品の視認性の向上、見栄えを華やかにする等
の目的で、ショーケース内で過度の蛍光灯照射を行って
いる。アイスクリーム、アイスミルク(以下、アイスク
リーム及びアイスミルクを含めアイスクリームとい
う。)中に含有される乳脂肪は、光により酸化されやす
く、酸化されるとアルデヒド類の生成に起因する風味劣
化が起きやすいことが知られている(畜産食品加工学、
斉藤喜一著)。そこで、アイスクリームミックスに、ビ
タミンC、ビタミンE(δ−トコフェロール)、β−カ
ロチン等の酸化防止剤を適当量添加して、乳脂肪の光に
よる酸化を抑制する試みや、容器の内側にアルミの層を
施したり、容器表面をチタンホワイトでコーティングす
る等して、容器中の製品に直接光が当たらないようにし
て、乳脂肪の光による酸化を抑制する試みがなされてい
る。
2. Description of the Related Art Regarding ice cream, "Ministerial Ordinance on Milk and Dairy Product Ingredient Standards"
Japanese Ministry of Health and Welfare Ordinance No. 52) "specifies the component standards and the standards for production methods. According to the report, ice cream (milk solid content 15.0% or more, milk fat content 8.0%, coliform group: negative, general bacteria: 100,000 or less per gram), ice milk (milk solid content 10.0% or more) , Milk fat content 3.0%, coliforms: negative, general bacteria: 50,000 or less per gram), lactoice (milk solids content 3.0% or more, coliforms: negative, general bacteria: 10,000 or less per 1 ml of dissolved water) )are categorized. recent years,
At major mass retailers, department stores, supermarkets, convenience stores, etc., ice cream is displayed in showcases and excessive fluorescent light irradiation is performed inside the showcases for the purpose of improving the visibility of products and making the appearance more gorgeous. ing. Milk fat contained in ice cream and ice milk (hereinafter, ice cream and ice cream including ice milk) is easily oxidized by light, and when oxidized, flavor deterioration due to the generation of aldehydes occurs. Is known to be easy (livestock food processing,
Kiichi Saito). Therefore, an appropriate amount of an antioxidant such as vitamin C, vitamin E (δ-tocopherol), and β-carotene is added to the ice cream mix to suppress the oxidation of milk fat by light. Attempts have been made to suppress the oxidation of milk fat by light, for example, by applying a layer of, or coating the surface of the container with titanium white so that the product in the container is not directly exposed to light.

【0003】しかしながら、前者においては、光照射に
よる乳脂肪の酸化は抑制されるものの、酸化防止剤を添
加することにより、風味が悪くなったり、コストが高く
なるといった問題がある。また、原材料表示に「酸化防
止剤」といった表示が必要となり、消費者に好まれない
傾向がある。後者においては、光照射による乳脂肪の酸
化は抑制できるものの、コストが高く、容器にアルミを
使用すると製造現場での品質検査で金属探知器が使用で
きないといった製造上の問題が生じる。
[0003] However, in the former, although oxidation of milk fat by light irradiation is suppressed, there is a problem that the addition of an antioxidant deteriorates flavor and increases costs. In addition, a label such as "antioxidant" is required for labeling raw materials, which tends to be unfavorable by consumers. In the latter, the oxidation of milk fat by light irradiation can be suppressed, but the cost is high, and when aluminum is used for the container, there arises a production problem that a metal detector cannot be used in a quality inspection at a production site.

【0004】[0004]

【発明が解決しようとする課題】このような現状におい
て、酸化防止剤を添加することなく、また容器に特別な
加工を施すことなく、ショーケース等で光照射されても
乳脂肪の酸化が抑制されたアイスクリームが求められて
いる。そこで本発明は、光照射による乳脂肪の酸化が抑
制され、ショーケース等で長期保存しても風味の良好な
アイスクリームを提供することを課題とする。本発明に
おいて光とは、蛍光灯、太陽光等をいう。本発明におい
て遊離脂肪率とは、アイスクリーム中に含有される全脂
肪重量に対する遊離脂肪重量の割合をいう。
Under these circumstances, the oxidation of milk fat is suppressed even when light is irradiated in a showcase or the like without adding an antioxidant and without specially processing the container. Ice cream is needed. Therefore, an object of the present invention is to provide an ice cream which suppresses the oxidation of milk fat by light irradiation and has a good flavor even when stored for a long time in a showcase or the like. In the present invention, light refers to fluorescent light, sunlight, and the like. In the present invention, the ratio of free fat refers to the ratio of the weight of free fat to the total weight of fat contained in ice cream.

