JP2001078705A - Production of tangle extract seasoning with good scent and flavor - Google Patents

Production of tangle extract seasoning with good scent and flavor

Info

Publication number
JP2001078705A
JP2001078705A JP25743199A JP25743199A JP2001078705A JP 2001078705 A JP2001078705 A JP 2001078705A JP 25743199 A JP25743199 A JP 25743199A JP 25743199 A JP25743199 A JP 25743199A JP 2001078705 A JP2001078705 A JP 2001078705A
Authority
JP
Japan
Prior art keywords
kelp
flavor
alcohol
seasoning
aroma
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP25743199A
Other languages
Japanese (ja)
Inventor
Motohisa Kuroda
素央 黒田
Fumihiko Odajima
文彦 小田嶋
Wataru Nosaka
亙 野坂
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ajinomoto Co Inc
Original Assignee
Ajinomoto Co Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ajinomoto Co Inc filed Critical Ajinomoto Co Inc
Priority to JP25743199A priority Critical patent/JP2001078705A/en
Publication of JP2001078705A publication Critical patent/JP2001078705A/en
Pending legal-status Critical Current

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  • Edible Seaweed (AREA)
  • Seasonings (AREA)

Abstract

PROBLEM TO BE SOLVED: To provide a method for producing a seasoning capable of reproducing the gustatoriness, scent and flavor each inherent in tangle. SOLUTION: This method for producing a seasoning comprises the following steps: soaking tangle powders with a hydrous alcohol followed by washing the resultant hydrous alcohol with carbon dioxide liquefied or in a subcritical state to collect the flavor ingredients from the hydrous alcohol; and then mixing the flavor ingredients with an extract liquid (or its concentrate) obtained by subjecting the residues left after collecting the flavor ingredients to hot water extraction.

Description

【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【0001】[0001]

【発明の属する技術分野】本発明は、昆布の呈味、香り
および風味を良好に再現する調味料の製造方法に関す
る。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a method for producing a seasoning which reproduces the taste, aroma and flavor of kelp well.

【0002】[0002]

【従来の技術】昆布などから香気成分を抽出する方法と
しては、抽出溶媒を昆布類に接触させることにより、香
気を抽出する方法が知られている。ここで、抽出溶媒と
して、水、アルコールを用いる方法が知られている。水
による抽出の場合には、香気成分の水への溶解性が低い
ために、香気成分の回収率が低く、また、抽出の際に加
熱を必要とするために、加熱により香気成分が失われて
しまうという欠点がある。また、アルコールによる抽出
の場合には、昆布など香気成分のうちで良い香りを有す
る芳香性の成分がアルコールへの可能性を有するため、
かかる芳香性の成分を効率良く抽出できる点で優れてい
る。しかし、抽出の際に多量のアルコールを必要とする
ために、抽出処理の最終段階においてアルコールを除去
しなければならず、この際に香気成分も失われてしまう
という欠点を有している。
2. Description of the Related Art As a method for extracting an aroma component from kelp or the like, a method of extracting an aroma by bringing an extraction solvent into contact with kelp is known. Here, a method using water or alcohol as an extraction solvent is known. In the case of extraction with water, the recovery rate of the fragrance component is low because the solubility of the fragrance component in water is low, and the fragrance component is lost by heating because heating is required during the extraction. There is a disadvantage that it will. In addition, in the case of extraction with alcohol, among aromatic components such as kelp, an aromatic component having a good scent has a possibility to alcohol,
It is excellent in that such aromatic components can be efficiently extracted. However, since a large amount of alcohol is required for the extraction, the alcohol must be removed at the final stage of the extraction process, and at this time, there is a disadvantage that the fragrance component is lost.

【0003】[0003]

【発明が解決しようとする課題】前項記載の従来技術の
背景下に、本発明は、昆布の呈味、香りおよび風味を良
好に再現する調味料の製造方法を提供することを目的と
する。
SUMMARY OF THE INVENTION Under the background of the prior art described in the preceding paragraph, an object of the present invention is to provide a method for producing a seasoning which reproduces the taste, aroma and flavor of kelp well.

