IT1256666B - Procedimento per la purificazione di n-alchil urea di grado tecnico. - Google Patents
Procedimento per la purificazione di n-alchil urea di grado tecnico.Info
- Publication number
- IT1256666B IT1256666B ITTO920022A ITTO920022A IT1256666B IT 1256666 B IT1256666 B IT 1256666B IT TO920022 A ITTO920022 A IT TO920022A IT TO920022 A ITTO920022 A IT TO920022A IT 1256666 B IT1256666 B IT 1256666B
- Authority
- IT
- Italy
- Prior art keywords
- urea
- alchil
- purifying
- alkyl urea
- alcoholic solvent
- Prior art date
Links
- 239000004202 carbamide Substances 0.000 title abstract 5
- 238000000034 method Methods 0.000 title abstract 2
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 title 1
- 230000001476 alcoholic effect Effects 0.000 abstract 3
- 239000002904 solvent Substances 0.000 abstract 3
- 229910052936 alkali metal sulfate Inorganic materials 0.000 abstract 2
- -1 alkyl urea Chemical compound 0.000 abstract 2
- RYECOJGRJDOGPP-UHFFFAOYSA-N Ethylurea Chemical compound CCNC(N)=O RYECOJGRJDOGPP-UHFFFAOYSA-N 0.000 abstract 1
- 238000000746 purification Methods 0.000 abstract 1
- 230000007928 solubilization Effects 0.000 abstract 1
- 238000005063 solubilization Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
- C07C273/18—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of substituted ureas
- C07C273/189—Purification, separation, stabilisation, use of additives
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Procedimento per la purificazione di N-alchil urea di grado tecnico, particolarmente mono-etilurea, comprendente solfato di metallo alcalino, caratterizzato dal fatto che comprende le fasi di:- trattare l'alchil urea tecnica con un solvente alcolico C1-C4 per causare la solubilizzazione selettiva dell'alchil urea,- separare la frazione solubile dal solfato di metallo alcalino insolubile nel solvente alcolico, e - rimuovere il solvente alcolico dalla frazione solubile per recuperare la N-alchil urea.
Priority Applications (6)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
ITTO920022A IT1256666B (it) | 1992-01-15 | 1992-01-15 | Procedimento per la purificazione di n-alchil urea di grado tecnico. |
US07/996,614 US5446200A (en) | 1992-01-15 | 1992-12-24 | Process for the purification of technical-grade N-alkyl urea |
ES93100264T ES2082525T3 (es) | 1992-01-15 | 1993-01-11 | Procedimiento para la purificacion de derivados de n-alquilo de urea. |
EP93100264A EP0552626B1 (en) | 1992-01-15 | 1993-01-11 | Process for the purification of technical-grade n-alkyl urea |
DE69301032T DE69301032T2 (de) | 1992-01-15 | 1993-01-11 | Verfahren zur Reinigung von technischem N-Alkyl-Harnstoff |
AT93100264T ATE131808T1 (de) | 1992-01-15 | 1993-01-11 | Verfahren zur reinigung von technischem n-alkyl- harnstoff |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
ITTO920022A IT1256666B (it) | 1992-01-15 | 1992-01-15 | Procedimento per la purificazione di n-alchil urea di grado tecnico. |
Publications (3)
Publication Number | Publication Date |
---|---|
ITTO920022A0 ITTO920022A0 (it) | 1992-01-15 |
ITTO920022A1 ITTO920022A1 (it) | 1993-07-15 |
IT1256666B true IT1256666B (it) | 1995-12-12 |
Family
ID=11409887
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ITTO920022A IT1256666B (it) | 1992-01-15 | 1992-01-15 | Procedimento per la purificazione di n-alchil urea di grado tecnico. |
Country Status (6)
Country | Link |
---|---|
US (1) | US5446200A (it) |
EP (1) | EP0552626B1 (it) |
AT (1) | ATE131808T1 (it) |
DE (1) | DE69301032T2 (it) |
ES (1) | ES2082525T3 (it) |
IT (1) | IT1256666B (it) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE19919482C2 (de) * | 1999-04-29 | 2001-04-26 | Byk Chemie Gmbh | Verfahren zur Herstellung eines Thixotropie-Mittels und dessen Verwendung |
US7720908B1 (en) * | 2000-03-07 | 2010-05-18 | Microsoft Corporation | System and method for multi-layered network communications |
PL3131962T3 (pl) | 2014-04-15 | 2018-09-28 | Byk-Chemie Gmbh | Kompozycja do regulowania właściwości reologicznych |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2673859A (en) * | 1950-09-15 | 1954-03-30 | Allied Chem & Dye Corp | Production of urea derivatives |
US3297753A (en) * | 1965-06-30 | 1967-01-10 | Atlas Chem Ind | Separation of alkyl ureas |
-
1992
- 1992-01-15 IT ITTO920022A patent/IT1256666B/it active IP Right Grant
- 1992-12-24 US US07/996,614 patent/US5446200A/en not_active Expired - Lifetime
-
1993
- 1993-01-11 AT AT93100264T patent/ATE131808T1/de not_active IP Right Cessation
- 1993-01-11 DE DE69301032T patent/DE69301032T2/de not_active Expired - Fee Related
- 1993-01-11 ES ES93100264T patent/ES2082525T3/es not_active Expired - Lifetime
- 1993-01-11 EP EP93100264A patent/EP0552626B1/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
DE69301032T2 (de) | 1996-05-02 |
DE69301032D1 (de) | 1996-02-01 |
ES2082525T3 (es) | 1996-03-16 |
EP0552626B1 (en) | 1995-12-20 |
EP0552626A1 (en) | 1993-07-28 |
US5446200A (en) | 1995-08-29 |
ITTO920022A0 (it) | 1992-01-15 |
ATE131808T1 (de) | 1996-01-15 |
ITTO920022A1 (it) | 1993-07-15 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
0001 | Granted | ||
TA | Fee payment date (situation as of event date), data collected since 19931001 |
Effective date: 19990129 |