JP2001058840A - Method for smoothing surface of optical fiber preform - Google Patents

Method for smoothing surface of optical fiber preform

Info

Publication number
JP2001058840A
JP2001058840A JP11232319A JP23231999A JP2001058840A JP 2001058840 A JP2001058840 A JP 2001058840A JP 11232319 A JP11232319 A JP 11232319A JP 23231999 A JP23231999 A JP 23231999A JP 2001058840 A JP2001058840 A JP 2001058840A
Authority
JP
Japan
Prior art keywords
glass
optical fiber
preform
fiber preform
glass material
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP11232319A
Other languages
Japanese (ja)
Inventor
Takeshi Hachiman
健 八幡
Tadakatsu Shimada
忠克 島田
Hideo Hirasawa
秀夫 平沢
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shin Etsu Chemical Co Ltd
Original Assignee
Shin Etsu Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shin Etsu Chemical Co Ltd filed Critical Shin Etsu Chemical Co Ltd
Priority to JP11232319A priority Critical patent/JP2001058840A/en
Publication of JP2001058840A publication Critical patent/JP2001058840A/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B37/00Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
    • C03B37/01Manufacture of glass fibres or filaments
    • C03B37/012Manufacture of preforms for drawing fibres or filaments
    • C03B37/01205Manufacture of preforms for drawing fibres or filaments starting from tubes, rods, fibres or filaments
    • C03B37/01225Means for changing or stabilising the shape, e.g. diameter, of tubes or rods in general, e.g. collapsing

Abstract

PROBLEM TO BE SOLVED: To provide a method for smoothing the surface of an optical fiber preform, by which the breakage of the optical fiber preform can be prevented when drawn, by covering and fusing the surface uneven portion of the optical fiber preform produced from quartz glass with a glass material having the same quality as the surface glass of the preform, thus burying the uneven portion. SOLUTION: Glass particles produced by the supply of a glass raw material gas to an oxyhydrogen flame burner are sequentially accumulated on a starting rod by a VAD method, and then passed through a heating oven to obtain the sintered optical fiber preform 1. A concave portion 2 such as a flaw or a recess or a convex portion such as a projection exits on the surface of the preform 1. A plate-like glass material 3 is melted and simultaneously fused to the concave portion 2 with the oxyhydrogen flame 4 of a burner 5. Thus, the concave portion 2 is wholly covered and buried with the glass material 3 to smooth the surface of the preform 1. On the other hand, when the glass material 3 is fused over a wide range around a convex portion, the convex portion is buried in a slope covered with the glass material 3 to smooth the surface of the preform 1.

Description

【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【0001】[0001]

【発明の属する技術分野】本発明は、光ファイバの原材
料となる光ファイバプリフォームの表面の凹凸を簡便か
つ確実に平滑化する方法に関するものである。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a method for simply and surely smoothing out irregularities on the surface of an optical fiber preform which is a raw material of an optical fiber.

【0002】[0002]

【従来の技術】光ファイバプリフォームは、気相軸付け
法(VAD法)等により酸水素火炎バーナから供給され
るガラス微粒子を堆積させた後、焼結させて透明ガラス
化したものである。これを所定径に延伸し、線引きする
と光ファイバが得られる。
2. Description of the Related Art An optical fiber preform is formed by depositing glass fine particles supplied from an oxyhydrogen flame burner by a vapor phase axial method (VAD method) or the like, and then sintering the glass fine particles into a transparent glass. This is stretched to a predetermined diameter and drawn to obtain an optical fiber.

【0003】光ファイバプリフォームの表面の局所に傷
やへこみ、または突起等の凹凸部があると、プリフォー
ムの線引きの際に断線が発生してしまう。プリフォーム
が、凸凹差で500μmを超える深い傷等を有している
と、図3に示すように、線引きの際の断線率が急増し、
生産効率が低下してしまう。
If the surface of the optical fiber preform has an uneven portion such as a scratch, a dent, or a projection, the preform will be broken when the preform is drawn. When the preform has a deep flaw or the like exceeding 500 μm in unevenness, as shown in FIG. 3, the disconnection rate at the time of drawing sharply increases,
Production efficiency decreases.

