JP2000123726A - Processing method for discharge lamp electrode and its device - Google Patents

Processing method for discharge lamp electrode and its device

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Publication number
JP2000123726A
JP2000123726A JP10316846A JP31684698A JP2000123726A JP 2000123726 A JP2000123726 A JP 2000123726A JP 10316846 A JP10316846 A JP 10316846A JP 31684698 A JP31684698 A JP 31684698A JP 2000123726 A JP2000123726 A JP 2000123726A
Authority
JP
Japan
Prior art keywords
discharge lamp
electrode
container
lamp electrode
heating
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP10316846A
Other languages
Japanese (ja)
Inventor
Nobuyuki Yamada
信幸 山田
Koichi Hayashi
浩一 林
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Toto Ltd
Original Assignee
Toto Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Toto Ltd filed Critical Toto Ltd
Priority to JP10316846A priority Critical patent/JP2000123726A/en
Publication of JP2000123726A publication Critical patent/JP2000123726A/en
Pending legal-status Critical Current

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Abstract

PROBLEM TO BE SOLVED: To simply remove impurities such as carbon stuck when electrodes are manufactured by applying high-frequency electromagnetic waves from an electromag netic wave generating device provided around a container to one or more electrodes stored in the container for heating them. SOLUTION: Electromagnetic waves from an electromagnetic wave generating device 3 such as a domestic microwave oven are applied to the inside 2a of a container 2 made of quartz which is a nonconductive material not induction-heated by electromagnetic waves and a discharge lamp electrode 1 made of a conductor and sealed in it for induction heating. When an electric discharge 4 generated from the tip of the discharge lamp electrode 1 is continued for some time, impurities such as carbon are deposited on the inner surface of the quartz container 2 kept at the low- temperature state together with tungsten as deposits 2b. Gases of one or more kinds, e.g., rare gas suck as argon and hydrogen, are preferably sealed at the inside 2a of the quartz container 2 at the prescribed gas pressure, and a discharge phenomenon by electromagnetic induction easily occurs. The impurities contained in the discharge lamp electrode 1 may be deposited on a separately provided member by evaporating them via electromagnetic wave heating.

Description

【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【0001】[0001]

【発明の属する技術分野】本発明は、放電灯用電極製造
時に付着する不純物、特に炭素を簡単に除去し、放電灯
に好適な放電灯用電極を提供する処理装置に関する。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a processing apparatus for easily removing impurities, particularly carbon, adhering during the production of a discharge lamp electrode and providing a discharge lamp electrode suitable for a discharge lamp.

【0002】[0002]

【従来の技術】放電灯用電極材としは、タングステンが
主に使用されている。その生産工程は、バインダーを入
れて粉末プレスし焼結された後、炭素のダイスを用いて
線引きされ、外周面を電解研磨、希望の長さに切断、研
磨加工や先端コイルを取り付けなどの工程を経て放電灯
用のタングステン電極とする。この際、上記生産工程を
経た状態のままで放電灯に組込むと、使用していくにつ
れて放電灯の黒化が早期の段階で起こり、放電灯の短寿
命と光束低下を招いていた。
2. Description of the Related Art Tungsten is mainly used as an electrode material for a discharge lamp. The production process is a process of putting a binder, powder pressing and sintering, drawing using a carbon die, electrolytic polishing the outer peripheral surface, cutting to the desired length, polishing and attaching the tip coil After that, a tungsten electrode for a discharge lamp is obtained. At this time, if the discharge lamp is incorporated into the discharge lamp in the state after the above-mentioned production process, the blackening of the discharge lamp occurs at an early stage as it is used, resulting in a short life of the discharge lamp and a decrease in luminous flux.

【0003】その大きな原因の1つとして、放電灯内に
不純物炭素が混在し、その炭素が、電極のタングステン
と反応し発光管内表面にタングステンカーバイドを付着
させ黒化を起こしていた。炭素は、元々、タングステン
電極の不純物として存在しており、故に、放電灯を組み
立てる前に、不純物除去を目的とし、タングステン電極
の処理を行なっていた。これに対し、従来は、放電灯に
組み込む前のタングステン電極を洗剤で脱脂洗浄し、1
600℃の水素雰囲気の炉内で熱処理し、その後、21
00℃の真空中の炉内で最終熱処理を行うといった処理
方法等を施して対処していた。
One of the major causes is that impurity carbon is mixed in the discharge lamp, and the carbon reacts with tungsten of the electrode to deposit tungsten carbide on the inner surface of the arc tube, causing blackening. Carbon originally exists as an impurity in the tungsten electrode, and therefore, before the discharge lamp is assembled, the tungsten electrode is treated for the purpose of removing impurities. On the other hand, conventionally, a tungsten electrode before being incorporated into a discharge lamp is degreased and washed with a detergent, and
Heat treatment in a furnace in a hydrogen atmosphere at 600 ° C.
A treatment method such as performing a final heat treatment in a furnace at 00 ° C. in a vacuum has been applied.

