JP2001103918A - Method for improving gustatoriness and gustatoriness- improved persimmon juice preparation - Google Patents

Method for improving gustatoriness and gustatoriness- improved persimmon juice preparation

Info

Publication number
JP2001103918A
JP2001103918A JP31866499A JP31866499A JP2001103918A JP 2001103918 A JP2001103918 A JP 2001103918A JP 31866499 A JP31866499 A JP 31866499A JP 31866499 A JP31866499 A JP 31866499A JP 2001103918 A JP2001103918 A JP 2001103918A
Authority
JP
Japan
Prior art keywords
persimmon
gustatoriness
persimmon juice
astringent
taste
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP31866499A
Other languages
Japanese (ja)
Inventor
浩誠 ▲桑▼原
Hiromoto Kuwabara
Yoshitaka Nakamura
喜孝 中村
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Maruzen Pharmaceutical Co Ltd
Original Assignee
Maruzen Pharmaceutical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Maruzen Pharmaceutical Co Ltd filed Critical Maruzen Pharmaceutical Co Ltd
Priority to JP31866499A priority Critical patent/JP2001103918A/en
Publication of JP2001103918A publication Critical patent/JP2001103918A/en
Pending legal-status Critical Current

Links

Abstract

PROBLEM TO BE SOLVED: To provide a means for improving the astringent taste or the like of persimmon juice and enabling persimmon juice to be easily taken as a food, and to obtain the subject gustatoriness-improved persimmon juice preparation. SOLUTION: This means for improving the gustatoriness of a persimmon juice comprises mixing preferably >=10 wt.% of a starch hydrolyzate with a molecular weight of 1,000-2,000 into a persimmon juice to dissolve it in the juice followed by drying the resultant mixture through e.g. spray drying method to obtain persimmon juice powder which is utilized as the other objective persimmon juice preparation.

Description

【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【発明の属する技術分野】本発明は、柿渋にデンプン加
水分解物を配合することにより、柿渋特有の渋味、収斂
味等の呈味を改善する方法及び呈味が改善された柿渋製
剤に関するものである。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a method for improving the taste, such as the astringency and astringency of persimmon astringent, by adding a starch hydrolyzate to persimmon astringent, and to a persimmon astringent preparation having an improved taste. It is.

【0002】[0002]

【従来の技術】柿渋は、古来より防虫防腐剤として、ま
た、樽・網・傘の塗料及び清酒の輸送・貯蔵・販売の過
程で生じる白濁を防止するための澱下げ剤として用いら
れていた。
2. Description of the Related Art Persimmon astringent has been used as an antiseptic and preservative since ancient times, and as a depressant to prevent cloudiness that occurs during the transportation, storage and sale of paint for barrels, nets and umbrellas, and sake. .

【0003】また、民間薬として、火傷や毒蛇の蛋白毒
の中和剤として用いらたり、経口的に服用することで、
血圧降下作用などの薬理作用を示すことが報告されてい
る。
[0003] In addition, as a folk medicine, it is used as a neutralizing agent for burns and poisonous snake protein poison, or taken orally.
It has been reported to exhibit pharmacological effects such as blood pressure lowering effects.

【0004】しかし、柿渋を経口的に服用する際、有機
酸臭が強く、その使用範囲が限られていたが、本発明者
らは、柿渋に水溶性多糖を混合し、加熱乾燥することに
より、柿渋の異臭を除くことに成功した(特願平10−
296231号)。
However, when persimmon juice is taken orally, the organic acid odor is strong and its use range is limited. However, the present inventors mixed water-soluble polysaccharide with persimmon juice and dried by heating. Succeeded in removing the off-flavor of persimmon juice (Japanese Patent Application No.
296231).

【0005】また、柿渋にはタンニン類に起因する渋
味、収斂味等も服用する際の問題となっていた。この渋
味等を取り除くため、カゼインなどのタンパク質との反
応が試みらているが、この方法では水不溶物が形成さ
れ、噴霧乾燥などの方法が採用できず、安価に生産する
ことが困難であると共に呈味改善の程度も十分ではなか
った。
[0005] In addition, astringency, astringency and the like caused by tannins have been a problem when taking persimmon juice. In order to remove such astringency, a reaction with a protein such as casein has been attempted. However, in this method, water-insoluble substances are formed, and methods such as spray-drying cannot be adopted. In addition, the degree of taste improvement was not sufficient.