【0005】[0005]

【課題を解決するための手段】本発明者らは、上記の課
題に鑑み鋭意研究を重ねた結果、アイスクリームの平均
脂肪粒子径を1.0〜1.5μm、及び遊離脂肪率を3
〜13%に調整することにより、光照射による乳脂肪の
酸化を抑制し、長期保存しても風味の良好なアイスクリ
ームが得られることを見出し、本発明を完成させるに至
った。通常、アイスクリームは、原料を混合してアイス
クリームミックスを調製した後、これを均質処理し、殺
菌、冷却、エージング、フリージング、充填、硬化する
ことにより製造される。均質処理により均質化されたア
イスクリームミックス中の脂肪球の平均脂肪粒子径は
0.7〜1.2μmとなる。そしてエージング中に脂肪
球は、数珠状に会合し、フリーザ中において低温下で高
速撹拌されるとブドウの房状に凝集して気泡表面に吸着
し、脂肪球の膜を作って気泡を安定化させる。この脂肪
球の連鎖がアイスクリームの骨格となり気泡を安定に保
ち、溶解しづらく保形性が良好で、貯蔵中に収縮せず、
しかも口溶けの良好な組織を有するアイスクリームとな
る。
Means for Solving the Problems The present inventors have conducted intensive studies in view of the above problems, and as a result, have found that the average fat particle diameter of ice cream is 1.0 to 1.5 μm and the free fat ratio is 3
By adjusting the content to 1313%, it was found that oxidation of milk fat due to light irradiation was suppressed, and ice cream with a good flavor was obtained even after long-term storage, and the present invention was completed. Usually, an ice cream is produced by mixing an ingredient to prepare an ice cream mix, homogenizing the mixture, sterilizing, cooling, aging, freezing, filling, and curing. The average fat particle diameter of fat globules in the ice cream mix homogenized by the homogenization treatment is 0.7 to 1.2 μm. During aging, the fat globules associate in a rosary, and when stirred at high speed in a freezer at low temperature, aggregate into a bunch of grapes and adsorb on the bubble surface, stabilizing the bubbles by forming a fat globule film. Let it. This chain of fat globules becomes a skeleton of ice cream, keeps bubbles stable, hardly melts, has good shape retention, does not shrink during storage,
Moreover, it becomes an ice cream having a tissue that melts well in the mouth.

【0006】しかしながら、上記の工程においてアイス
クリームミックスを低温下で高速撹拌すると、脂肪球の
皮膜が破壊され、その中から遊離脂肪と呼ばれる液状脂
肪が浸出する。この遊離脂肪は、脂肪球の皮膜が破壊さ
れた不安定な状態で存在するため、光照射による酸化を
受けやすい。そこで、アイスクリームミックスの均質処
理時の均質圧力を調整することで平均脂肪粒子径を0.
3〜0.6μmとし、フリーザーからの排出時の温度を
調整したところ、脂肪球が高速撹拌時に剪断を受けづら
くなり、脂肪球の皮膜の破壊も抑制されて、アイスクリ
ーム中の遊離脂肪率が3〜13%と低減され、光照射に
よる乳脂肪の酸化を抑制し、長期保存しても風味の良好
なアイスクリームが得られた。なお、アイスクリームミ
ックス中の脂肪球は、製造工程中で少しずつ凝集するた
め、最終製品中の脂肪球の平均脂肪粒子径は1.0〜
1.5μmとなる。
[0006] However, when the ice cream mix is stirred at a high speed at a low temperature in the above process, the film of the fat globules is broken, and liquid fat called free fat is leached out of the film. Since this free fat exists in an unstable state in which the film of the fat globule is broken, it is easily oxidized by light irradiation. Therefore, the average fat particle diameter is adjusted to 0.1 by adjusting the homogenous pressure during the homogenous treatment of the ice cream mix.
When the temperature at the time of discharge from the freezer is adjusted to 3 to 0.6 μm, the fat globules are hardly subjected to shearing during high-speed stirring, the destruction of the fat globule film is suppressed, and the free fat ratio in the ice cream is reduced. The content was reduced to 3 to 13%, the oxidation of milk fat by light irradiation was suppressed, and an ice cream having a good flavor was obtained even after long-term storage. In addition, since the fat globules in the ice cream mix are gradually agglomerated during the manufacturing process, the average fat particle diameter of the fat globules in the final product is 1.0 to
1.5 μm.