【0004】[0004]

【課題を解決するための手段】本発明者は、上記課題の
解決につき鋭意工夫を重ねた結果、昆布粉末を含水アル
コールに含浸させた後、香気成分を含む含水アルコール
を液体、亜臨界状態または超臨界状態の二酸化炭素によ
り洗浄・回収して香気成分と、香気成分回収工程後の残
さについて、熱水抽出を行うことによって得られた抽出
液またはその濃縮液を、前述の香気成分と混合すること
によって、昆布の呈味、香りおよび風味を良好に再現す
る調味料を得ることが可能で有ることを見い出し、本発
明を完成するに至った。
Means for Solving the Problems As a result of diligent efforts to solve the above-mentioned problems, the present inventor impregnated kelp powder with hydroalcohol, and then converted the hydroalcohol containing an aroma component into a liquid, subcritical state or The fragrance component is washed and recovered with carbon dioxide in a supercritical state, and the residue after the fragrance component recovery step is mixed with an extract obtained by performing hot water extraction or a concentrate thereof with the above-described fragrance component. As a result, the present inventors have found that it is possible to obtain a seasoning which can reproduce the taste, aroma and flavor of kelp satisfactorily, and have completed the present invention.

【0005】[0005]

【発明の実施の形態】本発明に用いる昆布類は、真昆
布、日高昆布、利尻昆布などであり、これらを単独、あ
るいは2種類以上組み合わせて使用することも可能であ
る。ここで、昆布は、アルコールに接触する面積を可能
な限り大きくして、より多量の香気成分を抽出できるよ
うにするため、細かく粉砕することが望ましい。
BEST MODE FOR CARRYING OUT THE INVENTION The kelp used in the present invention is Shin kelp, Hidaka kelp, Rishiri kelp and the like, and these can be used alone or in combination of two or more. Here, the kelp is desirably finely pulverized in order to make the area in contact with alcohol as large as possible so that a larger amount of aroma components can be extracted.

【0006】含水アルコールは、15〜95重量%のア
ルコールを含むものが使用されるが、香気成分の回収量
と抽出物の着色度の観点から、25〜75%であること
が望ましい。用いる含水アルコール中のアルコール濃度
については、抽出の対象となる昆布の種類によって異な
るが、事前のトライアルによって容易に設定することが
可能である。
As the hydrous alcohol, one containing 15 to 95% by weight of alcohol is used, and from the viewpoint of the recovery amount of the flavor component and the degree of coloring of the extract, it is desirably 25 to 75%. The alcohol concentration in the aqueous alcohol used varies depending on the type of kelp to be extracted, but can be easily set by a preliminary trial.

【0007】香気成分の抽出は、上記原料昆布を含水ア
ルコールと混合して、香気成分をアルコール中に抽出し
た後、該香気成分を含む含水アルコールを液体、亜臨界
または超臨界状態にある二酸化炭素と接触することによ
り、含水アルコール中の香気成分を洗浄、回収すること
により行う。抽出および洗浄・回収にてエキス抽出物を
得た後に、得られる残さから呈味成分を得るために熱水
抽出を行う。この時の条件は、使用する昆布によって異
なるが、通常は85〜100°C、15〜60分間の抽
出を行うことが望ましい。このようにして得られた熱水
抽出液をそのままでも用いることも可能であるが、調味
料の重量当りの香り・風味の力価を高くするためには、
濃縮を行うのが望ましい。濃縮操作は、工程中の褐変反
応を抑制するために、減圧濃縮あるいは逆浸透膜濃縮を
行うことが望ましい。
The fragrance component is extracted by mixing the raw material kelp with a hydroalcoholic solvent, extracting the fragrance component into the alcohol, and then removing the hydroalcohol containing the fragrance component from the liquid, subcritical or supercritical carbon dioxide. By contacting with water to wash and recover the fragrance component in the hydroalcoholic alcohol. After obtaining an extract extract by extraction, washing and recovery, hot water extraction is performed to obtain a taste component from the obtained residue. The conditions at this time vary depending on the kelp used, but it is usually desirable to perform extraction at 85 to 100 ° C. for 15 to 60 minutes. Although the hot water extract obtained in this way can be used as it is, in order to increase the fragrance / flavor titer per weight of the seasoning,
It is desirable to carry out concentration. In the concentration operation, in order to suppress the browning reaction in the process, it is desirable to perform vacuum concentration or reverse osmosis membrane concentration.