【0006】[0006]

【発明が解決しようとする課題】本発明の目的は、食品
に使用する柿渋の渋味等を改善することにより、固有の
渋味等により使用量及び用途範囲が制限されていた柿渋
の使用量及び用途を拡大することにある。
SUMMARY OF THE INVENTION It is an object of the present invention to improve the astringency of persimmon astringent used in foods, so that the amount of persimmon astringent used and the range of use are limited by the inherent astringency. And to expand applications.

【0007】[0007]

【課題を解決するための手段】本発明により提供された
呈味改善法及び呈味改善柿渋製剤は、柿渋に分子量が1
000〜2000のデンプン加水分解物を混合溶解した
後、噴霧乾燥、真空乾燥等の方法を行うことを特徴とす
る。
Means for Solving the Problems The taste improving method and the taste improving persimmon astringent preparation provided by the present invention have a molecular weight of 1 persimmon astringent.
After mixing and dissolving 000 to 2,000 starch hydrolysates, a method such as spray drying or vacuum drying is performed.

【0008】また、本発明により提供された呈味改善柿
渋製剤は、上記本発明の方法により、柿渋1に対して分
子量が1000〜2000のデンプン加水分解物10重
量%以上との混合物を乾燥したものである。
The taste-improved persimmon astringent preparation provided by the present invention is obtained by drying a mixture of persimmon astringent 1 and a starch hydrolyzate having a molecular weight of 1000 to 2000 by weight of 10% or more by the method of the present invention. Things.

【0009】[0009]

【発明の実施の形態】本発明に用いる柿渋は、直径3か
ら5cm位の未熟な柿(学名:Diospyros K
aki Linn.)を発酵して得た液体であって、高
分子化した縮合型タンニンを主成分とするものである。
この縮合型タンニンは通称柿タンニンと呼ばれる。この
柿タンニンは、蛋白質と強く結合して沈殿を生じたり、
鉄と反応して発色するという性質があり、水とエタノー
ル、メタノールにはよく溶けるが、n−ブタノール、イ
ソプロパノール、アセトン、酢酸エチルには解けにくい
ものである。
BEST MODE FOR CARRYING OUT THE INVENTION The persimmon astringent used in the present invention is an immature persimmon having a diameter of about 3 to 5 cm (scientific name: Diospyros K).
aki Linn. ) Is a liquid obtained by fermentation, and contains a polymerized condensed tannin as a main component.
This condensed tannin is commonly called persimmon tannin. This persimmon tannin binds strongly to the protein to form a precipitate,
It has the property of developing color by reacting with iron, and is soluble in water, ethanol and methanol, but hardly soluble in n-butanol, isopropanol, acetone and ethyl acetate.

【0010】柿渋は、柿を搾汁した後液部のみを取り出
し、糖質分解酵素を持つ酵母を添加し、3日から10日
発酵を行った後、この発酵液を1年から4年間熟成して
得られたものであり、固形分濃度が約8〜12重量%、
柿タンニン含有率が4〜7重量%程度である。
[0010] Persimmon astringent, after squeezing the persimmon, take out only the liquid part, add yeast having carbohydrate degrading enzyme, ferment for 3 to 10 days, and aged this fermented liquid for 1 to 4 years Having a solid content of about 8 to 12% by weight,
Persimmon tannin content is about 4-7% by weight.

【0011】また、本発明で言うデンプン加水分解物と
は、例えば、ばれいしょ、小麦粉、トウモロコシ、タピ
オカ等を原料とする澱粉を酵素または無機酸によって加
水分解処理して分子量が1000〜2000に分解した
ものを主成分としたものである。
[0011] The starch hydrolyzate referred to in the present invention is, for example, a starch obtained from a potato, flour, corn, tapioca or the like as a raw material, which is hydrolyzed with an enzyme or an inorganic acid to a molecular weight of 1,000 to 2,000. It is mainly composed of

【0012】分子量が1000以下のデンプン加水分解
物では、柿渋の呈味改善効果はほとんど無く、また、分
子量2000以上のデンプン加水分解物は、多少の改善
効果は見られるものの、十分な効果ではない。また、分
子量が2000以上のデンプン加水分解物は、水への溶
解性が悪く、取扱いの面でも本発明に用いることは難し
い。
A starch hydrolyzate having a molecular weight of 1,000 or less has almost no effect of improving the taste of persimmon astringent, and a starch hydrolyzate having a molecular weight of 2,000 or more has a slight improvement effect but is not a sufficient effect. . A starch hydrolyzate having a molecular weight of 2,000 or more has poor solubility in water, and is difficult to use in the present invention in terms of handling.