【0007】[0007]

【発明の実施の形態】本発明では、まず、アイスクリー
ムミックス(以下、ミックスと略す。)を調製する。ミ
ックスの配合は、通常のアイスクリームを製造する際に
用いられるミックスであればいずれでもよく、例えば、
生クリーム、脱脂粉乳、砂糖、乳化剤、安定剤、水を粉
体溶解機に投入し、粉体原料を液体原料に分散、溶解さ
せ、プレート式加熱殺菌機を用いて85〜90℃で15
〜30秒間加熱殺菌処理を行う。その後、ミックスを高
圧ホモゲナイザー等の高圧均質機に投入し、均質圧力5
00〜800kg/cm2 で均質処理し、プレート式熱
交換機を用いて5℃以下に冷却し、ストレージタンクで
一晩エージングを行う。均質処理時の均質圧力が500
kg/cm2 未満では、平均脂肪粒子径が0.8μmを
超え、その後のフリージング工程における高速撹拌で脂
肪球が剪断を受けやすくなり、遊離脂肪率が増加し、光
照射による乳脂肪の酸化を抑制できないことがあるため
好ましくない。また、均質圧力が800kg/cm2
超えると、微細な脂肪粒子が増加し、均質処理後に脂肪
粒子同士が凝集して平均脂肪粒子径が0.8μmを超
え、その後のフリージング工程における高速撹拌で脂肪
球が剪断を受けやすくなり、遊離脂肪率が増加し、光照
射による乳脂肪の酸化を抑制できないことがあるため好
ましくない。なお、ミックス中の乳脂肪含量により、平
均脂肪粒子径の大きさも変化するため、平均脂肪粒子径
が目標とする範囲内となるように、均質処理時の均質圧
力を500〜800kg/cm2 に調整することが好ま
しい。
BEST MODE FOR CARRYING OUT THE INVENTION In the present invention, first, an ice cream mix (hereinafter, abbreviated as mix) is prepared. Mixing of the mix may be any mix as long as it is used when producing ordinary ice cream, for example,
Raw cream, skim milk powder, sugar, emulsifier, stabilizer, and water are charged into a powder dissolver, and the powder raw material is dispersed and dissolved in the liquid raw material.
Perform heat sterilization for ~ 30 seconds. Thereafter, the mixture is charged into a high-pressure homogenizer such as a high-pressure homogenizer, and the homogenizing pressure is set to 5%.
The mixture is homogenized at 00 to 800 kg / cm 2 , cooled to 5 ° C. or lower using a plate heat exchanger, and aged in a storage tank overnight. Homogeneous pressure during homogenous processing is 500
When the weight is less than kg / cm 2 , the average fat particle diameter exceeds 0.8 μm, and the high-speed stirring in the subsequent freezing step makes the fat globules more susceptible to shearing, the free fat percentage increases, and the oxidation of milk fat by light irradiation reduces It is not preferable because it may not be able to be suppressed. When the homogenous pressure exceeds 800 kg / cm 2 , fine fat particles increase, the fat particles aggregate after homogenization, and the average fat particle diameter exceeds 0.8 μm. Fat globules are easily sheared, the free fat ratio increases, and oxidation of milk fat due to light irradiation may not be suppressed, which is not preferable. In addition, since the size of the average fat particle diameter changes depending on the milk fat content in the mix, the homogenous pressure during the homogenization treatment is set to 500 to 800 kg / cm 2 so that the average fat particle diameter is within a target range. Adjustment is preferred.