【0004】[0004]

【発明が解決しようとする課題】しかし、従来技術の処
理方法では、実際の放電灯に組み込まれた状態に比べタ
ングステン電極が経験する温度が低いなどの理由から、
炭素を完全に除去するのは不可能であった。また、高温
を維持する炉等、高度かつ複雑な設備が必要であり、そ
の作業も容易ではなかった。
However, in the conventional processing method, the temperature experienced by the tungsten electrode is lower than that in a state where the tungsten electrode is incorporated in an actual discharge lamp.
It was not possible to completely remove the carbon. In addition, sophisticated and complicated equipment such as a furnace for maintaining a high temperature was required, and the work was not easy.

【0005】本発明は上記課題を解決するためになされ
たもので、放電灯用電極製造時に付着する不純物、特に
炭素を簡単に除去し、放電灯に好適な放電灯用電極を得
ることを可能とする方法および装置を提供することを目
的とする。
SUMMARY OF THE INVENTION The present invention has been made to solve the above problems, and it is possible to easily remove impurities, particularly carbon, adhering during production of a discharge lamp electrode and obtain a discharge lamp electrode suitable for a discharge lamp. It is an object to provide a method and an apparatus.

【0006】[0006]

【課題を解決するための手段】上記目的を達成するた
め、請求項1では、放電灯用電極を内部に少なくとも1
本以上収納する容器からなり、その周囲に電磁波発生装
置を設け、その電磁波発生装置より高周波の電磁波を発
生させ容器内部の放電灯用電極に印加し、放電灯電極を
加熱するようにした。容器内部にある放電灯用電極は、
導体であるがゆえに前記電磁波発生装置から発生される
電磁場波よって誘導加熱の原理に基づいて加熱されると
共に、電磁誘導の原理により、前記容器内部にある放電
灯用電極から前記容器内部に放電現象が生じる。このた
め、本発明での現象状態に置かれた放電灯用電極は、点
灯中の放電灯内部と同じような状態となり、約2500
℃から3000℃の温度で加熱処理されるようになる。
In order to achieve the above object, according to the present invention, at least one electrode for a discharge lamp is provided therein.
An electromagnetic wave generator was provided around the container, and a high-frequency electromagnetic wave was generated from the electromagnetic wave generator and applied to a discharge lamp electrode inside the container to heat the discharge lamp electrode. The discharge lamp electrode inside the container is
Since the conductor is a conductor, it is heated based on the principle of induction heating by an electromagnetic field wave generated from the electromagnetic wave generator, and discharge phenomena are discharged from the discharge lamp electrode inside the container to the inside of the container by the principle of electromagnetic induction. Occurs. For this reason, the discharge lamp electrode placed in the phenomenon state according to the present invention is in the same state as the inside of the discharge lamp being lit, and is about 2,500.
Heat treatment is performed at a temperature of from 3000C to 3000C.

【0007】また、請求項2では、前記容器が非導電性
物質であるようにした。これにより、非導電性物質であ
るため電磁波による誘導加熱の影響を受けず、放電灯用
電極に比べ非常に低い温度となる。このため、高温で熱
処理された放電灯用電極の不純物、特に炭素は、蒸発
し、放電灯用電極よりも温度が低い前記容器の内表面に
放電灯用電極の主成分であるタングステンとともに蒸着
され、完全に放電灯用電極から除去することが可能とな
る。
Further, in the present invention, the container is made of a non-conductive material. Accordingly, the temperature is much lower than that of the discharge lamp electrode because it is a non-conductive substance and is not affected by induction heating by electromagnetic waves. For this reason, the impurities of the discharge lamp electrode heat-treated at a high temperature, particularly carbon, evaporate and are deposited on the inner surface of the vessel having a lower temperature than the discharge lamp electrode together with tungsten which is a main component of the discharge lamp electrode. , Can be completely removed from the discharge lamp electrode.