【0013】デンプン加水分解物は、呈味改善対象であ
る柿渋に対して10重量%以上、好ましくは10重量%
から200重量%を添加して、十分に混合し溶解する。
デンプン加水分解物の添加量が多い場合は、予めデンプ
ン加水分解物を水で溶解した液と柿渋を混合しても良
い。
[0013] The starch hydrolyzate is at least 10% by weight, preferably 10% by weight, based on persimmon astringency to be taste-improved.
To 200% by weight and thoroughly mixed and dissolved.
When the starch hydrolyzate is added in a large amount, a liquid obtained by dissolving the starch hydrolyzate in water and persimmon juice may be mixed.

【0014】柿渋とデンプン加水分解物の溶解液は、直
接乾燥するか必要に応じて濃縮した後、乾燥する。
The solution of persimmon astringent and starch hydrolyzate is dried directly or, if necessary, concentrated and then dried.

【0015】乾燥方法としては、加熱真空乾燥、凍結乾
燥、熱風乾燥、噴霧乾燥等の何れの方法を用いることも
できるが、コスト面や後工程の粉末化を考慮すると噴霧
乾燥が好ましい。
As a drying method, any method such as heating vacuum drying, freeze drying, hot air drying and spray drying can be used, but spray drying is preferable in consideration of cost and powdering in a later step.

【0016】このように得られた乾燥柿渋は、元の柿渋
特有の渋味や収斂味をほとんど呈せず、経口で服用する
に当たり、人に対し何ら不快感を感じることの無い製剤
である。
The dried persimmon astringent obtained in this way is a preparation which hardly exhibits the astringent or astringent taste peculiar to the original persimmon astringent and does not cause any discomfort to humans when taken orally.

【0017】さらに、本発明の方法を付した呈味改善柿
渋粉末は、服用した後、消化器官において容易にデンプ
ン加水分解物が消化され、柿渋本来の薬理を示す。
Further, after taking the taste-improved persimmon astringent powder to which the method of the present invention has been applied, starch hydrolyzate is easily digested in the digestive tract and exhibits the original pharmacology of persimmon astringent.

【0018】本発明の呈味改善された柿渋は、顆粒、錠
剤、粉末、チュアブル、カプセル等、各種形態に使用す
ることが出来る。また、使用用途しては、抗菌素材、消
臭素材、苦味素材に利用することが出来る。さらに、食
品や菓子類などに用いることが出来る。例えば、パン、
チューインガム、キャンディ、グミ、ゼリー、錠菓など
には容易に用いることが出来る。
The persimmon juice with improved taste of the present invention can be used in various forms such as granules, tablets, powders, chewables and capsules. In addition, it can be used for antibacterial materials, deodorant materials, and bitter materials. Furthermore, it can be used for foods and confectionery. For example, bread,
It can be easily used for chewing gum, candy, gummy, jelly, tablet confectionery and the like.

【0019】[0019]

【実施例】以下、実施例及び使用例を示して本発明を説
明するが本発明はこれに限定されるものではない。な
お、本実施例で用いる柿渋は、市販のものを使用し、固
形分濃度は10%のものを使用した。
The present invention will be described below with reference to examples and use examples, but the present invention is not limited to these examples. The persimmon juice used in this example was a commercially available persimmon juice having a solid content of 10%.

【0020】製造実施例1 平均分子量1500(商品名:パインデックスNo.
2、松谷化学工業社製)50gを水500mlに溶か
し、分画分子量1000の透析膜(商品名:スペクトラ
/ポアCE,MW1000、メデシナルインダストリー
社製)に入れ、水道水流水中で48時間透析し、膜内液
を減圧濃縮後、真空乾燥した。柿渋50gに透析内液乾
燥物5gを混合溶解し、減圧乾燥後、真空乾燥・粉砕に
より粉末柿渋製剤9.3gを得た。
Production Example 1 Average molecular weight 1500 (trade name: Paindex No.
2, 50 g of Matsutani Chemical Industry Co., Ltd.) is dissolved in 500 ml of water, put into a dialysis membrane having a molecular weight cut off of 1,000 (trade name: Spectra / Pore CE, MW1000, manufactured by Medicinal Industry), and dialyzed in running tap water for 48 hours. The solution in the membrane was concentrated under reduced pressure, and dried under vacuum. 5 g of dried dialysis solution was mixed and dissolved in 50 g of persimmon astringent, dried under reduced pressure, and then vacuum-dried and pulverized to obtain 9.3 g of a powdered persimmon astringent preparation.