【0008】次いで、エージング後のミックスをバッチ
式フリーザー、連続式フリーザー等を用いてオーバーラ
ンが30〜100%となるようにフリージングを行い、
適当な大きさの容器に充填して、約−20℃で硬化さ
せ、−20〜−30℃で貯蔵することにより、本発明の
アイスクリームを製造することができる。なお、フリー
ジング後はフリーザーから排出されるミックスの温度が
−3.0〜−5.0℃となるように調整することが好ま
しい。ミックスの温度が−3.0℃を超えると、ミック
スの凍結が不十分となりフリージング時における剪断を
受けづらくなり、遊離脂肪率が3%に満たなくなり、ア
イスクリームの組織が脆く、滑らかさに欠け、口溶けが
悪くなるのと、ミックスが柔らかくなりすぎて充填適性
が悪くなるため、好ましくない。また、ミックスの温度
が−5.0℃未満では、ミックスの凍結が進みすぎてフ
リージング時における剪断を受けすぎて遊離脂肪率が1
3%を超え、光照射による乳脂肪の酸化が起こりやすく
なるため好ましくない。また、フリーザーから排出され
るミックスの温度の調整は、フリーザーの蒸発圧力、ミ
ックス流量又はダッシャー回転数等を調節することによ
り調整することができ、例えば、フリーザーの蒸発圧力
は2.5kp、ミックス流量は160L/H、ダッシャ
ーの回転数は180rpmとすることが好ましい。
Next, the aged mix is subjected to freezing using a batch type freezer, a continuous type freezer or the like so that the overrun becomes 30 to 100%.
The ice cream of the present invention can be manufactured by filling a container of an appropriate size, curing at about -20 ° C, and storing at -20 to -30 ° C. In addition, after freezing, it is preferable to adjust the temperature of the mix discharged from the freezer to be -3.0 to -5.0 ° C. When the temperature of the mix exceeds -3.0 ° C., the mix is not sufficiently frozen, so that it is difficult to be subjected to shearing during freezing, the free fat ratio is less than 3%, and the texture of the ice cream is brittle and lacks smoothness. This is not preferred because the dissolution in the mouth deteriorates and the mix becomes too soft and the filling suitability deteriorates. If the temperature of the mix is lower than -5.0 ° C, the freezing of the mix proceeds too much and the mixture is subjected to excessive shearing during freezing, resulting in a free fat ratio of 1%.
If it exceeds 3%, oxidation of milk fat by light irradiation tends to occur, which is not preferable. Further, the temperature of the mix discharged from the freezer can be adjusted by adjusting the evaporating pressure of the freezer, the mixing flow rate, the number of rotations of the dasher, and the like. For example, the evaporating pressure of the freezer is 2.5 kp, and the mixing flow rate is adjusted. Is preferably 160 L / H, and the rotation speed of the dasher is preferably 180 rpm.

【0009】[0009]

【実施例】実施例1 表1に示す配合に従い、6種のアイスクリームを調製し
た。
EXAMPLES Example 1 Six types of ice cream were prepared according to the composition shown in Table 1.

【0010】[0010]

【表1】 [Table 1]