【0008】このようにして得られた、熱水抽出物液ま
たは濃縮液を、アルコール浸漬、液体、亜臨界または超
臨界二酸化炭素による洗浄、回収処理によって得られた
多量の香気成分を含む抽出物と混合することにより、昆
布の呈味、香りおよび風味を良好に再現する調味料を得
ることが可能である。
[0008] The extract containing a large amount of aroma components obtained by subjecting the hot water extract solution or the concentrated solution obtained as described above to alcohol immersion, washing with a liquid, subcritical or supercritical carbon dioxide, and recovery treatment. By mixing with, it is possible to obtain a seasoning that satisfactorily reproduces the taste, aroma and flavor of kelp.

【0009】以下に、本発明の実施形態を実施例にて説
明する。
Hereinafter, embodiments of the present invention will be described with reference to examples.

【0010】[0010]

【実施例1】昆布粉末(真昆布を粉砕したもの、平均粒
子径=450μm)2kgを50%(w/w)アルコー
ル水溶液1.2kgに25°C条件にて3時間浸漬させ
た後、香気成分を含む含水アルコールを液二酸化炭素
により洗浄・回収を行った。この時の条件は、25°
C、65気圧であり、2時間放置した後に、二酸化炭素
を気化させた。このときに得られた抽出液の重量は78
5gであった。この香気成分回収工程後の残さに、95
°Cの水8kgを加えて、95°C条件下で30分間の
抽出を行った(攪拌条件)。熱水抽出後、濾過により固
液分離を行い、逆浸透膜(日東電工社製、NTR−75
9HG)を用いた濃縮(液温45°C)を行い、固形分
20%の濃縮液1.6kgを得た。このようにして得ら
れた濃縮液と含水アルコール浸漬と二酸化炭素による洗
浄によって得られた抽出液とを混合させて本発明の調味
料2355gを得た。このようにして得られた、昆布エ
キス調味料をうどんつゆ(表1にうどんつゆの配合表を
示した)に添加して、専門パネル20名による官能評価
を行った。表2に評価結果を示した。表に示したよう
に、本発明の調味料は、有意に昆布の香り、風味を増強
するものであった。
Example 1 2 kg of kelp powder (pulverized true kelp, average particle size = 450 μm) was immersed in 1.2 kg of a 50% (w / w) alcohol aqueous solution at 25 ° C. for 3 hours, and then the odor was increased. the hydrous alcohol containing component was washed, recovered by the liquid body carbon dioxide. The condition at this time is 25 °
C, 65 atm. After standing for 2 hours, carbon dioxide was vaporized. The weight of the extract obtained at this time was 78
It was 5 g. 95% of the residue after this fragrance component recovery step
8 kg of water at 0 ° C was added, and extraction was performed for 30 minutes at 95 ° C (stirring conditions). After hot water extraction, solid-liquid separation was performed by filtration, and a reverse osmosis membrane (NTR-75, manufactured by Nitto Denko Corporation) was used.
9HG) (liquid temperature: 45 ° C.) to obtain 1.6 kg of a concentrated liquid having a solid content of 20%. The concentrated solution thus obtained was mixed with the extract obtained by immersion in aqueous alcohol and washing with carbon dioxide to obtain 2355 g of the seasoning of the present invention. The thus-obtained kelp extract seasoning was added to udon soup (the composition table of udon soup is shown in Table 1), and sensory evaluation was performed by 20 specialized panels. Table 2 shows the evaluation results. As shown in the table, the seasoning of the present invention significantly enhanced the aroma and flavor of kelp.