【0004】そこで従来、プリフォームには表面に円筒
研削や火炎研磨を施していた。この方法では、微小な傷
や突起は除去できるものの、凹凸差の大きな傷等は除去
できないため、線引きの際に断線が頻発し生産効率が悪
いうえ、高速で線引きができないという問題を有してい
た。
Conventionally, the surface of the preform has been subjected to cylindrical grinding or flame polishing. In this method, although fine scratches and projections can be removed, scratches with a large difference in unevenness cannot be removed, so that there is a problem that disconnection frequently occurs at the time of wire drawing, production efficiency is poor, and wire drawing cannot be performed at high speed. Was.

【0005】[0005]

【発明が解決しようとする課題】本発明は前記の課題を
解決するためなされたもので、線引きの際に断線を起こ
さないように、光ファイバプリフォームの表面を平滑化
する方法を提供することを目的とする。
SUMMARY OF THE INVENTION The present invention has been made to solve the above-mentioned problems, and it is an object of the present invention to provide a method for smoothing the surface of an optical fiber preform so as not to cause disconnection during drawing. With the goal.

【0006】[0006]

【課題を解決するための手段】前記の目的を達成するた
めになされた本発明の光ファイバプリフォーム表面の平
滑化方法は、実施例に対応する図1を参照して説明する
と、石英ガラス製の光ファイバプリフォーム1の表面の
凹凸部2を覆ってプリフォーム1の表面のガラスと同質
なガラス素材3を融着させ、凹凸部2を埋没させること
により、プリフォーム1の表面を平滑化するというもの
である。
A method for smoothing the surface of an optical fiber preform according to the present invention, which has been made to achieve the above object, will be described with reference to FIG. The glass material 3 having the same quality as the glass on the surface of the preform 1 is fused by covering the uneven portion 2 on the surface of the optical fiber preform 1, and the surface of the preform 1 is smoothed by burying the uneven portion 2. It is to do.

【0007】傷やへこみである凹部2は、図1に示すよ
うにガラス素材3で覆われることにより、凹部2近傍の
プリフォーム1の表面に対し平滑となる。突起である凸
部6は、図2に示すように突起6の周囲にガラス素材を
融着させて広範囲に形成された裾野7で覆われることに
より、プリフォーム1の表面に対し平滑となる。
[0007] As shown in FIG. 1, the concave portion 2, which is a scratch or a dent, becomes smooth with respect to the surface of the preform 1 near the concave portion 2 by being covered with the glass material 3. As shown in FIG. 2, the projections 6 serving as projections are covered with a foot 7 formed over a wide area by fusing a glass material around the projections 6, so that the surface of the preform 1 becomes smooth.

【0008】ガラス素材を融着させるにはガラスの溶融
温度である約2000℃以上に加熱することによって達
成することができる。
The fusion of the glass material can be achieved by heating the glass material to a temperature of about 2000 ° C. or higher, which is the melting temperature of the glass.

【0009】ガラス素材を融着させた後、表面研磨して
もよい。表面研磨は、円筒研削であってもよく、火炎研
磨であってもよい。ガラス素材の融着によりプリフォー
ム表面に新たに生じた微小な凹凸部は表面研磨により除
去されるので、プリフォーム1の表面は一層平滑化され
る。
After fusing the glass material, the surface may be polished. The surface polishing may be cylindrical grinding or flame polishing. Fine irregularities newly formed on the preform surface due to fusion of the glass material are removed by surface polishing, so that the surface of the preform 1 is further smoothed.

【0010】ガラス素材3は、塊状、板状、または粉状
のガラスであることが好ましい。塊状または板状のガラ
スを凹凸部に接触させつつバーナで加熱溶融させ凹凸部
を覆って融着させることにより好適に実施することがで
きる。粉状のガラスを凹凸部を覆って盛り、加熱炉を通
過させ溶融させることによっても実施することができ
る。
The glass material 3 is preferably a lump, plate, or powder glass. This can be suitably performed by bringing the block-shaped or plate-shaped glass into contact with the irregularities and heating and melting it with a burner to cover and fuse the irregularities. It can also be carried out by putting powdery glass over the uneven portion and passing it through a heating furnace to melt it.