【0011】試料1:クリーム(HFC:High Fat Cre
am、オーストラリア産)、脱脂粉乳、砂糖、乳化剤とし
てグリセリン脂肪酸エステル、安定剤として増粘多糖類
製剤(キャベロックス、トーエイ貿易)及び水を粉体溶
解機に投入し、分散、溶解させ、プレート式加熱殺菌機
を用い、85℃で加熱殺菌処理を行った。次いで、高圧
ホモゲナイザーを用い、均質圧力600kg/cm2
均質処理を行った。その後、一晩エージングを行い、ミ
ックスをフリーザー(WS−106G型、APVC−r
epaco社)に投入し、オーバーランを70%に設定
し、蒸発圧力2.5kp/cm2 、ミックス流量150
L/H、ダッシャー回転数160rpmに調節してフリ
ージングを行い、フリーザーから排出されるミックスの
温度を−3.5℃に調整し、円柱型白色容器(高さ2c
m、直径7cm)に充填し、−25℃にて一晩硬化させ
て、アイスクリームを製造した。 試料2:フリーザーの蒸発圧力を1.9kp/cm2
調節してフリーザーから排出されるミックスの温度を−
4.5℃に調整する以外は、試料1と同様の方法でアイ
スクリームを製造した。 試料3:フリーザーの蒸発圧力を1.6kp/cm2
調節してフリーザーから排出されるミックスの温度を−
5.0℃に調整する以外は、試料1と同様の方法でアイ
スクリームの製造した。
Sample 1: Cream (HFC: High Fat Cre)
am, made in Australia), skim milk powder, sugar, glycerin fatty acid ester as emulsifier, thickening polysaccharide preparation (Caverox, Toei Trading) and water as stabilizers, put into powder dissolver, disperse and dissolve, plate type Heat sterilization was performed at 85 ° C. using a heat sterilizer. Next, using a high-pressure homogenizer, homogenization treatment was performed at a homogenous pressure of 600 kg / cm 2 . Thereafter, aging was performed overnight, and the mix was frozen (WS-106G, APVC-r).
epaco), the overrun was set to 70%, the evaporation pressure was 2.5 kp / cm 2 , and the mix flow rate was 150.
L / H, Dasher rotation speed was adjusted to 160 rpm, freezing was performed, the temperature of the mix discharged from the freezer was adjusted to -3.5 ° C, and a cylindrical white container (height 2c)
m, 7 cm in diameter) and cured at -25 ° C overnight to produce an ice cream. Sample 2: the evaporating pressure of the freezer was adjusted to 1.9 kp / cm 2 and the temperature of the mix discharged from the freezer was −
An ice cream was produced in the same manner as in Sample 1, except that the temperature was adjusted to 4.5 ° C. Sample 3: The evaporating pressure of the freezer was adjusted to 1.6 kp / cm 2 and the temperature of the mix discharged from the freezer was −
Ice cream was produced in the same manner as in Sample 1, except that the temperature was adjusted to 5.0 ° C.

【0012】試料4:フリーザーの蒸発圧力を1.2k
p/cm2 に調節してフリーザーから排出されるミック
スの温度を−6.5℃に調整する以外は、試料1と同様
の方法でアイスクリームの製造を試みたが、チャーニン
グが発生し、アイスクリームを製造することができなか
った。 試料5:ミックスの均質処理を均質圧力200kg/c
2 で行い、さらにフリーザーの蒸発圧力を1.9kp
/cm2 に調節してフリーザーから排出されるミックス
の温度を−4.5℃に調整する以外は、試料1と同様の
方法でアイスクリームの製造した。 試料6:ミックスの均質処理を均質圧力900kg/c
2 で行い、さらにフリーザーの蒸発圧力を1.9kp
/cm2 に調節してフリーザーから排出されるミックス
の温度を−4.5℃に調整する以外は、試料1と同様の
方法でアイスクリームの製造を試みたが、チャーニング
が発生し、アイスクリームを製造することができなかっ
た。 試料1〜6のミックスについて、平均脂肪粒子径(メジ
アン径)とその粒径分布を粒度分布計SALD−200
0(島津製作所製)を用いて測定した。なお、ミックス
の平均脂肪粒子径の測定は、均質処理を行い一晩エージ
ングを行ったミックスについて行った。その結果を表2
に示す。
Sample 4: 1.2 k evaporating pressure of freezer
Ice cream was produced in the same manner as in Sample 1, except that the temperature of the mix discharged from the freezer was adjusted to -6.5 ° C by adjusting to p / cm 2 , but charring occurred. Could not produce ice cream. Sample 5: A homogenous treatment of the mix was performed at a homogeneous pressure of 200 kg / c.
performed in m 2, and more 1.9kp the evaporation pressure of the freezer
/ Except cm 2 adjusted to to adjust the temperature of the mix is discharged from the freezer to -4.5 ° C. was prepared ice cream in the same manner as Sample 1. Sample 6: A homogenous treatment of the mix was performed at a homogeneous pressure of 900 kg / c.
performed in m 2, and more 1.9kp the evaporation pressure of the freezer
/ Cm 2 and the temperature of the mix discharged from the freezer was adjusted to −4.5 ° C., except that ice cream was produced in the same manner as in Sample 1. The cream could not be manufactured. The average fat particle size (median size) and the particle size distribution of the mix of samples 1 to 6 were measured using a particle size distribution analyzer SALD-200.
0 (manufactured by Shimadzu Corporation). In addition, the measurement of the average fat particle diameter of the mix was performed on the mix that had been subjected to homogenous treatment and aged overnight. Table 2 shows the results.
Shown in