【0008】また、請求項3では、前記容器の内部に、
電極とともに希ガスまたは水素が、少なくとも1種類以
上存在するさせるようにした。これにより、電磁誘導に
よる放電現象をより起こさせやすくすることができる。
According to a third aspect of the present invention, in the container,
At least one kind of rare gas or hydrogen is present together with the electrodes. This makes it possible to more easily cause a discharge phenomenon due to electromagnetic induction.

【0009】また、請求項4では、放電灯用の電極に含
まれる不純物を、電磁波による電極の加熱により蒸発さ
せ、該電極とは別に設けた部材に蒸着させることにより
該電極より除去するようにした。これにより、従来技術
では除去されにくかった放電灯用電極の不純物、特に炭
素を簡単に除去することが可能となる。なお、含まれて
いる不純物を電磁波による加熱により蒸発させることが
可能な電極である場合、本発明の内容を放電灯用以外の
電灯用電極について用いてもよい。
According to a fourth aspect of the present invention, impurities contained in an electrode for a discharge lamp are evaporated by heating the electrode by electromagnetic waves, and are removed from the electrode by vapor deposition on a member provided separately from the electrode. did. This makes it possible to easily remove impurities, particularly carbon, of the discharge lamp electrode, which is difficult to remove in the prior art. In the case of an electrode capable of evaporating contained impurities by heating with an electromagnetic wave, the contents of the present invention may be applied to an electrode for an electric lamp other than for a discharge lamp.

【0010】[0010]

【発明の実施の形態】本発明をより理解しやすくするた
め、以下に実施例を用いて詳説する
DESCRIPTION OF THE PREFERRED EMBODIMENTS In order to make the present invention easier to understand, the present invention will be described in detail with reference to the following examples.

【0011】[0011]

【実施例】図1は、本発明の一実施形態を示す縦断面図
である。図1において、電磁波発生装置3の内側に、放
電灯用電極1を内部に配置し完全密封した石英製容器2
を固定する。ただし、固定するための冶具の記載は省略
している。石英製容器内部2aは放電灯用電極1が存在
すると共に、アルゴンをガス圧50Torrの状態にし
てある。なお、本実施例では希ガスとしてアルゴンを用
いているが、他のヘリウムガス、ネオンガス、クリプト
ンガス、キセノンガス、ラドンガス等の希ガスや水素ガ
スを用いても良い。また同様の作用を果たせるならば、
これ以外のガスを用いてもよい。また、複数のガスを組
み合わせて用いてもよい。
FIG. 1 is a longitudinal sectional view showing an embodiment of the present invention. In FIG. 1, a discharge vessel electrode 1 is disposed inside an electromagnetic wave generator 3 and a quartz container 2 completely sealed.
Is fixed. However, the description of the jig for fixing is omitted. Inside the quartz vessel 2a, the discharge lamp electrode 1 is present, and argon is kept at a gas pressure of 50 Torr. Although argon is used as the rare gas in this embodiment, other rare gases such as helium gas, neon gas, krypton gas, xenon gas, and radon gas, and hydrogen gas may be used. If you can also achieve the same effect,
Other gases may be used. Further, a plurality of gases may be used in combination.

【0012】電磁波発生装置3により石英製容器内部2
aおよび放電灯用電極1に電磁波を印加する。電磁波を
印加された石英製容器内部2aにおいて、導体である放
電灯用電極1は、誘導加熱の原理より加熱される。同時
に、放電灯用電極1の先端より放電4が発生する。そし
て、数秒から数分間この現象を続けることにより、放電
灯用電極1より温度の低い状態の石英製容器2の内表面
に付着物2bが蒸着させることによって、放電灯用電極
1から不純物を除去することが可能となる。
[0012] The electromagnetic wave generator 3 controls the inside 2 of the quartz container.
a and the discharge lamp electrode 1. In the interior 2a of the quartz container to which the electromagnetic wave is applied, the discharge lamp electrode 1 as a conductor is heated by the principle of induction heating. At the same time, a discharge 4 is generated from the tip of the discharge lamp electrode 1. By continuing this phenomenon for several seconds to several minutes, impurities are removed from the discharge lamp electrode 1 by depositing the deposit 2b on the inner surface of the quartz vessel 2 having a lower temperature than the discharge lamp electrode 1. It is possible to do.