【0021】製造実施例2 平均分子量2000(商品名:パインデックスNo.
1、松谷化学工業社製)50gを水1000mlに溶か
し、分画分子量2000の透析膜(商品名:スペクトラ
/ポアCE,MW2000、メデシナルインダストリー
社製)に入れ、各6000mlの水に対し、3回透析
(温度5℃、10時間、3回)し、透析外液を減圧濃縮
後、真空乾燥した。柿渋50gに透析内液乾燥物5gを
混合溶解し、減圧乾燥後、真空乾燥・粉砕により粉末柿
渋製剤9.6gを得た。
Production Example 2 Average molecular weight 2000 (trade name: Paindex No.
1, 50 g of Matsutani Chemical Industry Co., Ltd.) was dissolved in 1000 ml of water, and put into a dialysis membrane having a molecular weight cutoff of 2,000 (trade name: Spectra / Pore CE, MW2000, manufactured by Medicinal Industry). The dialysis was performed twice (temperature 5 ° C., 10 hours, three times), and the outer solution of the dialysis was concentrated under reduced pressure and then dried under vacuum. 5 g of dried dialysis solution was mixed and dissolved in 50 g of persimmon astringent, dried under reduced pressure, and vacuum-dried / pulverized to obtain 9.6 g of a powdered persimmon astringent preparation.

【0022】製造実施例3 柿渋1kgにデンプン加水分解物として、平均分子量:
1500(市販名:パインデックスNo.2、松谷化学
工業社製)200gを混合溶解し、165℃の噴霧乾燥
機で噴霧乾燥させ、粉末柿渋製剤284gを得た。
Production Example 3 1 kg of persimmon astringent as starch hydrolyzate, average molecular weight:
200 g of 1500 (commercial name: Paindex No. 2, manufactured by Matsutani Chemical Industry Co., Ltd.) was mixed and dissolved, and spray-dried with a spray dryer at 165 ° C. to obtain 284 g of a powdered persimmon astringent preparation.

【0023】製造実施例4 柿渋1kgにデンプン加水分解物として、平均分子量:
2000(パインデックスNo.1、松谷化学工業社
製)200gを混合溶解し、165℃の噴霧乾燥機で噴
霧乾燥させ、粉末柿渋製剤280gを得た。
Production Example 4 1 kg of persimmon persimmon as starch hydrolyzate, average molecular weight:
200 g (Paindex No. 1, manufactured by Matsutani Chemical Industry Co., Ltd.) was mixed and dissolved, and spray-dried with a spray drier at 165 ° C. to obtain 280 g of a powdered persimmon astringent preparation.

【0024】製造比較例1 柿渋1kgにデンプン加水分解物として、平均分子量6
50(パインデックスNo.3、松谷化学工業社製)2
00gを混合溶解し、165℃で噴霧乾燥し、乾燥粉末
281gを得た。
Comparative Production Example 1 1 kg of persimmon astringent was converted to a starch hydrolyzate with an average molecular weight of 6
50 (Paindex No. 3, manufactured by Matsutani Chemical Industry Co., Ltd.) 2
00 g was mixed and dissolved, and spray-dried at 165 ° C. to obtain 281 g of dry powder.

【0025】製造比較例2 柿渋1kgにデンプン加水分解物として、平均分子量2
000(パインデックスNo.1、松谷化学工業社製)
70gを混合溶解し、165℃で噴霧乾燥し、乾燥粉末
111gを得た。
Production Comparative Example 2 1 kg of persimmon astringent was converted to a starch hydrolyzate with an average molecular weight of 2
000 (Paindex No. 1, manufactured by Matsutani Chemical Industry Co., Ltd.)
70 g were mixed and dissolved, and spray-dried at 165 ° C. to obtain 111 g of a dry powder.

【0026】試験例1 呈味改善確認試験 製造実施例1から4及び製造比較例1、2で製造した柿
渋製剤を用いて、渋味のマスキングについて試験を行っ
た。パネラーは18歳から55歳までの男女各5人ずつ
で、各パネラーに供試粉末0.5gを直接口に含んで唾
液で口中に分散して呈味を確認し、「渋味、収斂味が強
い(味が強い)」「渋味、収斂味が感じられる(味を感
じる)」「渋味、収斂味なし(味がない)」の3段階評
価で行った。
Test Example 1 Test for Confirming Taste Improvement Using the persimmon astringent preparations produced in Production Examples 1 to 4 and Comparative Production Examples 1 and 2, a test was conducted for masking of astringency. The panelists consisted of 5 males and 5 females aged 18 to 55, each containing 0.5 g of the test powder directly in their mouth and dispersing in the mouth with saliva to confirm the taste. Is strong (has a strong taste), "astringent taste and astringent taste are felt (feel the taste)", and "no astringent taste and astringent taste (no taste)".