【0011】ガラス素材3は酸水素火炎バーナから供給
されるガラス微粒子であってもよい。このガラス微粒子
は、焼結されると同時に融着がされる。焼結は、加熱炉
を通過させることによって行われる。
The glass material 3 may be glass fine particles supplied from an oxyhydrogen flame burner. The glass fine particles are sintered and fused at the same time. Sintering is performed by passing through a heating furnace.

【0012】本発明の光ファイバプリフォームは、石英
ガラス製の光ファイバプリフォームの表面の凹凸部が、
該表面のガラスと同質なガラス素材の融着により埋没さ
れ、平滑化している。
In the optical fiber preform of the present invention, the irregularities on the surface of the optical fiber preform made of quartz glass are:
It is buried and smoothed by fusing a glass material of the same quality as the glass on the surface.

【0013】光ファイバプリフォームは、石英ガラス製
の光ファイバプリフォームの表面の凹凸部の最大の凹凸
差が500μm以下であることが好ましい。500μm
を超えると、線引きの際に断線率が急激に増加してしま
う。
[0013] In the optical fiber preform, it is preferable that the maximum unevenness difference of the uneven portion on the surface of the optical fiber preform made of quartz glass is 500 µm or less. 500 μm
If it exceeds, the disconnection rate will increase sharply during drawing.

【0014】この光ファイバプリフォームは線引きの際
に断線しないため、線引きして光ファイバを製造する際
の生産性が高い。
Since this optical fiber preform does not break at the time of drawing, the productivity in producing an optical fiber by drawing is high.

【0015】[0015]

【実施例】以下、本発明の実施例を詳細に説明する。図
1に、本発明を適用する光ファイバプリフォーム表面の
平滑化方法の実施例の概要図を示す。
Embodiments of the present invention will be described below in detail. FIG. 1 is a schematic diagram showing an embodiment of a method for smoothing the surface of an optical fiber preform to which the present invention is applied.

【0016】この平滑化方法は、光ファイバプリフォー
ム1の表面の凸凹部に、表面のガラスと同質なガラス素
材を融着させるものである。
In this smoothing method, a glass material of the same quality as the glass on the surface is fused to the concave and convex portions on the surface of the optical fiber preform 1.

【0017】先ず、VAD法により酸水素火炎バーナに
ガラス原料ガスを供給して生成したガラス微粒子を始発
棒に順次堆積させた後、加熱炉を通過させて焼結させ、
光ファイバプリフォーム1を得る。このプリフォームの
表面には、少なからず傷やへこみである凹部2、突起で
ある凸部6(図2参照)を有している。
First, glass fine particles generated by supplying a glass raw material gas to an oxyhydrogen flame burner by the VAD method are sequentially deposited on a starting rod, and then sintered by passing through a heating furnace.
An optical fiber preform 1 is obtained. On the surface of this preform, there are a concave portion 2 which is a scratch or a dent, and a convex portion 6 which is a projection (see FIG. 2).

【0018】へこみ2を平滑化するために、バーナ5の
酸水素火炎4により板状のガラス素材3を溶融させつ
つ、へこみ2に融着させる。へこみ2はガラス素材3で
覆われる。へこみ2の全体がガラス素材3で覆われて埋
没されると、プリフォームの表面は平滑化する。なお、
ガラス素材3は、へこみ2の深さと同じ厚さの板状のガ
ラスを融着させてへこみ2を埋めてもよく、へこみ2の
深さより薄い厚さの板状のガラスの複数枚を融着させて
へこみ2を平滑化していてもよい。
In order to smooth the dent 2, the plate-like glass material 3 is melted by the oxyhydrogen flame 4 of the burner 5 and fused to the dent 2. The dent 2 is covered with a glass material 3. When the entire dent 2 is covered with the glass material 3 and buried, the surface of the preform is smoothed. In addition,
The glass material 3 may fill the dent 2 by fusing a plate-like glass having the same thickness as the depth of the dent 2, and fusing a plurality of plate-like glasses having a thickness smaller than the depth of the dent 2. The dents 2 may be smoothed.