【0013】なお、電磁波を印加するために用いる電磁
場発生装置3としては、一般家庭で使用されている電子
レンジを用いても良い。本実施例では、放電灯用電極1
とアルゴン50Torrを共に封入密閉した石英製容器
2を一般用電子レンジ(NEC製MC−EV2定格高周
波出力500W)の内部に配置し、最大出力で6分間電
磁波を照射した。その後、石英製内部に付着物2bが蒸
着された。
As the electromagnetic field generator 3 used to apply the electromagnetic wave, a microwave oven used in ordinary households may be used. In this embodiment, the discharge lamp electrode 1 is used.
And a quartz container 2 sealed with argon and 50 Torr were placed inside a general-purpose microwave oven (NEC MC-EV2 rated high-frequency output 500 W), and irradiated with electromagnetic waves at the maximum output for 6 minutes. Thereafter, the deposit 2b was deposited inside the quartz.

【0014】図2に示す様に、蒸着された付着物2bの
エネルギー分散型X線分析装置を用いた元素の定性分析
の結果、放電灯用電極1の主成分であるタングステンと
放電灯用電極1の不純物である炭素が検出された。
As shown in FIG. 2, as a result of qualitative analysis of the deposited matter 2b using an energy dispersive X-ray analyzer, tungsten, which is the main component of the discharge lamp electrode 1, and the discharge lamp electrode Carbon, one of the impurities, was detected.

【0015】また、本発明の処理前と処理後の元素定性
分析結果を図3に示す。処理前には炭素が検出された放
電灯用電極1は、処理後には炭素が検出されてなかっ
た。
FIG. 3 shows the results of elemental qualitative analysis before and after the treatment of the present invention. In the discharge lamp electrode 1 in which carbon was detected before the treatment, no carbon was detected after the treatment.

【0016】以上述べてきたように、放電灯用電極1
は、点灯中の放電灯内部と同じような状態におかれ、約
2500℃から3000℃の温度で加熱処理される。そ
して、前記容器が非導電性物質であるため、電磁波によ
る誘導加熱の影響を受けず放電灯用電極に比べ非常に低
い温度となる。そして、高温で熱処理された放電灯用電
極の不純物、特に炭素は、蒸発し、放電灯用電極よりも
温度が低い前記容器の内表面に放電灯用電極の主成分で
あるタングステンとともに蒸着され、完全に放電灯用電
極から除去される。
As described above, the discharge lamp electrode 1
Is placed in the same state as the inside of the discharge lamp being lit, and is heated at a temperature of about 2500 ° C. to 3000 ° C. Since the container is made of a non-conductive material, the temperature is much lower than that of the discharge lamp electrode without being affected by induction heating by electromagnetic waves. And the impurities of the discharge lamp electrode heat-treated at a high temperature, particularly carbon, evaporate and are deposited together with tungsten which is a main component of the discharge lamp electrode on the inner surface of the container having a lower temperature than the discharge lamp electrode, It is completely removed from the discharge lamp electrode.

【0017】[0017]

【発明の効果】本発明は上記構成により次の効果を発揮
する。請求項1では、放電灯用電極を内部に少なくとも
1本以上収納する容器からなり、その周囲に電磁波発生
装置を設け、その電磁波発生装置より高周波の電磁波を
発生させ前記容器内部の放電灯用電極に印加し、放電灯
電極を加熱すると共に、電磁誘導の原理により、前記容
器内部にある放電灯用電極から前記容器内部に放電現象
が生じさせ、点灯中の放電灯内部と同じような状態とす
ることで、約2500℃から3000℃の温度で加熱処
理されることにより、放電灯用電極に含まれている不純
物を蒸発させることが可能となる。
According to the present invention, the following effects are exhibited by the above configuration. The discharge lamp electrode according to claim 1, comprising a container accommodating at least one electrode for a discharge lamp therein, an electromagnetic wave generator provided around the container, and a high frequency electromagnetic wave generated by the electromagnetic wave generator. To heat the discharge lamp electrode and, by the principle of electromagnetic induction, cause a discharge phenomenon inside the container from the discharge lamp electrode inside the container, and the same state as inside the discharge lamp being lit. By performing the heat treatment at a temperature of about 2500 ° C. to 3000 ° C., impurities contained in the discharge lamp electrode can be evaporated.