【0011】[0011]

【表1】 [Table 1]

【0012】[0012]

【表2】 [Table 2]

【0013】[0013]

【実施例2】昆布粉末(日高昆布を粉砕したもの、平均
粒子径=500μm)2kgを65%(w/w)アルコ
ール水溶液1.2kgに25°C条件にて3時間浸漬さ
せた後、香気成分を含む含水アルコールを液二酸化炭
素により洗浄・回収を行った。この時の条件は、25°
C、65気圧であり、2時間放置した後に、二酸化炭素
を気化させた。このときに得られた抽出液の重量は89
5gであった。この香気成分回収工程後の残さに、95
°Cの水8kgを加えて、95°C条件下で30分間の
抽出を行った(攪拌条件)。熱水抽出後、濾過により固
液分離を行い、減圧濃縮(液温45°C)を行い、固形
分30%の濃縮液1.1kgを得た。このようにして得
られた濃縮液と含水アルコール浸漬と二酸化炭素による
洗浄によって得られた抽出液とを混合させて本発明の調
味料1995gを得た。このようにして得られた、昆布
エキス調味料をうどんつゆ(表1の配合)に添加して、
専門パネル20名による官能評価を行った。表3に評価
結果を示した。表に示したように、本発明の調味料は、
有意に昆布の香り、風味を増強するものであった。
Example 2 2 kg of kelp powder (crushed Hidaka kelp, average particle size = 500 μm) was immersed in 1.2 kg of a 65% (w / w) alcohol aqueous solution at 25 ° C. for 3 hours. the hydrous alcohol containing aroma component was washed, recovered by the liquid body carbon dioxide. The condition at this time is 25 °
C, 65 atm. After standing for 2 hours, carbon dioxide was vaporized. The weight of the extract obtained at this time was 89
It was 5 g. 95% of the residue after this fragrance component recovery step
8 kg of water at 0 ° C was added, and extraction was performed for 30 minutes at 95 ° C (stirring conditions). After hot water extraction, solid-liquid separation was performed by filtration, and concentration under reduced pressure (liquid temperature 45 ° C) was performed to obtain 1.1 kg of a concentrated liquid having a solid content of 30%. The concentrate thus obtained was mixed with an extract obtained by immersion in aqueous alcohol and washing with carbon dioxide to obtain 1995 g of the seasoning of the present invention. Add the kelp extract seasoning thus obtained to the udon soup (combination in Table 1),
Sensory evaluation was performed by 20 specialized panels. Table 3 shows the evaluation results. As shown in the table, the seasoning of the present invention,
It significantly enhanced the aroma and flavor of kelp.

【0014】[0014]

【表3】 [Table 3]

【0015】[0015]

【発明の効果】以上に示したように、昆布粉末を含水ア
ルコールに含浸させた後、香気成分を含む含水アルコー
ルを液体、亜臨界状態または超臨界状態の二酸化炭素に
より洗浄・回収して得られた香気成分と、香気成分回収
工程後の残さについて、熱水抽出を行うことによって得
られた抽出液またはその濃縮液と混合することによっ
て、昆布の呈味、香りおよび風味を良好に再現する調味
料を得ることが可能である。
As described above, after the impregnated kelp powder is impregnated with hydrated alcohol, the hydrated alcohol containing fragrance components is washed and recovered with liquid, subcritical or supercritical carbon dioxide. The flavor and the residue after the aroma component recovery process are mixed with the extract obtained by performing hot water extraction or its concentrated solution to create a flavor that reproduces the taste, aroma and flavor of kelp well. It is possible to get a fee.

Claims (3)