【0019】一方、突起6を平滑化するために、酸水素
火炎によりガラス素材を溶融させ、突起6の周囲の広範
囲に渡ってガラス素材を融着させる。突起6がガラス素
材で覆われた裾野7に埋没されると、プリフォームの表
面は平滑化する。
On the other hand, in order to smooth the projections 6, the glass material is melted by an oxyhydrogen flame, and the glass material is fused over a wide area around the projections 6. When the protrusion 6 is buried in the foot 7 covered with the glass material, the surface of the preform is smoothed.

【0020】平滑化したプリフォーム表面に、円筒研削
および火炎研磨を施し、一層滑らかにする。なお、融着
後、鏝で整形した後、円筒研削や火炎研磨を施してもよ
い。
The surface of the smoothed preform is subjected to cylindrical grinding and flame polishing to make it even smoother. After fusion, after shaping with a trowel, cylindrical grinding or flame polishing may be performed.

【0021】前記実施例にしたがい、プリフォームの表
面の凹凸部を平滑化した例を示す。外径61.6mm
φ、長さ880mmの石英ガラス光ファイバープリフォ
ームを試作したところ、表面に950μmの局部的なへ
こみを有していた。プリフォーム表面のガラスと同質で
板状の石英ガラスを酸水素火炎バーナーにより溶融した
後、へこみに融着させてプリフォーム表面を平滑化し
た。さらにその表面を円筒研削した後、ガラス旋盤を用
いて火炎研磨し、プリフォーム表面をより一層平滑化し
たところ、凹凸のないプリフォームが得られた。このプ
リフォームを用いて、100m/分の速度で線引きを行
ったところ、断線は起きなかった。
An example in which the irregularities on the surface of the preform are smoothed according to the above embodiment will be described. Outer diameter 61.6mm
When a quartz glass optical fiber preform having a length of φ and a length of 880 mm was experimentally produced, the surface had a local dent of 950 μm. A plate-like quartz glass having the same quality as the glass on the surface of the preform was melted by an oxyhydrogen flame burner, and then fused to the dent to smooth the surface of the preform. Further, the surface of the preform was subjected to flame grinding using a glass lathe after cylindrical grinding, and the preform surface was further smoothed. As a result, a preform without irregularities was obtained. When wire drawing was performed at a speed of 100 m / min using this preform, no breakage occurred.

【0022】[0022]

【発明の効果】以上、詳細に説明したように本発明の光
ファイバプリフォーム表面の平滑化方法によれば、光フ
ァイバプリフォームは簡便かつ確実に平滑化できるの
で、生産効率がよい。得られる光ファイバは、引張強度
が強いため線引きの際に断線することがなく、高速で線
引きすることができる。
As described above in detail, according to the method for smoothing the surface of an optical fiber preform of the present invention, the optical fiber preform can be easily and reliably smoothed, so that the production efficiency is high. The resulting optical fiber has a high tensile strength and can be drawn at high speed without breaking during drawing.

【図面の簡単な説明】[Brief description of the drawings]

【図1】本発明を適用する光ファイバプリフォーム表面
の平滑化方法の実施例の実施途中を示す概要図である。
FIG. 1 is a schematic view showing an embodiment of a method for smoothing the surface of an optical fiber preform to which the present invention is applied, in the middle of execution.

【図2】本発明を適用する光ファイバプリフォーム表面
の平滑化方法の別な実施例を示す概要図である。
FIG. 2 is a schematic view showing another embodiment of a method for smoothing the surface of an optical fiber preform to which the present invention is applied.

【図3】光ファイバプリフォーム表面の凹凸差と断線率
との相関を示す図である。
FIG. 3 is a diagram showing a correlation between a difference in irregularities on the surface of an optical fiber preform and a disconnection rate.

【符号の説明】[Explanation of symbols]

1は光ファイバプリフォーム、2は凹部、3はガラス素
材、4は酸水素火炎、5はバーナ、6は凸部、7はガラ
ス素材である。
1 is an optical fiber preform, 2 is a concave portion, 3 is a glass material, 4 is an oxyhydrogen flame, 5 is a burner, 6 is a convex portion, and 7 is a glass material.

