IT1049374B - Acetylenes removal from hydrocarbons - by reaction with alcohol, phenol or acid in presence of mercury-contg. ion-exchange resin - Google Patents
Acetylenes removal from hydrocarbons - by reaction with alcohol, phenol or acid in presence of mercury-contg. ion-exchange resinInfo
- Publication number
- IT1049374B IT1049374B IT2151775A IT2151775A IT1049374B IT 1049374 B IT1049374 B IT 1049374B IT 2151775 A IT2151775 A IT 2151775A IT 2151775 A IT2151775 A IT 2151775A IT 1049374 B IT1049374 B IT 1049374B
- Authority
- IT
- Italy
- Prior art keywords
- acetylenes
- contg
- ion
- pref
- exchange resin
- Prior art date
Links
- 125000002534 ethynyl group Chemical class [H]C#C* 0.000 title abstract 5
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 title abstract 3
- 239000003456 ion exchange resin Substances 0.000 title abstract 3
- 229920003303 ion-exchange polymer Polymers 0.000 title abstract 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 title abstract 2
- 239000002253 acid Substances 0.000 title abstract 2
- 229930195733 hydrocarbon Natural products 0.000 title abstract 2
- 150000002430 hydrocarbons Chemical class 0.000 title abstract 2
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 title 1
- MYRTYDVEIRVNKP-UHFFFAOYSA-N 1,2-Divinylbenzene Chemical compound C=CC1=CC=CC=C1C=C MYRTYDVEIRVNKP-UHFFFAOYSA-N 0.000 abstract 2
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 abstract 2
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 abstract 2
- -1 Hg2+ ions Chemical class 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- 239000011347 resin Substances 0.000 abstract 2
- 229920005989 resin Polymers 0.000 abstract 2
- KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical compound [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 abstract 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 abstract 1
- 239000005977 Ethylene Substances 0.000 abstract 1
- 239000004793 Polystyrene Substances 0.000 abstract 1
- 125000002252 acyl group Chemical group 0.000 abstract 1
- 125000000217 alkyl group Chemical group 0.000 abstract 1
- 125000003118 aryl group Chemical group 0.000 abstract 1
- JXLHNMVSKXFWAO-UHFFFAOYSA-N azane;7-fluoro-2,1,3-benzoxadiazole-4-sulfonic acid Chemical compound N.OS(=O)(=O)C1=CC=C(F)C2=NON=C12 JXLHNMVSKXFWAO-UHFFFAOYSA-N 0.000 abstract 1
- 150000001732 carboxylic acid derivatives Chemical class 0.000 abstract 1
- 125000000753 cycloalkyl group Chemical group 0.000 abstract 1
- 150000002170 ethers Chemical class 0.000 abstract 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 abstract 1
- ORMNPSYMZOGSSV-UHFFFAOYSA-N mercury(II) nitrate Inorganic materials [Hg+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O ORMNPSYMZOGSSV-UHFFFAOYSA-N 0.000 abstract 1
- 239000005011 phenolic resin Substances 0.000 abstract 1
- 229920001568 phenolic resin Polymers 0.000 abstract 1
- 229920000779 poly(divinylbenzene) Polymers 0.000 abstract 1
- 229920002223 polystyrene Polymers 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 abstract 1
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 abstract 1
- 239000012264 purified product Substances 0.000 abstract 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Acetylenes are removed from satd. olefinic or dienic hydrocarbons or mixts. thereof by (a) reacting the acetylenes with ROH (R = alkyl. aryl, cycloalkyl or acyl) in the presence of an acid ion-exchange resin contg. Hg2+ ions; and (b) separating the products in known manner. The process is esp. useful for purifying butadiene, propylene and ethylene for use in polymerisation processes. Purified products contg. =10 ppm of acetylenes can be obtained. In step (a), the acetylenes are pref. etherified with an alcohol or glycol at -20 to +80 degrees (esp. 20-60 degrees C). The ion-exchange resin is pref. a sulphonate resin based on poly styrene, divinylbenzene or a phenolic resin, or can also be carboxylic acid resin. The Hg2+ ions are pref. introduced in the form of Hg(NO3)2 or Hg (OAc)2. The ethers formed are pref. removed by distn.