【0013】[0013]

【表2】 [Table 2]

【0014】試験例1 実施例1で得られた試料1〜3及び5のアイスクリーム
について、平均脂肪粒子径(メジアン径)及び遊離脂肪
率を測定した。平均脂肪粒子径の測定:粒度分布計SA
LD−2000(島津製作所製)を用いて測定した。 遊離脂肪率の測定:200mlの分液漏斗に約10gの
各試料を精秤し、四塩化炭素溶液30mlを加え、軽く
しん盪させ、5分間静置後、上層と下層に別れた層のう
ち、下層を採取した。残った上層に四塩化炭素溶液30
mlを加え、前記と同様の操作で下層を採取した。さら
に、この下層を200ml分液漏斗に移し、飽和食塩水
30mlを加え、前記と同様の操作で下層を採取した。
この下層に残留する四塩化炭素溶液をロータリーエバポ
レーターで減圧濃縮し、遊離脂肪を採取してその量を測
定した。また、全脂肪量をバブコック法により測定し、
全脂肪量に対する遊離脂肪量の割合を算出した。その結
果を表3に示す。
Test Example 1 The average fat particle diameter (median diameter) and the free fat percentage of the ice creams of Samples 1 to 3 and 5 obtained in Example 1 were measured. Measurement of average fat particle size: particle size distribution analyzer SA
It measured using LD-2000 (made by Shimadzu Corporation). Measurement of percentage of free fat: about 10 g of each sample was precisely weighed in a 200 ml separatory funnel, 30 ml of carbon tetrachloride solution was added, the mixture was gently shaken, and allowed to stand for 5 minutes. , The lower layer was collected. Carbon tetrachloride solution 30
ml was added, and the lower layer was collected in the same manner as above. Further, the lower layer was transferred to a 200 ml separating funnel, 30 ml of saturated saline was added, and the lower layer was collected in the same manner as above.
The carbon tetrachloride solution remaining in the lower layer was concentrated under reduced pressure using a rotary evaporator, and free fat was collected and its amount was measured. Also, the total fat mass was measured by the Babcock method,
The ratio of the amount of free fat to the amount of total fat was calculated. Table 3 shows the results.

【0015】[0015]

【表3】 [Table 3]

【0016】試験例2 実施例1で得られた試料1〜3及び5のアイスクリーム
について、光照射試験を行った。 光照射試験:アイスクリームを−18℃のマウンテンシ
ョーケース(SANDEN社製)にて約1000ルクス
の光照射を行いながら7日間保存し、保存0日後、保存
3日後、保存7日後の各試料のPOV(過酸化物価)を
鉄−チオシアネート法により測定した。なお、通常PO
Vの値がおおよそ2を超えると酸化臭が感じられる。さ
らに10名の熟練パネラーに各試料30g(品温−17
℃)を食してもらい、酸化臭について、製造直後のアイ
スクリームを10点とし、これと比較した点数で評価し
た。その結果を表4に示す。
Test Example 2 The ice creams of Samples 1 to 3 and 5 obtained in Example 1 were subjected to a light irradiation test. Light irradiation test: The ice cream was stored in a mountain showcase (manufactured by SANDEN) at −18 ° C. for 7 days while being irradiated with light of about 1000 lux, and after 0 day, 3 days, and 7 days after storage, POV (peroxide value) was measured by the iron-thiocyanate method. In addition, usually PO
When the value of V exceeds approximately 2, an odor of oxidation is felt. Furthermore, 30 g of each sample (product temperature -17) was sent to 10 skilled panelists.
° C), and the oxidative odor was evaluated on the basis of a score of 10 points for the ice cream immediately after production. Table 4 shows the results.