───────────────────────────────────────────────────── フロントページの続き (72)発明者 平沢 秀夫 群馬県安中市磯部2丁目13番1号 信越化 学工業株式会社精密機能材料研究所内 Fターム(参考) 4G015 DA01  ────────────────────────────────────────────────── ─── Continuing from the front page (72) Inventor Hideo Hirasawa 2-13-1, Isobe, Annaka-shi, Gunma F-term in the Shin-Etsu Chemical Co., Ltd. Precision Materials Laboratory 4G015 DA01

Claims (6)

【特許請求の範囲】[Claims] 【請求項1】 石英ガラス製の光ファイバプリフォー
ムの表面の凹凸部を覆って該プリフォーム表面のガラス
と同質なガラス素材を融着させ、該凹凸部を埋没させる
ことにより、光ファイバプリフォームの表面を平滑化す
る方法。
An optical fiber preform is formed by fusing a glass material of the same quality as the glass on the surface of the preform by covering the unevenness on the surface of the optical fiber preform made of quartz glass and burying the unevenness. Method to smooth the surface of
【請求項2】 前記融着の後、表面研磨することを特
徴とする請求項1に記載の光ファイバプリフォーム表面
の平滑化方法。
2. The method of claim 1, wherein the surface is polished after the fusion.
【請求項3】 前記ガラス素材が、塊状、板状、また
は粉状のガラスであることを特徴とする請求項1または
2に記載の光ファイバプリフォーム表面の平滑化方法。
3. The method for smoothing the surface of an optical fiber preform according to claim 1, wherein the glass material is a lump, plate, or powder glass.
【請求項4】 前記ガラス素材は酸水素火炎バーナか
ら供給されるガラス微粒子であって、該ガラス微粒子を
焼結することによって前記融着がなされることを特徴と
する請求項1または2に記載の光ファイバプリフォーム
表面の平滑化方法。
4. The glass material according to claim 1, wherein the glass material is glass fine particles supplied from an oxyhydrogen flame burner, and the fusion is performed by sintering the glass fine particles. Method for smoothing the surface of an optical fiber preform.
【請求項5】 石英ガラス製の光ファイバプリフォー
ムの表面の凹凸部が、該表面のガラスと同質なガラス素
材の融着により埋没され、平滑化していることを特徴と
する光ファイバプリフォーム。
5. An optical fiber preform characterized in that the irregularities on the surface of an optical fiber preform made of quartz glass are buried and smoothed by fusing a glass material of the same quality as the glass on the surface.
【請求項6】 石英ガラス製の光ファイバプリフォー
ムの表面の凹凸部の最大の凹凸差が500μm以下であ
ることを特徴とする光ファイバプリフォーム。
6. An optical fiber preform characterized in that the maximum unevenness difference of the unevenness on the surface of the optical fiber preform made of quartz glass is 500 μm or less.
JP11232319A 1999-08-19 1999-08-19 Method for smoothing surface of optical fiber preform Pending JP2001058840A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP11232319A JP2001058840A (en) 1999-08-19 1999-08-19 Method for smoothing surface of optical fiber preform

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP11232319A JP2001058840A (en) 1999-08-19 1999-08-19 Method for smoothing surface of optical fiber preform

Publications (1)

Publication Number Publication Date
JP2001058840A true JP2001058840A (en) 2001-03-06

Family

ID=16937347

Family Applications (1)

Application Number Title Priority Date Filing Date
JP11232319A Pending JP2001058840A (en) 1999-08-19 1999-08-19 Method for smoothing surface of optical fiber preform

Country Status (1)

Country Link
JP (1) JP2001058840A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2011144067A (en) * 2010-01-14 2011-07-28 Dainippon Printing Co Ltd Method for correcting defect part of glass substrate, and photomask

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2011144067A (en) * 2010-01-14 2011-07-28 Dainippon Printing Co Ltd Method for correcting defect part of glass substrate, and photomask

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