Priority Applications (30)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| AR258894A AR206714A1 (en) | 1974-05-21 | 1975-01-01 | PROCEDURE TO REMOVE ACETYLENE COMPOUNDS FROM OLEFINIC AND DIENIC SATURATED HYDROCARBONS OR MIXTURE OF THEM |
| IT2151775A IT1049374B (en) | 1975-03-21 | 1975-03-21 | Acetylenes removal from hydrocarbons - by reaction with alcohol, phenol or acid in presence of mercury-contg. ion-exchange resin |
| TR18762A TR18762A (en) | 1974-05-21 | 1975-05-03 | PROCEDURE FOR EXTRACTING ESSENTIAL COMPOSITIONS FROM SATURATED, OLEFINIC AND DIESEL HYDROCARBONS OR THEIR MIXTURES |
| DK209775AA DK140831B (en) | 1974-05-21 | 1975-05-13 | Process for removing acetylenic compounds from saturated, olefinic and dienic hydrocarbons or mixtures thereof. |
| YU01215/75A YU121575A (en) | 1974-05-21 | 1975-05-13 | Process for the separation of acetylene compounds from saturated olefinic and dienic hydrocarbons or mixtures thereof |
| GB2021175A GB1465015A (en) | 1974-05-21 | 1975-05-13 | Process for reducing the concentration of acetylenic compounds in a hydrocarbon mixture |
| IE1095/75A IE41364B1 (en) | 1974-05-21 | 1975-05-15 | Process for reducing the concentration of acetylenic compounds in a hydrocarbon mixture |
| DE19752521702 DE2521702C3 (en) | 1974-05-21 | 1975-05-15 | Process for the separation of acetylene compounds from other hydrocarbons |
| IN1000/CAL/75A IN140786B (en) | 1974-05-21 | 1975-05-19 | |
| CS368378A CS194250B2 (en) | 1975-03-21 | 1975-05-20 | Method for removing acetylenic compounds from unsaturated,olefinic and dienic hydrocarbons or mixtures thereof |
| ES438188A ES438188A1 (en) | 1974-05-21 | 1975-05-20 | Method for removing acetylenic compounds from saturated, olefinic and dienic hydrocarbons or mixtures thereof |
| FR7515720A FR2272054B1 (en) | 1974-05-21 | 1975-05-20 | |
| AU81326/75A AU492878B2 (en) | 1975-05-20 | Process for reducing the concentration of acetylenic compounds ina hydrocarbon mixture | |
| NO751786A NO144015C (en) | 1974-05-21 | 1975-05-20 | PROCEDURE FOR AA SEPARATE ACETYLENE COMPOUNDS FROM THEIR MIXTURES WITH Saturated, OLEFINUMETTED OR DIENUMETTED HYDROCARBONS OR MIXTURES THEREOF, BY ESTABLISHMENT AND DISPOSAL |
| AT381275A AT358541B (en) | 1974-05-21 | 1975-05-20 | METHOD FOR SEPARATING ALKINES FROM SATURED, OLEFINIC OR DIENIC HYDROCARBONS OR THEIR MIXTURES |
| CA227,298A CA1036182A (en) | 1974-05-21 | 1975-05-20 | Method for removing acetylenic compounds from saturated, olefinic and dienic hydrocarbons or mixtures thereof |
| LU72541A LU72541A1 (en) | 1974-05-21 | 1975-05-20 | |
| BG030038A BG24792A3 (en) | 1974-05-21 | 1975-05-20 | Method of separating acetylene combinations from saturated ethylene and dien hydrocarbons or their salts |
| SE7505803A SE396215B (en) | 1974-05-21 | 1975-05-21 | WAY TO REMOVE ACETYLENE COMPOUNDS FROM THE SATURATED CARBON, OLEFIN OR DIENE CARBON OR MIXTURES THEREFORE BY BRINGING THE ACETYLENE COMPOUNDS TO REACTION WITH COMPOUNDS OF TYPE R-OH ... |
| RO7582293A RO67330A (en) | 1974-05-21 | 1975-05-21 | PROCEDURE FOR INDEPENDENCE OF ACETYLENE COMPOUNDS FROM SATURATED, OLEFINIC OR DIENIC HYDROCARBONS, OR OF THEIR MIXTURES |
| BE156543A BE829301A (en) | 1974-05-21 | 1975-05-21 | PROCESS FOR REMOVING ACETYLENIC COMPOUNDS CONTAINED IN SATURATED, OLEFINIC AND DIENIC HYDROCARBONS OR MIXTURES OF SUCH HYDOCARBONS |
| SU752137590A SU1068030A3 (en) | 1974-05-21 | 1975-05-21 | Process for purifying propane, or propylene, or butadiene from impurities of acetylene hydrocarbons |
| US05/579,691 US4031157A (en) | 1974-05-21 | 1975-05-21 | Method for removing acetylenic compounds from saturated, olefinic and dienic hydrocarbons or mixtures thereof |
| NL7505993A NL7505993A (en) | 1974-05-21 | 1975-05-21 | PROCESS FOR THE REMOVAL OF ACETYLENE COMPOUNDS FROM SATURATED, ALKES AND DIESEL, HYDROCARBONS OR MIXTURES THEREOF. |
| CH649375A CH617100A5 (en) | 1974-05-21 | 1975-05-21 | |
| ZM63/75A ZM6375A1 (en) | 1974-05-21 | 1975-05-21 | Method for removing acetylenic compounds from saturated,olefinic and dienic hydrocarbons or mixtures thereof |
| DD186164A DD118056A5 (en) | 1974-05-21 | 1975-05-21 | |
| JP5979275A JPS554725B2 (en) | 1974-05-21 | 1975-05-21 | |
| BR4086/75A BR7503194A (en) | 1974-05-21 | 1975-05-22 | METHODS FOR REMOVING ACETYLENE COMPOUND FROM SATURATED HYDROCARBONS AND OLEFINS |
| US05/762,769 US4112009A (en) | 1974-05-21 | 1977-01-26 | Method for removing acetylenic compounds from saturated, olefinic and dienic hydrocarbons or mixtures thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IT2151775A IT1049374B (en) | 1975-03-21 | 1975-03-21 | Acetylenes removal from hydrocarbons - by reaction with alcohol, phenol or acid in presence of mercury-contg. ion-exchange resin |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| IT1049374B true IT1049374B (en) | 1981-01-20 |
Family
ID=11182972
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IT2151775A IT1049374B (en) | 1974-05-21 | 1975-03-21 | Acetylenes removal from hydrocarbons - by reaction with alcohol, phenol or acid in presence of mercury-contg. ion-exchange resin |
Country Status (2)
| Country | Link |
|---|---|
| CS (1) | CS194250B2 (en) |
| IT (1) | IT1049374B (en) |
-
1975
- 1975-03-21 IT IT2151775A patent/IT1049374B/en active
- 1975-05-20 CS CS368378A patent/CS194250B2/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| CS194250B2 (en) | 1979-11-30 |
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