【0017】[0017]

【表4】 [Table 4]

【0018】試料1〜3は、経時的なPOVの上昇も少
なく、光照射による乳脂肪の酸化が抑制されていること
が確認された。また、保存7日後でも酸化臭が感じられ
ないとの評価を得た。一方で、試料5は、経時的にPO
Vが上昇し、保存3日後で酸化臭が感じられ、好ましく
ないとの評価であった。
Samples 1 to 3 showed little increase in POV with time, confirming that the oxidation of milk fat by light irradiation was suppressed. In addition, it was evaluated that no odor of oxidation was felt even after 7 days of storage. On the other hand, Sample 5
V increased, and an odor of oxidation was felt 3 days after storage, which was evaluated as undesirable.

【0019】[0019]

【発明の効果】本発明によれば、光照射による乳脂肪の
酸化が抑制され、ショーケース等で長期間保存しても風
味が良好なアイスクリームを提供することができる。本
発明のアイスクリームは、酸化防止剤を添加することな
く、また、容器に特殊な加工を施さなくとも、アイスク
リームの製造工程において、平均脂肪粒子径及び遊離脂
肪率を調整することで、光照射による乳脂肪の酸化が抑
制されるものである。
According to the present invention, it is possible to provide an ice cream which suppresses the oxidation of milk fat by light irradiation and has a good flavor even when stored for a long time in a showcase or the like. The ice cream of the present invention can be obtained by adjusting the average fat particle diameter and the free fat percentage in the ice cream production process without adding an antioxidant and without specially processing the container. It suppresses the oxidation of milk fat by irradiation.

───────────────────────────────────────────────────── フロントページの続き (72)発明者 島田 勇一 東京都日野市神明4−1−12 プレステー ジビル205 (72)発明者 秦 博之 東京都府中市本町3−33−5 南乃家201 Fターム(参考) 4B014 GB18 GP02 GY01  ──────────────────────────────────────────────────続 き Continuing on the front page (72) Inventor Yuichi Shimada 4-1-12 Shinmei, Hino-shi, Tokyo Prestige Building 205 (72) Inventor Hiroyuki Hata 3-33-5, Honmachi, Fuchu-shi, Tokyo 201 Minanoya F-term ( Reference) 4B014 GB18 GP02 GY01

Claims (2)

【特許請求の範囲】[Claims] 【請求項1】 平均脂肪粒子径が1.0〜1.5μmで
あり、遊離脂肪率が3〜13%であることを特徴とする
アイスクリーム。
An ice cream having an average fat particle size of 1.0 to 1.5 μm and a free fat ratio of 3 to 13%.
【請求項2】 アイスクリームの製造工程において、ア
イスクリームミックスの均質処理を均質圧力500〜8
00kg/cm2 で行って平均脂肪粒子径を0.3〜
0.6μmとなるようにする工程、及びフリーザーから
アイスクリームミックスを−3.0〜−5.0℃で排出
する工程を含むことを特徴とする請求項1記載のアイス
クリームの製造方法。
2. In the ice cream manufacturing process, the ice cream mix is homogenized at a uniform pressure of 500-8.
Performing at 00 kg / cm 2 to reduce the average fat particle diameter to 0.3 to
2. The method for producing ice cream according to claim 1, further comprising a step of adjusting the thickness to 0.6 [mu] m and a step of discharging the ice cream mix from a freezer at -3.0 to -5.0 [deg.] C.
JP2000087304A 2000-03-27 2000-03-27 Ice cream and manufacturing method thereof Expired - Fee Related JP3999920B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2000087304A JP3999920B2 (en) 2000-03-27 2000-03-27 Ice cream and manufacturing method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2000087304A JP3999920B2 (en) 2000-03-27 2000-03-27 Ice cream and manufacturing method thereof

Publications (2)

Publication Number Publication Date
JP2001269123A true JP2001269123A (en) 2001-10-02
JP3999920B2 JP3999920B2 (en) 2007-10-31