【0018】請求項2では、容器を非導電性物質にする
ことにより、容器は電磁波による誘導加熱の影響を受け
ず容器内部に存在する放電灯用電極に比べ非常に低い温
度となり、高温で熱処理された放電灯用電極の不純物、
特に炭素が蒸発し、放電灯用電極よりも温度が低い前記
容器の内表面に放電灯用電極の主成分であるタングステ
ンとともに蒸着されるので、不純物を完全に放電灯用電
極から除去されるすることが可能となる。
According to the second aspect of the present invention, the container is made of a non-conductive material, so that the container is not affected by induction heating by electromagnetic waves and has a very low temperature as compared with the discharge lamp electrode existing inside the container. Discharge electrode impurities,
Particularly, carbon evaporates and is deposited together with tungsten which is a main component of the discharge lamp electrode on the inner surface of the container having a lower temperature than the discharge lamp electrode, so that impurities are completely removed from the discharge lamp electrode. It becomes possible.

【0019】請求項3では、容器の内部に電極とともに
不活性ガスを少なくとも1種類以上存在するさせること
により、電磁誘導による放電現象をより起こさせやすく
し、より効果的に放電灯用電極から不純物を除去するこ
とが可能となる。
According to the third aspect of the present invention, the presence of at least one kind of inert gas together with the electrode inside the container makes it easier to cause a discharge phenomenon by electromagnetic induction, and more effectively removes impurities from the discharge lamp electrode. Can be removed.

【0020】そして請求項4では、放電灯用の電極に含
まれる不純物を、電磁波による電極の加熱により蒸発さ
せ、該電極とは別に設けた部材に蒸着させることにより
該電極より除去するようにしたので、放電灯用電極から
不純物を簡単に除去することが可能となる。
According to the present invention, impurities contained in the electrode for the discharge lamp are evaporated by heating the electrode by electromagnetic waves, and are removed from the electrode by vapor deposition on a member provided separately from the electrode. Therefore, impurities can be easily removed from the discharge lamp electrode.

【図面の簡単な説明】[Brief description of the drawings]

【図1】本発明の実施の形態を示す縦断面図FIG. 1 is a longitudinal sectional view showing an embodiment of the present invention.

【図2】実施例によって得られた付着物の元素定性分析
結果
FIG. 2 shows the results of elemental qualitative analysis of the deposits obtained in the examples.

【図3】実施例によって得られた本発明による処理の実
施前と実施後の放電灯用電極の元素定性分析結果
FIG. 3 shows the results of elemental qualitative analysis of electrodes for a discharge lamp before and after the treatment according to the present invention obtained by the examples.

【符号の説明】[Explanation of symbols]

1…放電灯用電極 2…石英製容器、2a…石英製容器の内部、2b…付着
物 3…電磁波発生装置 4…放電
DESCRIPTION OF SYMBOLS 1 ... Electrode for discharge lamp 2 ... Quartz container, 2a ... Inside of quartz container, 2b ... Adhered matter 3 ... Electromagnetic wave generator 4 ... Discharge

Claims (4)

【特許請求の範囲】[Claims] 【請求項1】 放電灯用の電極を内部に少なくとも1本
以上収納する容器からなり、その周囲に電磁波発生装置
を設け、その電磁波発生装置より高周波の電磁波を発生
させ容器内部の放電灯用電極に印加し、放電灯電極を加
熱することを特徴とする放電灯用電極の処理装置。
1. An electrode for a discharge lamp inside a container, comprising a container in which at least one electrode for a discharge lamp is housed inside, an electromagnetic wave generator provided around the container, and a high-frequency electromagnetic wave generated by the electromagnetic wave generator. A discharge lamp electrode heating apparatus for heating a discharge lamp electrode.
【請求項2】 前記容器は、非導電性物質であることを
特徴とする請求項1の放電灯用電極の処理装置。
2. The apparatus according to claim 1, wherein the container is made of a non-conductive material.
【請求項3】 前記容器の内部には、前記電極とともに
希ガスまたは水素が、少なくとも1種類以上存在するこ
とを特徴とする請求項1の放電灯用電極の処理装置。
3. An apparatus for treating an electrode for a discharge lamp according to claim 1, wherein at least one kind of rare gas or hydrogen is present inside said container together with said electrode.
【請求項4】 放電灯用の電極に含まれる不純物を、電
磁波による電極の加熱により蒸発させ、該電極とは別に
設けた部材に蒸着させることにより該電極より除去する
ことを特徴とする放電灯用電極の処理方法。
4. A discharge lamp, wherein impurities contained in an electrode for a discharge lamp are evaporated by heating the electrode by electromagnetic waves, and are removed from the electrode by vapor deposition on a member provided separately from the electrode. Treatment method for electrodes.
JP10316846A 1998-10-19 1998-10-19 Processing method for discharge lamp electrode and its device Pending JP2000123726A (en)

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