【0026】 [0026]

【0027】上記の結果から明らかなように、柿渋に対
し、分子量1000〜2000のデンプン加水分解物を
10重量%以上混合溶解した液を乾燥した柿渋製剤は、
呈味が改善されていた。
As is clear from the above results, a persimmon juice preparation obtained by mixing and dissolving 10% by weight or more of a starch hydrolyzate having a molecular weight of 1,000 to 2,000 with respect to persimmon astringent was dried.
The taste was improved.

【0028】配合実施例1 常法に従い、錠剤状健康食
品を製造した。 粉糖 100g デキストリン 80g モノグリセリン脂肪酸エステル 20g 製造実施例3の粉末柿渋製剤 100g
Formulation Example 1 A tablet-shaped health food was produced according to a conventional method. Powdered sugar 100 g Dextrin 80 g Monoglycerin fatty acid ester 20 g Powdered persimmon juice preparation of Production Example 3 100 g

【0029】配合実施例2 常法に従い、柿渋製剤入り
キャンディーを製造した。 グラニュー糖 65g 酵素糖化水飴 35g サイクロデキストリン 0.5g 香料 0.1g 製造実施例4の粉末柿渋製剤 1g 水 20g
Blending Example 2 A candy containing a persimmon astringent formulation was produced according to a conventional method. Granulated sugar 65 g Enzymatic saccharified starch syrup 35 g Cyclodextrin 0.5 g Flavor 0.1 g Powder persimmon astringent preparation of Example 4 1 g Water 20 g

【0030】配合実施例3 常法に従い、柿渋製剤入り
チューインガムを製造した。 チューインガムベース 20g グラニュー糖 50g 水飴 15g 軟化剤 5g 香料 0.1g 製造実施例2の粉末柿渋製剤 1g
Formulation Example 3 A chewing gum containing a persimmon astringent formulation was produced according to a conventional method. Chewing gum base 20 g granulated sugar 50 g starch syrup 15 g softening agent 5 g flavoring 0.1 g powdered persimmon astringent preparation of Example 2 1 g

【0031】[0031]

【発明の効果】本発明により、柿渋特有の渋み、収斂味
が改善された柿渋製剤が提供され、それにより従来より
広い範囲の食品に利用することが可能となった。
According to the present invention, a persimmon astringent preparation with improved astringency and astringency specific to persimmon astringent is provided, thereby making it possible to use it in a wider range of foods than before.

Claims (2)

【特許請求の範囲】[Claims] 【請求項1】分子量が1000〜2000のデンプン加
水分解物と柿渋を混合溶解した後、乾燥することを特徴
とする柿渋の呈味を改善する方法。
1. A method for improving the taste of persimmon astringent, comprising mixing and dissolving a starch hydrolyzate having a molecular weight of 1,000 to 2,000 with persimmon astringent, followed by drying.
【請求項2】柿渋に対して、分子量が1000〜200
0のデンプン加水分解物10重量%以上を混合溶解した
後、乾燥してなる呈味改善柿渋製剤。 【0001】
2. The persimmon astringent has a molecular weight of 1,000 to 200.
No. 0 starch hydrolyzate of 10% by weight or more is mixed and dried, and then dried to improve taste. [0001]
JP31866499A 1999-10-05 1999-10-05 Method for improving gustatoriness and gustatoriness- improved persimmon juice preparation Pending JP2001103918A (en)

Priority Applications (1)

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Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
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Publications (1)

Publication Number Publication Date
JP2001103918A true JP2001103918A (en) 2001-04-17

Family

ID=18101666

Family Applications (1)

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Country Status (1)

Country Link
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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2001112417A (en) * 1999-10-14 2001-04-24 Ezaki Glico Co Ltd Tablet candy
JP2008118933A (en) * 2006-11-13 2008-05-29 Taiyo Kagaku Co Ltd Polyphenol composition
JP2009142267A (en) * 2007-11-19 2009-07-02 Bio I Kk Method for powdering plant subjected to unicellular treatment
JP2010227068A (en) * 2009-03-30 2010-10-14 Fukushima Prefecture Method for removing astringency from persimmon

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2001112417A (en) * 1999-10-14 2001-04-24 Ezaki Glico Co Ltd Tablet candy
JP2008118933A (en) * 2006-11-13 2008-05-29 Taiyo Kagaku Co Ltd Polyphenol composition
JP2009142267A (en) * 2007-11-19 2009-07-02 Bio I Kk Method for powdering plant subjected to unicellular treatment
JP2010227068A (en) * 2009-03-30 2010-10-14 Fukushima Prefecture Method for removing astringency from persimmon

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