Family

ID=18603337

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2000087304A Expired - Fee Related JP3999920B2 (en) 2000-03-27 2000-03-27 Ice cream and manufacturing method thereof

Country Status (1)

Country Link
JP (1) JP3999920B2 (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2006006195A (en) * 2004-06-25 2006-01-12 Fuji Oil Co Ltd Oil-in-water type emulsion
JP2006094801A (en) * 2004-09-30 2006-04-13 Fuji Oil Co Ltd Oil-in-water emulsified product containing nonfat milk solid
JP2009124985A (en) * 2007-11-22 2009-06-11 Morinaga & Co Ltd Method for producing chocolate ice cream
JP2011103906A (en) * 2011-03-11 2011-06-02 Fuji Oil Co Ltd Oil-in-water emulsified substance
JP2016119885A (en) * 2014-12-25 2016-07-07 太陽化学株式会社 Degradation odor inhibitor laurate-based oil and fat-containing food

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2006006195A (en) * 2004-06-25 2006-01-12 Fuji Oil Co Ltd Oil-in-water type emulsion
JP2006094801A (en) * 2004-09-30 2006-04-13 Fuji Oil Co Ltd Oil-in-water emulsified product containing nonfat milk solid
JP2009124985A (en) * 2007-11-22 2009-06-11 Morinaga & Co Ltd Method for producing chocolate ice cream
JP2011103906A (en) * 2011-03-11 2011-06-02 Fuji Oil Co Ltd Oil-in-water emulsified substance
JP2016119885A (en) * 2014-12-25 2016-07-07 太陽化学株式会社 Degradation odor inhibitor laurate-based oil and fat-containing food

Also Published As

Publication number Publication date
JP3999920B2 (en) 2007-10-31

Similar Documents

Publication Publication Date Title
JP3182557B2 (en) Dispersion stabilizer containing native gellan gum and its application
CN104472846B (en) A kind of soft ice cream milk slurry and preparation method thereof
JP2001502168A (en) Product, its manufacturing method and its use
TW201223454A (en) Gel composition
MX2014009625A (en) Ice-containing products.
CN107912016A (en) Low-fat frozen confectionery
CN109480134A (en) A kind of carbonated juice fruit syrup and preparation method thereof suitable for PET bottle dress production
JP2001269123A (en) Ice cream and method for producing the same
Hubbes et al. Sugar particles and their role in crystallization kinetics and structural properties in fats used for nougat creme production
JP6612491B2 (en) Edible cream and method for producing the same
JP2009148168A (en) Soft cream mix composition and method for producing the same
US20120121787A1 (en) Aerated food products
JPH0224512B2 (en)
JP2008506378A (en) Method for producing stable lactic acid metal salt in powder form and stable lactic acid metal salt
JP3411144B2 (en) Manufacturing method of jelly containing vegetables and fruits
JPH02207764A (en) Preparation of powdery cream readily dispersible in cold water
JP2008011784A (en) Frozen dessert stabilizer
JP2000014335A (en) Powdery thickening stabilizer composition
DE602004007323T2 (en) Gelatin and starch containing food
JP2974426B2 (en) Soft sherbet mix and method for producing the same
HU221776B1 (en) Process for producing of after - pasteurized curd products
EP1494544B1 (en) Spoonable water-continuous acidified food product
JPS611358A (en) Gelatinous food
EP3727005B1 (en) Edible water-continuous composition
JP4523956B2 (en) Dairy product and manufacturing method thereof

Legal Events

Date Code Title Description
A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20070110

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20070426

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20070502

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20070702

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20070802

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20070810

R150 Certificate of patent or registration of utility model

Free format text: JAPANESE INTERMEDIATE CODE: R150

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20100817

Year of fee payment: 3

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20100817

Year of fee payment: 3

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20110817

Year of fee payment: 4

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20110817

Year of fee payment: 4

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20140817

Year of fee payment: 7

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

S111 Request for change of ownership or part of ownership

Free format text: JAPANESE INTERMEDIATE CODE: R313111

R350 Written notification of registration of transfer

Free format text: JAPANESE INTERMEDIATE CODE: R350

LAPS Cancellation because of no payment of annual fees