【特許請求の範囲】[Claims] 【請求項1】 含水アルコールにより昆布粉末から香気
を抽出する方法において、昆布粉末を含水アルコールに
含浸させて得た香気成分を含む含水アルコールを液体、
亜臨界状態または超臨界状態の二酸化炭素により洗浄・
回収することを特徴とする昆布から香気を抽出する方法
および得られた香気成分を含有してなる調味料の製造方
法。
1. A method for extracting a fragrance from kelp powder with hydrated alcohol, wherein the hydrated alcohol containing a fragrance component obtained by impregnating the kelp powder with the hydrated alcohol is used as a liquid,
Cleaning with subcritical or supercritical carbon dioxide
A method for extracting a fragrance from kelp and a method for producing a seasoning containing the obtained fragrance component.
【請求項2】 含水アルコール中のアルコールの濃度
が、15〜95%(重量%)であることを特徴とする、
請求項1に示した、調味料の製造方法。
2. The method according to claim 1, wherein the concentration of the alcohol in the hydrous alcohol is 15 to 95% (% by weight).
The method for producing a seasoning according to claim 1.
【請求項3】 請求項1に記載した香気成分回収工程後
の残さに対し熱水抽出を行うことによって得られた呈味
成分を含む抽出液またはその濃縮液を、請求項1で得ら
れた香気成分と混合することを特徴とする、昆布の呈
味、香りおよび風味を良好に再現する調味料の製造方
法。
3. An extract containing a taste component obtained by performing hot water extraction on the residue after the aroma component recovery step described in claim 1 or a concentrate thereof is obtained in claim 1. A method for producing a seasoning which satisfactorily reproduces the taste, aroma and flavor of kelp, which is mixed with an aroma component.
JP25743199A 1999-09-10 1999-09-10 Production of tangle extract seasoning with good scent and flavor Pending JP2001078705A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP25743199A JP2001078705A (en) 1999-09-10 1999-09-10 Production of tangle extract seasoning with good scent and flavor

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP25743199A JP2001078705A (en) 1999-09-10 1999-09-10 Production of tangle extract seasoning with good scent and flavor

Publications (1)

Publication Number Publication Date
JP2001078705A true JP2001078705A (en) 2001-03-27

Family

ID=17306279

Family Applications (1)

Application Number Title Priority Date Filing Date
JP25743199A Pending JP2001078705A (en) 1999-09-10 1999-09-10 Production of tangle extract seasoning with good scent and flavor

Country Status (1)

Country Link
JP (1) JP2001078705A (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2005213327A (en) * 2004-01-28 2005-08-11 Japan Research & Development Association For New Functional Foods Vegetable essential oil, manufacturing method therefor and method for manufacturing thymol
EP2555638A1 (en) * 2010-04-08 2013-02-13 Takasago International Corporation Salty taste enhancer and kelp extract comprising the same
JP2014507502A (en) * 2010-12-23 2014-03-27 チャラボット Method for obtaining fresh flower and / or leaf aroma extracts using natural solvents
WO2015182144A1 (en) * 2014-05-30 2015-12-03 株式会社明治 Japanese-style-flavor enhancer and retort odor masking agent
JP5917763B1 (en) * 2015-12-22 2016-05-18 株式会社Mizkan Holdings Liquid seasoning and method for producing the same

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2005213327A (en) * 2004-01-28 2005-08-11 Japan Research & Development Association For New Functional Foods Vegetable essential oil, manufacturing method therefor and method for manufacturing thymol
JP4666923B2 (en) * 2004-01-28 2011-04-06 ニューフード・クリエーション技術研究組合 Method for producing Hosobayamajiso essential oil and method for producing thymol
EP2555638A1 (en) * 2010-04-08 2013-02-13 Takasago International Corporation Salty taste enhancer and kelp extract comprising the same
EP2555638A4 (en) * 2010-04-08 2014-11-12 Takasago Perfumery Co Ltd Salty taste enhancer and kelp extract comprising the same
JP2014507502A (en) * 2010-12-23 2014-03-27 チャラボット Method for obtaining fresh flower and / or leaf aroma extracts using natural solvents
JP2017088894A (en) * 2010-12-23 2017-05-25 チャラボット Method for obtaining scented extract of fresh flowers and/or leaves using natural solvent
WO2015182144A1 (en) * 2014-05-30 2015-12-03 株式会社明治 Japanese-style-flavor enhancer and retort odor masking agent
JPWO2015182144A1 (en) * 2014-05-30 2017-04-20 株式会社明治 Japanese flavor enhancer and retort odor masking agent
JP5917763B1 (en) * 2015-12-22 2016-05-18 株式会社Mizkan Holdings Liquid seasoning and method for producing the same
JP2017112864A (en) * 2015-12-22 2017-06-29 株式会社Mizkan Holdings Liquid seasoning and manufacturing method therefor

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